Zeitschrift für Kristallographie - New Crystal Structures

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Volume 235, Issue 2

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Zeitschrift für Kristallographie - New Crystal Structures

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Frontmatter

February 3, 2020

Page range: i-viii

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Open Access
Synthesis and crystal structure of bis{5-fluorine-2-(((4-(1-(methoxy-imino)ethyl)phenyl) imino)methyl)phenolato-κ²N,O}copper(II), C₃₂H₂₈CuF₂N₄O₄

October 31, 2019

Ji-Xing Zhao, Qin Wu

Page range: 257-258

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C 32 H 28 CuF 2 N 4 O 4 , monoclinic, P 2 1 / n (no. 14), a = 10.5489(3) Å, b = 6.2601(1) Å, c = 21.3299(7) Å, β = 99.401(1)°, V = 1389.65(6) Å 3 , Z = 2, R gt ( F ) = 0.0312, wR ref ( F 2 ) = 0.0849, T = 173(2) K.
Open Access
Redetermination of the crystal structure of N′-(3-ethoxy-2-hydroxybenzylidene)-4-fluorobenzohydrazide monohydrate, C₁₆H₁₇FN₂O₄

September 9, 2019

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 259-261

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C 16 H 17 FN 2 O 4 , monoclinic, P 2 1 / c (no. 14), a = 9.23280(10) Å, b = 12.9330(2) Å, c = 12.3477(2) Å, β = 97.383(1)°, V = 1462.19(4) Å 3 , Z = 4, R gt ( F ) = 0.0318, wR ref ( F 2 ) = 0.0861, T = 100(2) K.
Open Access
The crystal structure of (E)-N′-(1-(3-chloro-4-fluorophenyl) ethylidene)-2-hydroxybenzohydrazide, C₁₅H₁₂ClFN₂O₂

October 25, 2019

Xifeng Yan, Shibin Zhong, Hong Zhang

Page range: 263-265

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C 15 H 12 ClFN 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 13.9210(13) Å, b = 13.2329(15) Å, c = 18.7191(19) Å, β = 126.250(2)°, V = 2780.9(5) Å 3 , Z = 8, R gt ( F ) = 0.0499, wR ref ( F 2 ) = 0.1420, T = 293(2) K.
Open Access
Crystal structure of (E)-N-[4-(1H)-imidazolyl phenyl]-(2-methylphenyl)methanimine, C₁₇H₁₅N₃

November 2, 2019

Jie Liu, Ruo-Liu Cheng, Shu-Zhen Yu, Ying Zou

Page range: 267-268

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C 17 H 15 N 3 , monoclinic, P 2 1 / c (no. 14), a = 11.6325(11) Å, b = 7.8196(7) Å, c = 15.5644(11) Å, β = 106.288(2)°, V = 1358.9(2) Å 3 , Z = 4, R gt ( F ) = 0.0363, wR ref ( F 2 ) = 0.0975, T = 296(2) K.
Open Access
The crystal structure of 1-benzyl-4-(2-(phenylethynyl)phenyl)-1H-1,2,3-triazole, C₂₃H₁₇N₃

November 2, 2019

Quan Liu, Guowei Xiong, Yunfeng Chen, Yuanxiang Li

Page range: 269-270

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C 23 H 17 N 3 , monoclinic, P 2 1 (no. 4), a = 11.7817(14) Å, b = 5.3165(6) Å, c = 14.1747(16) Å, β = 95.731(2)°, V = 883.43(18) Å 3 , Z = 2, R gt ( F ) = 0.0663, wR ref ( F 2 ) = 1567, T = 298(2) K.
Open Access
Crystal structure of catena-poly[{μ₂-1,5-bis(diphenylphosphanyl)pentane-κ²P:P′}dichloridocadmium(II)], C₂₉H₃₀CdCl₂P₂

October 25, 2019

Yee Seng Tan, Edward R.T. Tiekink

Page range: 271-273

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C 29 H 30 CdCl 2 P 2 , orthorhombic, Pna 2 1 (no. 33), a = 15.84368(4) Å, b = 8.46281(2) Å, c = 20.88054(8) Å, V = 2799.705(14) Å 3 , Z = 4, R gt ( F ) = 0.0275, wR ref ( F 2 ) = 0.0719, T = 100(2) K.
Open Access
Crystal structure of methyl (E)-N²-((3-methylquinolin-8-yl)sulfonyl)-N^ω′-nitro-L-argininate - ethanol (1/1), C₁₉H₂₈N₆O₇S

October 25, 2019

Binli Jiang, Guo-Chun Zhou

Page range: 275-277

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C 19 H 28 N 6 O 7 S, monoclinic, P 2 1 (no. 4), a = 8.1573(1) Å, b = 17.4823(1) Å, c = 9.1162(1) Å, β = 116.432(1)°, V = 1164.14(2) Å 3 , Z = 2, R gt ( F ) = 0.0273, wR ref ( F 2 ) = 0.0732, T = 170(2) K.
Open Access
The crystal structure of trans-carbonyl-(diphenylcyclohexyl-phosphine-κP)iodidomethyl-(2-oxopyridin-1(2H)-olato-κ²O,O′)rhodium(III), C₂₅H₂₈INO₃PRh

December 5, 2019

Mohammed A. Elmakki, Orbett T. Alexander, Andreas Roodt

Page range: 279-281

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C 25 H 28 INO 3 PRh, monoclinic, P 2 1 / c (no. 14), a = 11.339(4) Å, b = 9.887(5) Å, c = 23.069(9) Å, β = 91.125(5)°, Z = 4, V = 2585.7(19) Å 3 , R gt ( F ) = 0.0463, wR ref ( F 2 ) = 0.1093, T = 293(2) K.
Open Access
Crystal structure of N-(amino(pyrazin-2-yl)methylene)-6-methylpyridin-1-ium-3-carbohydrazonate-κ³O,N,N′)-(dinitrato-κ¹O)zinc(II), C₁₂H₁₂N₈O₇Zn

November 8, 2019

Jin-Long Yan

Page range: 283-284

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C 12 H 12 N 8 O 7 Zn, monoclinic, P 2 1 / c (no. 14), a = 8.2116(3) Å, b = 11.1926(4) Å, c = 17.3488(7) Å, β = 96.2450(10)°, V = 1585.05(10) Å 3 , Z = 4, R gt ( F ) = 0.0263, wR ref ( F 2 ) = 0.0722, T = 150(2) K.
Open Access
The crystal structure of dichlorido-(tris(2-benzimidazolylmethyl)amine-κ⁴N,N′,N′′,N′′′)chromium(III) chloride — methanol (1/3), CrC₂₇H₃₃Cl₃N₇O₃

December 5, 2019

Ji Li, Siqi Wu

Page range: 285-287

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CrC 27 H 33 Cl 3 N 7 O 3 , triclinic, P 1̄ (no. 2), a = 9.7862(13) Å, b = 12.4690(17) Å, c = 12.8413(17), α = 84.163(2)°, β = 73.602(3)°, γ = 85.524(2)°, V = 1493.4(3) Å 3 , Z = 2, R gt ( F ) = 0.0472, wR ref ( F 2 ) = 0.1524, T = 100(2) K.
Open Access
Crystal structure of catena-poly[aqua(μ₄-piperazine-1,4-bis(2-hydroxypropanesulfonato-κ⁸O,O′:O′,N:N′,O′′:O′′,O′′′))silver(I)], C₁₀H₂₄Ag₂N₂O₁₀S₂

