Abstract
Taguchi experiment design in quality development studies, is an approach to engineering that supports research and development, product design and product development activities by enabling fewer trials of experiments to determine the best combinations of inputs that affect the outcome. In this study, the factors affecting the porosity were studied in a firm that produces ceramic tile. There were 6 factors considered to be important in total and 2 levels in each factor. L8 orthogonal array were used during the experiment design, which proposes 8 experiment types with different factor levels. The results of the experiments were analyzed so that important factors were determined. Significance of factors were tested by ANOVA and 4 of them were found to be significant. These factors were fuzzified by assessing the factors using linguistic expressions and then triangular fuzzy numbers. A model with 4 inputs and 1 output was built and 34 rules were generated for this model. The developed model was shown to be a useful approach in modeling the porosity permeability of ceramic tiles.
1 Introduction
Taguchi method was developed by Genichi Taguchi as a process improvement technique in the 1950s [1]. Taguchi method is an experimental design and optimization method based on parameter design, system design and tolerance design. It is commonly used to perform statistical analysis of collected data within quality assurance systems. Taguchi experiment design is an approach in engineering that supports product design and product development activities by enabling less trials of experiments to determine the most effective combinations of input values that yield better outcome [2].
There are various studies on the application of the Taguchi method in different areas. Savaşkan et al. aimed at finding the cost and quality benefits of maximizing the process parameters and increasing the life of the drill bits, based on the importance of drilling in the metalworking industry [3].
Baynal used the Signal to Noise (S/N) ratio in order to eliminate the bulge and slickness at the head of the products and to make the weight and dimensions close to the target values. By doing experiments with 3 levels of 13 factors (L27) in the study, it provided equipment, energy and labor savings as well as improved weight of produced parts [4].
Öztop investigated the impact rate and interactions of extrusion speed, temperature of the extrusion, rate of extrusion and profile of the die guide distance over the profile temperature, punch force and die surface pressure, which are decisive on die lifetime in aluminum extrusion process, using the Taguchi experiment design method. He determined the most important factors using the L8 orthogonal array [5].
Kiani et al. studied Zn (II) removal from aqueous solution using halloysite nanotubes. They found the optimum conditions for adsorption capacity and removal percent with Taguchi method using 4 levels of 5 control factors (L16) which are pH, contact time, adsorbent mass, temperature and initial concentration of Zn (II) [6].
Fuzzy Logic is a method for optimization which used in several engineering problems. This method can be used in Civil Engineering, Mechanical Engineering, Industrial Engineering, Chemical Engineering etc. Ibadov used Fuzzy Sets for determining the risk factors in the construction projects [7]. Adali et al. used Fuzzy for selecting the optimal shift numbers in a paint factory [8]. Erdem used Fuzzy analytical hierarchy process for personnel selection in IT companies [9]. Toklu determined the customer loyalty levels by Fuzzy multi criteria decision making approaches [10]. Akinrotimi and Oladele used fuzzy logic to classify patients with typhoid fever disease in five different severity by generating explainable rules for diagnosis [11]. Srivastava et al. implemented fuzzy logic to predict the rainfall using temperature and humidity as parameters [12].
Jenatabadi et al. combined fuzzy analytical hierarchy process and Taguchi method to determine a pattern for willingness to pay characteristics of public transportation users based on their satisfaction [13]. Ngo et al. combined fuzzy theory with Taguchi method to optimize in fly cutting process and applied to hobbing process [14]. Ethical approval: The conducted research is not related to either human or animal use.
2 Problem Definition
In this study, tile production process of a ceramic company was analyzed. Tile is a construction material used for floor and wall coating in closed and open areas regardless of shape and size. Decorative tile consists of four parts in structural aspect; mass, liner, glost and decor. The raw materials in the mass are shaped by pressing, plastic extrusion or casting at normal room temperature after being processed through grinding, sieving and mixing processes. The shaped body is then cooked at high temperature [15].
Porosity has a great importance in ceramics. Porosity is defined as the ratio of the amount of water that the tile can contain to the weight of the tile, expressed in percentage [15]. Low degree of porosity is a desirable condition for ceramic materials. Low porosity indicates good quality of ceramics. For this reason, the factors affecting the porosity of tiles are examined and the most important factors are determined using the Taguchi experiment design method. After the factors with the greatest effect on the porosity are determined, a fuzzy model is suggested to calculate the porosity for any value of these factors.
3 Suggested Model
There are 6 factors that affect the porosity of tiles. Engineers in the factory may prefer one of two levels of value for each factor, during operations. Therefore, normally, 2^6 combinations of experiment is required in order to find out the most effective factor levels. However, with the Taguchi experimental design, using L8 orthogonal array that proposes only 8 experiment combinations will be sufficient to analyze effective combinations of factor levels. The factors affecting the porosity, as well as their level values given in Table 1.
Factors and their level values that affects the porosity.
| Factors | Level 1 | Level 2 | |
|---|---|---|---|
| A | Alcali ratio | 3% | 6% |
| B | Grain size of mud | 10μ | 20μ |
| C | Size distribution of mass | >250μ rate 80% | >250μ rate 90% |
| D | Pressure of press | 250 bar | 300 bar |
| E | Furnace temperature | 1100°C | 1200°C |
| F | Firing time | 35 min | 40 min |
The L8 orthogonal array was generated with the help of the Minitab program and the experiments were performed according to the experiment combinations proposed by this array. Experiments were repeated 4 times for each combination. L8 orthogonal array and observed values of the experiments given in Table 2.
