Zeitschrift für Kristallographie - New Crystal Structures

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Volume 235, Issue 1

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Zeitschrift für Kristallographie - New Crystal Structures

Contents

Open Access
The crystal structure of 3,5-dicarboxybenzenaminium perchlorate monohydrate, C₈H₈ClNO₉

October 23, 2019

Bin Cai, Shu-Jing Li, Meng-En Zhu, Meng-Qi Li, Yuning Meng

Page range: 1-2

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C 8 H 8 ClNO 9 , monoclinic, P 2 1 / n (no. 14), a = 7.1284(3) Å, b = 8.5538(5) Å, c = 18.7089(10) Å, β = 99.760(2)°, V = 1124.26(10) Å 3 , Z = 4, R gt (F) = 0.0381, wR ref (F 2 ) = 0.1031, T = 150 K.
Open Access
The crystal structure of poly[(m₄-4-bromoisophthalato-κ⁴O: O′:O′′:O′′′)zinc(II)], C₈H₃BrO₄Zn

October 2, 2019

Xin-Hong Chang

Page range: 3-4

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C 8 H 3 BrO 4 Zn, monoclinic, P 2 1 / c (no. 14), a = 4.7134(4) Å, b = 15.4354(13) Å, c = 12.0064(9) Å, β = 98.942(8)°, V = 862.89(12) Å 3 , Z = 4, R gt ( F ) = 0.0445, wR ref ( F 2 ) = 0.1193, T = 292.67(10) K.
Open Access
Crystal structure of (E)-2-(2-chloro-6-hydroxybenzylidene)hydrazine-1-carbothioamide, C₈H₈ClN₃O₄S

August 23, 2019

Xia Li, Shangjun Liu, Weihong Yan, Mingle Shen, Chaohui Xue

Page range: 5-6

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C 8 H 8 ClN 3 O 4 S, monoclinic, P 2 1 / c (no. 14), a = 12.662(2) Å, b = 5.2782(8) Å, c = 14.841(2) Å, β = 94.103(3)°, V = 989.3(3) Å 3 , Z = 4, R gt ( F ) = 0.0317, wR ref ( F 2 ) = 0.1232, T = 293(2) K.
Open Access
Crystal structure of 1,1′-methylenebis(3-ethyl-1H-imidazol-3-ium) bis(hexafluorophosphate(V)), C₁₁H₁₈F₁₂N₄P₂

September 21, 2019

Wan-Ming Xiong, Jing Chen, Wen Zhao, Yao-Hong Zhou, Chen Jing, Xu-Liang Nie

Page range: 7-9

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C 11 H 18 F 12 N 4 P 2 , monoclinic, P 2 1 / c (no. 14), a = 14.975(3) Å, b = 9.897(2) Å, c = 13.525(3) Å, β = 105.507(3)°, V = 1931.5(7) Å 3 , Z = 4, R gt ( F ) = 0.0590, wR ref ( F 2 ) = 0.1843, T = 296(2) K.
Open Access
The crystal structure of hexakis(1-isopropyl-1H-imidazole-κ¹N)copper(II) dichloride, C₃₆H₅₈Cl₂CuN₁₂

September 18, 2019

Miao Cheng, Shuang Cheng

Page range: 11-13

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C 36 H 58 Cl 2 CuN 12 , monoclinic, P 2 1 / c (no. 14), a = 8.1490(8) Å, b = 17.0301(15) Å, c = 16.8649(14) Å, β = 101.629(3)°, Z = 2, V = 2292.4(4) Å 3 , R gt ( F ) = 0.0419, wR ref ( F 2 ) = 0.1121, T = 298(2) K.
Open Access
Crystal structure of catena-poly[μ₂-4,4′-bipyridine-κ²N:N′)-tetrakis(μ₂-2-((3,5,6-trichloropyridin-2-yl)oxy)acetato-κ²O:O′)dicobalt(II)], C₁₉H₁₀Cl₆CoN₃O₆

October 11, 2019

Zhong-Xiang Du, Jun-Xia Li, Ruo-Fei Bai

Page range: 15-17

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C 19 H 10 Cl 6 CoN 3 O 6 , tetragonal, I 4̄ (no. 82), a = 13.1152(4) Å, c = 14.2497(6) Å, V = 2451.07(18) Å 3 , Z = 4, R gt ( F ) = 0.0359, wR ref ( F 2 ) = 0.0843, T = 293.2(3) K.
Open Access
Crystal structure of (E)-1-(4-(((E)-2-bromo-6-hydroxybenzylidene)amino)phenyl)ethan-1-one O-methyl oxime, C₁₆H₁₅BrN₂O₂

August 23, 2019

Jin-Xia Ma, Ping Wei, Qing-Lin Li, Tao Fu, Ji-Xing Zhao, Li Zhao

Page range: 19-20

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C 16 H 15 BrN 2 O 2 , monoclinic, P 2 1 (no. 4), a = 10.9311(8) Å, b = 3.9554(3) Å, c = 16.5215(12) Å, β = 92.743(2)°, V = 713.52(9) Å 3 , Z = 2, R gt ( F ) = 0.0335, wR ref ( F 2 ) = 0.0655, T = 173(2) K.
Open Access
Crystal structure of ethyl 2-methyl-4-(5-methylthiophen-2-yl)-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate, C₁₈H₂₁NO₃S

August 17, 2019

Han-Sheng Luo, Yao Liu

Page range: 21-22

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C 18 H 21 NO 3 S, triclinic, P 1̄ (no. 2), a = 7.2345(18) Å, b = 10.842(3) Å, c = 11.573(3) Å, α = 69.174(4)°, β = 77.335(4)°, γ = 79.555(4)°. V = 822.5(4) Å 3 , Z = 2, R gt ( F ) = 0.0471, wR ref ( F 2 ) = 0.1419, T = 296(2) K.
Open Access
The crystal structure of 5-bromo-2-(1-methyl-1H-tetrazol-5-yl)pyridine, C₇H₆BrN₅

September 14, 2019

Hang-Jun Tang, Yang-Rong Xu, Xiao-Hui Wang, Feng-Lan Zhao, Qing-Guo Meng

Page range: 23-25

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C 7 H 6 BrN 5 , orthorhombic, Acam (no. 64; unconventional setting of Cmce formerly known as Cmca ), a = 12.3735(8) Å, b = 20.8690(11) Å, c = 6.8385(6) Å, V = 1765.9(2) Å 3 , Z = 8, R gt ( F ) = 0.0471, wR ref ( F 2 ) = 0.1152, T = 293(2) K.
Open Access
Crystal structure of Bis(acetato-κ²O,O′)-bis[4-(dimethylamino)pyridine-κN]nickel(II), C₁₈H₂₆N₄NiO₄

September 27, 2019

Zhuang-Yu Li, E. Liu, Fang-fang Jian, Tong-ling Liang

Page range: 27-28

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C 18 H 26 N 4 NiO 4 , triclinic, P 1̄ (no. 2), a = 7.7547(16) Å, b = 7.8666(16) Å, c = 8.2798(17) Å, α = 90.46(3)°, β = 96.24(3)°, γ = 93.25(3)°, V = 501.24(18) Å 3 , Z = 1, R gt ( F ) = 0.0294, wR ref ( F 2 ) = 0.0873, T = 310 K.
Open Access
Crystal structure of (E)-3-chloro-2-(((4-chlorophenyl)imino)methyl)phenol, C₁₃H₉Cl₂NO

