Zeitschrift für Kristallographie - New Crystal Structures

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Volume 235, Issue 6

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Zeitschrift für Kristallographie - New Crystal Structures

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Frontmatter

October 28, 2020

Page range: i-viii

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Open Access
Crystal structure of poly[tetraaqua-bis(μ₄-5-(4-carboxy-benzylamino)-isophthalato-κ⁴O,O′:O′′:O′′′)-(μ₂-4,4′-di(1H-imidazol-1-yl)-1,1′-biphenyl-κ²N:N′)dicadmium(II)], C₂₅H₂₂N₃O₈Cd

August 4, 2020

Shi-Hui Li, Guan-Feng Li, Li Zhang

Page range: 1271-1273

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C 25 H 22 N 3 O 8 Cd, triclinic, P 1̄ (no. 2), a = 10.2722(10) Å, b = 10.6897(11) Å, c = 12.5667(13) Å, α = 79.698(9)°, β = 72.168(9)°, γ = 63.166(10)°, V = 1170.8(2) Å 3 , Z = 2, R gt ( F ) = 0.0618, wR ref ( F 2 ) = 0.1078, T = 293(2) K.
Open Access
The crystal structure of 2-(2-(2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-2-ium-1-yl)phenoxy)acetate, C₁₉H₁₈N₂O₃

July 22, 2020

Wang Li-Hua, Tai Xi-Shi

Page range: 1275-1276

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C 19 H 18 N 2 O 3 , monoclinic, P 2 1 / c (no. 14), a = 12.6187(7) Å, b = 9.4445(5) Å, c = 13.7424(8) Å, β = 99.248(5)°, V = 1616.49(16) Å 3 , Z = 4, R gt ( F ) = 0.0793, wR ref ( F 2 ) = 0.2220, T = 100(10) K.
Open Access
Crystal structure of poly[aqua-μ₂-4,4′-bipyridine-κ²N:N′)-μ₂-bis(2-(2-((2,6-dichlorophenyl)amino)phenyl)acetato-κ²O,O′)zinc(II)], C₃₈H₂₈Cl₄N₄O₄Zn

July 7, 2020

Qian-Qian Tang, Shi-Hui Li

Page range: 1277-1278

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C 38 H 28 Cl 4 N 4 O 4 Zn, monoclinic, C 2/ c (no. 19), a = 33.2980(15) Å, b = 7.8254(3) Å, c = 13.8939(9) Å, β = 92.506(5)°, V = 3616.9(3) Å 3 , Z = 4, R gt ( F ) = 0.0702, wR ref ( F 2 ) = 0.1774, T = 293(2) K.
Open Access
Crystal structure of 1-(2-(1H-indol-3-yl)ethyl)-4-benzyl-3-hydroxy-3,6-diphenylpiperazine-2,5-dione, C₃₃H₂₉N₃O₃

July 14, 2020

Ying Fen Li, Xian Wei, Song Bai, Meng Lan Lv

Page range: 1279-1280

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C 33 H 29 N 3 O 3 , triclinic, P 1̅ (no. 2), a = 7.1229(8) Å, b = 12.8851(13) Å, c = 15.0472(15) Å, α = 92.354(2)°, β = 103.338(2)°, γ = 91.502(2)°, V = 1341.7(2) Å 3 , Z = 2, R gt ( F ) = 0.0364, wR ref ( F 2 ) = 0.1074, T = 296(2) K.
Open Access
The crystal structure 2,2′-bipyridine-κ²N,N′-(2-(3-amino-4-chlorobenzoyl)benzoato-κ¹O)-(2-(3-amino-4-chlorobenzoyl)benzoato-κ²O,O′)zinc(II) — ethanol (1/1), C₄₀H₃₂Cl₂N₄O₇Zn

August 25, 2020

Wang Li-Hua, Liang Lei, Tai Xi-Shi

Page range: 1281-1283

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C 40 H 32 Cl 2 N 4 O 7 Zn, monoclinic, P 2 1 / c (no. 14), a = 13.5114(8) Å, b = 16.5735(7) Å, c = 17.0403(9) Å, β = 107.528(6)°, V = 3638.7(3) Å 3 , Z = 4, R gt ( F ) = 0.0398, wR ref ( F 2 ) = 0.0831, T = 100 K.
Open Access
Crystal structure of catena-poly[(μ₃-2-carboxy-4-(3-carboxy-5-carboxylatophenoxy)benzoato-κ³O:O′:O′′)-bis(μ₂-4,4′-bis(pyrid-4-yl)biphenyl-k¹N)copper(II)], C₆₀H₄₀N₄O₉Cu

August 20, 2020

Shi-Hui Li, Qian-Qian Tang

Page range: 1285-1287

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C 60 H 40 N 4 O 9 Cu, triclinic, P 1̄ (no. 2), a = 9.6569(8) Å, b = 10.3941(7) Å, c = 24.9421(16) Å, α = 97.162(5)°, β = 90.953(6)°, γ = 107.788(7)°, V = 2361.3(3) Å 3 , Z = 2, R gt ( F ) = 0.0729, wR ref ( F 2 ) = 0.1609, T = 293(2) K.
Open Access
The crystal structure of dimethylammonium catena-[di(μ-aqua)-bis(μ₉-benzene-1,3,5-tricarboxylato)pentalithium], C₂₀H₁₆Li₅NO₁₃

September 9, 2020

Ying Li, Yu-Cai Qin, Bao-Kuan Chen

Page range: 1289-1291

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C 20 H 16 Li 5 NO 13 , orthorhombic, Pnma (no. 62), a = 9.9218(8) Å, b = 14.6941(11) Å, c = 13.5697(10) Å, V = 1978.4(3) Å 3 , Z = 4, R gt ( F ) = 0.0439, wR ref ( F 2 ) = 0.0960, T = 173(2) K.
Open Access
Crystal structure of tetraaqua-bis(3,5-di(pyridin-4-yl)-1,2,4-triazol-1-ido-κ¹N)nickel(II) dihydrate, C₂₄H₂₈O₆N₁₀Ni

August 20, 2020

Xue-Li Xu, Shi-Hui Li

Page range: 1293-1294

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C 24 H 28 O 6 N 10 Ni, monoclinic, P 2 1 / c (no. 14), a = 7.3274(4) Å, b = 15.6403(5) Å, c = 11.8035(6) Å, β = 106.966(5)°, V = 1293.85(10) Å 3 , Z = 2, R gt ( F ) = 0.0397, wR ref ( F 2 ) = 0.1002, T = 293(2) K.
Open Access
The crystal structure of tetrakis(1-methylimidazole-κ¹N)-oxido-(sulfato-κ¹O)vanadium(IV), C₁₆H₂₄N₈O₅SV

July 22, 2020

Gang Zhang, Jian Luan, Xiao-Jie Wang

Page range: 1295-1296

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C 16 H 24 N 8 O 5 SV, monoclinic, P 2 1 / c (no. 14), a = 9.6165(6) Å, b = 16.6705(10) Å, c = 15.2726(7) Å, β = 121.630(3)°, V = 2084.7(2) Å 3 , Z = 4, R gt ( F ) = 0.0417, wR ref ( F 2 ) = 0.1443, T = 296(2) K.
Open Access
Crystal structure of methyl 2-(6,11-dioxo-2,3,6,11-tetrahydro-1H-benzo[f]pyrrolo[2,1-a]isoindole-5-carbonyl)benzoate, C₂₄H₁₇NO₅

