Zeitschrift für Kristallographie - New Crystal Structures

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Volume 235, Issue 4

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Zeitschrift für Kristallographie - New Crystal Structures

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Frontmatter

June 13, 2020

Page range: i-viii

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Open Access
Crystal structure of bis [1-(phenylsulfonyl)-2-(1-(pyrazin-2-yl)ethylidene)hydrazin-1-ido-κ³N,N′,O]cobalt(II), C₂₄H₂₂N₈O₄S₂Co

March 18, 2020

Wan-Wan Wang, Xiao-Wei Deng, Wei-Na Wu

Page range: 763-764

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C 24 H 22 N 8 O 4 S 2 Co, orthorhombic, Aba 2 (no. 41), a = 12.043(5) Å, b = 21.723(9) Å, c = 9.961(4) Å, V = 2605.9(18) Å 3 , Z = 4, R gt ( F ) = 0.0366, wR ref ( F 2 ) = 0.0764, T = 296(2) K.
Open Access
The crystal structure of 1,3-bis(4-(methoxycarbonyl)benzyl)-2-methyl-1H-benzo[d]imidazol-3-ium bromide, C₂₆H₂₅BrN₂O₄

May 11, 2020

Bin Cai, Chun-Yan Fu, Xin-Yu Guo, Ying Wang

Page range: 765-766

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C 26 H 25 BrN 2 O 4 , triclinic, P 1̄ (no. 2), a = 9.4202(5) Å, b = 9.7871(5) Å, c = 15.0135(9) Å, α = 106.775(3)°, β = 92.534(3)°, γ = 117.424(3)°, V = 1150.52(11) Å 3 , Z = 2, R gt ( F ) = 0.0316, wR ref ( F 2 ) = 0.0671, T = 150(2) K.
Open Access
Crystal structure of {tris((1H-benzo[d]imidazol-2-yl)methyl)amine-κ⁴N,N′,N′′,N′′′}-(nitrito-κ²O,O′)nickel(II) perchlorate – ethanol (1/1), C₂₆H₂₇ClN₈NiO₇

March 25, 2020

Xin-Lun Li, Zhong-Ping Luo, Jun-Chao Zhang, Feng-Mei Nie

Page range: 767-769

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C 26 H 27 ClN 8 NiO 7 , triclinic, P 1̄ (no. 2), a = 9.893(2) Å, b = 11.503(2) Å, c = 13.295(3) Å, α = 78.77(3)°, β = 70.52(3)°, γ = 83.40(3)°, V = 1397.0(6) Å 3 , Z = 2, R gt ( F ) = 0.0423, wR ref ( F 2 ) = 0.1032, T = 153.15 K.
Open Access
Crystal structure of catena-poly[aqua[(μ₂-4,5-dicarboxylato-2-(2-carboxylatophenyl)imidazol-1-ido-κ⁴N,O,O′:N′)](μ₂-4,4′-bipyridine-κ²N:N′)dicopper(II)], C₂₂H₁₄Cu₂N₄O₇

March 26, 2020

Xiao-Yu Guo, Ji-Hong Chen, Xiang-Ru Meng

Page range: 771-773

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C 22 H 14 Cu 2 N 4 O 7 , monoclinic, P 2 1 / n (no. 14), a = 7.7885(4) Å, b = 14.9974(8) Å, c = 17.7464(10) Å, β = 102.184(2)°, V = 2026.22(19) Å 3 , Z = 4, R gt ( F ) = 0.0357, wR ref ( F 2 ) = 0.0936, T = 300(2) K.
Open Access
Crystal structure of chlorido-tris(4-methylbenzyl-κC)-(triphenylarsine oxide-κO)tin(IV), C₄₂H₄₂AsClOSn

April 7, 2020

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 775-777

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C 42 H 42 AsClOSn, monoclinic, P 2 1 / n (no. 14), a = 17.5342(1) Å, b = 11.1174(1) Å, c = 18.5675(1) Å, β = 95.405(1)°, V = 3603.36(4) Å 3 , Z = 4, R gt ( F ) = 0.0184, wR ref ( F 2 ) = 0.0465, T = 100(2) K.
Open Access
The crystal structure of 4,4′-bipyridinium bis(3-carboxy-2-nitrobenzoate) tetrahydrate, C₁₃H₁₃N₂O₈