October 25, 2019

Jin-Ke Jiang, Xin-Yue Xu, Xi-Xi Li, Jing-Jie Du, Hui Jiang, Xian-Wu Dong

Page range: 289-290

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C 10 H 24 Ag 2 N 2 O 10 S 2 , triclinic, P 1̄ (no. 2), a = 6.9547(9) Å, b = 8.4684(12) Å, c = 8.9563(15) Å, α = 117.888(15)°, β = 101.740(13)°, γ = 93.026(11)°, V = 449.75(13) Å 3 , Z = 1, R gt ( F ) = 0.0365, wR ref ( F 2 ) = 0.0858, T = 293(2) K.
Open Access
Crystal structure of bis(μ₃-oxido)-bis(μ₂–2,3,4,5-tetrafluorobenzoato-κ²O:O′)-bis(2,3,4,5-tetrafluorobenzoato-κO)-oktakis(3-chlorobenzyl-κC)tetratin(IV), C₈₄H₅₂Cl₈F₁₆O₁₀Sn₄

January 3, 2020

Junshan Sun

Page range: 291-292

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C 84 H 52 Cl 8 F 16 O 10 Sn 4 , triclinic, P 1̄ (no. 2), a = 11.2999(9) Å, b = 14.1471(11) Å, c = 15.2378(12) Å, α = 67.656(1)°, β = 72.115(1)°, γ = 69.730(1)°, V = 2069.9(3) Å 3 , Z = 1, R gt ( F ) = 0.0284, wR ref ( F 2 ) = 0.0732, T = 293(2) K.
Open Access
Crystal structure of (E)-1-{4-[(4-fluoro-2-hydroxybenzylidene)amino]phenyl}ethanone O-methyl oxime, C₁₆H₁₅FN₂O₂

December 20, 2019

Tao Fu, Jin-Xia Ma, Qing-Lin Li, Ping Wei, Ji-Xing Zhao, Li Zhao

Page range: 293-295

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C 16 H 15 FN 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 6.0573(3) Å, b = 13.8341(6) Å, c = 33.0876(15) Å, β = 92.837(2)°, Z = 8, V = 2769.3(2) Å 3 , R gt ( F ) = 0.0581, wR ref ( F 2 ) = 0.1605, T = 173(2) K.
Open Access
Crystal structure of catena-[(bis(O,O′-diethyl dithiophosphato-S,S′)-μ₂-1,2-bis(3-pyridylmethylene)hydrazine-N,N′)zinc(II)], {C₂₀H₃₀N₄O₄P₂S₄Zn}_n

October 25, 2019

Yee Seng Tan, Edward R.T. Tiekink

Page range: 297-299

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C 20 H 30 N 4 O 4 P 2 S 4 Zn, triclinic, P 1̄ (no. 2), a = 8.01840(1) Å, b = 8.4326(1) Å, c = 23.5086(2) Å, α = 80.478(1)°, β = 80.679(1)°, γ = 76.112(1)°, V = 1509.37(3) Å 3 , Z = 2, R gt ( F ) = 0.0449, wR ref ( F 2 ) = 0.1182, T = 100(2) K.
Open Access
Crystal structure of methyl 2-(4-(3-iodopyrazolo[1,5-a]pyrimidin-6-yl)phenyl)acetate, C₁₅H₁₂IN₃O₂

November 2, 2019

Bo Fang, Fang Fang Jiang, Jiang Ping Meng

Page range: 301-302

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C 15 H 12 IN 3 O 2 , triclinic, P 1̄ (no. 2), a = 4.511(2) Å, b = 11.891(6) Å, c = 14.557(7) Å, α = 109.709(9)°, β = 96.971(9)°, γ = 97.054(9)°, V = 718.4(6) Å 3 , Z = 2, R gt ( F ) = 0.0449, wR ref ( F 2 ) = 0.1052, T = 293(2) K.
Open Access
Crystal structure of hexacarbonyl-(μ₂-methanoato-k²O:O′)-(μ₂–bis(di-p-tolylphosphino)cyclohexylamine-κ²P:P′)dirhenium(I), C₄₂H₄₅NO₈P₂Re₂

November 9, 2019

Dumisani V. Kama, Alice Brink, Roger Alberto, Andreas Roodt

Page range: 303-305

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C 42 H 45 NO 8 P 2 Re 2 , monoclinic, C 2/ c (no. 15), a = 24.1612(7) Å, b = 13.0229(3) Å, c = 14.9180(4) Å, β = 121.383(3)°, V = 4007.2(2) Å 3 , Z = 4, R gt ( F ) = 0.0235, wR ref ( F 2 ) = 0.0596, T = 173(2) K.
Open Access
The cocrystal structure of 1′-hydroxy-1H,1′H-[5,5′-bitetrazol]-1-olate and 1,10-phenanthrolin-1-ium, C₁₄H₁₀N₁₀O₂

November 2, 2019

Zhu Jiaping, Wang Gang, Wu Dang

Page range: 307-308

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C 14 H 10 N 10 O 2 , monoclinic, P 2 1 / n (no. 14), a = 9.6366(19) Å, b = 9.5098(19) Å, c = 16.095(3) Å, β = 103.59(3)°, V = 1433.7(5) Å 3 , Z = 4, R gt ( F ) = 0.0579, wR ref ( F 2 ) = 0.1309, T = 153(2) K.
Open Access
The crystal structure of 1-benzyl-2-((4-(tert-butyl)phenyl)ethynyl)pyridin-1-ium bromide,C₂₄H₂₄BrN

October 25, 2019

Juan Liao, Fei Zeng, Man-Hua Ding

Page range: 309-310

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C 24 H 24 BrN, orthorhombic, P 2 1 / n (no. 14), a = 9.875(6) Å, b = 10.415(6) Å, c = 20.562(12) Å, β = 98.130(7)°, V = 2094(2) Å 3 , Z = 4, R gt ( F ) = 0.0367, wR ref ( F 2 ) = 0.1044, T = 273(2) K.
Open Access
Crystal structure of (5,5′-bitetrazole-1,1′-diolate)-bis(1,10-phenanthroline)-copper(II), C₂₆H₁₆CuN₁₂O₂

November 8, 2019

Zhu Jiaping, Wang Gang, Wu Dang

Page range: 311-312

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C 26 H 16 CuN 12 O 2 , monoclinic, C 2/ c (no. 15), a = 18.800(4) Å, b = 21.224(4) Å, c = 14.436(3) Å, β = 112.094(6)°, V = 5337.1(18) Å 3 , Z = 8, R gt ( F ) = 0.0468, wR ref ( F 2 ) = 0.1287, T = 296(2) K.
Open Access
Crystal structure of bis(ammonium) diaqua-tetrakis(4-hydroxybenzoato)-manganese(II) tetrahydrate, [NH₄]₂[C₂₈H₂₄MnO₁₄] ⋅ 4(H₂O)

November 2, 2019

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 313-315

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C 28 H 40 MnN 2 O 18 , monoclinic, P 2 1 / c (no. 14), a = 7.1069(1) Å, b = 20.5238(2) Å, c = 10.8978(1) Å, β = 96.029(1)°, V = 1580.77(3) Å 3 , Z = 2, R gt ( F ) = 0.0255, wR ref ( F 2 ) = 0.0746, T = 294(2) K.
Open Access
The crystal structure of 3-chloro-1-hydrazino-2,4,6-trinitrobenzene, C₆H₄ClN₅O₆