July 3, 2020

Bo Fang, Jiang Ping Meng, Yan Luo

Page range: 1297-1299

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C 24 H 17 NO 5 , triclinic, P 1̄ (no. 2), a = 8.5858(2) Å, b = 9.2397(4) Å, c = 13.7831(8) Å, α = 97.11(3)°, β = 103.23(3)°, γ = 113.33(3)°, V = 948.8(2) Å 3 , Z = 2, R gt ( F ) = 0.0545, wR ref ( F 2 ) = 0.1669, T = 296(2) K.
Open Access
Crystal structure of (E)-N′-(2-hydroxy-4-(2-(piperidin-1-yl)ethoxy)benzylidene) nicotinohydrazide monohydrate, C₂₀H₂₄N₄O₃ ⋅ H₂O

July 22, 2020

Xiao-Li Chen, Le-Tao Sun, Qi-Long Zhang, Hong Xu, Xian-Jiong Yang

Page range: 1301-1302

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C 20 H 26 N 4 O 4 , monoclinic, P 2 1 / a (no. 14), a = 12.107(3) Å, b = 7.8431(19) Å, c = 21.794(5) Å, β = 98.233(5)°, V = 2048.1(8) Å 3 , Z = 4, R gt ( F ) = 0.0458, wR ref ( F 2 ) = 0.1208, T = 293(2) K.
Open Access
Crystal structure of poly[bis(μ₃-(1-(3,5-di(1H-imidazol-1-yl)phenyl)-1H-imidazole-κ³N:N′:N′′)cobalt(II)] dinitrate — N,N-dimethylformamide (1/4), C₄₂H₅₂N₁₈O₁₀Co

July 27, 2020

Yabin Sun, Yan Chen, Daguang Wang

Page range: 1303-1305

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C 42 H 52 N 18 O 10 Co, monoclinic, P 2 1 / c (no. 14), a = 11.3692(7) Å, b = 17.5938(10) Å, c = 12.1825(7) Å, β = 108.6360(10)°, V = 2309.1(2) Å 3 , Z = 2, R gt ( F ) = 0.0308, wR ref ( F 2 ) = 0.0765, T = 120(2) K.
Open Access
The crystal structure bis{hexakis(1-methyl-1H-imidazole-κ¹N)cobalt(II)} tetrakis(μ₃-oxido)-octakis(μ₂-oxido)-tetradecaoxido-octamolybdate(VI), C₂₄H₃₆CoMo₄N₁₂O₁₃

September 2, 2020

Gang Zhang, Jian Luan, Xiao-Jie Wang

Page range: 1307-1309

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C 24 H 36 CoMo 4 N 12 O 13 , triclinic, P 1̄ (no. 2), a = 11.155(5) Å, b = 13.889(6) Å, c = 14.081(6) Å, α = 64.544(12)°, β = 79.558(14)°, γ = 87.084(14)°, V = 1936.3(15) Å 3 , Z = 2, R gt ( F ) = 0.0365, wR ref ( F 2 ) = 0.1171, T = 293(2) K.
Open Access
Crystal structure of di-μ-nicotinato-κ²N:O; κ²O:N-bis-[aqua-bis(benzyl)(nicotinato-κ²O,O′)tin(IV)], C₅₂H₄₈N₄O₁₀Sn₂

September 29, 2020

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 1311-1313

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C 52 H 48 N 4 O 10 Sn 2 , triclinic, P 1̄ (no. 2), a = 8.4845(1) Å, b = 9.2814(1) Å, c = 15.5517(2) Å, α = 83.005(1)°, β = 81.918(1)°, γ = 74.690(1)°, V = 1164.87(2) Å 3 , Z = 1, R gt ( F ) = 0.0173, wR ref ( F 2 ) = 0.0453, T = 100(2) K.
Open Access
Crystal structure of dichlorido-bis[2-(2-(3-(pyridin-2-yl)-1H-1,2,4-triazol-5-yl)phenoxy)benzoic acidmanganese(II) monohydrate, C₄₀H₃₀N₈O₇MnCl₂

July 23, 2020

Qiang Xu, Hong Yan Zhang, Xiao fang Luo, Guo qiang Li

Page range: 1315-1317

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C 40 H 30 N 8 O 7 MnCl 2 , monoclinic, C 2/ c (no. 15), a = 13.0864(7) Å, b = 25.6216(9) Å, c = 12.2253(7) Å, β = 112.027(6)°, V = 3799.9(3) Å 3 , Z = 4, R gt ( F ) = 0.0413, wR ref ( F 2 ) = 0.1001, T = 293(2) K.
Open Access
The crystal structure of benzyl 3β-acetylglycyrrhetate, C₃₉H₅₄O₅

August 1, 2020

Ruo-Lin Zhao, Hui-Yun Wang, Xiao-Hui Wang, Li Liu, Qing-Guo Meng

Page range: 1319-1321

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C 39 H 54 O 5 , monoclinic, P 2 1 (no. 4), a = 6.98138(17) Å, b = 37.9050(6) Å, c = 7.28644(16) Å, β = 117.789(3)°, V = 1705.82(8) Å 3 , Z = 2, R gt ( F ) = 0.0326, wR ref ( F 2 ) = 0.0872, T = 293(2) K.
Open Access
Synthesis and crystal structure of (E)-1-benzyl-3-(4-methoxystyryl)quinoxalin-2(1H)-one, C₂₄H₂₀N₂O₂

July 15, 2020

Mohcine Missioui, El Mokhtar Essassi, Joel T. Mague, Youssef Ramli

Page range: 1323-1325

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C 24 H 20 N 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 11.1713(3) Å, b = 17.7718(5) Å, c = 10.9852(3) Å, β = 118.990(1)°, V = 1907.67(9) Å 3 , Z = 4, R gt ( F ) = 0.0538, wR ref ( F 2 ) = 0.1582, T = 296(2) K.
Open Access
Crystal structure of trans-dichloridobis(4-chlorophenyl-κC¹)(1,10-phenanthroline-κ²N,N′)tin(IV) dimethylsulphoxide solvate, C₂₆H₂₂Cl₄N₂OSSn

July 24, 2020

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 1327-1329

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C 26 H 22 Cl 4 N 2 OSSn, triclinic, P 1̄ (no. 2), a = 8.2966(1) Å, b = 11.4971(2) Å, c = 14.3311(2) Å, α = 90.322(2)°, β = 101.783(1)°, γ = 95.780(1)°, V = 1330.91(3) Å 3 , Z = 2, R gt ( F ) = 0.0258, wR ref ( F 2 ) = 0.0684, T = 100 K.
Open Access
Crystal structure of phenyl(1,3,4a-triphenyl-4a,5,6,10b-tetrahydro-1H-[1,4]oxazino[2,3-c]quinolin-5-yl)methanone, C₃₆H₂₈N₂O₂

July 27, 2020

Xue Li, Chao Chen, Mei-Hang Zhang, Jin-Min Wang, Fu-Min Feng

Page range: 1331-1333

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C 36 H 28 N 2 O 2 , triclinic, P 1̄ (no. 2), a = 9.6248(18) Å, b = 10.848(2) Å, c = 14.099(3) Å, α = 95.822(2)°, β = 105.907(2)°, γ = 102.404(2)°, V = 1362.4(5) Å 3 , Z = 2, R gt ( F ) = 0.0497, wR ref ( F 2 ) = 0.1205, T = 296 K.
Open Access
Crystal structure of (4aS,5S,6aS,6a¹S, 10aS)-4a,5,6a,6a¹,9,10-hexahydro-7H-4,5-methanocyclobuta[4,5]naphtho[8a,1-b]pyran-6(2H)-one, C₁₅H₁₆O₂