March 12, 2020

Chun-Xia Chai, Peng Peng, Bin Cai

Page range: 779-781

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C 13 H 13 N 2 O 8 , triclinic, P 1̄ (no. 2), a = 7.8590(6) Å, b = 9.3108(8) Å, c = 11.0816(8) Å, α = 66.950(3)°, β = 71.558(3)°, γ = 77.203(4)°, V = 703.38(10) Å 3 , Z = 2, R gt (F) = 0.0389, wR ref (F 2 ) = 0.1075, T = 149(2) K.
Open Access
Crystal structure of 1-(3-chlorophenyl)-4-(4-(((2,3-dihydro-1H-inden-5-yl)oxy)methyl)phenethyl)piperazine, C₂₈H₃₁ClN₂O

March 25, 2020

Aiqing Feng, Bin Lv

Page range: 783-785

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C 28 H 31 ClN 2 O, monoclinic, P 1̄ (no. 2), a = 21.9309(11) Å, b = 9.9648(5) Å, c = 11.0049(7) Å, β = 93.403(6)°, V = 2400.7(2) Å 3 , Z = 4, R gt ( F ) = 0.0566, wR ref ( F 2 ) = 0.1355, T = 293 K.
Open Access
Crystal structure of catena-poly[diaqua-bis(μ₂-5,5′-(1H-imidazole-4,5-diyl)bis(tetrazol-2-ido)-κ⁴N,N′:N′′,N′′′)magnesium], C₁₀H₈N₂₀O₂Mg

March 5, 2020

Ting Li, Zheng Xing

Page range: 787-788

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C 10 H 8 N 20 O 2 Mg, orthorhombic, Pnma (no. 62), a = 12.4217(8) Å, b = 7.3444(6) Å, c = 10.6063(7) Å, V = 967.61(12) Å 3 , Z = 2, R gt ( F ) = 0.0411, wR ref ( F 2 ) = 0.1147, T = 293(2) K.
Open Access
The crystal structure of (E)-2-((2-hydroxy-4-ethoxybenzylidene)amino)-2-methylpropane-1,3-diol monohydrate, C₁₃H₂₁NO₅

March 9, 2020

Yang Liguo, Zhang Zhen, Niu Yongsheng, Wang Fang, Tian Dayong

Page range: 789-791

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C 13 H 21 NO 5 , orthorhombic, Pca 2 1 (no. 29), a = 19.718(8) Å, b = 9.102(4) Å, c = 8.091(4) Å, V = 1452.1(11) Å 3 , Z = 4, R gt ( F ) = 0.0452, wR ref ( F 2 ) = 0.1289, T = 298 K [1–3].
Open Access
Crystal structure of catena-poly[diaqua-(μ₂-bipyridine-κ²N:N′)-bis(3,5-dichloroisonicotinato-κO)cadmium(II)] dihydrate, C₂₂H₂₀CdCl₄N₄O₈

March 5, 2020

Sun Xiao-Tian, Lei Zheng

Page range: 793-795

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C 22 H 20 CdCl 4 N 4 O 8 , monoclinic, C 2/ c (no. 15), a = 14.9908(5) Å, b = 11.6786(3) Å, c = 15.4664(5) Å, β = 95.448(3)°, V = 2695.50(14) Å 3 , Z = 4, R gt ( F ) = 0.0226, wR ref ( F 2 ) = 0.0516, T = 291.5(2) K.
Open Access
The crystal structure of 4-(4-chlorophenyl)cyclohexane-1-carboxylic acid, C₁₃H₁₅ClO₂

March 25, 2020

Chao-Jun Du, Zong-Dong Wang, Xiao-Ke Wang, Yan Zeng

Page range: 797-799

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C 13 H 15 ClO 2 , monoclinic, P 2 1 / n (no. 14), a = 14.4696(7) Å, b = 9.5385(4) Å, c = 18.7042(11) Å, β = 112.619(2)°, V = 2383.0(2) Å 3 , Z = 8, R gt ( F ) = 0.0414, wR ref ( F 2 ) = 0.1090, T = 150(2) K.
Open Access
Redetermination of the crystal structure of yttrium(III) trinitrate(V) pentahydrate, Y(NO₃)₃ ⋅ 5 H₂O, H₁₀N₃O₁₄Y

March 25, 2020

Wilhelm Klein

Page range: 801-802

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H 10 N 3 O 14 Y, triclinic, P 1̄ (no. 2), a = 6.5965(12) Å, b = 9.5374(17) Å, c = 10.5249(19) Å, α = 63.809(13)°, β = 84.677(15)°, γ = 76.397(19)°, V = 577.46(18) Å 3 , Z = 2, R gt ( F ) = 0.0330, wR ref ( F 2 ) = 0.0697, T = 223 K.
Open Access
Crystal structure of catena-poly[di-μ₂-chlorido-1,10-phenanthroline-κ²N,N′-cadmium(II)], C₁₂H₈Cl₂CdN₂