L8 orthogonal array and observed values.
| Factors and their levels | Observed values (%) | |||||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Exp | A | B | C | D | E | F | 1 | 2 | 3 | 4 |
| 1 | 3 | 10 | 80 | 250 | 1100 | 35 | 14 | 16 | 16.3 | 17.2 |
| 2 | 3 | 10 | 80 | 300 | 1200 | 40 | 11.2 | 10 | 10.8 | 11.5 |
| 3 | 3 | 20 | 90 | 250 | 1100 | 40 | 19.2 | 18.7 | 19 | 18 |
| 4 | 3 | 20 | 90 | 300 | 1200 | 35 | 8.3 | 9.1 | 7.9 | 8.9 |
| 5 | 6 | 10 | 90 | 250 | 1200 | 35 | 1.1 | 0.7 | 1 | 1.3 |
| 6 | 6 | 10 | 90 | 300 | 1100 | 40 | 5 | 5.4 | 5.5 | 5.4 |
| 7 | 6 | 20 | 80 | 250 | 1200 | 40 | 2 | 2.5 | 2.1 | 2.3 |
| 8 | 6 | 20 | 80 | 300 | 1100 | 35 | 4.6 | 4.8 | 4.8 | 4.5 |
4 Application
The signal to noise (S/N) ratio indicates variability of response values relative to the target value under different noise conditions. S/N ratio of factors given in Figure 1. Since the best result can be obtained with lowest porosity, the “smaller is better” approach was used to calculate the S/N ratio. The greatest levels in the S/N ratio graph indicate the best values of factors to obtain better porosity. It is seen that among all the factors, the most effective factors on the porosity are A and E. On the other hand, the effect of using different levels of factor B or C is close to zero. Factors D and F seem to have small effect on porosity.

S/N ratios of factors.
The results of the ANOVA test performed on the Minitab program are given in Table 3. Values of P less than 0.05 denote that related factor significantly affects the porosity. For this reason, the fuzzification process was performed on factors A, D, E and F, which were found to be effective in ANOVA.
ANOVA test results.
| Source | DF | Seq. SS | Adj. SS | Adj. MS | F | P |
|---|---|---|---|---|---|---|
| A | 1 | 831.30 | 831.30 | 831.30 | 1428.32 | 0.000 |
| B | 1 | 0.58 | 0.58 | 0.58 | 0.99 | 0.329 |
| C | 1 | 0.00 | 0.00 | 0.00 | 0.00 | 0.982 |
| D | 1 | 35.49 | 35.49 | 35.49 | 60.98 | 0.000 |
| E | 1 | 240.35 | 240.35 | 240.35 | 412.97 | 0.000 |
| F | 1 | 24.68 | 24.68 | 24.68 | 42.40 | 0.000 |
| Error | 25 | 14.55 | 14.55 | 0.58 |
The values of factors found to be significant in the ANOVA test were fuzzified by classifying the values into linguistic expressions as “very low”, “low”, “medium”, “high” and “very high”. Then, these expressions were transformed into triangular fuzzy numbers within range of lower and upper limits. Linguistic rules were formed between these expressions and porosity.
34 rules related to the porosity model with 4 inputs and 1 output were established. Some of these rules are given below:
If the alkali ratio is low and the press pressure is not high and the furnace temperature is low and the firing time is not high, then the porosity is high.
If the alkali ratio is low and the press pressure is not high and the furnace temperature is low and the firing time is high, then the porosity is very high.
⁝
34. If the alkali ratio is high and the press pressure is high and the furnace temperature is high and the firing time is high, then the porosity is very low.
5 Conclusion
The linguistic expressions and rules treated with the defuzzification process using the Matlab program to obtain crisp results. At this stage, unlike in Taguchi method, the porosity value can be calculated for any value of each factor in the interval between two levels, as well as for all value combinations of all factors.
The effect of the A and E factors, which are the most effective on the porosity is shown in Figure 2. Porosity is very low at the blue region and gets higher as the region color turns to yellow.

Effect of A (Alkali rate) and E (Furnace temperature) to porosity.
Integrating fuzzy logic into Taguchi method enables the decision maker to apply enhanced analysis. This approach could be used in any Taguchi implementation in different areas.
Acknowledgements
We would like to thank Ind. Eng. Lütfiye Hamamcı for providing the data necessary to carry out this study.
Conflict of interest Authors state no conflict of interest.
References
[1] Roy R.K., A Primer on the Taguchi Method, 1st ed., Society of Manufacturing Engineers, New York 1990.Search in Google Scholar
[2] Güral G., Gazaltı Kaynağında Proses Parametrelerinin Optimizasyonu, MSc Thesis, Dokuz Eylül University, The Graduate School of Natural and Applied Sciences, Department of Mechanical Engineering, 2003.Search in Google Scholar
[3] Savaşkan M., Taptık, Y., Ürgen M., Deney tasarımı yöntemi ile matkap uçlarında performans optimizasyonu. İTÜ Dergisid 2010, 3, 117–128.Search in Google Scholar
[4] Baynal, K., Çok Yanıtlı Kalite Karakteristiklerinin Eşzamanlı Eniyilenmesinde Taguchi Yöntemi ve Otomotiv Endüstrisinde Bir Uygulama. End. Mühendisliği Derg. 2005, 16, 1–24.Search in Google Scholar
[5] Öztop, M., Taguchi Deney Tasarımı Yöntemi ile alüminyum ekstrüzyon prosesinin iyileştirilmesi, MSc Thesis, Erciyes University, Graduate School of Natural and Applied Sciences, Department of Mechanical Engineering, 2007.Search in Google Scholar
[6] Kiani, G., Soltanzadeh, M., Ahadzadeh, I., Adsorption study of Zinc ion onto halloysite nanotubes using taguchi’s design of experimental methodology. Int. J. Nano Dimens. Tonekabon 2018, 9, 246–259.Search in Google Scholar
[7] Ibadov, N., Determination of the Risk Factors Impact on the Construction Projects Implementation Using Fuzzy Sets Theory. Acta Phys. Pol. A 2016, 130, 107–111.10.12693/APhysPolA.130.107Search in Google Scholar
[8] Adali, M.R., Taşkin, M.F., Taşkin, H., Selecting the optimal shift numbers using fuzzy control model: a paint factory’s facility application. J. Intell. Manuf. 2009, 20, 267–272.10.1007/s10845-008-0231-0Search in Google Scholar