July 23, 2020

Shengxian Zhai, Youzhu Yu, Yongsheng Niu, Chuchu Han

Page range: 1335-1337

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C 15 H 16 O 2 , triclinic, P 1̄ (no. 2), a = 5.6034(7) Å, b = 8.7105(11) Å, c = 12.5661(16) Å, α = 92.790(7)°, β = 100.516(7)°, γ = 106.105(6)°, V = 576.15(13) Å 3 , Z = 2, R gt ( F ) = 0.0476, wR ref ( F 2 ) = 0.1348, T = 296.15 K.
Open Access
Crystal structure of [(Z)-O-isopropyl N-(4-chlorophenyl)thiocarbamato-κS]-(triphenylphosphine-κP)-gold(I), C₂₈H₂₆AuClNOPS

July 21, 2020

Chien Ing Yeo, Edward R.T. Tiekink

Page range: 1339-1341

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C 28 H 26 AuClNOPS, monoclinic, P 2 1 / c (no. 14), a = 9.7445(3) Å, b = 12.4105(4) Å, c = 21.9727(9) Å, β = 100.113(1)°, V = 2615.96(16) Å 3 , Z = 4, R gt ( F ) = 0.0292, wR ref ( F 2 ) = 0.0677, T = 100 K.
Open Access
Crystal structure of (μ₂-1,1′-bis(diphenylphosphino)ferrocene-P,P′)-bis[(Z)-O-isopropyl N-(4-chlorophenyl)thiocarbamato-S]-di-gold(I) acetonitrile di-solvate, C₅₄H₅₀Au₂Cl₂FeN₂O₂P₂S₂⋅2(C₂H₃N)

July 22, 2020

Chien Ing Yeo, Edward R.T. Tiekink

Page range: 1343-1345

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C 58 H 56 Au 2 Cl 2 FeN 4 O 2 P 2 S 2 , triclinic, P 1̄ (no. 2), a = 8.5422(3) Å, b = 13.2143(4) Å, c = 14.0226(4)) Å, α = 65.764(3)°, β = 78.311(2)°, γ = 80.090(3)°, V = 1406.39(8) Å 3 , Z = 1, R gt ( F ) = 0.0213, wR ref ( F 2 ) = 0.0477, T = 100 K.
Open Access
Crystal structure of (6aR,6a¹S,10aS)-2,4a,6a,6a¹,9,10-hexahydro-7H-4,5-methanocyclobuta[4,5]naphtho[8a,1-b]pyran, C₁₅H₁₆O

July 23, 2020

Shengxian Zhai, Lunjian Chen, Yongsheng Niu, Chuchu Han

Page range: 1347-1348

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C 15 H 16 O, monoclinic, P 2 1 / c (no. 14), a = 5.4371(7) Å, b = 17.567(2) Å, c = 11.8840(18) Å, β = 101.043(9)°, V = 1114.1(3) Å 3 , Z = 4, R gt ( F ) = 0.0422, wR ref ( F 2 ) = 0.1155, T = 296(2) K.
Open Access
Crystal structure of 5,17-diformyl-25,26,27,28-tetrahydroxycalix[4]arene- dichloromethane, C₃₁H₂₆Cl₂O₆

July 18, 2020

Chong Wu, Xiao-Long Liu, Rui An, Ye Yang

Page range: 1349-1350

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C 30 H 24 O 6 ⋅ CH 2 Cl 2 , orthorhombic, Pbcn (no. 60), a = 11.6965(10) Å, b = 13.8078(11) Å, c = 16.3257(14) Å, V = 2636.6(4) Å 3 , Z = 4, R gt ( F ) = 0.0765, wR ref ( F 2 ) = 0.1487, T = 296(2) K.
Open Access
Crystal structure of 2-tert-butyl 1-methyl 5-{4-[(methoxycarbonyl)amino]phenyl}-2,5-dihydro-1H-pyrrole-1,2-dicarboxylate, C₁₉H₂₄N₂O₆

July 18, 2020

Ignez Caracelli, Julio Zukerman-Schpector, Ariel L. Llanes Garcia, Carlos Roque D. Correia, Edward R.T. Tiekink

Page range: 1351-1354

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C 19 H 24 N 2 O 6 , monoclinic, P 2 1 (no. 4), a = 8.3611(7) Å, b = 9.0521(8) Å, c = 13.8988(8) Å, β = 106.710(5)°, V = 1007.52(14) Å 3 , Z = 2, R gt ( F ) = 0.0428, wR ref ( F 2 ) = 0.1174, T = 293(2) K.
Open Access
Crystal structure of [2-carboxybenzene-1-thiolato-S]-(triethylphosphane-P)-gold(I), C₁₃H₂₀AuO₂PS

August 4, 2020

Chien Ing Yeo, Edward R.T. Tiekink

Page range: 1355-1358

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C 13 H 20 AuO 2 PS, triclinic, P 1̄ (no. 2), a = 7.7509(2) Å, b = 12.7840(3) Å, c = 15.8689(4) Å, α = 89.087(2)°, β = 87.065(2)°, γ = 84.797(2)°, V = 1563.78(7) Å 3 , Z = 4, R gt ( F ) = 0.0282, wR ref ( F 2 ) = 0.0795, T = 100 K.
Open Access
Synthesis and crystal structure of bis(5-methyl-2-aldehyde-phenolato-κ²O¹,O²)copper(II), C₁₆H₁₄CuO₄

July 28, 2020

Qin Wu

Page range: 1359-1360

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C 16 H 14 CuO 4 , monoclinic, P 2 1 / c (no. 14), a = 12.7831(4) Å, b = 4.71970(10) Å, c = 12.1802(4) Å, β = 114.557(1)°, Z = 2, V = 668.39(3) Å 3 , R gt ( F ) = 0.0211, wR ref ( F 2 ) = 0.0624, T = 173(2) K
Open Access
Crystal structure of poly[triaqua-(di(2,2′-bipyridine-κ²N,N′)-μ₄-silanetetrayltetrakis(benzene-4,1-diyl)tetrakis (hydrogen phosphonato)-κ⁴O:O′:O′′:O′′′) dicadmium(II)], C₄₄H₄₂N₄O₁₅P₄Cd₂Si

September 12, 2020

Baogang Wang, Xiaxia Man

Page range: 1361-1363

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C 44 H 42 N 4 O 15 P 4 Cd 2 Si, triclinic, P 1̄ (no. 2), a = 13.4778(9) Å, b = 14.2036(9) Å, c = 15.2206(10) Å, α = 69.637(1)°, β = 72.355(1)°, γ = 64.861(1)°, V = 2431.1(3) Å 3 , Z = 2, R gt ( F ) = 0.0428, wR ref ( F 2 ) = 0.0987, T = 120(2) K.
Open Access
Crystal structure of bis[μ₂-(N,N-diethylcarbamodithioato-κS:κS,κS′)]-bis(triethylphosphine-P)-di-silver(I), C₂₂H₅₀Ag₂N₂P₂S₄

July 27, 2020

Chien Ing Yeo, Yi Jiun Tan, Aya Shiomitsu, Jactty Chew, Nathan R. Halcovitch, Edward R.T. Tiekink

Page range: 1365-1368

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C 22 H 50 Ag 2 N 2 P 2 S 4 , triclinic, P 1̄ (no. 2), a = 9.0672(2) Å, b = 11.2091(3) Å, c = 16.6853(4) Å, α = 91.097(2)°, β = 90.363(2)°, γ = 110.989(2)°, V = 1582.85(7) Å 3 , Z = 2, R gt ( F ) = 0.0241, wR ref ( F 2 ) = 0.0653, T = 100(2) K.
Open Access
Crystal structure of bis[μ₂-(pyrrolidine-1-carbodithioato-κS:κS,κS′)]-bis(triethylphosphine-κP)disilver(I), C₂₂H₄₆Ag₂N₂P₂S₄