September 11, 2019

Wei Song, Yanju Yang

Page range: 29-30

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C 13 H 9 Cl 2 NO, monoclinic, P 2 1 / c (no. 14), a = 21.039(6) Å, b = 4.0172(12) Å, c = 14.561(4) Å, β = 97.849(5)°, V = 1219.1(6) Å 3 , Z = 4, R gt ( F ) = 0.0378, wR ref ( F 2 ) = 0.1211, T = 293(2) K.
Open Access
The co-crystal structure of (17b)-estra-1,3,5(10)-triene-3,17diol – acetamide (1/1), a Z′ = 4 structure, C₂₀H₂₉NO₃

August 17, 2019

Xiao F. Gong, Tao Song, Li F. Ning, Xiao F. Chen, Juan Xu, Peng Li, Ying Z. Gou, Hui P. Wang

Page range: 31-34

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C 20 H 29 NO 3 , monoclinic, P 2 1 (no. 4), a = 16.167(3) Å, b = 9.3424(19) Å, c = 25.656(5) Å, β = 108.27(3)°, V = 3679.8(14) Å 3 , Z = 8, R gt ( F ) = 0.1030, wR ref ( F 2 ) = 0.2296, T = 153(2) K.
Open Access
Crystal structure of 3-(3-(pyridin-3-yl)ureido)benzoic acid, C₁₃H₁₁N₃O₃

August 23, 2019

Qi-Long Zhang, Hai-Fang Xie, Qing Yu, Xiao-Sheng Yang

Page range: 35-36

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C 13 H 11 N 3 O 3 , Orthorhombic, Pna 2 1 (no. 33), a = 9.2062(6) Å, b = 11.5258(7) Å, c = 11.5263(7) Å, V = 1223.04(13) Å 3 , Z = 4, R gt ( F ) = 0.0377, wR ref ( F 2 ) = 0.1006, T = 293(2) K.
Open Access
The crystal structure of 1,1′-(9-ethyl-9H-carbazole-3,6-diyl)bis(3-ethyl-1H-imidazol-3-ium) bis(hexafluorophosphate(IV)), C₂₄H₂₇N₅F₁₂P₂

August 5, 2019

Zhang Shilu, Zhao Bo, Luo Jiewei

Page range: 37-39

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C 24 H 27 N 5 F 12 P 2 , monoclinic, P 2 1 / n (no. 14), a = 12.395(4) Å, b = 16.630(6) Å, c = 26.899(10) Å, β = 90.395(7)°, V = 5545(4) Å 3 , Z = 8, R gt ( F ) = 0.0650, wR ref ( F 2 ) = 0.1651, T = 113(2) K.
Open Access
The crystal structure of 2-bromoisophthalic acid, C₈H₅BrO₄

September 11, 2019

Shu-Jing Li, Ke Li, Yi-Wen Li

Page range: 41-42

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C 8 H 5 BrO 4 , triclinic, P 1̄ (no. 2), a = 4.8161(3) Å, b = 7.3727(5) Å, c = 12.1230(7) Å, α = 81.004(3)°, β = 78.897(3)°, γ = 72.829(3)°, V = 401.30(4) Å 3 , Z = 2, R gt (F) = 0.0201, wR ref (F 2 ) = 0.0479, T = 150(2) K.
Open Access
The crystal structure of 13-ethoxycarbonyl-9-methyl-4-chlor-11-thioxo-8-oxa-10,12-diazatricyclo[7.3.1.0^2,7]trideca-2,4,6-triene, C₁₄H₁₅ClN₂O₃S

September 9, 2019

Chuansheng Cui, Haichao Zhang, Xiaoyu Gu

Page range: 43-44

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C 14 H 15 ClN 2 O 3 S, monoclinic C 2/ c (no. 15), a = 17.0104(15) Å, b = 8.6786(7) Å, c = 20.4283(18) Å, β = 93.977(1)°, V = 3008.5(4) Å 3 , Z = 8, R gt ( F ) = 0.0363, wR ref ( F 2 ) = 0.0937, T = 298(2) K.
Open Access
The crystal structure of (E)-4-((4-(diethylamino)benzylidene)amino)-N,N-diphenylaniline, C₂₉H₂₉N₃

September 17, 2019

Yue Liu, Zhou-Hua Yang, Jian-Jun Ni, Zhaod-Di Liu

Page range: 45-47

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C 29 H 29 N 3 , triclinic, P 1̄ (no. 2), a = 10.677(4) Å, b = 11.325(4) Å, c = 21.530(8) Å, α = 88.026(5)°, β = 75.646(5)°, γ = 71.504(4)°, V = 2389.0(15) Å 3 , Z = 4, R gt ( F ) = 0.0663, wR ref ( F 2 ) = 0.2002, T = 293(2) K.
Open Access
Crystal structure of 2-(3-(2-(4-phenylpiperazin-1-yl)ethyl)benzyl)isoindoline-1,3-dione, C₂₇H₂₇N₃O₂

September 11, 2019

Aiqing Feng, Bin Lv

Page range: 49-51

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C 27 H 27 N 3 O 2 , triclinic, P 1̄ (no. 2), a = 6.9263(4) Å, b = 10.0832(7) Å, c = 17.3531(10) Å, α = 75.708(5)°, β = 87.142(5)°, γ = 74.935(6)°, V = 1133.92(13) Å 3 , Z = 2, R gt ( F ) = 0.0605, wR ref ( F 2 ) = 0.1661, T = 290(1) K.
Open Access
Crystal structure of 2-ethoxy-6-((E)-((3-(((E)-3-ethoxy-2-hydroxybenzylidene)amino)-2-hydroxypropyl)iminio)methyl)phenolate, C₂₁H₂₆N₂O₅

September 17, 2019

Su Wenhui, Tian Dayong, Yu Zhichao, Yang Liguo, Niu Yongsheng

Page range: 53-54

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C 21 H 26 N 2 O 5 , monoclinic, P 2 1 / c (no. 14), a = 19.779(9) Å, b = 5.332(2) Å, c = 18.945(8) Å, β = 94.572(6)°, V = 1991.4(15) Å 3 , Z = 4, R gt ( F ) = 0.0425, wR ref ( F 2 ) = 0.1179, T = 298(2) K.
Open Access
The crystal structure of catena-poly(μ₂-4,4′-bipyridine-κ²N:N′)-tetrakis(μ₂-2-((3,5,6-trichloropyridin-2-yl)oxy)acetato-κ²O:O′)dinickel(II)], C₁₉H₁₀Cl₆N₃NiO₆

September 18, 2019

Zhong-Xiang Du, Jun-Xia Li, Ruo-Fei Bai

Page range: 55-56

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C 19 H 10 Cl 6 N 3 NiO 6 , tetragonal, I 4̄ (no. 82), a = 13.1205(4) Å, c = 14.2717(6) Å, V = 2456.84(18) Å 3 , Z = 4, R gt ( F ) = 0.0384, wR ref ( F 2 ) = 0.0756, T = 293.2(3) K.
Open Access
Crystal structure of hexakis(μ₂-azido-κ²N:N)-diazido-κ¹N-tetrakis(phenanthroline-κ²N,N′)tetrazinc(II), C₄₈H₃₂N₃₂Zn₄