November 8, 2019

Xue Mei, Xiang Yong, Wang Jian, Zhang Yushan, Yao Yuehua, Wang Jianlong

Page range: 317-318

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C 6 H 4 ClN 5 O 6 , monoclinic, P 2 1 / n (no. 14), a = 10.2139(13) Å, b = 5.6835(6) Å, c = 17.597(2) Å, β = 106.484(4)°, V = 979.6(2) Å 3 , Z = 4, R gt ( F ) = 0.0497, wR ref ( F 2 ) = 0.1138, T = 173 K.
Open Access
Crystal structure of catena-[(μ₂-pyrazine-κ²N:N′)-bis(O,O′-di-ethyldithiophosphato-κ²S,S′)cadmium(II)], {C₁₂H₂₄CdN₂O₄P₂S₄}_n

November 6, 2019

Yee Seng Tan, Edward R.T. Tiekink

Page range: 319-321

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C 12 H 24 CdN 2 O 4 P 2 S 4 , monoclinic, P 2/ n (no. 13), a = 11.7844(2) Å, b = 7.6063(1) Å, c = 13.1965(2) Å, β = 111.594(2)°, V = 1099.86(3) Å 3 , Z = 2, R gt ( F ) = 0.0171, wR ref ( F 2 ) = 0.0467, T = 100 K.
Open Access
Crystal structure of catena-poly[(μ₂-pyrazine-N,N′)-bis(O,O′-di-isopropyldithiophosphato-S,S′)cadmium(II) acetonitrile di-solvate], [C₁₆H₃₂CdN₂O₄P₂S₄⋅2(C₂H₃N)]_n

October 31, 2019

Yee Seng Tan, Edward R.T. Tiekink

Page range: 323-325

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C 20 H 38 CdN 4 O 4 P 2 S 4 , triclinic, P 1̄ (no. 2), a = 9.6352(2) Å, b = 11.3986(2) Å, c = 14.8017(3) Å, α = 85.713(2)°, β = 89.877(2)°, γ = 86.048(2)°, V = 1617.23(6) Å 3 , Z = 2, R gt ( F ) = 0.0285, wR ref ( F 2 ) = 0.0829, T = 100 K.
Open Access
Crystal structure of catena-poly{(μ₂-N¹,N²-bis[(pyridin-4-yl)methyl]ethanediamide-κ²N:N′)-bis(O,O′-di-isopropyldithiophosphato-κ¹S)zinc(II)} — acetonitrile (1/1), C₂₆H₄₂N₄O₆P₂S₄Zn⋅C₂H₃N

November 2, 2019

Yee Seng Tan, Edward R.T. Tiekink

Page range: 327-329

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C 28 H 45 N 5 O 6 P 2 S 4 Zn, monoclinic, P 2 1 / c (no. 14), a = 7.73670(10) Å, b = 21.56370(10) Å, c = 23.1184(2) Å, β = 99.121(1)°, V = 3808.12(6) Å 3 , Z = 4, R gt ( F ) = 0.0210, wR ref ( F 2 ) = 0.0580, T = 100(2) K.
Open Access
Crystal structure of tetraqua-bis(4-(hydroxymethyl)benzoato-κO)cobalt(II), C₁₆H₂₂O₁₀Co

November 14, 2019

Haixia Pang, Zhucan Xie, Hong Zhang, Baoming Xu, Hongyu Gan

Page range: 331-333

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C 16 H 22 O 10 Co, monoclinic, P 2 1 / c (no. 14), a = 9.811(2) Å, b = 15.530(3) Å, c = 13.639(3) Å, β = 122.122(3)°, V = 1760.0(6) Å 3 , Z = 4, R gt ( F ) = 0.0243, wR ref ( F 2 ) = 0.0821, T = 297(2) K.
Open Access
Crystal structure of catena-[(bis(O,O′-diethyl dithiophosphato-S,S′)-μ₂-1,2-bis(4-pyridylmethylene)hydrazine-N,N′)cadmium(II)], {C₂₀H₃₀CdN₄O₄P₂S₄}_n

November 9, 2019

Yee Seng Tan, Edward R.T. Tiekink

Page range: 335-337

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C 20 H 30 CdN 4 O 4 P 2 S 4 , triclinic, P 1̄ (no. 2), a = 9.3353(2) Å, b = 9.7725(2) Å, c = 10.6884(2) Å, α = 63.153(2)°, β = 64.193(2)°, γ = 62.710(2)°, V = 740.43(3) Å 3 , Z = 1, R gt ( F ) = 0.0171, wR ref ( F 2 ) = 0.0465, T = 100 K.
Open Access
Crystal structure of catena-poly[(μ₂-1,2-bis(3-pyridylmethylene)hydrazine-κ²N:N′)-bis(O,O′-dimethyl dithiophosphato-κ²-S,S′)cadmium(II)], {C₁₆H₂₂CdN₄O₄P₂S₄}_n

November 6, 2019

Yee Seng Tan, Edward R.T. Tiekink

Page range: 339-341

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C 16 H 22 CdN 4 O 4 P 2 S 4 , orthorhombic, Pbca (no. 61), a = 12.66410(10) Å, b = 13.00140(10) Å, c = 15.30720(10) Å, V = 2520.35(3) Å 3 , Z = 4, R gt ( F ) = 0.0186, wR ref ( F 2 ) = 0.0503, T = 100(2) K.
Open Access
Crystal structure of catena-poly[(bis(O,O′-diethyl dithiophosphato-κ²S,S′)-μ₂-1,2-bis(3-pyridylmethylene)hydrazine-κ²N:N′)cadmium(II)], {C₂₀H₃₀CdN₄O₄P₂S₄}_n

November 14, 2019

Yee Seng Tan, Edward R.T. Tiekink

Page range: 343-345

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C 20 H 30 CdN 4 O 4 P 2 S 4 , triclinic, P 1̄ (no. 2), a = 9.0764(3) Å, b = 9.3969(3) Å, c = 9.6964(3) Å, α = 86.516(3)°, β = 63.362(3)°, γ = 75.250(3)°, V = 713.50(4) Å 3 , Z = 1, R gt ( F ) = 0.0166, wR ref ( F 2 ) = 0.0462, T = 100(2) K.
Open Access
The crystal structure of catena-poly[(E)-2-(((5-((trimethylstannyl)thio)-1,3,4-thiadiazol-2-yl)imino)methyl)phenol], C₁₂H₁₅N₃OS₂Sn

December 5, 2019

Junshan Sun

Page range: 347-348

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C 12 H 15 N 3 OS 2 Sn, orthorhombic, Pbca (no. 61), a = 13.101(6) Å, b = 11.151(5) Å, c = 20.855(10) Å, V = 3047(2) Å 3 , Z = 8, R gt ( F ) = 0.0440, wR ref ( F 2 ) = 0.1560, T = 298(2) K.
Open Access
Crystal structure of dichlorido(N-o-tolyl-1,1-di-p-tolylphosphanamine–κ¹P)-(methoxydi-p-tolylphosphane-κ¹P)palladium(II), C₃₆H₃₉Cl₂NOP₂Pd

November 2, 2019

Dumisani V. Kama, Alice Brink, Andreas Roodt

Page range: 349-352

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C 36 H 39 Cl 2 NOP 2 Pd, orthorhombic, Pbca (no. 61), a = 19.209(13) Å, b = 15.144(11) Å, c = 24.011(19) Å, V = 6985(9) Å 3 , Z = 8, R gt ( F ) = 0.0292, wR ref ( F 2 ) = 0.0867, T = 100 K.
Open Access
The crystal structure of the triclinic polymorph of hexameric (trimethylsilyl)methyllithium, C₂₄H₆₆Li₆Si₆