July 21, 2020

Yi Jiun Tan, Chien Ing Yeo, Nathan R. Halcovitch, Edward R.T. Tiekink

Page range: 1369-1371

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C 22 H 46 Ag 2 N 2 P 2 S 4 , triclinic, P 1̄ (no. 2), a = 10.2008(3) Å, b = 12.2058(3) Å, c = 13.2466(4) Å, α = 88.155(2)°, β = 87.256(2)°, γ = 69.324(2)°, V = 1541.12(8) Å 3 , Z = 2, R gt ( F ) = 0.0237, wR ref ( F 2 ) = 0.0621, T = 100(2) K.
Open Access
Crystal structure of bis[μ₂-(N-(2-hydroxyethyl)-N-methylcarbamodithioato-κS:κS,κS′)]-bis(triethylphosphine-P)-di-silver(I), C₂₀H₄₆Ag₂N₂O₂P₂S₄

July 28, 2020

Chien Ing Yeo, Kong Mun Lo, Edward R.T. Tiekink

Page range: 1373-1376

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C 20 H 46 Ag 2 N 2 O 2 P 2 S 4 , triclinic, P 1̄ (no. 2), a = 9.3895(1) Å, b = 13.1597(2) Å, c = 13.1803(2) Å, α = 88.119(1)°, β = 86.601(1)°, γ = 70.173(1)°, V = 1529.22(4) Å 3 , Z = 2, R gt ( F ) = 0.0162, wR ref ( F 2 ) = 0.0406, T = 100(2) K.
Open Access
The crystal structure of (2E,2′E)-,2,2′-bis[1-(2-pyrazinyl)ethylidene]carbonimidic dihydrazide, C₁₃H₁₅N₉

July 18, 2020

Xiao-Hui Ji, Ye Liu, Mei-Ling Liu, Juan Zhao, Jiu-Fu Lu

Page range: 1377-1379

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C 13 H 15 N 9 , monoclinic, C 2/ c (no. 15), a = 22.827(5) Å, b = 7.8830(16) Å, c = 16.020(3) Å, β = 98.95(3)°, V = 2847.6(10) Å 3 , Z = 8, R gt ( F ) = 0.0416, wR ref ( F 2 ) = 0.1331, T = 293(2) K.
Open Access
The crystal structure of (E)-1-(quinolin-2-ylmethyl)-2-((1-(quinolin-2-ylmethyl)pyridin-2(1H)-ylidene)amino)pyridin-1-ium, C₃₀H₂₅BrN₅

August 7, 2020

Orbett T. Alexander, Andreas Roodt

Page range: 1381-1383

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C 30 H 25 BrN 5 , monoclinic, P 2 1 / c (no. 14), a = 15.685(4) Å, b = 9.317(2) Å, c = 18.373(4) Å, β = 114.422(7)°, V = 2444.8(10) Å 3 , Z = 4, R gt ( F ) = 0.0377, wR ref ( F 2 ) = 0.0849, T = 112(2) K.
Open Access
Crystal structure of catena-poly[(μ₂-1-((benzotriazol-1-yl)methyl)-1H-1,3-imdazole-κ²N:N′)-(1-((benzotriazol-1-yl)methyl)-1H-1,3-imdazole-κ¹N)-(methanol-κ¹O)mercury(II)] dinitrate, C₂₁H₂₂N₁₂O₇Hg

August 26, 2020

Shu-Xiang Sun, Zhi-Min Lu, Ke-Qing Zhang, Pei Yao

Page range: 1385-1387

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C 21 H 22 N 12 O 7 Hg, monoclinic, P 2/ n (no. 13), a = 13.655(3) Å, b = 8.7038(17) Å, c = 23.260(5) Å, β = 102.51(3)°, V = 2698.8(10) Å 3 , Z = 4, R gt ( F ) = 0.0446, wR ref ( F 2 ) = 0.0875, T = 293(2) K.
Open Access
Crystal structure of 1-(6-hydroxy-2-phenylbenzofuran-5-yl)ethan-1-one, C₁₆H₁₂O₃

August 1, 2020

Temitope O. Olomola, Marole M. Maluleka, Malose J. Mphahlele

Page range: 1389-1391

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C 16 H 12 O 3 , orthorhombic, Pbca (no. 61), a = 10.7095(3) Å, b = 8.1455(2) Å, c = 27.5374(8) Å, V = 2402.20(11) Å 3 , Z = 8, R gt ( F ) = 0.0369, wR ref ( F 2 ) = 0.0947, T = 173(2) K.
Open Access
The crystal structure of oxonium hexaquaaluminium disulfate hexahydrate

October 5, 2020

Yan Liu, Min Hao, Jianfeng Gao, Jianghui Liu, Juan Cui

Page range: 1393-1394

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AlH 27 S 2 O 21 , cubic, Pa 3̄ (no. 205), a = 12.2403(14) Å, V = 1833.9(6) Å 3 , Z = 4, R gt ( F ) = 0.0507, wR ref ( F 2 ) = 0.1458, T = 298 K.
Open Access
Crystal structure of catena{(μ₂-1,10-phenanthroline-κ⁴N,N,N′,N′)-(μ₂-1,10-phenanthroline-κ³N,N,N′)potassium(I) {[bis(2-hydroxyethyl)iminiumyl](sulfanidyl)methyl}sulfanide hemi(1,10-phenanthroline)}, {C₂₄H₁₆KN₄, 0.5(C₁₂H₈N₂), C₅H₁₀NO₂S₂}

August 1, 2020

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 1395-1397

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C 35 H 30 KN 6 O 2 S 2 , monoclinic, C 2/ c (no. 15), a = 32.8001(4) Å, b = 7.1562(1) Å, c = 26.0400(3) Å, β = 94.385(1)°, V = 6094.32(13) Å 3 , Z = 8, R gt ( F ) = 0.0315, wR ref ( F 2 ) = 0.0911, T = 100(2) K.
Open Access
Crystal structure of chlorido-[(N,N-di-isobutyl)dithiocarbamato-κ²S,S′]-di(4-methylbenzyl-κC)tin(IV), C₂₅H₃₆ClNS₂Sn

July 30, 2020

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Page range: 1399-1401

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C 25 H 36 ClNS 2 Sn, monoclinic, P 2 1 / n (no. 14), a = 12.7694(1) Å, b = 9.7283(1) Å, c = 21.5640(2) Å, β = 97.978(1)°, V = 2652.85(4) Å 3 , Z = 4, R gt ( F ) = 0.0167, wR ref ( F 2 ) = 0.0444, T = 100(2) K.
Open Access
Crystal structure of chlorido-(η⁵-pentamethylcyclopentadienyl)-(4-chloro-4-pyridyl-2,2′:6′,2′′-terpyridine-κ²N,N′) rhodium(III) hexaflourophosphate, C₃₁H₂₉Cl₂F₆N₃PRh

September 15, 2020

Joel M. Gichumbi, Sizwe J. Zamisa, Holger B. Friedrich

Page range: 1403-1405

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C 31 H 29 Cl 2 F 6 N 3 PRh, monoclinic, P 2 1 / c (no. 14), a = 7.4069(7) Å, b = 13.245(1) Å, c = 32.141(3) Å, β = 93.924(2)°, V = 3145.8(5) Å 3 , Z = 4, R gt ( F ) = 0.0386, wR ref ( F 2 ) = 0.0962, T = 123.15 K.
Open Access
The crystal structure of catena-poly[bis-(3,5-dinitro-1,2,4-triazolato-κ²N:O)-(μ₂-1,4-bis(1-imidazolyl)benzene-κ²N:N′)copper(II)], C₁₆H₁₀CuN₁₄O₈