April 9, 2020

Ling-Chuan Li, Xiao-Li Zhou, Yan-Li Liu, Li-Ping Wang

Page range: 803-804

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C 12 H 8 Cl 2 CdN 2 , monoclinic, C 2/ c (no. 15), a = 16.969(5) Å, b = 10.515(3) Å, c = 7.238(2) Å, β = 110.710(10)°, V = 1208.0(6) Å 3 , Z = 4, R gt ( F ) = 0.0245, wR ref ( F 2 ) = 0.0806, T = 298(2) K.
Open Access
Crystal structure of 4-((2-methyl-6-(trifluoromethyl)pyrimidin-4-yl)oxy)benzoic acid, C₁₃H₉F₃N₂O₃

March 25, 2020

Wen-Neng Wu, Qiang Fei, Yong-Hui Ge, Xiu-Hai Gan

Page range: 805-806

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C 13 H 9 F 3 N 2 O 3 , monoclinic, P 2 1 / c (no. 14), a = 8.6952(7) Å, b = 19.6715(18) Å, c = 8.0995(8) Å, β = 110.691(3)°, V = 1296.0(2) Å 3 , Z = 4, R gt ( F ) = 0.0558, wR ref ( F 2 ) = 0.1358, T = 298(2) K.
Open Access
Crystal structure of 3-acetyl-4-hydroxybenzoic acid, C₁₈H₁₆O₈

March 25, 2020

Jia Gu, Cui-Xin Huang, Yan-Ling Zheng, Xu-Liang Nie, Jin-Zhu Chen

Page range: 807-809

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C 18 H 16 O 8 , monoclinic, P 2 1 / c (no. 14), a = 5.3210(8) Å, b = 5.1825(8) Å, c = 29.598(5) Å, β = 93.875(2)°, V = 814.3(2) Å 3 , Z = 2, R gt ( F ) = 0.0340, wR ref ( F 2 ) = 0.1011, T = 296(2) K.
Open Access
Crystal structure of bis(N,2-bis(4-ethoxybenzylidene)hydrazine-1-carbohydrazonothioato-κ²N,S)nickel(II) — N,N-dimethylformamide (1/2), C₄₄H₅₆N₁₀S₂O₆Ni

March 25, 2020

Zhuang-Yu Li, E. Liu, Xiao-Jing Liu, Fang-Fang Jian, Tong-ling Liang

Page range: 811-813

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C 44 H 56 N 10 S 2 O 6 Ni, triclinic, P 1̄ (no. 2), a = 9.3077(14) Å, b = 9.9624(14) Å, c = 14.0449(19) Å, α = 70.889(3)°, β = 75.532(2)°, γ = 87.544(3)°, V = 1190.5(3) Å 3 , Z = 1, R gt ( F ) = 0.0528, wR ref ( F 2 ) = 0.1279, T = 293 K.
Open Access
The crystal structure of 5-chloro-4,6-dimethoxypyrimidin-2-amine, C₆H₈ClN₃O₂

March 18, 2020

Sheng Yan, Mei Xue, Xinyuan He, Chengqian Wang, Zixin Wang, Jianlong Wang

Page range: 815-816

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C 6 H 8 ClN 3 O 2 , monoclinic, P 2 1 / n (no. 14), a = 5.066(3) Å, b = 12.775(8) Å, c = 12.587(8) Å, β = 94.060(8)°, V = 812.5(9) Å 3 , Z = 4, R gt ( F ) = 0.0597, wR ref ( F 2 ) = 0.1990, T = 296(2) K.
Open Access
Crystal structure of poly[aqua-(μ₄-benzene-1,2,4,5-tetracarboxylato-κ⁴O,O′,O′′,O′′′)bis(μ₂-1-(4-(1H-imidazol-1-yl)benzyl)-1H-1,2,4-triazole-κ²N:N)dinickel(II)], NiC₁₇H₁₄N₅O₅

March 20, 2020

Rui Shi, Xia Zhu, Shi-Yong Lin, Yi Su, Yu-Yang He, Song-Yao Zhang

Page range: 817-819

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NiC 17 H 14 N 5 O 5 , triclinic, P 1̄ (no. 2), a = 7.8199(8) Å, b = 8.6969(8) Å, c = 13.1934(13) Å, α = 93.955(1)°, β = 99.951(1)°, γ = 109.946(1)°, V = 822.79(14) Å 3 , Z = 2, R gt ( F ) = 0.0316, wR ref ( F 2 ) = 0.0688, T = 150 K.
Open Access
Crystal structure of poly[aqua(5-dimethylamino)naphthalene-1-sulfonato-κ²N:O)(μ₂-4,4′-bipyridyl -κ²N:N′)silver(I)], C₄₄H₄₄Ag₂N₆O₈S₂