[9] Erdem, M.B., A Fuzzy Analytical Hierarchy Process Application in Personnel Selection in IT Companies: A Case Study in a Spin-off Company. Acta Phys. Pol. A 2016, 130, 331–334.10.12693/APhysPolA.130.331Search in Google Scholar
[10] Cengiz Toklu, M., Determination of Customer Loyalty Levels by Using Fuzzy MCDM Approaches. Acta Phys. Pol. A 2017, 132, 650–654.10.12693/APhysPolA.132.650Search in Google Scholar
[11] Akinrotimi, A.O., Oladele, R.O., Modeling and Diagnosis of Typhoid Fever Using a Fuzzy Logic Controlled Inference System. J. Comput. Sci. Control Syst. Oradea 2018, 11, 5–8.Search in Google Scholar
[12] Srivastava, R., Sharma, P., Daniel, A.K., Fuzzy Logic Based Prediction Model for Rainfall Over Agriculture in Northeast Region. Int. J. Adv. Res. Comput. Sci. Udaipur 2018, 9, 191–195.Search in Google Scholar
[13] Jenatabadi, H.S., Babashamsi, P., Yusoff, N.I.M., The Combination of a Fuzzy Analytical Hierarchy Process and the Taguchi Method to Evaluate the Malaysian Users’ Willingness to Pay for Public Transportation. Symmetry Basel 2016, 8, 90.10.3390/sym8090090Search in Google Scholar
[14] Ngo, M.T., Link to external site, this link will open in a new window, Hoang, V., Hoang, S.V., Taguchi-fuzzy multi-response optimization in fly cutting process and applying in the actual hobbing process. Int. J. Mech. Mater. Eng. Heidelb. 2018, 13, 1–10.10.1186/s40712-018-0092-zSearch in Google Scholar
[15] Tefek, M., Bilgeç, Ç., Yer Karoları. Kim. Mühendisliği Derg. 1997, 27–31.Search in Google Scholar
© 2018 Abdullah Hulusi Kokcam et al., published by De Gruyter
This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 License.
Articles in the same Issue
- Regular Articles
- The effect of CuO modification for a TiO2 nanotube confined CeO2 catalyst on the catalytic combustion of butane
- The preparation and antibacterial activity of cellulose/ZnO composite: a review
- Linde Type A and nano magnetite/NaA zeolites: cytotoxicity and doxorubicin loading efficiency
- Performance and thermal decomposition analysis of foaming agent NPL-10 for use in heavy oil recovery by steam injection
- Spectroscopic (FT-IR, FT-Raman, UV, 1H and 13C NMR) insights, electronic profiling and DFT computations on ({(E)-[3-(1H-imidazol-1-yl)-1-phenylpropylidene] amino}oxy)(4-nitrophenyl)methanone, an imidazole-bearing anti-Candida agent
- A Simplistic Preliminary Assessment of Ginstling-Brounstein Model for Solid Spherical Particles in the Context of a Diffusion-Controlled Synthesis
- M-Polynomials And Topological Indices Of Zigzag And Rhombic Benzenoid Systems
- Photochemical Transformation of some 3-benzyloxy-2-(benzo[b]thiophen-2-yl)-4Hchromen-4-ones: A Remote Substituent Effect
- Dynamic Changes of Secondary Metabolites and Antioxidant Activity of Ligustrum lucidum During Fruit Growth
- Studies on the flammability of polypropylene/ammonium polyphosphate and montmorillonite by using the cone calorimeter test
- DSC, FT-IR, NIR, NIR-PCA and NIR-ANOVA for determination of chemical stability of diuretic drugs: impact of excipients
- Antioxidant and Hepatoprotective Effects of Methanolic Extracts of Zilla spinosa and Hammada elegans Against Carbon Tetrachlorideinduced Hepatotoxicity in Rats
- Prunus cerasifera Ehrh. fabricated ZnO nano falcates and its photocatalytic and dose dependent in vitro bio-activity
- Organic biocides hosted in layered double hydroxides: enhancing antimicrobial activity
- Experimental study on the regulation of the cholinergic pathway in renal macrophages by microRNA-132 to alleviate inflammatory response
- Synthesis, characterization, in-vitro antimicrobial properties, molecular docking and DFT studies of 3-{(E)-[(4,6-dimethylpyrimidin-2-yl)imino]methyl} naphthalen-2-ol and Heteroleptic Mn(II), Co(II), Ni(II) and Zn(II) complexes
- M-Polynomials and Topological Indices of Dominating David Derived Networks
- Human Health Risk Assessment of Trace Metals in Surface Water Due to Leachate from the Municipal Dumpsite by Pollution Index: A Case Study from Ndawuse River, Abuja, Nigeria
- Analysis of Bowel Diseases from Blood Serum by Autofluorescence and Atomic Force Microscopy Techniques
- Hydrographic parameters and distribution of dissolved Cu, Ni, Zn and nutrients near Jeddah desalination plant
- Relationships between diatoms and environmental variables in industrial water biotopes of Trzuskawica S.A. (Poland)
- Optimum Conversion of Major Ginsenoside Rb1 to Minor Ginsenoside Rg3(S) by Pulsed Electric Field-Assisted Acid Hydrolysis Treatment
- Antioxidant, Anti-microbial Properties and Chemical Composition of Cumin Essential Oils Extracted by Three Methods
- Regulatory mechanism of ulinastatin on autophagy of macrophages and renal tubular epithelial cells
- Investigation of the sustained-release mechanism of hydroxypropyl methyl cellulose skeleton type Acipimox tablets
- Bio-accumulation of Polycyclic Aromatic Hydrocarbons in the Grey Mangrove (Avicennia marina) along Arabian Gulf, Saudi Coast
- Dynamic Change of Secondary Metabolites and spectrum-effect relationship of Malus halliana Koehne flowers during blooming
- Lipids constituents from Gardenia aqualla Stapf & Hutch
- Effect of using microwaves for catalysts preparation on the catalytic acetalization of glycerol with furfural to obtain fuel additives
- Effect of Humic Acid on the Degradation of Methylene Blue by Peroxymonosulfate
- Serum containing drugs of Gua Lou Xie Bai decoction (GLXB-D) can inhibit TGF-β1-Induced Epithelial to Mesenchymal Transition (EMT) in A549 Cells
- Antiulcer Activity of Different Extracts of Anvillea garcinii and Isolation of Two New Secondary Metabolites
- Analysis of Metabolites in Cabernet Sauvignon and Shiraz Dry Red Wines from Shanxi by 1H NMR Spectroscopy Combined with Pattern Recognition Analysis