September 4, 2020

Li Yajin, Xie Wuxi, Song Kuanguang, Zhao Yu

Page range: 1407-1408

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C 16 H 10 CuN 14 O 8 , monoclinic, C 2/ c (no. 15), a = 13.4851(13) Å, b = 12.3808(12) Å, c = 13.2151(13) Å, β = 97.3040(10)°, V = 2188.4(4) Å 3 , Z = 4, R gt ( F ) = 0.0310, wR ref ( F 2 ) = 0.1127, T = 296(2) K.
Open Access
Crystal structure of poly[triaqua-bis(μ₃-3,3′-((5-carboxylato-1,3-phenylene)bis(oxy))dibenzoato)-tris(1,10-phenanthroline)cobalt(II)], C₇₈H₄₆N₆O₂₀Co₃

September 28, 2020

Pei-xuan Li, Wei Hui

Page range: 1409-1411

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C 78 H 46 N 6 O 20 Co 3 , monoclinic, P 2 1 / c (no. 14), a = 10.789(4) Å, b = 48.885(18) Å, c = 15.205(4) Å, β = 124.604(19)°, V = 6601(4) Å 3 , Z = 4, R gt ( F ) = 0.0539, wR ref ( F 2 ) = 0.1205, T = 293(2) K.
Open Access
The crystal structure of 2,4-dihydroxybenzoic acid–nicotinamide–methanol (1/1/1), C₁₅H₁₈N₂O₆

August 26, 2020

Bencai Dai, Yang Zhou, Jin Chen, Changchun Liu, Zhihao Shen, Junming Tang

Page range: 1413-1415

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C 2 H 6 O⋅C 6 H 6 N 2 O⋅C 7 H 6 O 4 , triclinic, P 1̄ (no. 2), a = 7.4217(18) Å, b = 7.7021(18) Å, c = 15.362(4) Å, α = 79.223(2)°, β = 82.086(3)°, γ = 65.182(2)°, V = 781.2(3) Å 3 , Z = 2, R gt ( F ) = 0.0444, wR ref ( F 2 ) = 0.1341, T = 296(2) K.
Open Access
The crystal structure of aqua{N,N,N′,N′-tetrakis[(1H-benzimidazol-κN³) methyl]cyclohexane-1,2-diamine}lead(II) diacetate–methanol (1/2), C₄₄H₅₄N₁₀O₇Pb

August 20, 2020

Ji Li, Ming-Zhi Miao

Page range: 1417-1420

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PbC 44 H 54 N 10 O 7 , triclinic, P 1̄ (no. 2), a = 12.096(2) Å, b = 12.916(2) Å, c = 16.5904(7) Å, α = 101.163(2)°, β = 110.634(2)°, γ = 100.698(2)°, V = 2287.0(4) Å 3 , Z = 2, R gt ( F ) = 0.0604, wR ref ( F 2 ) = 0.1409, T = 298(2) K.
Open Access
Crystal structure of (2-amino-5-bromo-3-iodophenyl)(3-(4-chlorophenyl)oxiran-2-yl)methanone, C₁₅H₁₀BrClINO₂

August 18, 2020

Marole M. Maluleka, Malose J. Mphahlele

Page range: 1421-1423

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C 15 H 10 BrClINO 2 , monoclinic, P 2 1 / n (no. 14), a = 5.0083(2) Å, b = 9.7548(3) Å, c = 31.9640(10) Å, β = 92.576(2)°, V = 1560.02(9) Å 3 , Z = 4, R gt ( F ) = 0.0416, wR ref ( F 2 ) = 0.1059, T = 173 K.
Open Access
Synthesis and crystal structure of 3-octyl-5,5-diphenylimidazolidine-2,4-dione, C₂₃H₂₈N₂O₂

August 18, 2020

Walid Guerrab, Joel T. Mague, Youssef Ramli

Page range: 1425-1427

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C 23 H 28 N 2 O 2 , orthorhombic, Pbca (no. 61), a = 10.713(2) Å, b = 15.689(3) Å, c = 24.485(5) Å, V = 4115.2(14) Å 3 , Z = 8, R gt ( F ) = 0.0581, wR ref ( F 2 ) = 0.1734, T = 120(2) K.
Open Access
Synthesis and crystal structure of 2-azido-N-(4-nitrophenyl)acetamide, C₈H₇N₅O₃

August 8, 2020

Mohcine Missioui, Walid Guerrab, Joel T. Mague, Youssef Ramli

Page range: 1429-1430

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C 8 H 7 N 5 O 3 , monoclinic, P 2 1 / n (no. 14), a = 5.0340(2) Å, b = 21.1023(9) Å, c = 9.2880(4) Å, β = 94.909(1)°, V = 983.04(7) Å 3 , Z = 4, R gt ( F ) = 0.0470, wR ref ( F 2 ) = 0.1496, T = 298(2) K.
Open Access
Crystal structure of tert-butyl (1S,2R,5R)-2-(hydroxymethyl)-4-(4-methoxyphenyl)-6-oxa-3-azabicyclo[3.1.0]hexane-3-carboxylate, C₁₇H₂₃NO₅

August 12, 2020

Ignez Caracelli, Julio Zukerman-Schpector, Ariel L. Llanes Garcia, Carlos Roque D. Correia, Edward R.T. Tiekink

Page range: 1431-1433

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C 17 H 23 NO 5 , monoclinic, P 2 1 (no. 4), a = 6.0479(9) Å, b = 9.7032(10) Å, c = 14.711(2) Å, β = 94.174(9)°, V = 861.0(2) Å 3 , Z = 2, R gt ( F ) = 0.0440, wR ref ( F 2 ) = 0.1436, T = 293(2) K.
Open Access
Crystal structure of 4-[(4-methoxy-2-nitrophenyl)carbamoyl]butanoic acid, C₁₂H₁₄N₂O₆

August 12, 2020

Bibi Hanifa, Muhammad Sirajuddin, Kong Mun Lo, Edward R.T. Tiekink

Page range: 1435-1437

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C 12 H 14 N 2 O 6 , triclinic, P 1̄ (no. 2), a = 4.8835(4) Å, b = 9.2111(7) Å, c = 14.6655(7) Å, α = 76.135(5)°, β = 82.693(6)°, γ = 87.379(7)°, V = 635.19(8) Å 3 , Z = 2, R gt ( F ) = 0.0449, wR ref ( F 2 ) = 0.1297, T = 293(1) K.
Open Access
Crystal structure of 3-ethyl-1-[(E)-[(2E)-3-phenylprop-2-en-1-ylidene]amino]thiourea, C₁₂H₁₅N₃S

August 21, 2020

Ming Yueh Tan, Sheng Zhou Ho, Kong Wai Tan, Edward R.T. Tiekink

Page range: 1439-1441

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C 12 H 15 N 3 S, orthorhombic, Pbca (no. 61), a = 11.9612(5) Å, b = 8.1215(3) Å, c = 27.5865(12) Å, V = 2679.83(19) Å 3 , Z = 8, R gt ( F ) = 0.0520, wR ref ( F 2 ) = 0.1514, T = 293(2) K.
Open Access
Crystal structure of 4,4′-bipyridin-1,1′-dium poly[bis(μ₄-benzene-1,3,5-triyltris(hydrogen phosphonato-κ⁴O:O′:O′′:O′′′))zinc(II)], C₁₁H₁₁NO₉P₃Zn