October 9, 2019

Yu-Quan Feng, Zhi-Guo Zhong, Zi-Long Yue

Page range: 57-58

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C 48 H 32 N 32 Zn 4 , triclinic, P 1̄ (no. 2), a = 9.9928(14) Å, b = 10.1374(14) Å, c = 14.2362(19) Å, α = 71.710(2)°, β = 76.166(2)°, γ = 71.086(2)°, V = 1280.1(3) Å 3 , Z = 1, R gt ( F ) = 0.0314, wR ref ( F 2 ) = 0.0795, T = 296(2) K.
Open Access
Synthesis and crystal structure of bis{2-bromo-6-(((4-(1-(methoxyimino)ethyl)phenyl)imino)methyl)phenolato-κ²N,O}cobalt(II)–dichloromethane(1/1), C₃₄H₃₂Br₂Cl₄CoN₄O₄

October 18, 2019

Tao Fu, Jin-Xia Ma, Ping Wei, Qing-Lin Li, Ji-Xing Zhao, Li Zhao

Page range: 59-60

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C 34 H 32 Br 2 Cl 4 CoN 4 O 4 , monoclinic, C 2/ c (no. 15), a = 30.281(3) Å, b = 8.9971(8) Å, c = 13.9050(13) Å, β = 107.053(5)°, Z = 4, V = 3621.7(6) Å 3 , R gt ( F ) = 0.0648, wR ref ( F 2 ) = 0.1629, T = 173(2) K.
Open Access
Crystal structure of (E)-3-chloro-2-(((4-nitrophenyl)imino)methyl)phenol, C₁₃H₉ClN₂O₃

September 11, 2019

Wei Song, Yanju Yang, Jin Li

Page range: 61-62

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C 13 H 9 ClN 2 O 3 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 7.401(3) Å, b = 12.005(5) Å, c = 13.808(5) Å, V = 1226.8(8) Å 3 , Z = 4, R gt ( F ) = 0.0673, wR ref ( F 2 ) = 0.1473, T = 293(2) K.
Open Access
Crystal structure of aqua-bis(5-bromo-6-methyl-picolinato-κ²N,O)zinc(II) dihydrate, C₁₄H₁₆Br₂N₂O₇Zn

September 26, 2019

Jun-Xia Li, Zhong-Xiang Du, Ruo-Fei Bai

Page range: 63-65

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C 14 H 16 Br 2 N 2 O 7 Zn, orthorhombic, Pna 2 1 (no. 33), a = 15.4300(3) Å, b = 10.6264(2) Å, c = 11.4638(2) Å, V = 1879.66(6) Å 3 , Z = 4, R gt ( F ) = 0.0328, wR ref ( F 2 ) = 0.0709, T = 293 K.
Open Access
Crystal structure of biaqua(2,2′-bipyridine-4,4′-dicarboxylato-κ²N,N′)(pyridine-2,6-dicarboxylato-κ³O,N,O′)nickel(II) hydrate, C₁₉H₁₅N₃NiO₁₀

October 4, 2019

Jin-Ke Jiang, Ying-Wen Yang, Hui Jiang

Page range: 67-68

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C 19 H 15 N 3 NiO 10 , monoclinic, P 2 1 / c (no. 14), a = 12.7175(10) Å, b = 10.6780(10) Å, c = 15.0802(16) Å, β = 96.786(9)°, V = 2033.5(3) Å 3 , Z = 4, R gt ( F ) = 0.0358, wR ref ( F 2 ) = 0.0960, T = 293(2) K.
Open Access
Synthesis and crystal structure of bis(2-(((4-(1-(ethoxyimino)ethyl)phenyl)imino)methyl)-5-fluorophenolato-κ²N,O)zinc(II) - methanol (1/1), C₃₃H₃₂F₂N₄O₄Zn

October 9, 2019

Ji-Xing Zhao

Page range: 69-71

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C 33 H 32 F 2 N 4 O 5 Zn, triclinic, P 1̄ (no. 2), a = 9.5132(5) Å, b = 13.0781(6) Å, c = 14.0448(6) Å, α = 63.0950(10)°, β = 73.5640(10)°, γ = 78.870(2)°, V = 1490.24(12) Å 3 , Z = 2, R gt ( F ) = 0.0459, wR ref ( F 2 ) = 0.1004, T = 173(2) K.
Open Access
Crystal structure of tetraaqua-bis(μ₂-5-aminoisophthalato-κ³N:O,O′)-bis(4,4′-dipyridylsulfide-κ¹N)dizinc(II), C₃₆H₃₄N₆O₁₂S₂Ni₂

September 20, 2019

Xin-Hong Chang, Zhi-Min Zhai, Xiao-Min Lu

Page range: 73-75

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C 36 H 34 N 6 O 12 S 2 Ni 2 , monoclinic, C 2/ c (no. 15), a = 29.642(4) Å, b = 6.2241(4) Å, c = 21.667(2) Å, β = 108.592(13)°, V = 3788.9(7) Å 3 , Z = 4, R gt ( F ) = 0.0907, wR ref ( F 2 ) = 0.1605, T = 293(2) K.
Open Access
Crystal structure of (1,4,8,11-tetraazacyclotetradecane-κ⁴N,N′,N′′,N′′′)palladium(II) tetracyanonickelate(II), C₁₄H₂₄N₈NiPd

August 17, 2019

Kwang Ha

Page range: 77-78

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C 14 H 24 N 8 NiPd, monoclinic, P 2 1 / n (no. 14), a = 8.9786(9) Å, b = 8.3191(9) Å, c = 11.9489(12) Å, β = 94.772(3)°, V = 889.42(16) Å 3 , Z = 2, R gt ( F ) = 0.0161, wR ref ( F 2 ) = 0.0401, T = 223(2) K.
Open Access
The crystal structure of 3-benzyl-1-((8-(benzyloxy)quinolin-2-yl)methyl)-1H-imidazol-3-ium hexafluorophosphate, C₂₇H₂₄N₃OF₆P

October 14, 2019

Luo Jiewei, Zhang Shilu, Liu Yiming, Zhao Bo

Page range: 79-80

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C 27 H 24 N 3 OF 6 P, monoclinic, Cc (no. 9), a = 18.0589(18) Å, b = 12.5100(9) Å, c = 13.3659(12) Å, β = 124.522(7)°, V = 2487.9(4) Å 3 , Z = 4, R gt ( F ) = 0.0437, wR ref ( F 2 ) = 0.1141, T = 113(2) K.
Open Access
Crystal structure of 1-(4-chloro-2-hydroxy-5-iodophenyl)ethan-1-one, C₈H₆ClIO₂

September 18, 2019

Malose J. Mphahlele

Page range: 81-83

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C 8 H 6 ClIO 2 , orthorhombic, Pbcn (no. 60), a = 13.3204(7) Å, b = 7.2517(4) Å, c = 18.5627(9) Å, V = 1793.07(16) Å 3 , Z = 8, R gt ( F ) = 0.0195, wR ref (F2) = 0.0483, T = 173 K.
Open Access
Crystal structure of hexaaquamagnesium(II) bis((E)-4-((4-(dimethylamino)phenyl)diazenyl)benzenesulfonate), C₂₈H₄₀MgN₆O₁₂S₂