- Can water temperature impact litter decomposition under pollution of copper and zinc mixture
- Released from ZrO2/SiO2 coating resveratrol inhibits senescence and oxidative stress of human adipose-derived stem cells (ASC)
- Validated thin-layer chromatographic method for alternative and simultaneous determination of two anti-gout agents in their fixed dose combinations
- Fast removal of pollutants from vehicle emissions during cold-start stage
- Review Article
- Catalytic activities of heterogeneous catalysts obtained by copolymerization of metal-containing 2-(acetoacetoxy)ethyl methacrylate
- Antibiotic Residue in the Aquatic Environment: Status in Africa
- Regular Articles
- Mercury fractionation in gypsum using temperature desorption and mass spectrometric detection
- Phytosynthetic Ag doped ZnO nanoparticles: Semiconducting green remediators
- Epithelial–Mesenchymal Transition Induced by SMAD4 Activation in Invasive Growth Hormone-Secreting Adenomas
- Physicochemical properties of stabilized sewage sludge admixtures by modified steel slag
- In Vitro Cytotoxic and Antiproliferative Activity of Cydonia oblonga flower petals, leaf and fruit pellet ethanolic extracts. Docking simulation of the active flavonoids on anti-apoptotic protein Bcl-2
- Synthesis and Characterization of Pd exchanged MMT Clay for Mizoroki-Heck Reaction
- A new selective, and sensitive method for the determination of lixivaptan, a vasopressin 2 (V2)-receptor antagonist, in mouse plasma and its application in a pharmacokinetic study
- Anti-EGFL7 antibodies inhibit rat prolactinoma MMQ cells proliferation and PRL secretion
- Density functional theory calculations, vibration spectral analysis and molecular docking of the antimicrobial agent 6-(1,3-benzodioxol-5-ylmethyl)-5-ethyl-2-{[2-(morpholin-4-yl)ethyl] sulfanyl}pyrimidin-4(3H)-one
- Effect of Nano Zeolite on the Transformation of Cadmium Speciation and Its Uptake by Tobacco in Cadmium-contaminated Soil
- Effects and Mechanisms of Jinniu Capsule on Methamphetamine-Induced Conditioned Place Preference in Rats
- Calculating the Degree-based Topological Indices of Dendrimers
- Efficient optimization and mineralization of UV absorbers: A comparative investigation with Fenton and UV/H2O2
- Metabolites of Tryptophane and Phenylalanine as Markers of Small Bowel Ischemia-Reperfusion Injury
- Adsorption and determination of polycyclic aromatic hydrocarbons in water through the aggregation of graphene oxide
- The role of NR2C2 in the prolactinomas
- Chromium removal from industrial wastewater using Phyllostachys pubescens biomass loaded Cu-S nanospheres
- Hydrotalcite Anchored Ruthenium Catalyst for CO2 Hydrogenation Reaction
- Preparation of Calcium Fluoride using Phosphogypsum by Orthogonal Experiment
- The mechanism of antibacterial activity of corylifolinin against three clinical bacteria from Psoralen corylifolia L
- 2-formyl-3,6-bis(hydroxymethyl)phenyl benzoate in Electrochemical Dry Cell
- Electro-photocatalytic degradation of amoxicillin using calcium titanate
- Effect of Malus halliana Koehne Polysaccharides on Functional Constipation
- Structural Properties and Nonlinear Optical Responses of Halogenated Compounds: A DFT Investigation on Molecular Modelling
- DMFDMA catalyzed synthesis of 2-((Dimethylamino)methylene)-3,4-dihydro-9-arylacridin-1(2H)-ones and their derivatives: in-vitro antifungal, antibacterial and antioxidant evaluations
- Production of Methanol as a Fuel Energy from CO2 Present in Polluted Seawater - A Photocatalytic Outlook
- Study of different extraction methods on finger print and fatty acid of raw beef fat using fourier transform infrared and gas chromatography-mass spectrometry
- Determination of trace fluoroquinolones in water solutions and in medicinal preparations by conventional and synchronous fluorescence spectrometry
- Extraction and determination of flavonoids in Carthamus tinctorius
- Therapeutic Application of Zinc and Vanadium Complexes against Diabetes Mellitus a Coronary Disease: A review
- Study of calcined eggshell as potential catalyst for biodiesel formation using used cooking oil
- Manganese oxalates - structure-based Insights
- Topological Indices of H-Naphtalenic Nanosheet
- Long-Term Dissolution of Glass Fibers in Water Described by Dissolving Cylinder Zero-Order Kinetic Model: Mass Loss and Radius Reduction
- Topological study of the para-line graphs of certain pentacene via topological indices
- A brief insight into the prediction of water vapor transmissibility in highly impermeable hybrid nanocomposites based on bromobutyl/epichlorohydrin rubber blends
- Comparative sulfite assay by voltammetry using Pt electrodes, photometry and titrimetry: Application to cider, vinegar and sugar analysis
- MicroRNA delivery mediated by PEGylated polyethylenimine for prostate cancer therapy
- Reversible Fluorescent Turn-on Sensors for Fe3+ based on a Receptor Composed of Tri-oxygen Atoms of Amide Groups in Water
- Sonocatalytic degradation of methyl orange in aqueous solution using Fe-doped TiO2 nanoparticles under mechanical agitation
- Hydrotalcite Anchored Ruthenium Catalyst for CO2 Hydrogenation Reaction
- Production and Analysis of Recycled Ammonium Perrhenate from CMSX-4 superalloys
- Topical Issue on Agriculture
- New phosphorus biofertilizers from renewable raw materials in the aspect of cadmium and lead contents in soil and plants
- Survey of content of cadmium, calcium, chromium, copper, iron, lead, magnesium, manganese, mercury, sodium and zinc in chamomile and green tea leaves by electrothermal or flame atomizer atomic absorption spectrometry