August 20, 2020

Yabin Sun, Yan Chen, Daguang Wang

Page range: 1443-1444

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C 11 H 11 NO 9 P 3 Zn, monoclinic, P 2 1 / n (no. 14), a = 12.619(2) Å, b = 8.4948(12) Å, c = 13.954(2) Å, β = 90.588(3)°, V = 1495.7(4) Å 3 , Z = 4, R gt ( F ) = 0.0413, wR ref ( F 2 ) = 0.0965, T = 120(2) K.
Open Access
Crystal structure of (μ₂-1,1′-bis(diphenylphosphino)butane-κ²P,P′)-bis[(Z)-N-(3-fluorophenyl)-O-methylthiocarbamato-κS]-di-gold(I), C₄₄H₄₂Au₂F₂N₂O₂P₂S₂

August 21, 2020

Chien Ing Yeo, Edward R.T. Tiekink

Page range: 1445-1448

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C 44 H 42 Au 2 F 2 N 2 O 2 P 2 S 2 , triclinic, P 1̄ (no. 2), a = 8.8035(2) Å, b = 11.4764(3) Å, c = 21.2293(6) Å, α = 83.550(2)°, β = 82.256(2)°, γ = 83.793(2)°, V = 2102.40(10) Å 3 , Z = 2, R gt ( F ) = 0.0268, wR ref ( F 2 ) = 0.0577, T = 100(2) K.
Open Access
Crystal structure of (μ₂-1,1′-bis(diphenylphosphino)hexane-κ²P,P′)-bis[(Z)-N-(3-fluorophenyl)-O-methylthiocarbamato-κS]digold(I), C₄₆H₄₆Au₂F₂N₂O₂P₂S₂

August 18, 2020

Chien Ing Yeo, Edward R.T. Tiekink

Page range: 1449-1451

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C 46 H 46 Au 2 F 2 N 2 O 2 P 2 S 2 , triclinic, P 1̄ (no. 2), a = 8.2496(3) Å, b = 11.4366(4) Å, c = 12.9504(4) Å, α = 109.171(3)°, β = 92.496(3)°, γ = 100.208(3)°, V = 1128.98(7) Å 3 , Z = 1, R gt ( F ) = 0.0246, wR ref ( F 2 ) = 0.0560, T = 100(2) K.
Open Access
Crystal structure of tetrakis (N-(2-hydroxyethyl)-N-isopropylcarbamodithioato-κS,S′)-(μ₂(2-(pyridin-4-yl)vinyl)pyridine-κN,N′)dicadmium(II), C₃₆H₅₈Cd₂N₆O₄S₈

August 13, 2020

Chien Ing Yeo, Edward R.T. Tiekink

Page range: 1453-1456

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C 36 H 58 Cd 2 N 6 O 4 S 8 , monoclinic, P 2 1 / c (no. 14), a = 7.82927(4) Å, b = 11.64209(5) Å, c = 26.2493(1) Å, β = 95.6985(4)°, V = 2380.775(18) Å 3 , Z = 2, R gt ( F ) = 0.0158, wR ref ( F 2 ) = 0.0411, T = 100(2) K.
Open Access
Crystal structure of 4-(2-(benzo[b]thiophen-2-yl)-3,3,4,4,5,5-hexafluorocyclopent-1-en-1-yl)-1,5-dimethyl-1H-pyrrole-2-carbonitrile, C₂₀H₁₂F₆N₂S

August 27, 2020

Ying Li

Page range: 1457-1459

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C 20 H 12 F 6 N 2 S, monoclinic, P 2 1 / c (no. 14), a = 8.2091(9) Å, b = 13.9215(16) Å, c = 16.5280(19) Å, β = 94.0670(10)°, V = 1884.1(4) Å 3 , Z = 4, R gt ( F ) = 0.0421, wR ref ( F 2 ) = 0.1226, T = 296(2) K.
Open Access
Crystal structure of bis(octahydrocyclopenta[c]pyrrolium)pentachlorobismuthate(III), (C₇NH₁₄)₂BiCl₅

August 28, 2020

Yuxin Ma, Munan Hao, Xin Zhong, Junyan Zhou, Zeyu Zhang, Shifeng Jin, Changchun Zhao

Page range: 1461-1462

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(C 7 NH 14 ) 2 BiCl 5 , monoclinic, P 2 1 / n (no. 14), a = 13.6087(3) Å, b = 7.4645(2) Å, c = 21.7967(6) Å, β = 104.3220(9)°, V = 2145.34(10) Å 3 , Z = 4, R gt ( F ) = 0.0205, wR ref ( F 2 ) = 0.0528, T = 293(2) K.
Open Access
The crystal structure of diaqua-tris(nitrato-κ²O,O′)-bis(4,4,5,5-tetramethyl-2-(p-pyridyl)imidazoline-1-oxyl 3-oxide-κN)samarium(III), C₂₄H₃₆N₉O₁₅Sm

September 3, 2020

Dongjiao Li

Page range: 1463-1464

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C 24 H 36 N 9 O 15 Sm, monoclinic, C 2/ c (no. 14), a = 23.625(3) Å, b = 11.6837(12) Å, c = 11.9293(12) Å, β = 94.6460(10)°, V = 3281.9(6) Å 3 , Z = 4, R gt ( F ) = 0.0173, wR ref ( F 2 ) = 0.0449, T = 293(2) K.
Open Access
Synthesis and crystal structure of methyl 2-(2-((tert-butoxycarbonyl)amino)phenyl)-2-(4-oxo-4H-chromen-3-yl)acetate, C₂₃H₂₃NO₆

August 21, 2020

Wu-Wu Li, Xiong-Li Liu

Page range: 1465-1467

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C 23 H 23 NO 6 , monoclinic, P 2 1 / n (no. 14), a = 7.5845(4) Å, b = 14.7024(5) Å, c = 18.1433(6) Å, β = 98.753(4)°, V = 1999.62(14) Å 3 , Z = 4, R gt ( F ) = 0.0389, wR ref ( F 2 ) = 0.0965, T = 293 K.
Open Access
Crystal structure of O-hexyl benzoylcarbamothioate, C₁₄H₁₉NO₂S

August 21, 2020

Ignez Caracelli, Julio Zukerman-Schpector, Ariel L. Llanes Garcia, Heiddy Márquez Alvarez, Edward R.T. Tiekink

Page range: 1469-1471

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C 14 H 19 NO 2 S, monoclinic, P 2 1 / c (no. 14), a = 8.6849(10) Å, b = 18.740(2) Å, c = 10.0465(12) Å, β = 112.845(3)°, V = 1506.9(3) Å 3 , Z = 4, R gt ( F ) = 0.0685, wR ref ( F 2 ) = 0.2023, T = 293(2) K.
Open Access
Crystal structure of chlorido-(O-methyl phenylcarbamothioamide-κS)-bis(triphenylphosphane-κP)silver(I), C₄₄H₃₉AgClNOP₂S

September 18, 2020

Chien Ing Yeo, Sin-Yeang Teow, Li Yuan Liew, Jactty Chew, Edward R.T. Tiekink

Page range: 1473-1475

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C 44 H 39 AgClNOP 2 S, triclinic, P 1̄ (no. 2), a = 10.2520(3) Å, b = 13.2252(4) Å, c = 14.9378(3) Å, α = 78.424(2)°, β = 78.388(2)°, γ = 84.534(3)°, V = 1940.35(9) Å 3 , Z = 2, R gt ( F ) = 0.0382, wR ref ( F 2 ) = 0.0807, T = 100(2) K.
Open Access
Crystal structure of chlorido-(O-ethyl phenylcarbamothioamide-κS)-bis(triphenylphosphane-κP)-silver(I), C₄₅H₄₁AgClNOP₂S