September 25, 2019

Garam Park, In-Hwan Oh, Seong-Hun Park

Page range: 85-86

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C 28 H 40 MgN 6 O 12 S 2 , monoclinic, P 2 1 / c (no. 14), a = 6.1988(3) Å, b = 7.1103(4) Å, c = 38.7135(4) Å, β = 91.519(3)°, V = 1705.71(13) Å 3 , Z = 2, R gt ( F ) = 0.0360, wR ref ( F 2 ) = 0.0755, T = 293 K.
Open Access
Crystal structure of the coordination polymer catena-poly[(1,2-di(pyridin-4-yl)ethane-κN)-(μ₂-2-nitroisophthalato-κ²O:O′)zinc(II)], C₂₀H₁₇N₃O₇Zn

October 9, 2019

Guang-Zhen Liu, Lu-Ping Ma, Ru Jia

Page range: 87-89

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C 20 H 17 N 3 O 7 Zn, monoclinic, P 2 1 / n (no. 14), a = 10.4368(3) Å, b = 15.1527(5) Å, c = 12.9007(3) Å, β = 101.900(3)°, V = 1996.36(10) Å 3 , Z = 4, R gt ( F ) = 0.0410, wR ref ( F 2 ) = 0.0898, T = 293(2) K.
Open Access
Crystal structure of catena-{[tri-aqua-di-sodium bis(2-{[n-butyl(methyl)carbamothioyl]sulfanyl}acetate)]}_n, [C₁₆H₃₄N₂Na₂O₇S₄]_n

October 4, 2019

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 91-94

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[C 16 H 34 N 2 Na 2 O 7 S 4 ] n , triclinic, P 1̄ (no. 2), a = 5.3734(1) Å, b = 11.0473(2) Å, c = 22.2264(5) Å, α = 102.075(2)°, β = 96.202(2)°, γ = 97.383(2)°, V = 1267.06(5) Å 3 , Z = 2, R gt ( F ) = 0.0335, wR ref ( F 2 ) = 0.0941, T = 100(2) K.
Open Access
The crystal structure of diaqua-bis(μ₂-3-((3-acetyl-5-carboxyphenyl)oxidophosphoryl)-5-carboxybenzoato-κ²O:O′)bis(5,5′-dimethyl-2,2′-bipyridine-k²N,N′)zinc(II), C₅₆H₄₆N₄O₂₂P₂Zn₂

October 9, 2019

Yesheng Li, Huating Chen, Han Chen, Xingen Hu, Hongping Xiao

Page range: 95-97

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C 56 H 46 N 4 O 22 P 2 Zn 2 , monoclinic, P 2 1 / c (no. 14), a = 9.6537(4) Å, b = 31.1374(11) Å, c = 9.8927(4) Å, β = 112.709(2)°, V = 2743.13(19) Å 3 , Z = 2, R gt ( F ) = 0.0341, wR ref ( F 2 ) = 0.0934, T = 296(2) K.
Open Access
Crystal structure of N′,2-bis((E)-2-chloro-6-hydroxybenzylidene)hydrazine-1-carbothiohydrazide, C₁₅H₁₂Cl₂N₄O₂S

September 19, 2019

Weiping Liu

Page range: 99-100

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C 15 H 12 Cl 2 N 4 O 2 S, monoclinic, P 2 1 / c (no. 14), a = 12.236(7) Å, b = 20.199(10) Å, c = 6.992(4) Å, β = 105.987(9)°, V = 1661.2(16) Å 3 , Z = 4, R gt ( F ) = 0.0707, wR ref ( F 2 ) = 0.1917, T = 293(2) K.
Open Access
Crystal structure of 2-[(1E)-{[1,3-dihydroxy-2-(hydroxymethyl)propan-2-yl]iminiumyl}methyl]-5-(dodecyloxy)benzen-1-olate, C₂₃H₃₉NO₅

October 14, 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 101-103

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C 23 H 39 NO 5 , monoclinic, P 2 1 / c (no. 14), a = 26.1698(4) Å, b = 9.4863(2) Å, c = 9.0929(2) Å, β = 97.376(2)°, V = 2238.67(8) Å 3 , Z = 4, R gt ( F ) = 0.0539, wR ref ( F 2 ) = 0.1580, T = 100(2) K.
Open Access
Crystal structure of 12-(2-hydroxybenzoyl)benzo[f]pyrido[1,2-a]indole-6,11-dione, C₂₃H₁₃NO₄

September 27, 2019

Peng Luo, Amar G. Chittiboyina, Mei Wang, Ikhlas A. Khan, Wei-Gao Pan, Wan-Xing Wei

Page range: 105-107

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C 23 H 13 NO 4 , monoclinic, P 2 1 / n (no. 14), a = 11.6537(6) Å, b = 5.1315(2) Å, c = 26.8047(13) Å, β = 96.266(3)°, V = 1593.4(13) Å 3 , Z = 4, R gt ( F ) = 0.0531, wR ref ( F 2 ) = 0.1432, T = 90.0(5) K.
Open Access
Crystal structure of chlorido-(4-chloro-6-(p-tolyl)pyrimidine-κ²C,N)-(triphenylphosphane-κP)palladium(II), C₂₉H₂₃Cl₂N₂PPd

October 23, 2019

Chen Xu, Xin-Hua Lou

Page range: 109-111

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C 29 H 23 Cl 2 N 2 PPd, monoclinic, P 2 1 / c (no. 14), a = 9.4028(16) Å, b = 30.928(5) Å, c = 9.3071(16) Å, β = 103.222(2)°, V = 2634.8(8) Å 3 , Z = 4, R gt ( F ) = 0.0423, wR ref ( F 2 ) = 0.1047, T = 296(2) K.
Open Access
Crystal structure of catena-poly[diaqua-bis(3,4,5,6-tetrabromo-carboxybenzoato-κ¹O)-(μ₂-4,4′-bipyridine-κ²N:N′)cobalt(II)], C₂₆H₁₄Br₈CoN₂O₁₀

October 4, 2019

Yong-Shuang Li, Jia-Yang Luo, Man-Qiu He, Min-Le Han

Page range: 113-115

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C 26 H 14 Br 8 CoN 2 O 10 , orthorhombic, Pbcn (no. 60), a = 24.3935(3) Å, b = 11.4505(1) Å, c = 11.7004(1) Å, V = 3268.13(6) Å 3 , Z = 4, R gt ( F ) = 0.0313, wR ref ( F 2 ) = 0.0819, T = 293 K.
Open Access
Crystal structure of catena-poly[dibenzyl-dichlorido-(μ₂-[4,4′-bipyridine]1,1′-dioxide-κ²O:O′)tin(IV)], C₂₄H₂₂Cl₂N₂O₂Sn