November 9, 2019

Jonathan O. Bauer

Page range: 353-356

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C 24 H 66 Li 6 Si 6 , triclinic, P 1̄ (no. 2), a = 12.2492(9) Å, b = 12.4617(9) Å, c = 14.3841(11) Å, α = 74.189(6), β = 74.543(7), γ = 85.970(6), V = 2036.2(3) Å 3 , Z = 2, R gt ( F ) = 0.0465, wR ref ( F 2 ) = 0.0802, T = 173(2) K.
Open Access
Crystal structure of bis(hydroxydi(pyridin-2-yl)methanolato-κ³N,N′O)cobalt(III) 7,7,8,8-tetracyanoquinodimethane, C₃₄H₂₂CoN₈O₄

November 6, 2019

Junjie Huang, Yang Lu, Hui Lu, Jianhua Sun

Page range: 357-358

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C 34 H 22 CoN 8 O 4 , triclinic, P 1̄ (no. 2), a = 6.8423(10) Å, b = 8.8919(13) Å, c = 12.6319(18) Å, α = 104.743(2)°, β = 94.606(2)°, γ = 90.934(2)°, V = 740.30(19) Å 3 , Z = 1, R gt ( F ) = 0.0369, wR ref( F 2 ) = 0.1179, T = 296(2) K.
Open Access
Synthesis and crystal structure of benzyl 5-oxo-5-phenyl-2-(quinolin-2-yl)pentanoate, C₂₇H₂₃NO₃

December 3, 2019

Li Wang, Xiao-Xin An, Yong-Fan Cui, Wen-Kui Dong

Page range: 359-360

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C 27 H 23 NO 3 , monoclinic, P 2 1 (no. 4), a = 5.8236(4) Å, b = 16.7277(13) Å, c = 10.5963(7) Å, β = 96.022(2)°, V = 1026.55(13) Å 3 , Z = 2, R gt ( F ) = 0.0396, wR ref ( F 2 ) = 0.0953, T = 153(2) K.
Open Access
Crystal structure of 5,5-dimethyl-3-oxocyclohex-1-en-1-yl 4-(2,2-dichloroacetyl)-3,4-dihydro-2 H-benzo[b][1,4]oxazine-7-carboxylate, C₁₉H₁₉Cl₂NO₅

November 9, 2019

You-Yuan Guo, Huan Wang, Xin Ma, Ying Fu

Page range: 361-363

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C 19 H 19 Cl 2 NO 5 , orthorhombic, Pbca (no. 61), a = 12.6750(18) Å, b = 11.0927(17) Å, c = 28.400(4) Å, V = 3993.0(10) Å 3 , Z = 8, R gt ( F ) = 0.0700, wR ref ( F 2 ) = 0.2011, T = 293(2) K.
Open Access
Crystal structure of dipentyl 2,5-dihydroxycyclohexa-1,4-diene-1,4-dicarboxylate, C₁₈H₂₈O₆

November 8, 2019

Zhuang-Yu Li, Xiao-Jing Liu, Zi-Yu Guo, Wen-Yu Li, E. Liu, Fang-Fang Jian

Page range: 365-366

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C 18 H 28 O 6 , monoclinic, C 2/ c (no. 15), a = 15.061(3) Å, b = 13.791(3) Å, c = 10.106(2) Å, β = 118.60(3)°, V = 1843.0(8) Å 3 , Z = 4, R gt ( F ) = 0.0462, wR ref ( F 2 ) = 0.1315, T = 294.3 K.
Open Access
The crystal structure of catena-poly[diaqua-(μ₄-5-(benzo[d]thiazol-2-yl)benzene-1,3-dicarboxylate-κ⁴O,O′:O′′,O′′′)-(μ₄-5-(benzo[d]thiazol-2-yl)benzene-1,3-dicarboxylate-κ⁴O,O′:O′′,O′′′)dicadmium(II)], C₃₀H₁₈Cd₂N₂O₁₀S₂

November 14, 2019

Min Zheng

Page range: 367-369

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C 30 H 18 Cd 2 N 2 O 10 S 2 , monoclinic, P 2 1 / c (no. 14), a = 14.9275(2) Å, b = 10.18003(11) Å, c = 18.3497(2) Å, β = 92.0808(13)°, V = 2786.63(6) Å 3 , Z = 4, R gt ( F ) = 0.0285, wR ref ( F 2 ) = 0.0679, T = 290.3(9) K.
Open Access
Crystal structure of 2,7-diiodo-1,3,6,8-tetramethyl-bis(difluoroboron)-1,2-bis((1H-pyrrol-2-yl)methylene)hydrazine, C₁₄H₁₄B₂F₄I₂N₄

November 8, 2019

Yingfan Liu, Xiaochuan Li, Saisai Sun, Guangqian Ji, Young-A. Son

Page range: 371-372

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C 14 H 15 B 2 F 4 I 2 N 4 , triclinic, P 1̄ (no. 2), a = 7.5458(7) Å, b = 8.5659(6) Å, c = 8.6089(5) Å, α = 108.189(6)°, β = 110.492(7)°, γ = 98.678(7)°, V = 473.6 Å 3 , Z = 1, R gt ( F ) = 0.0334, wR ref ( F 2 ) = 0.0831, T = 296.5 K.
Open Access
A dinuclear Eu(III) complex in the crystal structure of dodecaaqua-bis(μ₂-4-(1H-tetrazol-5-yl)benzoato-κ²O:O′) bis(5-(4-carboxylatophenyl)tetrazol-1-ide) tetrahydrate, C₃₂H₅₀Eu₂N₁₆O₂₄

January 1, 2020

Min Zhu, Wen-Qi Song, Zong-Cheng Miao

Page range: 373-375

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C 32 H 50 Eu 2 N 16 O 24 , monoclinic, P 2 1 / c (no. 14), a = 7.685(5) Å, b = 13.482(5) Å, c = 23.240(5) Å, β = 93.578(5)°, V = 2403.2(19) Å 3 , Z = 2, R gt ( F ) = 0.0235, wR ref ( F 2 ) = 0.0577, T = 293 K.
Open Access
Crystal structure and anti-inflammatory activity of (3E,5E)-3-(2-fluorobenzylidene)-1-((4-fluorophenyl)sulfonyl)-5-(pyridin-3-ylmethylene)piperidin-4-one, C₂₄H₁₈F₂N₂O₃S

December 7, 2019

Yue Sun, Yin-Kai Liu, Jia-Dong Li, Qing-Guo Meng, Gui-Ge Hou

Page range: 377-379

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C 24 H 18 F 2 N 2 O 3 S, monoclinic, P 2 1 / c (no. 14), a = 15.180(5) Å, b = 10.221(3) Å, c = 13.556(4) Å, β = 106.628(4)°, V = 2015.3(10) Å 3 , Z = 4, R gt ( F ) = 0.0530, wR ref ( F 2 ) = 0.1342, T = 173(2) K.
Open Access
Crystal structure and anti-inflammatory activity of (3E,5E)-3-(2-fluorobenzylidene)-1-((4-acetamidophenyl)sulfonyl)-5-(pyridin-3-ylmethylene)piperidin-4-one-methanol-hydrate (2/1/1), C₅₃H₅₀F₂N₆O₁₀S₂