August 21, 2020

Chien Ing Yeo, Li Yuan Liew, Jactty Chew, Sin-Yeang Teow, Edward R.T. Tiekink

Page range: 1477-1480

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C 45 H 41 AgClNOP 2 S, monoclinic, P 2 1 / c (no. 14), a = 10.1930(3) Å, b = 18.3087(6) Å, c = 21.3088(6) Å, β = 94.516(3)°, V = 3964.3(2) Å 3 , Z = 4, R gt ( F ) = 0.0353, wR ref ( F 2 ) = 0.0810, T = 100(2) K.
Open Access
Crystal structure of 4-[(2-methoxyphenyl)carbamoyl]butanoic acid, C₁₂H₁₅NO₄

August 7, 2020

Bibi Hanifa, Muhammad Sirajuddin, Hizbullah Khan, Kong Mun Lo, Edward R.T. Tiekink

Page range: 1481-1483

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C 12 H 15 NO 4 , triclinic, P 1̄ (no. 2), a = 7.4325(3) Å, b = 7.5171(3) Å, c = 23.7377(9) Å, α = 87.780(3)°, β = 89.105(3)°, γ = 61.299(4)°, V = 1162.42(9) Å 3 , Z = 4, R gt ( F ) = 0.0566, wR ref ( F 2 ) = 0.1652, T = 100(2) K.
Open Access
Crystal structure of ethyl 4-methyl-2-oxo-5-phenyl-1,3,4-oxadiazinane-3-carboxylate, C₁₃H₁₆N₂O₄

September 1, 2020

Ignez Caracelli, Julio Zukerman-Schpector, Alessandro Rodrigues, Elisângela Vinhato, Paulo R. Olivato, Edward R.T. Tiekink

Page range: 1485-1487

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C 13 H 16 N 2 O 4 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 6.7876(2) Å, b = 8.8984(2) Å, c = 22.3399(6) Å, V = 1349.30(6) Å 3 , Z = 4, R gt ( F ) = 0.0384, wR ref ( F 2 ) = 0.0947, T = 293(2) K.
Open Access
Crystal structure of catena-poly[diaqua(μ₂-2-(hydroxymethyl)-1H-imidazole-4,5-dicarboxylato)cadmium(II)], C₆H₈CdN₂O₇

September 2, 2020

Xiao-Ying Huang, Shu-Xiang Sun, Chuan-Qi Wang, Pei Yao

Page range: 1489-1491

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C 6 H 8 CdN 2 O 7 , monoclinic, P 2 1 / c (no. 14), a = 7.3428(15) Å, b = 11.272(2) Å, c = 12.764(4) Å, β = 118.73(2)°, V = 926.4(4) Å 3 , Z = 4, R gt ( F ) = 0.0261, wR ref ( F 2 ) = 0.0609, T = 293(2) K.
Open Access
Crystal structure of (1S)-N-(chloromethyl)-1-((4S,6aR,8aS, 8bR,9aR)-4-methoxy-6a,8a-dimethyl-1,3,4, 5,6,6a,6b,7,8,8a,9a,10,10a,10b-tetradecahydro-8bH-naphtho[2′,1′:4,5] indeno[1,2-b]oxiren-8b-yl)-N-methylethan-1-amine, C₂₄H₄₆ClNO₅

August 22, 2020

Xue-Jing Ning, Xiao-Bin Yang, Jiang Du

Page range: 1493-1494

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C 24 H 46 ClNO 5 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 7.5992(3) Å, b = 9.6634(5) Å, c = 34.7499(7) Å, V = 2551.8(10) Å 3 , Z = 4, R gt ( F ) = 0.0554, wR ref ( F 2 ) = 0.1479, T = 170 K.
Open Access
Crystal structure of 4-[(3,5-dichlorophenyl)carbamoyl]butanoic acid, C₁₁H₁₁Cl₂NO₃

September 18, 2020

Bibi Hanifa, Muhammad Sirajuddin, Kong Mun Lo, Edward R.T. Tiekink

Page range: 1495-1497

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C 11 H 11 Cl 2 NO 3 , monoclinic, P 2 1 / c (no. 14), a = 17.2336(3) Å, b = 4.9604(1) Å, c = 14.3696(3) Å, β = 100.970(2)°, V = 1205.95(4) Å 3 , Z = 4, R gt ( F ) = 0.0313, wR ref ( F 2 ) = 0.0848, T = 293(2) K.
Open Access
Crystal structure of (2Z)-2-amino-3-[(E)-[(2,4-dihydroxyphenyl)methylidene]-amino]but-2-enedinitrile, C₁₁H₈N₄O₂

August 21, 2020

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 1499-1501

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C 11 H 8 N 4 O 2 , triclinic, P 1̄ (no. 2), a = 6.9017(4) Å, b = 6.9496(2) Å, c = 11.2372(7) Å, α = 88.218(4)°, β = 76.489(5)°, γ = 77.575(4)°, V = 511.69(5) Å 3 , Z = 2, R gt ( F ) = 0.0417, wR ref ( F 2 ) = 0.1200, T = 100(2) K.
Open Access
Crystal structure of 3-methyl-1-[(E)-(4-phenylbutan-2-ylidene)amino]thiourea, C₁₂H₁₇N₃S

August 20, 2020

Ming Yueh Tan, Huey Chong Kwong, Karen A. Crouse, Thahira B.S.A. Ravoof, Edward R.T. Tiekink

Page range: 1503-1505

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C 12 H 17 N 3 S, monoclinic, P 2 1 / c (no. 14), a = 9.3084(19) Å, b = 7.9523(16) Å, c = 16.905(3) Å, β = 92.26(3)°, V = 1250.4(4) Å 3 , Z = 4, R gt ( F ) = 0.0330, wR ref ( F 2 ) = 0.0914, T = 100(2) K.
Open Access
Crystal structure of carbonyl{hydridotris[3-phenyl-5-methylpyrazol-1-yl]borato-κ³N,N′N′′}copper(I), C₃₁H₂₈BCuN₆O

August 28, 2020

Kiyoshi Fujisawa, Makoto Yabe, Edward R.T. Tiekink

Page range: 1507-1509

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C 31 H 28 BCuN 6 O, monoclinic, P 2 1 / n (no. 14), a = 11.506(3) Å, b = 16.122(3) Å, c = 15.805(3) Å, β = 99.433(3)°, V = 2892.2(11) Å 3 , Z = 4, R gt ( F ) = 0.0501, wR ref ( F 2 ) = 0.1260, T = 193(2) K.
Open Access
Crystal structure of ethane-1,2-diylbis(diphenylphosphine oxide) – dihydrogenperoxide (1/2), C₂₆H₂₈O₆P₂

August 21, 2020

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 1511-1513

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C 26 H 28 O 6 P 2 , monoclinic, C 2/ c (no. 15), a = 12.8582(1) Å, b = 12.4664(1) Å, c = 15.4358(1) Å, β = 95.738(1)°, V = 2461.89(3) Å 3 , Z = 4, R gt ( F ) = 0.0296, wR ref ( F 2 ) = 0.0809, T = 100(2) K.
Open Access
Crystal structure of 2-(pyridin-2-ylamino)pyridinium chloride dibenzyldichlorostannane, [C₁₀H₁₀N₃]Cl, C₁₄H₁₄Cl₂Sn

August 28, 2020

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 1515-1517

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C 24 H 24 Cl 3 N 3 Sn, triclinic, P 1̄ (no. 2), a = 10.2029(2) Å, b = 10.6071(2) Å, c = 12.1389(3) Å, α = 71.395(2)°, β = 82.665(2)°, γ = 73.340(2)°, V = 1191.84(5) Å 3 , Z = 2, R gt ( F ) = 0.0175, wR ref ( F 2 ) = 0.0447, T = 100(2) K.
Open Access
Crystal structure of 4-[(3-methoxyphenyl)carbamoyl]butanoic acid, C₁₂H₁₅NO₄