September 11, 2019

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 117-119

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C 24 H 22 Cl 2 N 2 O 2 Sn, monoclinic, P 2 1 / n (no. 14), a = 12.6418(1) Å, b = 13.2422(1) Å, c = 13.6364(1) Å, β = 104.6370(10)°, V = 2208.72(3) Å 3 , Z = 4, R gt ( F ) = 0.0292, wR ref ( F 2 ) = 0.0778, T = 100(2) K.
Open Access
Crystal structure of benzyl-chlorido-(4-chloro-N-[(2-oxidophenyl)methylidene]benzenecarbohydrazonato)-methanol-tin(IV), C₂₂H₂₀Cl₂N₂O₃Sn

September 17, 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 121-124

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C 22 H 20 Cl 2 N 2 O 3 Sn, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 8.1234(3) Å, b = 10.7966(3) Å, c = 24.9785(8) Å, V = 2190.74(12) Å 3 , Z = 4, R gt ( F ) = 0.0271, wR ref ( F 2 ) = 0.0645, T = 293(2) K.
Open Access
Crystal structure of catena-poly[triaqua-(1,3-di(1H-imidazol-1-yl)benzene-κ²N:N′)-(3-nitrophthalato-κ¹O)cobalt(II)] — water (2/3), C₂₀H₂₂N₅O_10.5Co

October 18, 2019

Wei-Dong Yin, Qian-Long Liu, Gui-Lian Li

Page range: 125-128

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C 20 H 22 N 5 O 10.5 Co, triclinic, P 1̄ (no. 2), a = 7.9667(3) Å, b = 11.5847(4) Å, c = 13.5305(5) Å, α = 81.096(3)°, β = 83.110(3)°, γ = 69.997(4)°, V = 1156.26(8) Å 3 , Z = 2, R gt ( F ) = 0.0439, wR ref ( F 2 ) = 0.1096, T = 292(1) K.
Open Access
Crystal structure of (3R,5R,8R,9R,10R,12R,13R,14R)-4,4,8,10,14-pentamethyl-17-((R)-2,6,6-trimethyltetrahydro-2H-pyran-2-yl)hexadecahydro-1H-cyclopenta[a]phenanthrene-3,12-diol, C₃₀H₅₂O₃

October 14, 2019

Ruo-Lin Zhao, Hui-Yun Wang, Ming-Zhu Luan, Xia Zheng, Feng-Lan Zhao, Qing-Guo Meng

Page range: 129-131

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C 30 H 52 O 3 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 6.71147(14) Å, b = 16.6565(4) Å, c = 25.0815(6) Å, V = 2803.85(11) Å 3 , Z = 4, R gt ( F ) = 0.0405, wR ref ( F 2 ) = 0.1092, T = 293(2) K.
Open Access
Crystal structure of 3-(3-(4-carboxyphenyl)ureido)pyridin-1-ium perchlorate, C₂₆H₂₄Cl₂N₆O₁₄

September 28, 2019

Qi-Long Zhang, Qing Yu, Hai-Fang Xie, Xiao-Sheng Yang

Page range: 133-134

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C 26 H 24 Cl 2 N 6 O 14 , monoclinic, P 2 1 / c (no. 14), a = 15.7471(18) Å, b = 14.1486(15) Å, c = 13.7894(15) Å, β = 109.588(3)°, V = 2894.5(6) Å 3 , Z = 4, R gt ( F ) = 0.0744, wR ref ( F 2 ) = 0.2246, T = 293(2) K.
Open Access
Crystal structure of 8-hydroxy-2-methylquinolin-1-ium chloride dihydrate, C₁₀H₁₄ClNO₃

September 11, 2019

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 135-137

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C 10 H 14 ClNO 3 , monoclinic, P 2 1 / c (no. 14), a = 7.2706(2) Å, b = 14.8440(5) Å, c = 10.3910(3) Å, β = 101.101(2)°, V = 1100.46(6) Å 3 , Z = 4, R gt ( F ) = 0.0268, wR ref ( F 2 ) = 0.0735, T = 100(2) K.
Open Access
Crystal structure of (dibenzyl sulphoxide-κO)dibromido-bis(4-bromobenzyl-κC)tin(IV), C₂₈H₂₆Br₄OSSn

September 9, 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 139-141

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C 28 H 26 Br 4 OSSn, monoclinic, Cm (no. 8), a = 8.4055(1) Å, b = 26.9988(3) Å, c = 6.4207(1) Å, β = 98.164(1)°, V = 1442.34(3) Å 3 , Z = 2, R gt ( F ) = 0.0174, wR ref ( F 2 ) = 0.0454, T = 100(2) K.
Open Access
Crystal structure of bromido-tri(4-chlorophenyl-κ¹C)-(ethanol-κ¹O)tin(IV) — 4,4′-dimethyl-2,2′-bipyridine (2/1), C₅₂H₄₈Br₂Cl₆N₂O₂Sn₂

October 18, 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 143-145

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C 52 H 48 Br 2 Cl 6 N 2 O 2 Sn 2 , triclinic, P 1̄ (no. 2), a = 8.8297(1) Å, b = 12.2632(2) Å, c = 12.6884(2) Å, α = 84.191(1)°, β = 83.940(1)°, γ = 76.086(1)°, V = 1322.04(3) Å 3 , Z = 1, R gt ( F ) = 0.0222, wR ref ( F 2 ) = 0.0621, T = 100(2) K.
Open Access
Crystal structure of 2-butyl-6-(ethylamino)-1H-benzo[de]isoquinoline-1,3(2H)-dione, C₁₈H₂₀N₂O₂

September 20, 2019

Peilian Liu, Fangru Jiang, Guiyuan Huang, Ying Sun, Liping Huang

Page range: 147-149

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C 18 H 20 N 2 O 2 , monoclinic, C 2/ c (no. 15), a = 27.5693(13) Å, b = 8.3005(4) Å, c = 16.8797(8) Å, β = 127.0225(12)°, V = 3084.0(3) Å 3 , Z = 8, R gt ( F ) = 0.0642, wR ref ( F 2 ) = 0.2248, T = 293(2) K.
Open Access
Crystal structure of (4-chloro-N-[(2-oxido-5-chlorophenyl)methylidene] benzene-carbohydrazonato-κ³N,O,O′)bis(2-fluorobenzyl)tin(IV), C₂₈H₂₀Cl₂F₂N₂O₂Sn

September 9, 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 151-153

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C 28 H 20 Cl 2 F 2 N 2 O 2 Sn, monoclinic, P 2 1 / c (no. 14), a = 27.8125(4) Å, b = 8.4443(2) Å, c = 10.7891(1) Å, β = 91.074(1)° V = 2533.45(7) Å 3 , Z = 4, R gt ( F ) = 0.0600, wR ref ( F 2 ) = 0.1608, T = 100(2) K.
Open Access
Crystal structure of aqua-chlorido-(4-fluorobenzyl-κC)-(N′-(4-methoxy-2-oxidobenzylidene)-3-hydroxy-2-naphthohydrazidato-κ³N,O,O′)tin(IV), C₂₆H₂₂ClFN₂O₅Sn