April 16, 2020

Xi-Xi Li, Jin-Ke Jiang, Jing-Jie Du, Wei Guo, Hui Jiang, Xian-Wu Dong

Page range: 821-823

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abstract C 44 H 44 Ag 2 N 6 O 8 S 2 , triclinic, P 1̄ (no. 2), a = 11.3967(5) Å, b = 12.6953(6) Å, c = 14.9539(7) Å, α = 80.903(4)°, β = 89.801(4)°, γ = 83.911(4)°, V = 2124.14(17) Å 3 , Z = 2, R gt ( F ) = 0.0421, wR ref ( F 2 ) = 0.1130, T = 293(2) K.
Open Access
Crystal structure of 1-[3-(trifluoromethyl)cinnamoyl]-3-(pyridin-2-yl-κN)pyrazole-κ²N-bis(2-phenylpyridinato-k²C,N)iridium(III) hexafluorophosphate complex, [C₄₀H₂₈F₃IrN₅O]PF₆

March 25, 2020

Yan Yi Chong, Wun Fui Mark-Lee, Ishak Ahmad, Mohammad B. Kassim

Page range: 825-829

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[C 40 H 28 F 3 IrN 5 O]PF 6 , monoclinic, P 2 1 / c (no. 14), a = 20.2282(19) Å, b = 14.5095(11) Å, c = 12.6091(10) Å, β = 96.937(3)°, V = 3673.7(5) Å 3 , Z = 4, R gt (F) = 0.0498, wR ref (F 2 ) = 0.1250, T = 107(2) K.
Open Access
Crystal structure of catena-poly[aqua(μ₆-piperazine-1,4-bisethanesulfonato-κ⁶N:N′:O:O′:O′′:O′′′)(μ₂-pyrazinyl-κ²N:N′)disilver(I)sesquihydrate], C₁₂H₃₀Ag₂N₄O₁₁S₂

April 25, 2020

Jin-Ke Jiang, Xi-Xi Li, Hua Wu, Xian-Wu Dong, Hui Jiang

Page range: 831-832

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C 12 H 30 Ag 2 N 4 O 11 S 2 , monoclinic, I 2/ a (no. 15), a = 12.2643(8) Å, b = 7.1481(4) Å, c = 26.2858(16) Å, β = 93.119(6)°, V = 2301.0(2) Å 3 , Z = 4, R gt ( F ) = 0.0186, wR ref ( F 2 ) = 0.0462, T = 298(2) K.
Open Access
Crystal structure of (E)-1-(2-nitrophenyl)-N-(o-tolyl)methanimine, C₁₄H₁₂N₂O₂

April 16, 2020

Sulaiman A. Olagboye, Tunde L. Yusuf, Segun D. Oladipo, Sizwe J. Zamisa

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C 14 H 12 N 2 O 2 , monoclinic, P 2 1 , a = 8.3844(1) Å, b = 20.0465(3) Å, c = 14.0511(2) Å, β = 94.786(1)°, V = 2353.44(6) Å 3 , Z = 4, R gt ( F ) = 0.0356, wR ref ( F 2 ) = 0.1022, T = 150(2) K.
Open Access
Crystal structure of 4′-amino-3′,5′-diisopropyl-(1,1′-biphenyl)-4-carbonitrile, C₁₉H₂₂N₂

April 16, 2020

Shuang-Ming Mo, Da-Bin Shi

Page range: 837-839

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C 19 H 22 N 2 , triclinic, P 1̄ (no. 2), a = 8.1330(5) Å, b = 9.3474(5) Å, c = 12.1520(8) Å, α = 87.278(5)°, β = 71.092(6)°, γ = 66.190(6)°, V = 795.88(9) Å 3 , Z = 2, R gt ( F ) = 0.0498, wR ref ( F 2 ) = 0.1415, T = 293(2) K.
Open Access
The crystal structure of poly[bis(N,N-dimethylformamide-κ¹O)-tetrakis(μ₂-cyanido-κ²C:N)dinickel(II)], C₁₀H₁₄N₆O₂Ni₂

March 12, 2020

Shuang-Hua Yang

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C 10 H 14 N 6 O 2 Ni 2 , monoclinic, I 2/ m (no. 12), a = 6.7377(1) Å, b = 7.3500(1) Å, c = 14.8647(2) Å, β = 96.051(1)°, V = 732.030(18) Å 3 , Z = 8, R gt ( F ) = 0.0314, wR ref ( F 2 ) = 0.0996, T = 150.01(10) K.
Open Access
Crystal structure of rac-trans-N,N′-bis(3-bromo-5-chlorosalicylidene)-1,2-cyclohexanediamine, C₂₀H₁₈Br₂Cl₂N₂O₂