August 22, 2020

Muhammad Sirajuddin, Bibi Hanifa, Sharif Ullah, Kong Mun Lo, Edward R.T. Tiekink

Page range: 1519-1521

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C 12 H 15 NO 4 , triclinic, P 1̄ (no. 2), a = 5.0167(2) Å, b = 7.9264(5) Å, c = 15.2073(7) Å, α = 98.909(4)°, β = 92.060(4)°, γ = 101.800(4)°, V = 583.36(5) Å 3 , Z = 2, R gt ( F ) = 0.0403, wR ref ( F 2 ) = 0.1179, T = 293(2) K.
Open Access
Crystal structure of dichlorido-bis(tri-4-tolylphosphane oxide-κO)-di(4-chlorophenyl-κC)tin(IV), C₅₄H₅₀Cl₄O₂P₂Sn

August 21, 2020

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 1523-1525

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C 54 H 50 Cl 4 O 2 P 2 Sn, triclinic, P 1̄ (no. 2), a = 10.6360(2) Å, b = 10.8406(2) Å, c = 12.5727(2) Å, α = 94.152(1)°, β = 107.195(2)°, γ = 112.549(2)°, V = 1250.31(4) Å 3 , Z = 1, R gt ( F ) = 0.0194, wR ref ( F 2 ) = 0.0529, T = 100(2) K.
Open Access
Crystal structure of dichloridodimethylbis(tri-4-tolylphosphane oxide-κO)-tin(IV), C₄₄H₄₈Cl₂O₂P₂Sn

August 27, 2020

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 1527-1529

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C 44 H 48 Cl 2 O 2 P 2 Sn, orthorhombic, Pbca (no. 61), a = 17.8312(1) Å, b = 12.0291(1) Å, c = 18.5895(1) Å, V = 3987.32(5) Å 3 , Z = 4, R gt ( F ) = 0.0196, wR ref ( F 2 ) = 0.0564, T = 100(2) K.
Open Access
Crystal structure of chlorido(2-methylquinolin-8-olato-κ²N,O)-bis(4-tolyl-κC)tin(IV), C₂₄H₂₂ClNOSn

August 27, 2020

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 1531-1533

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C 24 H 22 ClNOSn, monoclinic, P 2 1 / c (no. 14), a = 13.7584(1) Å, b = 13.5542(1) Å, c = 13.0912(1) Å, β = 115.778(1)°, V = 2198.36(3) Å 3 , Z = 4, R gt ( F ) = 0.0170, wR ref ( F 2 ) = 0.0448, T = 100(2) K.
Open Access
Crystal structure of (E)-dichloro(1-chloro-3-methoxyprop-1-en-2-yl)(4-methoxyphenyl)-λ⁴-tellane, C₁₁H₁₃Cl₃O₂Te

September 18, 2020

Ignez Caracelli, Julio Zukerman-Schpector, Rodrigo L.O.R. Cunha, Edward R.T. Tiekink

Page range: 1535-1537

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C 11 H 13 Cl 3 O 2 Te, monoclinic, P 2 1 / c (no. 14), a = 11.0098(8) Å, b = 16.471(1) Å, c = 8.4975(7) Å, β = 99.421(7)°, V = 1520.17(19) Å 3 , Z = 4, R gt ( F ) = 0.0306, wR ref ( F 2 ) = 0.0852, T = 293(2) K.
Open Access
Crystal structure of bis{N-methyl-N′-[3-(4-methoxyphenyl)-1-methylpropane-1-ylidene]carbamohydrazonothioato}zinc(II), C₂₆H₃₆N₆O₂S₂Zn

August 21, 2020

Ming Yueh Tan, Huey Chong Kwong, Karen A. Crouse, Thahira B.S.A. Ravoof, Edward R.T. Tiekink

Page range: 1539-1541

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C 26 H 36 N 6 O 2 S 2 Zn, triclinic, P 1̄ (no. 2), a = 9.1777(5) Å, b = 12.3828(7) Å, c = 13.3137(7) Å, α = 102.157(5)°, β = 101.395(4)°, γ = 100.771(4)°, V = 1408.14(14) Å 3 , Z = 2, R gt ( F ) = 0.0489, wR ref ( F 2 ) = 0.1147, T = 100(2) K.
Open Access
Crystal structure of (2-carboxy-4-(3-carboxy-5-carboxylatophenoxy)benzoato-κ²O,O′)bis(1,10-phenantroline-κ²N,N′)cobalt(II), C₄₀H₂₄N₄O₉Co

September 4, 2020

Jie Luo, Guang-Na Gu, Xiao-Wei Wang

Page range: 1543-1545

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C 40 H 24 N 4 O 9 Co, triclinic, P 1̄ (no. 2), a = 11.5623(9) Å, b = 11.5732(12) Å, c = 13.4379(11) Å, α = 82.003(8)°, β = 77.597(7)°, γ = 76.048(8)°, V = 1697.1(3) Å 3 , Z = 2, R gt ( F ) = 0.0462, wR ref ( F 2 ) = 0.1021, T = 293(2) K.
Open Access
The crystal structure of (3S,8R,10R,14R)-17-((2S,5S)-5-(2-hydroxypropan-2-yl)-2-methyltetrahydrofuran-2-yl)-4,4,8,10,14-pentamethyl-12-oxohexadecahydro-1H-cyclopenta[a]phenanthren-3-yl acetate, C₃₂H₅₂O₅

September 26, 2020

Li Liu, Hui-yun Wang, Xia Zhou, Sheng-Nan Zhang, Xiao-Qian Chen, Feng-Lan Zhao, Qing-Guo Meng

Page range: 1547-1549

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C 32 H 52 O 5 , monoclinic, P 2 1 (no. 4), a = 11.816(2) Å, b = 7.4064(15) Å, c = 17.101(3) Å, β = 97.01(3)°, V = 1485.5(5) Å 3 , Z = 2, R gt ( F ) = 0.0543, wR ref ( F 2 ) = 0.1501, T = 293(2) K.
Open Access
Crystal structure of (μ₂-1,1′-bis(diphenylphosphino)ferrocene-κ²P,P′)-bis[(Z)N-(3-fluorophenyl)-O-methylthiocarbamato-S]digold(I) chloroform solvate, C₅₀H₄₂Au₂F₂FeN₂O₂P₂S₂, CHCl₃

August 27, 2020

Chien Ing Yeo, Yee Seng Tan, Edward R.T. Tiekink

Page range: 1551-1553

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C 51 H 43 Au 2 Cl 3 F 2 FeN 2 O 2 P 2 S 2 , triclinic, P 1̄ (no. 2), a = 8.3276(1) Å, b = 13.1116(1) Å, c = 13.5547(1) Å, α = 110.309(1)°, β = 103.132(1)°, γ = 105.601(1)°, V = 1249.86(2) Å 3 , Z = 1, R gt ( F ) = 0.0153, wR ref ( F 2 ) = 0.0387, T = 100(2) K.
Open Access
Crystal structure of poly[bis(μ₂-1,4-di(1H-imidazol-1-yl)benzene-κ²N:N′)-(μ₂-tetraoxidomolybdato(VI)-κ²O:O′)cobalt(II)], C₂₄H₂₀N₈O₄MoCo

September 18, 2020

Cheng-Yong Zhou, Yu-Jie Du, Feng Su, Bao-Xiu Zhang, Shao-Dong Li

Page range: 1555-1557

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C 24 H 20 N 8 O 4 MoCo, monoclinic, C 2/ c (no. 15), a = 19.3535(7) Å, b = 10.0870(4) Å, c = 12.4174(5) Å, β = 97.3700(10)°, V = 2404.08(16) Å 3 , Z = 4, R gt ( F ) = 0.0218, wR ref ( F 2 ) = 0.0577, T = 298(2) K.

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