September 27, 2019

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 155-157

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C 26 H 22 ClFN 2 O 5 Sn, triclinic, P 1̄ (no. 2), a = 7.1473(6) Å, b = 12.8246(11) Å, c = 13.2899(11) Å, α = 97.541(5)°, β = 94.503(6)°, γ = 96.247(5)°, V = 1195.13(18) Å 3 , Z = 2, R gt ( F ) = 0.0325, wR ref ( F 2 ) = 0.0756, T = 296(2) K.
Open Access
Crystal structure of catena-poly[tri(4-chlorophenyl)-(μ₂-hydroxido)tin(IV)] – 2-propanol (1/1), C₂₁H₂₁Cl₃O₂Sn

September 18, 2019

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 159-161

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C 21 H 21 Cl 3 O 2 Sn, monoclinic, P 2 1 / n (no. 14), a = 13.3360(1) Å, b = 8.2332(1) Å, c = 20.2443(2) Å, β = 104.070(1)°, V = 2156.10(4) Å 3 , Z = 4, R gt ( F ) = 0.0199, wR ref ( F 2 ) = 0.0544, T = 100(2) K.
Open Access
Crystal structure of bromido-dimethyl-4-tolyl-(triphenylphosphine oxide)tin(IV), C₂₇H₂₈BrOPSn

September 14, 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 163-165

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C 27 H 28 BrOPSn, monoclinic, P 2 1 / n (no. 14), a = 10.9369(1) Å, b = 12.2170(1) Å, c = 18.8402(1) Å, β = 91.869(1)°, V = 2516.01(3) Å 3 , Z = 4, R gt ( F ) = 0.0279, wR ref ( F 2 ) = 0.0754, T = 100(2) K.
Open Access
Crystal structure of 2-(bis(2-hydroxyethyl)ammonio)ethane-1-sulfonate, C₆H₁₅NO₅S

October 2, 2019

Baogang Wang, Xiaxia Man

Page range: 167-168

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C 6 H 15 NO 5 S, monoclinic, Cc (no. 9), a = 15.167(5) Å, b = 6.422(5) Å, c = 10.969(5) Å, β = 117.407(5)°, V = 948.5(9) Å 3 , Z = 4, R gt ( F ) = 0.0278, wR ref ( F 2 ) = 0.0755, T = 293(2) K.
Open Access
Crystal structure of bis[triaqua-(μ₂-1,2-di(4-pyridyl)ethylene-κ²N:N′)-(4-sulfonatobenzoato-κ²O,O′)zinc(II)], C₁₃H₁₅NO₈SZn

October 11, 2019

Xiao-Ling Li, Ling-Yun Xin, Yue-Yi Yu, Qing-Qing Yang, Meng-Ke Liu

Page range: 169-170

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C 13 H 15 NO 8 SZn, monoclinic, C 2/ c (no. 15), a = 12.3456(3) Å, b = 13.7680(4) Å, c = 19.9125(5) Å, β = 107.051(2)°, V = 3235.85(14) Å 3 , Z = 8, R gt ( F ) = 0.0325, wR ref ( F 2 ) = 0.0819, T = 293(2) K.
Open Access
Crystal structure of 2-((2-(3-hydroxy-7-methylene-2,3-dihydro-7H-furo[3,2-g]chromen-2-yl)propan-2-yl)oxy)-6-(hydroxymethyl)tetrahydro-2H-pyran-3,4,5-triol – a marmesin derivative, C₂₀H₂₄O₁₀

October 9, 2019

Yu-Yan Li, Xu-Liang Nie, Xiao-Xiang Fu, Bao-Tong Li, Wen-Wen Peng

Page range: 171-173

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C 20 H 24 O 10 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 6.3728(6) Å, b = 14.3835(14) Å, c = 20.453(2) Å, V = 1874.8(3) Å 3 , Z = 4, R gt ( F ) = 0.0272, wR ref ( F 2 ) = 0.0558, T = 296(2) K.
Open Access
Crystal structure of octa(4-chlorobenzyl)-dichlorido-bis(μ₂-methanolato)-bis(μ₃-oxo)-tetratin(IV), C₅₈H₅₄Cl₁₀O₄Sn₄

September 19, 2019

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 175-177

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C 58 H 54 Cl 10 O 4 Sn 4 , monoclinic, C 2/ c (no. 15), a = 27.6269(8) Å, b = 9.0623(2) Å, c = 24.7099(7) Å, β = 103.070(1)°, V = 6026.2(3) Å 3 , Z = 4, R gt ( F ) = 0.0259, wR ref ( F 2 ) = 0.0671, T = 296(2) K.
Open Access
Crystal structure of iodido-triphenyl-(triphenylphosphine oxide)tin(IV), C₃₆H₃₀IOPSn

October 11, 2019

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 179-181

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C 36 H 30 IOPSn, monoclinic, P 2 1 (no. 4), a = 9.7251(6) Å, b = 17.3609(11) Å, c = 10.0542(6) Å, β = 114.379(1)°, V = 1546.16(17) Å 3 , Z = 2, R gt ( F ) = 0.0113, wR ref ( F 2 ) = 0.0301, T = 296(2) K.
Open Access
Crystal structure of dichlorido-bis(4-methylphenyl-κC)-bis(triphenylarsine oxide-κO)tin(IV), C₅₀H₄₄As₂Cl₂O₂Sn

October 9, 2019

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 183-185

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C 50 H 44 As 2 Cl 2 O 2 Sn, monoclinic, P 2 1 / n (no. 14), a = 10.84633(6) Å, b = 14.61376(9) Å, c = 13.53951(8) Å, β = 91.5073(6)°, V = 2145.35(2) Å 3 , Z = 2, R gt ( F ) = 0.0237, wR ref ( F 2 ) = 0.0642, T = 100(2) K.
Open Access
Crystal structure of 4-benzyl-1-oxo-N-phenethyl-1H-[1,4]oxazino [4,3-b]indazole-3-carboxamide, C₂₆H₂₁N₃O₃

October 18, 2019

Xian Wei, Ying Fen Li, You Lin Xu, Meng Lan Lv

Page range: 187-188

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C 26 H 21 N 3 O 3 , triclinic, P 1̄ (no. 2), a = 9.149(4) Å, b = 9.249(4) Å, c = 13.508(7) Å, α = 91.995(9)°, β = 101.158(8)°, γ = 108.392(8)°, V = 1058.5(9) Å 3 , Z = 2, R gt ( F ) = 0.0628, wR ref ( F 2 ) = 0.1668, T = 296(2) K.
Open Access
Crystal structure of bis{(N-[(5-chloro-2-oxidophenyl)methylidene]-2-hydroxybenzenecarbohydrazonato)-dioxo-molybdenum(VI)}(μ₂-4,4′-bipyridine), C₃₈H₂₆Cl₂Mo₂N₆O₁₀

October 11, 2019

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 189-191

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C 38 H 26 Cl 2 Mo 2 N 6 O 10 , triclinic, P 1̄ (no. 2), a = 7.7151(2) Å, b = 10.5336(2) Å, c = 12.5668(2) Å, α = 73.027(2)°, β = 76.226(2)°, γ = 72.269(2)°, V = 917.83(4) Å 3 , Z = 1, R gt ( F ) = 0.0234, wR ref ( F 2 ) = 0.0612, T = 100(2) K.
Open Access
Crystal structure of dichlorido-octamethyl-bis(μ₃-oxido)-bis(μ₂-2-(phenylamino)ethanolato-κ²O:O)tetratin(IV), C₂₄H₄₄Cl₂N₂O₄Sn₄