May 4, 2020

Fang Jiang, Yan Xu, Xun Ma, Jiayi Li, Qiong Wu

Page range: 845-846

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C 20 H 18 Br 2 Cl 2 N 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 10.6105(8) Å, b = 17.1664(9) Å, c = 11.9848(9) Å, β = 97.682(3)°, V = 2163.4(3) Å 3 , Z = 4, R gt ( F ) = 0.0330, wR ref ( F 2 ) = 0.0823, T = 100(2) K.
Open Access
Crystal structure of rac-trans-N,N′-bis(3,5-dibromosalicylidene)-1,2-cyclohexanediamine, C₂₀H₁₈Br₄N₂O₂

March 20, 2020

Liang Jiao, Hui Tan, Jinrong Sun, Longduo Zhang, Qiong Wu

Page range: 847-848

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C 20 H 18 Br 4 N 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 9.1119(6) Å, b = 17.8211(12) Å, c = 13.5228(8) Å, β = 90.809(2)°, V = 2195.7(2) Å 3 , Z = 4, R gt ( F ) = 0.0448, wR ref ( F 2 ) = 0.0963, T = 273(2) K.
Open Access
The crystal structure of (dichromato-κ²O,O′)bis(1,10-phenanthroline-κ²N,N′)nickel(II), C₁₂H₁₆N₄O₇Cr₂Ni

May 4, 2020

Chen Wu-Hua, Xie Gui-Xiang, Chen Qin, Ruan Yan-Ming

Page range: 849-850

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C 12 H 16 N 4 O 7 Cr 2 Ni, orthorhombic, Pbcn (no. 60), a = 13.7804(5) Å, b = 10.3110(5) Å, c = 16.4118(6) Å, V = 2331.96(17) Å 3 , Z = 4, R gt ( F ) = 0.0438, wR ref ( F 2 ) = 0.1111, T = 293(2) K.
Open Access
The crystal structure of 3-((1R,2S)-1-methylpyrrolidin-1-ium-2-yl)pyridin-1-ium tetrachloridozincate(II) monohydrate, C₁₀H₁₈Cl₄ZnN₂O

April 9, 2020

Guido J. Reiss, Alena Sergeeva

Page range: 851-854

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C 10 H 18 Cl 4 ZnN 2 O, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 7.0752(1) Å, b = 7.5085(1) Å, c = 29.3383(5) Å, V = 1558.57(4) Å 3 , Z = 4, R gt ( F ) = 0.0330, wR ref ( F 2 ) = 0.0672, T = 290(2) K.
Open Access
Crystal structure of bis(μ₂-azido-k²N,N)-bis(2-amino-1-(N-(3-bromosalicylaldiminato))ethane)-dicopper(II), C₂₀H₁₈Br₄N₂O₂

March 25, 2020

Jiayi Li, Yan Xu, Fang Jiang, Jinrong Sun, Qiong Wu

Page range: 855-856

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C 20 H 18 Br 4 N 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 9.5994(7) Å, b = 11.9156(10) Å, c = 10.3508(7) Å, β = 91.025(6)°, V = 1183.76(15) Å 3 , Z = 2, R gt ( F ) = 0.0472, wR ref ( F 2 ) = 0.1008, T = 293(2) K.
Open Access
Crystal structure of (η⁶-1-methyl-4-isopropylbenzene)-[5-bromo-2-(2-pyridyl)phenyl-κ²C,N]-chloro-ruthenium(II), C₂₁H₂₁BrClNRu

March 25, 2020

Chen Xu, Xin-Hua Lou

Page range: 857-859

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C 21 H 21 BrClNRu, triclinic, P 1̄ (no. 2), a = 8.2185(4) Å, b = 10.1626(5) Å, c = 11.9356(6) Å, α = 100.399(4)°, β = 90.005(4)°, γ = 93.434(4)°, V = 978.68(9) Å 3 , Z = 2, R gt ( F ) = 0.0353, wR ref ( F 2 ) = 0.0676, T = 291(2) K.
Open Access
Crystal structure of N-(methyl(oxo)(1-(6-(trifluoromethyl)pyridin-3-yl)ethyl)-λ⁶-sulfanylidene)cyanamide, C₁₀H₁₀F₃N₃OS

March 18, 2020

Xu Ning, Yun-Lian Shi, Xu-Gen Shi, Wen-Li Yang, Da-Yong Peng

Page range: 861-862

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[C 10 H 10 F 3 N 3 OS], monoclinic, P 2 1 / c (no. 14), a = 18.555(10) Å, b = 6.785(4) Å, c = 10.139(5) Å, β = 105.86°, V = 1227.9(11) Å 3 , Z = 4, R gt ( F ) = 0.0571, wR ref ( F 2 ) = 0.1785, T = 296(2) K.
Open Access
Crystal structure of 6,6′-((cyclohexane-1,2-diylbis(azanylylidene))bis(methanylylidene))bis(2-bromo-4-chlorophenolato-κ⁴N,N′,O,O′)nickel(II), C₂₀H₁₆Br₂Cl₂NiN₂O₂