November 9, 2019

An-Qi Wang, Ru-Ning Gao, Qing-Hao Luan, Ze-Ping Wang, Xiao-Ming Li, Gui-Ge Hou

Page range: 381-384

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C 53 H 50 F 2 N 6 O 10 S 2 , monoclinic, P 2 1 / n (no. 14), a = 15.088(5) Å, b = 23.560(9) Å, c = 15.401(6) Å, β = 112.254(5)°, V = 5067(3) Å 3 , Z = 4, R gt ( F ) = 0.0509, wR ref ( F 2 ) = 0.1336, T = 298(2) K.
Open Access
Crystal structure of 4-dimethylamino-pyridin-1-ium uracil-1-acetate, C₁₃H₁₆N₄O₄

December 20, 2019

Xiao Zhang, Lin Wang, Sen Liang

Page range: 385-386

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C 13 H 16 N 4 O 4 , monoclinic, P 2 1 / n (no. 14), a = 4.7965(12) Å, b = 10.053(2) Å, c = 27.570(6) Å, β = 90.292(8)°, V = 1329.3(5) Å 3 , Z = 4, R gt ( F ) = 0.0426, wR ref ( F 2 ) = 0.1115, T = 292(3) K.
Open Access
Crystal structure of dimethylammonium 5-fluorouracil-1-acetate, C₈H₁₂N₃O₄F

December 20, 2019

Xiao Zhang, Kaiyun Li, Sen Liang

Page range: 387-388

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C 8 H 12 N 3 O 4 F, monoclinic, P 2 1 / c (no. 14), a = 4.8090(3) Å, b = 9.9340(6) Å, c = 22.2437(13) Å, β = 90.138(8)°, V = 1062.64(11) Å 3 , Z = 4, R gt ( F ) = 0.0452, wR ref ( F 2 ) = 0.1227, T = 293(2) K.
Open Access
Crystal structure of bis(N′-((5-(ethoxycarbonyl)-1H-pyrrol-2-yl)methylene)-N-ethylcarbamohydrazonothioato-κ²N,O)nickel(II), C₂₂H₃₀N₈O₄S₂Ni

December 31, 2019

Kui-Kui Chen, Jing-Tao Huang, Long Lin, Wei-Na Wu

Page range: 389-390

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C 22 H 30 N 8 O 4 S 2 Ni, monoclinic, P 2 1 / c (no. 14), a = 10.635(2) Å, b = 10.308(2) Å, c = 12.444(3) Å, β = 101.205(4)°, V = 1338.2(5) Å 3 , Z = 2, R gt ( F ) = 0.0417, wR ref ( F 2 ) = 0.0937, T = 296(2) K.
Open Access
Crystal structure of chlorido-(η⁵-pentamethylcyclopentadienyl)-((bis-pyrazol-1-yl)methane-κ²N,N′) rhodium(III) hexafluorophosphate. (C₁₇H₂₃ClN₄RhF₆P)

November 13, 2019

Joel M. Gichumbi, Sizwe J. Zamisa, Holger B. Friedrich

Page range: 391-393

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C 17 H 23 ClN 4 RhF 6 P, monoclinic, P 2 1 / c (no. 14), a = 10.6954(2) Å, b = 15.3868(3) Å, c = 12.6130(2) Å, β = 90.5590(10)°, V = 2075.60(7) Å 3 , Z = 4, R gt ( F ) = 0.0296, wR ref ( F 2 ) = 0.0727, T = 100(2) K.
Open Access
The crystal structure of 5-(benzofuran-2-carbonyl)-N-cyclohexyl-5,6-dihydrophenanthridine-6-carboxamide, C₂₉H₂₆N₂O₃

November 8, 2019

Weiwei Han

Page range: 395-396

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C 29 H 26 N 2 O 3 , triclinic, P 1̄ (no. 2), a = 9.6533(8) Å, b = 11.3185(9) Å, c = 11.4469(10) Å, α = 83.747(3)°, β = 85.810(2)°, γ = 71.445(2)°, V = 1177.65(17) Å 3 , Z = 2, R gt ( F ) = 0.0464, wR ref ( F 2 ) = 0.1621, T = 296(2) K.
Open Access
The crystal structure of 2-oxo-2H-chromen-4-yl acetate, C₁₁H₈O₄

November 9, 2019

Siya T. Hulushe, Meloddy H. Manyeruke, Eric C. Hosten, Perry T. Kaye, Gareth M. Watkins, Rui W. M. Krause

Page range: 397-398

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C 11 H 8 O 4 , monoclinic, P 2 1 / c (no. 14), a = 4.5947(2) Å, b = 10.5414(3) Å, c = 19.1611(7) Å, β = 94.084(2)°, V = 925.70(6) Å 3 , Z = 4, R gt ( F ) = 0.0376, wR ref ( F 2 ) = 0.1109, T = 200(2) K.
Open Access
The crystal structure of 2-nitroisophthalic acid, C₈H₅NO₆

December 5, 2019

Shu-Jing Li, Ke Li, Yi-Wen Li

Page range: 399-400

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C 8 H 5 NO 6 , monoclinic, C 2/ c (no. 15), a = 5.4755(12) Å, b = 14.377(3) Å, c = 11.143(3) Å, β = 99.096(9)°, V = 866.2(3) Å 3 , Z = 4, R gt ( F ) = 0.0455, wR ref ( F 2 ) = 0.1341, T = 150(2) K.
Open Access
Crystal structure of 3-fluoro-9-methoxy-4b,5,14,15-tetrahydro-6H-isoquinolino [2′,1′:1,6]pyrazino[2,3-b]quinoxaline, C₁₉H₁₇FN₄O

December 14, 2019

Yu Hang Chen, Yan Rong Dan, Lin Ling Gan, Yu Yu

Page range: 401-402

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C 19 H 17 FN 4 O, orthorhombic, Pbca (no. 61), a = 7.0607(2) Å, b = 18.4459(5) Å, c = 23.8955(7) Å, V = 3112.17(15) Å 3 , Z = 8, R gt ( F ) = 0.0543, wR ref ( F 2 ) = 0.1540, T = 100(2) K.
Open Access
Crystal structure of (4-fluorobenzyl-κC)(bis(2-hydroxyethyl) carbamodithioato-κ²S,S′)(2,2′-imino-diethanolato-κ³N,O,O′)tin(IV), C₁₆H₂₅FN₂O₄S₂Sn

November 8, 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 403-405

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C 16 H 25 FN 2 O 4 S 2 Sn, monoclinic, P 2 1 / n (no. 14), a = 11.2227(1) Å, b = 12.6793(1) Å, c = 13.8731(1) Å, β = 98.282(1)°, V = 1953.50(3) Å 3 , Z = 4, R gt ( F ) = 0.0198, wR ref ( F 2 ) = 0.0507, T = 100(2) K.
Open Access
Crystal structure and anti-inflammatory activity of (3E,5E)-1-((4-bromophenyl)sulfonyl)-3-(pyridin-4-ylmethylene)-5-(2-(trifluoromethyl)benzylidene)piperidin-4-one, C₂₅H₁₈BrF₃N₂O₃S

December 18, 2019

Xian-Yong Bai, Qing-Guo Meng, Gui-Ge Hou, Yun Hou

Page range: 407-409

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C 25 H 18 BrF 3 N 2 O 3 S, monoclinic, P 2 1 / n (no. 14), a = 9.9295(11) Å, b = 21.755(2) Å, c = 10.2358(11) Å, β = 95.022(10)°, V = 2202.6(4) Å 3 , Z = 4, R gt ( F ) = 0.0373, wR ref ( F 2 ) = 0.0795, T = 100(1) K.
Open Access
Crystal structure and anti-inflammatory activity of (3E,5E)-1-((4-chlorophenyl)sulfonyl)-3-(pyridin-4-ylmethylene)-5-(2-(trifluoromethyl)benzylidene)piperidin-4-one, C₂₅H₁₈ClF₃N₂O₃S