- Biogas digestate – benefits and risks for soil fertility and crop quality – an evaluation of grain maize response
- A numerical analysis of heat transfer in a cross-current heat exchanger with controlled and newly designed air flows
- Freshwater green macroalgae as a biosorbent of Cr(III) ions
- The main influencing factors of soil mechanical characteristics of the gravity erosion environment in the dry-hot valley of Jinsha river
- Free amino acids in Viola tricolor in relation to different habitat conditions
- The influence of filler amount on selected properties of new experimental resin dental composite
- Effect of poultry wastewater irrigation on nitrogen, phosphorus and carbon contents in farmland soil
- Response of spring wheat to NPK and S fertilization. The content and uptake of macronutrients and the value of ionic ratios
- The Effect of Macroalgal Extracts and Near Infrared Radiation on Germination of Soybean Seedlings: Preliminary Research Results
- Content of Zn, Cd and Pb in purple moor-grass in soils heavily contaminated with heavy metals around a zinc and lead ore tailing landfill
- Topical Issue on Research for Natural Bioactive Products
- Synthesis of (±)-3,4-dimethoxybenzyl-4-methyloctanoate as a novel internal standard for capsinoid determination by HPLC-ESI-MS/MS(QTOF)
- Repellent activity of monoterpenoid esters with neurotransmitter amino acids against yellow fever mosquito, Aedes aegypti
- Effect of Flammulina velutipes (golden needle mushroom, eno-kitake) polysaccharides on constipation
- Bioassay-directed fractionation of a blood coagulation factor Xa inhibitor, betulinic acid from Lycopus lucidus
- Antifungal and repellent activities of the essential oils from three aromatic herbs from western Himalaya
- Chemical composition and microbiological evaluation of essential oil from Hyssopus officinalis L. with white and pink flowers
- Bioassay-guided isolation and identification of Aedes aegypti larvicidal and biting deterrent compounds from Veratrum lobelianum
- α-Terpineol, a natural monoterpene: A review of its biological properties
- Utility of essential oils for development of host-based lures for Xyleborus glabratus (Coleoptera: Curculionidae: Scolytinae), vector of laurel wilt
- Phenolic composition and antioxidant potential of different organs of Kazakh Crataegus almaatensis Pojark: A comparison with the European Crataegus oxyacantha L. flowers
- Isolation of eudesmane type sesquiterpene ketone from Prangos heyniae H.Duman & M.F.Watson essential oil and mosquitocidal activity of the essential oils
- Comparative analysis of the polyphenols profiles and the antioxidant and cytotoxicity properties of various blue honeysuckle varieties
- Special Issue on ICCESEN 2017
- Modelling world energy security data from multinomial distribution by generalized linear model under different cumulative link functions
- Pine Cone and Boron Compounds Effect as Reinforcement on Mechanical and Flammability Properties of Polyester Composites
- Artificial Neural Network Modelling for Prediction of SNR Effected by Probe Properties on Ultrasonic Inspection of Austenitic Stainless Steel Weldments
- Calculation and 3D analyses of ERR in the band crack front contained in a rectangular plate made of multilayered material
- Improvement of fuel properties of biodiesel with bioadditive ethyl levulinate
- Properties of AlSi9Cu3 metal matrix micro and nano composites produced via stir casting
- Investigation of Antibacterial Properties of Ag Doped TiO2 Nanofibers Prepared by Electrospinning Process
- Modeling of Total Phenolic contents in Various Tea samples by Experimental Design Methods
- Nickel doping effect on the structural and optical properties of indium sulfide thin films by SILAR
- The effect mechanism of Ginnalin A as a homeopathic agent on various cancer cell lines
- Excitation functions of proton induced reactions of some radioisotopes used in medicine
- Oxide ionic conductivity and microstructures of Pr and Sm co-doped CeO2-based systems
- Rapid Synthesis of Metallic Reinforced in Situ Intermetallic Composites in Ti-Al-Nb System via Resistive Sintering
- Oxidation Behavior of NiCr/YSZ Thermal Barrier Coatings (TBCs)
- Clustering Analysis of Normal Strength Concretes Produced with Different Aggregate Types
- Magnetic Nano-Sized Solid Acid Catalyst Bearing Sulfonic Acid Groups for Biodiesel Synthesis
- The biological activities of Arabis alpina L. subsp. brevifolia (DC.) Cullen against food pathogens
- Humidity properties of Schiff base polymers
- Free Vibration Analysis of Fiber Metal Laminated Straight Beam
- Comparative study of in vitro antioxidant, acetylcholinesterase and butyrylcholinesterase activity of alfalfa (Medicago sativa L.) collected during different growth stages
- Isothermal Oxidation Behavior of Gadolinium Zirconate (Gd2Zr2O7) Thermal Barrier Coatings (TBCs) produced by Electron Beam Physical Vapor Deposition (EB-PVD) technique
- Optimization of Adsorption Parameters for Ultra-Fine Calcite Using a Box-Behnken Experimental Design
- The Microstructural Investigation of Vermiculite-Infiltrated Electron Beam Physical Vapor Deposition Thermal Barrier Coatings
- Modelling Porosity Permeability of Ceramic Tiles using Fuzzy Taguchi Method
- Experimental and theoretical study of a novel naphthoquinone Schiff base
- Physicochemical properties of heat treated sille stone for ceramic industry
- Sand Dune Characterization for Preparing Metallurgical Grade Silicon
- Catalytic Applications of Large Pore Sulfonic Acid-Functionalized SBA-15 Mesoporous Silica for Esterification
- One-photon Absorption Characterizations, Dipole Polarizabilities and Second Hyperpolarizabilities of Chlorophyll a and Crocin
- The Optical and Crystallite Characterization of Bilayer TiO2 Films Coated on Different ITO layers