October 9, 2019

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 193-195

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C 24 H 44 Cl 2 N 2 O 4 Sn 4 , orthorhombic, Pbca (no. 61), a = 13.9593(2) Å, b = 11.1227(2) Å, c = 21.6656(3) Å, V = 3363.91(9) Å 3 , Z = 4, R gt ( F ) = 0.0252, wR ref ( F 2 ) = 0.0642, T = 100(2) K.
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The crystal structure of 1-(2-(2-(imidazo[1,5-a]pyridine-4-ium)ethoxy)ethyl)-imidazo[1,5-a]pyridine-4-ium bis(hexafluorophosphate) — acetonitrile (1/1), C₁₈H₂₀ON₄F₁₂P₂

October 18, 2019

Zhao Bo, Zhong Yue, Luo Jiewei

Page range: 197-199

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C 18 H 20 ON 4 F 12 P 2 , triclinic, P 1̄ (no. 2), a = 9.393(8) Å, b = 10.894(10) Å, c = 13.716(12) Å, α = 107.741(14)°, β = 100.379(15)°, γ = 92.869(14)°, V = 1306.7(19) Å 3 , Z = 2, R gt ( F ) = 0.0916, wR ref ( F 2 ) = 0.1970, T = 296(2) K.
Open Access
Crystal structure of cyclo[tetra(μ₂-cyanido)-tetracyanido-bis(1,4,7,10-tetraazacyclododecane-κ⁴N,N′,N′′,N′′′)dinickel(II)dipalladium(II)] hexahydrate, C₂₄H₅₂N₁₆Ni₂O₆Pd₂

October 2, 2019

Kwang Ha

Page range: 201-202

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C 24 H 52 N 16 Ni 2 O 6 Pd 2 , monoclinic, P 2 1 / c (no. 14), a = 8.6416(3) Å, b = 14.2237(5) Å, c = 15.5573(5) Å, β = 93.8054(12)°, V = 1908.02(11) Å 3 , Z = 2, R gt ( F ) = 0.0312, wR ref ( F 2 ) = 0.0915, T = 223(2) K.
Open Access
Crystal structure of (dimethyl sulfoxide)-dioxido-[2-hydroxy-N′-(4-oxo-4-phenylbutan-2-ylidene)benzohydrazidato κ³N,O,O′]molybdenum(VI), C₁₉H₂₀MoN₂O₆S

October 9, 2019

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 203-205

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C 19 H 20 MoN 2 O 6 S, orthorhombic, Pbca (no. 61), a = 13.4060(1) Å, b = 16.5112(1) Å, c = 17.6357(1) Å, V = 3903.65(4) Å 3 , Z = 8, R gt ( F ) = 0.0217, wR ref ( F 2 ) = 0.0602, T = 100(2) K.
Open Access
Crystal structure of bis(acetylacetonato-κ²O,O′)-(ethanolamine-κ²N,O)copper(II), C₁₄H₂₅CuNO₅

October 11, 2019

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 207-209

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C 14 H 25 CuNO 5 , triclinic, P 1̄ (no. 2), a = 7.7319(3) Å, b = 9.9198(5) Å, c = 11.6827(5) Å, α = 81.866(4)°, β = 75.576(4)°, γ = 74.562(4)°, V = 833.78(7) Å 3 , Z = 2, R gt ( F ) = 0.0287, wR ref ( F 2 ) = 0.0807, T = 100(2) K.
Open Access
Crystal structure of chlorido-diphenyl-(isopropyl(propyl)carbamodithioato-κ²S,S′)tin(IV), C₁₉H₂₄ClNS₂Sn

October 18, 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 211-214

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C 19 H 24 ClNS 2 Sn, triclinic, P 1̄ (no. 2), a = 10.1894(1) Å, b = 14.0236(2) Å, c = 14.5114(2) Å, α = 91.070(1)°, β = 96.997(1)°, γ = 98.222(1)°, V = 2035.59(5) Å 3 , Z = 4, R gt ( F ) = 0.0211, wR ref ( F 2 ) = 0.0556, T = 100(2) K.
Open Access
The crystal structure of bis(imidazole-1-yl)methane monohydrate, C₇H₁₀N₄O

October 18, 2019

Yong Wang, Jun Yuan, Duanlin Cao, Jianlong Wang, Lizhen Chen

Page range: 215-216

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C 7 H 10 N 4 O, monoclinic, I 2 (no. 5), a = 15.7815(13) Å, b = 4.3242(3) Å, c = 12.4658(9) Å, β = 106.301(8)°, V = 816.50(10) Å 3 , Z = 4, R gt ( F ) = 0.0473, wR ref ( F 2 ) = 0.1067, T = 113.25(10) K.
Open Access
The crystal structure of bis(4-nitroimidazole-1-1yl)methane, C₇H₆N₆O₄

October 18, 2019

Wang Yong, Yuan Jun, Cao Duanlin, Wang Jianlong, Chen Lizhen

Page range: 217-218

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C 7 H 6 N 6 O 4 , monoclinic, P 2 1 / c (no. 14), a = 21.0402(7) Å, b = 7.9959(3) Å, c = 11.8012(4) Å, β = 102.379(1)°, V = 1939.22(12) Å 3 , Z = 8, R gt ( F ) = 0.0481, wR ref ( F 2 ) = 0.1296, T = 170 K.
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Crystal structure of di(naphthalen-2-yl)sulfane, C₂₀H₁₄S

October 18, 2019

Wen Ma, Pu-Bo Li, Sen Liang

Page range: 219-220

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C 20 H 14 S, monoclinic, C 2/ c (no. 15), a = 31.155(3) Å, b = 5.8419(6) Å, c = 7.7505(8) Å, β = 94.664(4)°, V = 1405.9(3) Å 3 , Z = 4, R gt ( F ) = 0.0480, wR ref ( F 2 ) = 0.1352, T = 193(2) K.
Open Access
Crystal structure of 3-acetyl-6-bromo-4-hydroxy-2H-chromen-2-one, C₁₁H₇BrO₄

October 11, 2019

Siya T. Hulushe, Meloddy H. Manyeruke, Eric C. Hosten, Perry T. Kaye

Page range: 221-222

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C 11 H 7 BrO 4 , triclinic, P 1̄ (no. 2), a = 4.3164(5) Å, b = 10.7922(12) Å, c = 11.1521(11) Å, α = 98.075(4)°, β = 100.741(4)°, γ = 95.325(5)°, V = 501.55(9) Å 3 , Z = 2, R gt ( F ) = 0.0203, wR ref ( F 2 ) = 0.0544, T = 200(2) K.
Open Access
Crystal structure of N′²,N′⁶-bis((E)-1-(pyrazin-2-yl)ethylidene)pyridine-2,6-dicarbohydrazide — methanol (1/2), C₂₁H₂₅N₉O₄