December 20, 2019

Yan-Qiu Zhou, Gui-Ge Hou, Qing-Guo Meng, Yun Hou

Page range: 411-413

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C 25 H 18 ClF 3 N 2 O 3 S, monoclinic, P 2 1 / n (no. 14), a = 9.9087(5) Å, b = 21.7843(10) Å, c = 10.2512(6) Å, β = 94.749(5)°, V = 2205.2(2) Å 3 , Z = 4, R gt ( F ) = 0.0448, wR ref ( F 2 ) = 0.1028, T = 100 K.
Open Access
The crystal structure of 3-((1R,2S)-1-methylpyrrolidin-1-ium-2-yl)pyridin-1-ium tetrachloridomanganate(II), C₁₀H₁₆Cl₄MnN₂

November 9, 2019

Guido J. Reiss

Page range: 415-417

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C 10 H 16 Cl 4 MnN 2 , monoclinic, P 2 1 (no. 4), a = 7.28276(7) Å, b = 13.22972(12) Å, c = 8.01007(7) Å, β = 97.5018(9)°, V = 765.155(12) Å 3 , Z = 2, R gt ( F ) = 0.0165, wR ref ( F 2 ) = 0.0392, T = 123(2) K.
Open Access
The crystal structure of 3-carboxy-5-methylpyridin-1-ium-2-carboxylate, C₈H₇NO₄

December 20, 2019

Yuanliang Zhu, Jingwei Ma, Shaofeng Li, Bin Cai

Page range: 419-420

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C 8 H 7 NO 4 , orthorhombic, Pccn (no. 56), a = 14.1361(10) Å, b = 15.8923(12) Å, c = 6.6410(6) Å, V = 1491.9(2) Å 3 , Z = 8, R gt ( F ) = 0.0406, wR ref ( F 2 ) = 0.1155, T = 150(2) K.
Open Access
Crystal structure of bis(3-methoxy-N-(1-(pyridin-2-yl)ethylidene)benzohydrazonato κ³O,N,N′)zinc(II), C₃₀H₂₈N₆O₄Zn

December 7, 2019

Xiao-Wei Deng, Wei-Na Wu

Page range: 421-422

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C 30 H 28 N 6 O 4 Zn, orthorhombic, Aba 2 (no. 41), a = 12.040(9) Å, b = 22.596(18) Å, c = 10.344(10) Å, V = 2814(4) Å 3 , Z = 4, R gt ( F ) = 0.0463, wR ref ( F 2 ) = 0.1435, T = 296(2) K.
Open Access
Crystal structure of dichlorido-(4,4′-dichloro-2,2′-bipyridine-κ²N,N′)platinum(II) — acetone (1/1), C₁₃H₁₂Cl₄N₂PtO

November 9, 2019

Tatsuto Kiwada, Aika Hirasaki, Akira Odani

Page range: 423-424

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C 13 H 12 Cl 4 N 2 PtO, monoclinic, C 2/ m (no. 12), a = 17.497(4) Å, b = 6.8214(15) Å, c = 14.183(3) Å, β = 93.441(7)°, Z = 4, V = 1689.7(6) Å 3 , R gt ( F ) = 0.0309, wR ref ( F 2 ) = 0.0696, T = 93 K.
Open Access
Crystal structure of diethyl 6,12-bis(4-fluorophenyl)-2,10-dimethoxy-3,9-diphenyl-3,9-diazatetracyclo[6.4.0.0^2,7.0^4,11]dodecane-1,5-dicarboxylate, C₄₂H₄₂F₂N₂O₆

December 5, 2019

Yu-Kun Guo, Shi-Jun Chen, Meng-Meng Zhang, Han-Yang Lan, Yu-Cai Wang, Qi-Di Zhong

Page range: 425-427

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C 42 H 42 F 2 N 2 O 6 , monoclinic, P 2 1 / c (no. 14), a = 20.159(3) Å, b = 8.3357(10) Å, c = 21.372(3) Å, β = 103.130(3)°, V = 3497.4(8) Å 3 , Z = 4, R gt ( F ) = 0.0414, wR ref ( F 2 ) = 0.1083, T = 113(2) K.
Open Access
Synthesis and crystal structure of (1E,3E)-2-hydroxy-5-methylisophthalaldehyde O,O-di(2-((((E)-(2-hydroxynaphthalen-1-yl)methylene)amino)oxy)ethyl) dioxime, C₃₅H₃₂N₄O₇

December 5, 2019

Ying-Qi Pan, Meng Yu, Yu Zhang, Wen-Kui Dong

Page range: 429-431

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C 35 H 32 N 4 O 7 , triclinic, P 1̄ (no. 2), a = 9.3625(6) Å, b = 12.7558(7) Å, c = 14.5965(9) Å, α = 68.833(2)°, β = 80.891(2)°, γ = 69.242(2)°, V = 1519.15(16) Å 3 , Z = 2, R gt ( F ) = 0.0447, wR ref ( F 2 ) = 0.1500, T = 296(2) K.
Open Access
The crystal structure of 2-phenyl-4,6-bis(prop-2-yn-1-yloxy)-1,3,5-triazine, C₁₅H₁₁N₃O₂

December 13, 2019

Jin Li, Yan Chen, Ziqing Wu, Yali Liu, Dachuan Yin, Zhenyu Zuo

Page range: 433-435

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C 15 H 11 N 3 O 2 , triclinic, P 1̄ (no. 2), a = 8.4680(5) Å, b = 9.7578(5) Å, c = 10.2101(6) Å, α = 104.578(5)°, β = 111.882(6)°, γ = 106.589(5)°, V = 686.77(8) Å 3 , Z = 2, R gt ( F ) = 0.0394, wR ref ( F 2 ) = 0.1261, T = 250(2) K.
Open Access
Crystal structure of 7-(2-{4-[(4-bromophenyl)methyl]piperazin-1-yl}ethoxy)-2H-chromen-2-one, C₂₂H₂₃BrN₂O₃

December 5, 2019

Jacques Joubert, Germaine B. Foka

Page range: 437-439

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C 22 H 23 BrN 2 O 3 , monoclinic, P 2 1 / c (no. 14), a = 5.9023(9) Å, b = 14.554(2) Å, c = 22.801(4) Å, β = 90.801(2)°, V = 1958.5(5) Å 3 , Z = 4, R gt ( F ) = 0.0388, wR ref ( F 2 ) = 0.0961, T = 100(2) K.
Open Access
Crystal structure of bis-[N-(3-ethyl-1-pyrazin-2-yl-ethylidene)-3-bromo-benzoic acid-hydrazonato-κ³O,N,N′)]-cadmium(II), C₃₀H₂₈N₈O₂Br₂Cd

December 14, 2019

Liangjun Lv, Long Lin, Wei-Na Wu

Page range: 441-443

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C 30 H 28 N 8 O 2 Br 2 Cd, triclinic, P 1̄ (no. 2), a = 8.359(7) Å, b = 12.394(10) Å, c = 15.189(12) Å, α = 95.757(14)°, β = 90.593(16)°, γ = 106.961(15)°, V = 1496(2) Å 3 , Z = 2, R gt ( F ) = 0.0467, wR ref ( F 2 ) = 0.0998, T = 296(2) K.
Open Access
Crystal structure of 6-(4-fluorophenyl)-4-methoxy-2H-pyran-2-one, C₁₂H₉FO₃