- Topical Issue on Bond Activation
- Metal-mediated reactions towards the synthesis of a novel deaminolysed bisurea, dicarbamolyamine
- The structure of ortho-(trifluoromethyl)phenol in comparison to its homologues – A combined experimental and theoretical study
- Heterogeneous catalysis with encapsulated haem and other synthetic porphyrins: Harnessing the power of porphyrins for oxidation reactions
- Recent Advances on Mechanistic Studies on C–H Activation Catalyzed by Base Metals
- Reactions of the organoplatinum complex [Pt(cod) (neoSi)Cl] (neoSi = trimethylsilylmethyl) with the non-coordinating anions SbF6– and BPh4–
- Erratum
- Investigation on Two Compounds of O, O’-dithiophosphate Derivatives as Corrosion Inhibitors for Q235 Steel in Hydrochloric Acid Solution
Articles in the same Issue
- Regular Articles
- The effect of CuO modification for a TiO2 nanotube confined CeO2 catalyst on the catalytic combustion of butane
- The preparation and antibacterial activity of cellulose/ZnO composite: a review
- Linde Type A and nano magnetite/NaA zeolites: cytotoxicity and doxorubicin loading efficiency
- Performance and thermal decomposition analysis of foaming agent NPL-10 for use in heavy oil recovery by steam injection
- Spectroscopic (FT-IR, FT-Raman, UV, 1H and 13C NMR) insights, electronic profiling and DFT computations on ({(E)-[3-(1H-imidazol-1-yl)-1-phenylpropylidene] amino}oxy)(4-nitrophenyl)methanone, an imidazole-bearing anti-Candida agent
- A Simplistic Preliminary Assessment of Ginstling-Brounstein Model for Solid Spherical Particles in the Context of a Diffusion-Controlled Synthesis
- M-Polynomials And Topological Indices Of Zigzag And Rhombic Benzenoid Systems
- Photochemical Transformation of some 3-benzyloxy-2-(benzo[b]thiophen-2-yl)-4Hchromen-4-ones: A Remote Substituent Effect
- Dynamic Changes of Secondary Metabolites and Antioxidant Activity of Ligustrum lucidum During Fruit Growth
- Studies on the flammability of polypropylene/ammonium polyphosphate and montmorillonite by using the cone calorimeter test
- DSC, FT-IR, NIR, NIR-PCA and NIR-ANOVA for determination of chemical stability of diuretic drugs: impact of excipients
- Antioxidant and Hepatoprotective Effects of Methanolic Extracts of Zilla spinosa and Hammada elegans Against Carbon Tetrachlorideinduced Hepatotoxicity in Rats
- Prunus cerasifera Ehrh. fabricated ZnO nano falcates and its photocatalytic and dose dependent in vitro bio-activity
- Organic biocides hosted in layered double hydroxides: enhancing antimicrobial activity
- Experimental study on the regulation of the cholinergic pathway in renal macrophages by microRNA-132 to alleviate inflammatory response
- Synthesis, characterization, in-vitro antimicrobial properties, molecular docking and DFT studies of 3-{(E)-[(4,6-dimethylpyrimidin-2-yl)imino]methyl} naphthalen-2-ol and Heteroleptic Mn(II), Co(II), Ni(II) and Zn(II) complexes
- M-Polynomials and Topological Indices of Dominating David Derived Networks
- Human Health Risk Assessment of Trace Metals in Surface Water Due to Leachate from the Municipal Dumpsite by Pollution Index: A Case Study from Ndawuse River, Abuja, Nigeria
- Analysis of Bowel Diseases from Blood Serum by Autofluorescence and Atomic Force Microscopy Techniques
- Hydrographic parameters and distribution of dissolved Cu, Ni, Zn and nutrients near Jeddah desalination plant
- Relationships between diatoms and environmental variables in industrial water biotopes of Trzuskawica S.A. (Poland)
- Optimum Conversion of Major Ginsenoside Rb1 to Minor Ginsenoside Rg3(S) by Pulsed Electric Field-Assisted Acid Hydrolysis Treatment
- Antioxidant, Anti-microbial Properties and Chemical Composition of Cumin Essential Oils Extracted by Three Methods
- Regulatory mechanism of ulinastatin on autophagy of macrophages and renal tubular epithelial cells
- Investigation of the sustained-release mechanism of hydroxypropyl methyl cellulose skeleton type Acipimox tablets
- Bio-accumulation of Polycyclic Aromatic Hydrocarbons in the Grey Mangrove (Avicennia marina) along Arabian Gulf, Saudi Coast
- Dynamic Change of Secondary Metabolites and spectrum-effect relationship of Malus halliana Koehne flowers during blooming
- Lipids constituents from Gardenia aqualla Stapf & Hutch
- Effect of using microwaves for catalysts preparation on the catalytic acetalization of glycerol with furfural to obtain fuel additives
- Effect of Humic Acid on the Degradation of Methylene Blue by Peroxymonosulfate
- Serum containing drugs of Gua Lou Xie Bai decoction (GLXB-D) can inhibit TGF-β1-Induced Epithelial to Mesenchymal Transition (EMT) in A549 Cells
- Antiulcer Activity of Different Extracts of Anvillea garcinii and Isolation of Two New Secondary Metabolites
- Analysis of Metabolites in Cabernet Sauvignon and Shiraz Dry Red Wines from Shanxi by 1H NMR Spectroscopy Combined with Pattern Recognition Analysis
- Can water temperature impact litter decomposition under pollution of copper and zinc mixture
- Released from ZrO2/SiO2 coating resveratrol inhibits senescence and oxidative stress of human adipose-derived stem cells (ASC)
- Validated thin-layer chromatographic method for alternative and simultaneous determination of two anti-gout agents in their fixed dose combinations
- Fast removal of pollutants from vehicle emissions during cold-start stage
- Review Article
- Catalytic activities of heterogeneous catalysts obtained by copolymerization of metal-containing 2-(acetoacetoxy)ethyl methacrylate
- Antibiotic Residue in the Aquatic Environment: Status in Africa
- Regular Articles
- Mercury fractionation in gypsum using temperature desorption and mass spectrometric detection