October 14, 2019

Fang Xiangqing, Wang Ren, Du Kai, Gu Jia, Yang Liguo

Page range: 223-224

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C 21 H 25 N 9 O 4 , monoclinic, P 2/ n (no. 13), a = 10.277(3) Å, b = 10.081(3) Å, c = 11.264(4) Å, β = 104.582(4)°, V = 1129.4(6) Å 3 , Z = 2, R gt ( F ) = 0.0452, wR ref ( F 2 ) = 0.1278, T = 296(2) K [1], [2], [3].
Open Access
The crystal structure of 3-nitro-4-(p-tolylamino)-2H-chromen-2-one, C₁₆H₁₂N₂O₄

October 14, 2019

Vidoslav S. Dekić, Marko V. Rodić, Niko S. Radulović, Milenko N. Ristić, Biljana R. Dekić, Dejan M. Gurešić, Novica R. Ristić

Page range: 225-227

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C 16 H 12 N 2 O 4 , triclinic, P 1̄ (no. 2), a = 10.7105(5) Å, b = 11.2685(5) Å, c = 13.0145(6) Å, α = 99.292(4)°, β = 109.607(4)°, γ = 96.771(4)°, V = 1435.01(12) Å 3 , Z = 4, R gt (F) = 0.0427, wR ref (F 2 ) = 0.1124, T = 295(2) K.
Open Access
The crystal structure of 1,2-bis((4-methoxyphenyl)ethynyl)benzene, C₂₄H₁₈O₂

October 11, 2019

Shuai Wu, Ling Peng, Pan Zhou, Zhigang Zeng

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C 24 H 18 O 2 , orthorhombic, Ccc 2 (no. 37), a = 9.7401(14) Å, b = 34.509(5) Å, c = 21.970(3) Å, V = 7384.7(19) Å 3 , Z = 16, R gt ( F ) = 0.0738, wR ref ( F 2 ) = 0.1559, T = 298(2) K.
Open Access
Crystal structure of a low-temperature (100 K) polymorph of catena-poly[(μ₂-4,4′-bipyridine-κ²N,N′)-bis(O,O′-diethyldithiophosphato-κ¹S)zinc(II)], C₁₈H₂₈N₂O₄P₂S₄Zn

October 18, 2019

Yee Seng Tan, Edward R.T. Tiekink

Page range: 233-237

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C 18 H 28 N 2 O 4 P 2 S 4 Zn, triclinic, P 1̄ (no. 2), a = 15.2379(1) Å, b = 17.3322(2) Å, c = 21.8829(1) Å, α = 75.919(1)°, β = 78.050(1)°, γ = 68.170(1)°, V = 5159.97(8) Å 3 , Z = 8, R gt ( F ) = 0.0246, wR ref ( F 2 ) = 0.0681, T = 100 K.
Open Access
The pseudosymmetric low temperature polymorph of catena-poly[(μ₂-4,4′-bipyridyl-κN,N′)-bis(O,O′-diethyldithiophosphato-κS)-cadmium(II)], {C₁₈H₂₈CdN₂O₄P₂S₄}_n

October 19, 2019

Yee Seng Tan, Edward R.T. Tiekink

Page range: 239-242

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C 18 H 28 CdN 2 O 4 P 2 S 4 , triclinic, P 1̄ (no. 2), a = 10.3735(1) Å, b = 15.2066(2) Å, c = 26.5231(2) Å, α = 85.178(1)°, β = 81.311(1)°, γ = 71.541(1)°, V = 3920.17(7) Å 3 , Z = 6, R gt ( F ) = 0.0214, wR ref ( F 2 ) = 0.0556, T = 100(2) K.
Open Access
Crystal structure of 3-iodophthalic acid, C₈H₅IO₄

October 18, 2019

Chao-Jun Du, Zong-Dong Wang, Da-Feng Zhu, Yuan-Liang Zhu, Yan Zeng

Page range: 243-244

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C 8 H 5 IO 4 , triclinic, P 1̄ (no. 2), a = 4.5570(3) Å, b = 7.7720(5) Å, c = 12.7660(8) Å, α = 99.906(3)°, β = 97.718(3)°, γ = 105.651(3)°, V = 421.02(5) Å 3 , Z = 2, R gt ( F ) = 0.0191, wR ref ( F 2 ) = 0.0433, T = 150(2) K.
Open Access
The crystal structure of tert-butyl (tert-butoxy(oxo)methyl)(5-bromo-2-fluorophenyl)carbamate, C₁₆H₂₁BrFNO₄

October 19, 2019

Chun Ji, Yu-Mei Qin

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C 16 H 21 BrFNO 4 , monoclinic, P 2 1 / n (no. 14), a = 9.0896(4) Å, b = 10.8609(4) Å, c = 18.5637(8) Å, β = 99.5050(10)°, V = 1807.47(13) Å 3 , Z = 4, R gt ( F ) = 0.0382, wR ref ( F 2 ) = 0.0900, T = 170 K.
Open Access
The crystal structure of bis(μ₂-5,7-dichloroquinolin-8-olato-κ³N,O:O)-tetrakis(5,7-dichloroquinolin-8-olato-κ²N,O)bis(methanol-κ¹O)dieuropium(III) — toluene (1/1), C₆₃H₃₉Cl₁₂Eu₂N₆O₈

October 25, 2019

Orbett T. Alexander, Alice Brink, Hendrik G. Visser

Page range: 247-249

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C 63 H 39 Cl 12 Eu 2 N 6 O 8 , triclinic, P 1̄ (no. 2), a = 10.720(5) Å, b = 12.232(5) Å, c = 14.267(5) Å, α = 65.288(32)°, β = 71.325(5)°, γ = 88.067(5)°, V = 1599.1(11) Å3, Z = 1, R gt ( F ) = 0.0358, wR ref ( F 2 ) = 0.0785, T = 293(2) K.
Open Access
Crystal structure of dichlorido-(N′-(1-(3-ethylpyrazin-2-yl)ethylidene)-4-methoxybenzohydrazide-κ³N,N′,O)cadmium(II), C₁₆H₁₈N₄O₂Cl₂Cd

October 18, 2019

Wei-Guo Duan, Yi-Peng Guo, Long Lin, Wei-Na Wu

Page range: 251-252

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C 16 H 18 N 4 O 2 Cl 2 Cd, monoclinic, P 2 1 / n (no. 14), a = 9.833(2) Å, b = 17.404(4) Å, c = 11.694(3) Å, β = 112.901(3)°, V = 1843.5(8) Å 3 , Z = 4, R gt ( F ) = 0.0280, wR ref ( F 2 ) = 0.0728, T = 296(2) K.
Open Access
A redetermination of the crystal structure of catena-poly[(bis(O,O′-isopropyl dithiophosphato-κ²S,S′)-(μ₂-1,2-bis(3-pyridylmethylene)hydrazine-κ²N,N′)cadmium(II)], {C₂₄H₃₈CdN₄O₄P₂S₄}_n

October 17, 2019

Yee Seng Tan, Edward R.T. Tiekink

Page range: 253-255

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C 24 H 38 CdN 4 O 4 P 2 S 4 , monoclinic, P 2 1 / n (no. 14), a = 12.2264(1) Å, b = 10.8805(1) Å, c = 12.9590(1) Å, β = 108.172(1)°, V = 1637.95(3) Å 3 , Z = 2, R gt ( F ) = 0.0183, wR ref ( F 2 ) = 0.0468, T = 100(2) K.

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