December 5, 2019

Grace Obi, Sizwe J. Zamisa, Fanie R. van Heerden

Page range: 445-446

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C 12 H 9 FO 3 , triclinic, P 1̄ (no. 2), a = 7.1983(6) Å, b = 7.3732(6) Å, c = 9.6439(8) Å, α = 81.489(5)°, β = 88.634(4)°, γ = 71.065(4)°, V = 478.66(7) Å 3 , Z = 2, R gt ( F 2 ) = 0.0362, wR ref ( F 2 ) = 0.1015, T = 100(2) K.
Open Access
Crystal structure of 3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanoic acid, C₁₄H₁₈O₄

December 5, 2019

Peilian Liu, Lijun Chen, Jieping Chen, Guiyuan Huang, Ying Sun, Guohua Zhou

Page range: 447-449

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C 14 H 18 O 4 , monoclinic, P 2 1 / n (no. 14), a = 10.8905(6) Å, b = 9.9903(5) Å, c = 12.7101(6) Å, β = 104.912(2)°, V = 1336.28(12) Å 3 , Z = 4, R gt ( F ) = 0.0502, wR ref ( F 2 ) = 0.1504, T = 296(2) K.
Open Access
The crystal structure of 3-bromo-6-methoxy-2-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine, C₁₃H₁₉BBrNO₃

December 13, 2019

Ji-Run Zhang, Hao Deng, Tong Liu

Page range: 451-452

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C 13 H 19 BBrNO 3 , triclinic, P 1̄ (no. 2), a = 6.5459(3) Å, b = 11.2565(5) Å, c = 11.8529(5) Å, α = 106.938(2)°, β = 105.657(2)°, γ = 106.628(2)°, V = 738.71(6) Å 3 , Z = 2, R gt ( F ) = 0.0286, wR ref ( F 2 ) = 0.0641, T = 173 K.
Open Access
The crystal structure of 6-methyl-3,20-dioxo-19-norpregna-4,6-dien-17-yl acetate–2,4-dihydroxybenzoic acid (1/1), C₃₀H₃₆O₈

December 7, 2019

Xiao F. Chen, Peng Li, Juan Xu, Hui P. Wang, Li F. Ning

Page range: 453-455

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C 30 H 36 O 8 , monoclinic, P 2 1 (no. 4), a = 10.899(2) Å, b = 11.002(2) Å, c = 11.847(2) Å, V = 1310.3(5) Å 3 , Z = 2, R gt ( F ) = 0.0504, wR ref ( F 2 ) = 0.1161, T = 163(2) K.
Open Access
The crystal structure of (5-chloro-2-hydroxy-N-(4-methoxy-2-oxidobenzylidene)benzohydrazonato-κ³N,O,O′)-(pyridine-κ¹N)copper(II), C₂₀H₁₆ClCuN₃O₄

December 5, 2019

Wang Xin, Li Shuli, Yang Liguo, Song Haixiang, Niu Yongsheng

Page range: 457-458

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C 20 H 16 ClCuN 3 O 4 , triclinic, P 1̄ (no. 2), a = 7.629(4) Å, b = 8.893(5) Å, c = 14.193(8) Å, α = 88.603(6)°, β = 81.093(6)°, γ = 83.715(6)°, V = 945.6(9) Å 3 , Z = 2, R gt ( F ) = 0.0245, wR ref ( F 2 ) = 0.0709, T = 296(2) K.
Open Access
Crystal structure of (E)-2-cyano-N′-(1-(3-ethylpyrazin-2-yl)ethylidene)acetohydrazide, C₁₁H₃N₅O

December 7, 2019

Xiao-Li Gao

Page range: 459-460

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C 11 H 3 N 5 O, monoclinic, P 2 1 / c (no. 14), a = 15.727(4) Å, b = 5.0572(12) Å, c = 15.452(4) Å, β = 105.007(4)°, V = 1187.1(5) Å 3 , Z = 4, R gt ( F ) = 0.0408, wR ref ( F 2 ) = 0.1123, T = 296 K.
Open Access
Crystal structure of (2,7-dihexyl-9,9-dimethyl-9H-xanthene-4,5-diyl)bis(diphenylphosphane), C₅₁H₅₆OP₂

December 20, 2019

Nonjabulo Nyalungu, Saba Alapour, Holger B. Friedrich, Muhammad D. Bala

Page range: 461-463

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C 51 H 56 OP 2 , monoclinic, C 2/ c (no. 15), a = 20.1788(4) Å, b = 13.0247(4) Å, c = 18.0172(5) Å, β = 119.874(2)°, V = 4106.1(2) Å 3 , Z = 4, R gt ( F ) = 0.0363, wR ref ( F 2 ) = 0.0981, T = 173(2) K.
Open Access
Crystal structure of 5-((bis(pyridin-2-ylmethyl)amino)methyl)quinolin-8-ol, C₂₂H₂₀N₄O

December 7, 2019

Liu Jia, Nie Xu-Liang, Yin Zhong-Ping, Peng Da-Yong, Shi Xu-Gen

Page range: 465-467

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C 22 H 20 N 4 O, monoclinic, P 2 1 / n (no. 14), a = 11.1861(14) Å, b = 8.1418(10) Å, c = 20.461(3) Å, β = 97.433(1)°, V = 1847.8(4) Å 3 , Z = 4, R gt ( F ) = 0.0357, wR ref ( F 2 ) = 0.1002, T = 296(2) K.
Open Access
Crystal structure of 3-(2-(5-(4-fluorophenyl)-3-(4-methylphenyl)-4,5-dihydro-1H-pyrazol-1-yl)thiazol-4-yl)-2H-chromen-2-one, C₂₈H₂₀FN₃O₂S

December 5, 2019

Mohammed F. Alotibi, Bakr F. Abdel-Wahab, Emad Yousif, Amany S. Hegazy, Benson M. Kariuki, Gamal A. El-Hiti

Page range: 469-471

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C 28 H 20 FN 3 O 2 S, triclinic, P 1̄ (no. 2), a = 9.1325(7) Å, b = 11.5184(9) Å, c = 11.6535(9) Å, α = 74.682(7)°, β = 84.253(6)°, γ = 76.720(6)°, V = 1149.68(15) Å 3 , Z = 2, R gt ( F ) = 0.0574, wR ref ( F 2 ) = 0.1438, T = 296(2) K.
Open Access
The crystal structure of [(tetra-μ₂-2,6-difluorobenzoato-κ²O:O′)-bis-(2,6-difluorobenzoato-κ²O:O′)-bis-(1,10-phenanthroline-κ²N:N′)]dierbium(III) C₆₆H₃₄N₄O₁₂F₁₂Er₂

December 3, 2019

Zhong Yu-Fei, Wang Wen-Min, Peng Xiong-Xin, Bao Guang-Ming, Hu Chun-Yan, Yuan Hou-Qun

Page range: 473-475

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C 66 H 34 N 4 O 12 F 12 Er 2 , triclinic, P 1̄ (no. 2), a = 11.8934(5) Å, b = 12.0041(4) Å, c = 12.4578(5) Å, α = 68.718(4)°, β = 64.205(4)°, γ = 87.053(3)°, V = 1480.09(12) Å 3 , Z = 1, R gt ( F ) = 0.0326, wR ref ( F 2 ) = 0.0626, T = 293(2) K.
Open Access
Crystal structure of bis(3-chloro-N-(1-(pyrazin-2-yl)ethylidene)benzohydrazonato-k³N,N′,O)nickel(II), C₂₆H₂₀N₈O₂Cl₂Ni