- Phytosynthetic Ag doped ZnO nanoparticles: Semiconducting green remediators
- Epithelial–Mesenchymal Transition Induced by SMAD4 Activation in Invasive Growth Hormone-Secreting Adenomas
- Physicochemical properties of stabilized sewage sludge admixtures by modified steel slag
- In Vitro Cytotoxic and Antiproliferative Activity of Cydonia oblonga flower petals, leaf and fruit pellet ethanolic extracts. Docking simulation of the active flavonoids on anti-apoptotic protein Bcl-2
- Synthesis and Characterization of Pd exchanged MMT Clay for Mizoroki-Heck Reaction
- A new selective, and sensitive method for the determination of lixivaptan, a vasopressin 2 (V2)-receptor antagonist, in mouse plasma and its application in a pharmacokinetic study
- Anti-EGFL7 antibodies inhibit rat prolactinoma MMQ cells proliferation and PRL secretion
- Density functional theory calculations, vibration spectral analysis and molecular docking of the antimicrobial agent 6-(1,3-benzodioxol-5-ylmethyl)-5-ethyl-2-{[2-(morpholin-4-yl)ethyl] sulfanyl}pyrimidin-4(3H)-one
- Effect of Nano Zeolite on the Transformation of Cadmium Speciation and Its Uptake by Tobacco in Cadmium-contaminated Soil
- Effects and Mechanisms of Jinniu Capsule on Methamphetamine-Induced Conditioned Place Preference in Rats
- Calculating the Degree-based Topological Indices of Dendrimers
- Efficient optimization and mineralization of UV absorbers: A comparative investigation with Fenton and UV/H2O2
- Metabolites of Tryptophane and Phenylalanine as Markers of Small Bowel Ischemia-Reperfusion Injury
- Adsorption and determination of polycyclic aromatic hydrocarbons in water through the aggregation of graphene oxide
- The role of NR2C2 in the prolactinomas
- Chromium removal from industrial wastewater using Phyllostachys pubescens biomass loaded Cu-S nanospheres
- Hydrotalcite Anchored Ruthenium Catalyst for CO2 Hydrogenation Reaction
- Preparation of Calcium Fluoride using Phosphogypsum by Orthogonal Experiment
- The mechanism of antibacterial activity of corylifolinin against three clinical bacteria from Psoralen corylifolia L
- 2-formyl-3,6-bis(hydroxymethyl)phenyl benzoate in Electrochemical Dry Cell
- Electro-photocatalytic degradation of amoxicillin using calcium titanate
- Effect of Malus halliana Koehne Polysaccharides on Functional Constipation
- Structural Properties and Nonlinear Optical Responses of Halogenated Compounds: A DFT Investigation on Molecular Modelling
- DMFDMA catalyzed synthesis of 2-((Dimethylamino)methylene)-3,4-dihydro-9-arylacridin-1(2H)-ones and their derivatives: in-vitro antifungal, antibacterial and antioxidant evaluations
- Production of Methanol as a Fuel Energy from CO2 Present in Polluted Seawater - A Photocatalytic Outlook
- Study of different extraction methods on finger print and fatty acid of raw beef fat using fourier transform infrared and gas chromatography-mass spectrometry
- Determination of trace fluoroquinolones in water solutions and in medicinal preparations by conventional and synchronous fluorescence spectrometry
- Extraction and determination of flavonoids in Carthamus tinctorius
- Therapeutic Application of Zinc and Vanadium Complexes against Diabetes Mellitus a Coronary Disease: A review
- Study of calcined eggshell as potential catalyst for biodiesel formation using used cooking oil
- Manganese oxalates - structure-based Insights
- Topological Indices of H-Naphtalenic Nanosheet
- Long-Term Dissolution of Glass Fibers in Water Described by Dissolving Cylinder Zero-Order Kinetic Model: Mass Loss and Radius Reduction
- Topological study of the para-line graphs of certain pentacene via topological indices
- A brief insight into the prediction of water vapor transmissibility in highly impermeable hybrid nanocomposites based on bromobutyl/epichlorohydrin rubber blends
- Comparative sulfite assay by voltammetry using Pt electrodes, photometry and titrimetry: Application to cider, vinegar and sugar analysis
- MicroRNA delivery mediated by PEGylated polyethylenimine for prostate cancer therapy
- Reversible Fluorescent Turn-on Sensors for Fe3+ based on a Receptor Composed of Tri-oxygen Atoms of Amide Groups in Water
- Sonocatalytic degradation of methyl orange in aqueous solution using Fe-doped TiO2 nanoparticles under mechanical agitation
- Hydrotalcite Anchored Ruthenium Catalyst for CO2 Hydrogenation Reaction
- Production and Analysis of Recycled Ammonium Perrhenate from CMSX-4 superalloys
- Topical Issue on Agriculture
- New phosphorus biofertilizers from renewable raw materials in the aspect of cadmium and lead contents in soil and plants
- Survey of content of cadmium, calcium, chromium, copper, iron, lead, magnesium, manganese, mercury, sodium and zinc in chamomile and green tea leaves by electrothermal or flame atomizer atomic absorption spectrometry
- Biogas digestate – benefits and risks for soil fertility and crop quality – an evaluation of grain maize response
- A numerical analysis of heat transfer in a cross-current heat exchanger with controlled and newly designed air flows
- Freshwater green macroalgae as a biosorbent of Cr(III) ions
- The main influencing factors of soil mechanical characteristics of the gravity erosion environment in the dry-hot valley of Jinsha river
- Free amino acids in Viola tricolor in relation to different habitat conditions
- The influence of filler amount on selected properties of new experimental resin dental composite
- Effect of poultry wastewater irrigation on nitrogen, phosphorus and carbon contents in farmland soil
- Response of spring wheat to NPK and S fertilization. The content and uptake of macronutrients and the value of ionic ratios