March 25, 2020

Fang Jiang, Yan Lei, Liu Ting, Xiongzi Yang, Qiong Wu

Page range: 863-864

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C 20 H 16 Br 2 Cl 2 NiN 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 12.6946(7) Å, b = 11.9262(7) Å, c = 14.9398(9) Å, β = 115.1400°, V = 2047.6(2) Å 3 , Z = 4, R gt ( F ) = 0.0386, wR ref ( F 2 ) = 0.0834, T = 273(2) K.
Open Access
Redetermination of the crystal structure of catena-poly[aqua-(1,10-phenanthroline-κ²N,N′)-(μ₂-tetraoxidomolybdato(VI)-κ²O:O′)manganese(II) monohydrate, C₁₂H₁₂N₂O₆MoMn

April 9, 2020

Chen Wu-Hua, Zhou Ji, Wang Yu-Fan

Page range: 865-866

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C 12 H 12 N 2 O 6 MoMn, triclinic, P 1̄ (no. 2), a = 7.0427(3) Å, b = 10.4459(7) Å, c = 10.5778(6) Å, α = 73.233(6)°, β = 83.372(4)°, γ = 77.340(4)°, V = 725.85(7) Å 3 , Z = 2, R gt ( F ) = 0.0386, wR ref ( F 2 ) = 0.0916, T = 293(2) K.
Open Access
The crystal structure tetrakis(μ₂-o-chlorobenzoato-κ²O:O′)-bis(methanol-κ¹O)dirhodium(II), C₃₀H₂₄Cl₄O₁₀Rh₂

April 10, 2020

Guangyuan Zhu, Miao Meng

Page range: 867-868

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C 30 H 24 Cl 4 O 10 Rh 2 , monoclinic, P 2 1 / n (no. 14), a = 7.5270(4) Å, b = 12.3533(6) Å, c = 17.4904(8) Å, β = 91.780(4)°, V = 1625.52(14) Å 3 , Z = 2, R gt ( F ) = 0.0458, wR ref ( F 2 ) = 0.1285, T = 150(1) K.
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Crystal structure of bis(2,3-diphenyltetrazolidine-5-thione-κ¹S)-(nitrato-κ¹O)-(nitrato-κ²O,O′)lead(II), C₂₆H₂₀N₁₀O₆S₂Pb

April 10, 2020

Zhuang-yu Li, E Liu, Xiao-jing Liu, Fang-fang Jian

Page range: 869-871

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C 26 H 20 N 10 O 6 S 2 Pb, triclinic, P 1̄ (no. 2), a = 9.3480(19) Å, b = 12.985(3) Å, c = 14.278(3) Å, α = 113.14(3)°, β = 92.05(3)°, γ = 102.75(3)°, V = 1539.8(7) Å 3 , Z = 2, R gt ( F ) = 0.0336, wR ref ( F 2 ) = 0.0874, T = 293.0 K.
Open Access
Crystal structure of bis(3-bromo-N-(1-(3-methylpyrazin-2-yl)ethylidene)benzohydrazonato-κ³O,N,N′)cadmium(II) hemihydrate, C₂₈H₂₅N₈O_2.5Br₂Cd

April 10, 2020

Yi-Peng Guo, Xiao Liu

Page range: 873-874

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C 28 H 25 N 8 O 2.5 Br 2 Cd, triclinic, P 1̄ (no. 2), a = 8.7233(16) Å, b = 11.655(2) Å, c = 15.374(3) Å, α = 82.225(4)°, β = 86.125(3)°, γ = 76.300(3)°, V = 1503.6(5) Å 3 , Z = 2, R gt ( F ) = 0.0459, wR ref ( F 2 ) = 0.1102, T = 296 K.
Open Access
Crystal structure of catena-poly[tetrakis(μ₂-trifluoroacetato-κ²O:O′)(μ₂-2,5-dimethylpyrazine-κ²N,N′)dicopper(II)], C₇H₄CuF₆NO₄