December 7, 2019

Zhen-Li Hao, Cun-Han Huang

Page range: 477-478

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C 26 H 20 N 8 O 2 Cl 2 Ni, orthorhombic, Pbcn (no. 60), a = 11.737(10) Å, b = 9.309(8) Å, c = 23.72(2) Å, V = 2592(4) Å 3 , Z = 4, R gt ( F ) = 0.0361, wR ref ( F 2 ) = 0.0934, T = 296 K.
Open Access
Crystal structure of (E)-3-(3-(5-methyl-1-phenyl-1H-1,2,3-triazol-4-yl)-1-phenyl-1H-pyrazol-4-yl)-1-phenylprop-2-en-1-one, C₂₇H₂₁N₅O

December 10, 2019

Mohammed F. Alotibi, Bakr F. Abdel-Wahab, Emad Yousif, Amany S. Hegazy, Benson M. Kariuki, Gamal A. El-Hiti

Page range: 479-481

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C 27 H 21 N 5 O, triclinic, P 1̄ (no. 2), a = 8.1464(7) Å, b = 10.3861(8) Å, c = 13.2507(9) Å, α = 84.898(6)°, β = 89.413(6)°, γ = 80.351(7)°, V = 1100.88(15) Å 3 , Z = 2, R gt ( F ) = 0.0648, wR ref ( F 2 ) = 0.1726, T = 296(2) K.
Open Access
Crystal structure of (E)-N′-((4-aminophenyl)sulfonyl)-N,N-dimethylformimidamide, C₉H₁₃N₃O₂S

December 5, 2019

Alaa A.-M. Abdel-Aziz, Adel S. El-Azab, Hazem A. Ghabbour, Ahmad J. Obaidullaha

Page range: 483-484

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C 9 H 13 N 3 O 2 S, monoclinic, P 2 1 / c (no. 14), a = 8.0984(4) Å, b = 17.3203(10) Å, c = 9.6802(4) Å, β = 124.031(3)°, V = 1125.26(10) Å 3 , Z = 4, R gt ( F ) = 0.0504, wR ref ( F 2 ) = 0.1275, T = 293(2) K.
Open Access
Crystal structure of η⁶-p-cymene-iodido-(N-isopropyl-1-(pyridin-2-yl)methanimine-κ²N,N′)ruthenium(II) hexafluorophosphate(V), C₁₉H₂₆IN₂F₆Ru

December 7, 2019

Joel M. Gichumbi, Bernard Omondi, Holger B. Friedrich

Page range: 485-487

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C 19 H 26 IN 2 F 6 Ru, triclinic, P 1̄ (no. 2), a = 9.240(2) Å, b = 10.019(3) Å, c = 12.689(3) Å, α = 78.921°, β = 81.596(10)°, γ = 83.654°, V = 1136.30(5) Å 3 , Z = 2, R gt ( F ) = 0.0174, wR ref ( F 2 ) = 0.0440, T = 173 K.
Open Access
Crystal structure of 6-iodo-3-phenyl-2-propylquinazolin-4(3H)-one, C₁₇H₁₅IN₂O

December 5, 2019

Adel S. El-Azab, Hazem A. Ghabbour, Alaa A.-M. Abdel-Aziz, Hamad M. Alkahtani

Page range: 489-491

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C 17 H 15 IN 2 O, monoclinic, C 2 (no. 5), a = 23.6958(12) Å, b = 5.5334(2) Å, c = 15.9712(9) Å, β = 132.329(3)°, V = 1548.16(13) Å 3 , Z = 4, R gt ( F ) = 0.046, wR ref ( F 2 ) = 0.093, T = 296(2) K.
Open Access
Low temperature redetermination of the crystal structure of catena-poly[[tri-4-fluorobenzyltin(IV)]μ₂-pyridine-4-carboxylato-κ²N:O], {C₂₇H₂₂F₃NO₂Sn}_n

December 7, 2019

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 493-496

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C 27 H 22 F 3 NO 2 Sn, monoclinic, P 2 1 / n (no. 14), a = 8.7913(2) Å, b = 19.0856(5) Å, c = 13.9417(4) Å, β = 91.017(2)°, V = 2338.87(11) Å 3 , Z = 4, R gt ( F ) = 0.0324, wR ref ( F 2 ) = 0.0873, T = 100(2) K.
Open Access
Crystal structure of bis(2-propyl-1H-benzo[d]imidazol-3-ium) tetrachloridozincate(II), C₁₀H₁₃Cl₄N₂Zn

December 5, 2019

Xiao-Ming Shi, Shu-Jing Li, Li-Na Xiao, Meng-Jing Li

Page range: 497-499

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C 10 H 13 Cl 4 N 2 Zn, monoclinic, P 2 1 / c (no. 14), a = 13.370(2) Å, b = 10.0304(14) Å, c = 17.913(2) Å, β = 93.950(4)°, V = 2396.5(6) Å 3 , Z = 4, R gt ( F ) = 0.0461, wR ref ( F 2 ) = 0.1038, T = 150(2) K.
Open Access
The crystal structure of (Z)-3-hydrazono-5-nitroindolin-2-one – dimethyl sulfoxide (1/1), C₈H₆N₄O₃

December 7, 2019

Abdulrahman M. Al-Obaid, Saeed Ali Syed, Bari Ahmed, Eric C. Hosten

Page range: 501-502

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C 8 H 6 N 4 O 3 ⋅ C 2 H 6 OS, orthorhombic, Pnma (no. 62), a = 10.4813(5) Å, b = 6.8663(4) Å, c = 17.2605(9) Å, V = 1242.20(11) Å 3 , Z = 4, R gt ( F ) = 0.0506, wR ref ( F 2 ) = 0.1590, T = 200(2) K.
Open Access
Crystal structure of bis-[N-(1-pyrazin-2-yl-ethylidene)-cyanoacetic acid-hydrazonato-κ³O,N,N′)]-zinc(II), C₁₈H₁₆N₁₀O₂Zn

December 27, 2019

Xiao-Li Gao, Rong-Li Geng, Pai Chen

Page range: 503-504

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C 18 H 16 N 10 O 2 Zn, triclinic, P 1̄ (no. 2), a = 10.218(7) Å, b = 10.490(7) Å, c = 11.101(8) Å, α = 79.590(11)°, β = 65.913(12)°, γ = 66.785(10)°, V = 998.0(12) Å 3 , Z = 2, R gt ( F ) = 0.0516, wR ref ( F 2 ) = 0.1323, T = 293(2) K.
Open Access
Crystal structure and photochromism of 1-(2,5-dimethyl-3-thienyl)-2-[2-methyl-5-(benzaldoxime)-3-thienyl] perfluorocyclopentene, C₂₃H₁₇F₆NOS₂

December 31, 2019

Xiaoxiao Wu, Hongliang Liu, Yuping Yang, Shouzhi Pu

Page range: 505-507

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C 23 H 17 F 6 NOS 2 , triclinic, P 1̄ (no. 2), a = 8.379(3) Å, b = 11.509(2) Å, c = 12.817(3) Å, α = 71.272(3)°, β = 81.342(4)°, γ = 77.553(3)°, V = 1138.7(5) Å 3 , Z = 2, R gt ( F ) = 0.0489, wR ref ( F 2 ) = 0.1296, T = 296(2) K.

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