- The Effect of Macroalgal Extracts and Near Infrared Radiation on Germination of Soybean Seedlings: Preliminary Research Results
- Content of Zn, Cd and Pb in purple moor-grass in soils heavily contaminated with heavy metals around a zinc and lead ore tailing landfill
- Topical Issue on Research for Natural Bioactive Products
- Synthesis of (±)-3,4-dimethoxybenzyl-4-methyloctanoate as a novel internal standard for capsinoid determination by HPLC-ESI-MS/MS(QTOF)
- Repellent activity of monoterpenoid esters with neurotransmitter amino acids against yellow fever mosquito, Aedes aegypti
- Effect of Flammulina velutipes (golden needle mushroom, eno-kitake) polysaccharides on constipation
- Bioassay-directed fractionation of a blood coagulation factor Xa inhibitor, betulinic acid from Lycopus lucidus
- Antifungal and repellent activities of the essential oils from three aromatic herbs from western Himalaya
- Chemical composition and microbiological evaluation of essential oil from Hyssopus officinalis L. with white and pink flowers
- Bioassay-guided isolation and identification of Aedes aegypti larvicidal and biting deterrent compounds from Veratrum lobelianum
- α-Terpineol, a natural monoterpene: A review of its biological properties
- Utility of essential oils for development of host-based lures for Xyleborus glabratus (Coleoptera: Curculionidae: Scolytinae), vector of laurel wilt
- Phenolic composition and antioxidant potential of different organs of Kazakh Crataegus almaatensis Pojark: A comparison with the European Crataegus oxyacantha L. flowers
- Isolation of eudesmane type sesquiterpene ketone from Prangos heyniae H.Duman & M.F.Watson essential oil and mosquitocidal activity of the essential oils
- Comparative analysis of the polyphenols profiles and the antioxidant and cytotoxicity properties of various blue honeysuckle varieties
- Special Issue on ICCESEN 2017
- Modelling world energy security data from multinomial distribution by generalized linear model under different cumulative link functions
- Pine Cone and Boron Compounds Effect as Reinforcement on Mechanical and Flammability Properties of Polyester Composites
- Artificial Neural Network Modelling for Prediction of SNR Effected by Probe Properties on Ultrasonic Inspection of Austenitic Stainless Steel Weldments
- Calculation and 3D analyses of ERR in the band crack front contained in a rectangular plate made of multilayered material
- Improvement of fuel properties of biodiesel with bioadditive ethyl levulinate
- Properties of AlSi9Cu3 metal matrix micro and nano composites produced via stir casting
- Investigation of Antibacterial Properties of Ag Doped TiO2 Nanofibers Prepared by Electrospinning Process
- Modeling of Total Phenolic contents in Various Tea samples by Experimental Design Methods
- Nickel doping effect on the structural and optical properties of indium sulfide thin films by SILAR
- The effect mechanism of Ginnalin A as a homeopathic agent on various cancer cell lines
- Excitation functions of proton induced reactions of some radioisotopes used in medicine
- Oxide ionic conductivity and microstructures of Pr and Sm co-doped CeO2-based systems
- Rapid Synthesis of Metallic Reinforced in Situ Intermetallic Composites in Ti-Al-Nb System via Resistive Sintering
- Oxidation Behavior of NiCr/YSZ Thermal Barrier Coatings (TBCs)
- Clustering Analysis of Normal Strength Concretes Produced with Different Aggregate Types
- Magnetic Nano-Sized Solid Acid Catalyst Bearing Sulfonic Acid Groups for Biodiesel Synthesis
- The biological activities of Arabis alpina L. subsp. brevifolia (DC.) Cullen against food pathogens
- Humidity properties of Schiff base polymers
- Free Vibration Analysis of Fiber Metal Laminated Straight Beam
- Comparative study of in vitro antioxidant, acetylcholinesterase and butyrylcholinesterase activity of alfalfa (Medicago sativa L.) collected during different growth stages
- Isothermal Oxidation Behavior of Gadolinium Zirconate (Gd2Zr2O7) Thermal Barrier Coatings (TBCs) produced by Electron Beam Physical Vapor Deposition (EB-PVD) technique
- Optimization of Adsorption Parameters for Ultra-Fine Calcite Using a Box-Behnken Experimental Design
- The Microstructural Investigation of Vermiculite-Infiltrated Electron Beam Physical Vapor Deposition Thermal Barrier Coatings
- Modelling Porosity Permeability of Ceramic Tiles using Fuzzy Taguchi Method
- Experimental and theoretical study of a novel naphthoquinone Schiff base
- Physicochemical properties of heat treated sille stone for ceramic industry
- Sand Dune Characterization for Preparing Metallurgical Grade Silicon
- Catalytic Applications of Large Pore Sulfonic Acid-Functionalized SBA-15 Mesoporous Silica for Esterification
- One-photon Absorption Characterizations, Dipole Polarizabilities and Second Hyperpolarizabilities of Chlorophyll a and Crocin
- The Optical and Crystallite Characterization of Bilayer TiO2 Films Coated on Different ITO layers
- Topical Issue on Bond Activation
- Metal-mediated reactions towards the synthesis of a novel deaminolysed bisurea, dicarbamolyamine
- The structure of ortho-(trifluoromethyl)phenol in comparison to its homologues – A combined experimental and theoretical study
- Heterogeneous catalysis with encapsulated haem and other synthetic porphyrins: Harnessing the power of porphyrins for oxidation reactions
- Recent Advances on Mechanistic Studies on C–H Activation Catalyzed by Base Metals
- Reactions of the organoplatinum complex [Pt(cod) (neoSi)Cl] (neoSi = trimethylsilylmethyl) with the non-coordinating anions SbF6– and BPh4–
- Erratum
- Investigation on Two Compounds of O, O’-dithiophosphate Derivatives as Corrosion Inhibitors for Q235 Steel in Hydrochloric Acid Solution