April 10, 2020

Lan Zhang, Yong Ren, Qiang Wang, Wu-Xiu Ding, Wen-Bo Fei

Page range: 875-877

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C 7 H 4 CuF 6 NO 4 , triclinic, P 1̄ (no. 2), a = 8.5122(5) Å, b = 8.5458(6) Å, c = 8.8674(6) Å, α = 75.042(3)°, β = 68.601(2)°, γ = 89.809(3)°, V = 577.26(7) Å 3 , Z = 2, R gt ( F ) = 0.0247, wR ref ( F 2 ) = 0.0625, T = 152.41 K.
Open Access
The crystal structure of catena-poly[bis[3-azoniapentane-1,5-diammonium][bis(μ₄-oxo)-tetrakis(μ₃-oxo)-heptakis(μ₂-oxo)-tetradecaoxo-octa-molybdenum] dihydrate], (C₈H₃₆N₆O₂₉Mo₈)_n

April 16, 2020

Chen Wu-Hua, Yang Dai-Bin, Jiang Zhao-Bin

Page range: 879-880

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(C 8 H 36 N 6 O 29 Mo 8 ) n , monoclinic, P 2 1 / n (no. 14), a = 10.5883(4) Å, b = 9.4385(3) Å, c = 16.5154(7) Å, β = 94.616(4)°, V = 1645.15(11) Å 3 , Z = 2, R gt ( F ) = 0.0359, wR ref ( F 2 ) = 0.0887, T = 293(2) K.
Open Access
Crystal structure of tetraaqua-bis(2-((3,5,6-trichloropyridin-2-yl)oxy)acetato-κO)-nickel(II)—diaqua-bis(2-((3,5,6-trichloropyridin-2-yl)oxy)acetato-nickel(II), C₂₈H₂₄Cl₁₂N₄Ni₂O₁₈

April 16, 2020

Zhong-Xiang Du, Jun-Xia Li

Page range: 881-883

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C 28 H 24 Cl 12 N 4 Ni 2 O 18 , monoclinic, I 2 / a (no. 15), a = 37.8040(12) Å, b = 6.0860(2) Å, c = 19.3025(6) Å, β = 98.104(3)°, V = 4396.7(2) Å 3 , Z = 4, R gt ( F ) = 0.0498, wR ref ( F 2 ) = 0.1039, T = 291.8(2) K.
Open Access
The crystal structure of bis(2-hydroxypyrimidinium) pentachloridobismuthate(III), (C₄N₂H₅O)₂BiCl₅

May 5, 2020

Munan Hao, Shifeng Jin, Yuxin Ma, Junyan Zhou, Zeyu Zhang, Changchun Zhao

Page range: 885-886

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C 8 N 4 H 10 O 2 BiCl 5 , monoclinic, P 2 1 / a (no. 14, non-standard setting of P 2 1 / c ), a = 9.1065(5) Å, b = 14.5950(8) Å, c = 12.7159(8) Å, β = 93.557(2)°, V = 1687.28(17) Å 3 , Z = 4, R gt ( F ) = 0.0249, wR ref ( F 2 ) = 0.0612, T = 273 K.
Open Access
The crystal structure of catena-poly[(μ₂-4,4′-dipyridine-κ²N,N′)-bis(3,5,6-trichloropyridine-2-oxyacetato-κO)-bis(ethanol-κO)nickel(II)], C₂₈H₂₆Cl₆N₄NiO₈

April 24, 2020

Jun-Xia Li, Zhong-Xiang Du

Page range: 887-890

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C 28 H 26 Cl 6 N 4 NiO 8 , monoclinic, I 2 / a (no. 15), a = 15.7577(10) Å, b = 12.6174(7) Å, c = 16.7333(10) Å, β = 99.609(6)Å, V = 3280.3(3) Å 3 , Z = 4, R gt ( F ) = 0.0674, wR ref ( F 2 ) = 0.1665, T = 291.2(3) K.
Open Access
Crystal structure and anti-inflammatory activity of (3E,5E)-1-((4-chlorophenyl)sulfonyl)-3,5-bis(4-fluorobenzylidene)piperidin-4-one-dichloromethane (1/1), C₂₆H₂₀Cl₃F₂NO₃S

April 25, 2020

Li-Xia Zhang, Yun Hou

Page range: 891-893

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C 26 H 20 Cl 3 F 2 NO 3 S, triclinic, P 1̄ (no. 2), a = 8.6281(7) Å, b = 11.3695(9) Å, c = 14.3529(11) Å, α = 68.166(7)°, β = 80.707(7)°, γ = 71.169(7)°, V = 1235.65(19) Å 3 , Z = 2, R gt ( F ) = 0.0564, wR ref ( F 2 ) = 0.1376, T = 100.00(10) K.
Open Access
The crystal structure of 5-bromopicolinic acid monohydrate, C₆H₆BrNO₃

April 9, 2020

Bin Cai, Meng-En Zhu, Xin Bai, Yan-Ru Lin, Qian-Qian Guo, Yu-Ning Meng

Page range: 895-896

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C 6 H 6 BrNO 3 , triclinic, P 1̄ (no. 2), a = 7.0407(5) Å, b = 7.1597(6) Å, c = 8.3808(7) Å, α = 75.844(4)°, β = 94.562(4)°, γ = 76.306(4)°, V = 373.61(5) Å 3 , Z = 4, R gt ( F ) = 0.0205, wR ref ( F 2 ) = 0.0527, T = 150(2) K.
Open Access
The crystal structure of 2-(3-(4-bromophenyl)-5-(4-fluorophenyl)-4,5-dihydro-1H-pyrazol-1-yl)-8H-indeno[1,2-d]thiazole, C₂₅H₁₇BrFN₃S

April 9, 2020

Abdullah A. Alotaibi, Bakr F. Abdel-Wahab, Amany S. Hegazy, Benson M. Kariuki, Gamal A. El-Hiti

Page range: 897-899

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C 25 H 17 BrFN 3 S, triclinic, P 1̄ (no. 2), a = 11.2926(6) Å, b = 11.5832(4) Å, c = 16.9974(9) Å, α = 109.211(4)°, β = 90.211(4)°, γ = 95.290(4))°, V = 2089.21(18) Å 3 , Z = 4, R gt ( F ) = 0.0580, wR ref ( F 2 ) = 0.1797, T = 296 K.
Open Access
The crystal structure of catena-poly[(μ₂-2-((3-bromo-2-oxidobenzylidene)amino)acetato-κ⁴O,N,O′:O′′)-(dimethylformamide-κ¹O)]zinc(II), C₁₂H₁₃N₂O₄BrZn

April 9, 2020

Tai Xi-Shi, Zhou Xiao-Jing, Liu Li-Li, Cao Shu-Hua, Wang Li-Hua

Page range: 901-902

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C 12 H 13 N 2 O 4 BrZn, monoclinic, P 2 1 / n (no. 14), a = 12.0182(12) Å, b = 6.9735(7) Å, c = 16.2510(14) Å, β = 93.572(9)°, V = 1359.3(2) Å 3 , Z = 4, R gt ( F ) = 0.0279, wR ref ( F 2 ) = 0.0613, T = 293(2) K.
Open Access
Crystal structure of aqua-azido-κ¹N-(6,6′-((propane-1,3-diylbis(azanylylidene))bis(methanylylidene))bis(3-bromophenolato)-κ⁴N,N′,O,O′iron(III), C₁₇H₁₆Br₂FeN₅O₃

April 23, 2020

Jianchang Xiao, Cun Zhou, Meifen Huang, Hui Tan, Qiong Wu

Page range: 903-904

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C 17 H 16 Br 2 FeN 5 O 3 , orthorhombic, Pbca (no. 61), a = 11.9307(9) Å, b = 14.8166(17) Å, c = 22.923(2) Å, V = 4052.2(7) Å 3 , Z = 8, R gt ( F ) = 0.0750, wR ref ( F 2 ) = 0.2497, T = 293(2) K.
Open Access
The crystal structure of tris(1-ethylimidazole-κ¹N)-(sulfato-κ²O,O′)vanadium(IV), C₁₅H₂₄N₆O₅SV

April 9, 2020

Yi-Ru Fu, Jian Luan, Xiao-Jie Wang

Page range: 905-906

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C 15 H 24 N 6 O 5 SV, monoclinic, P 2 1 / c (no. 14), a = 16.0059 Å, b = 9.1008 Å, c = 14.2686 Å, β = 100.352°, V = 2044.6(2) Å 3 , Z = 4, R gt ( F ) = 0.0400, wR ref ( F 2 ) = 0.0852, T = 173(2) K.
Open Access
Crystal structure of (E)-3-methoxy-N′-(1-(pyridin-2-yl)ethylidene)benzohydrazide, C₁₅H₁₅N₃O₂

March 25, 2020

Valeri V. Mossine, Steven P. Kelley, Thomas P. Mawhinney

Page range: 907-909

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C 15 H 15 N 3 O 2 , orthorhombic, Pca 2 1 (no. 29), a = 7.9831(2) Å, b = 10.6486(3) Å, c = 15.7222(4) Å, V = 1336.53(6) Å 3 , Z = 4, R gt ( F ) = 0.0340, wR ref ( F 2 ) = 0.0799, T = 100 K.
Open Access
Crystal structure of dichloro-bis-(1-butyl-1H-benzo[d]imidazole)-nickel(II), C₂₂H₂₈Cl₂N₄Ni

April 21, 2020

Zhuang-yu Li, Xiao-jing Liu, E. Liu, Fang-fang Jian, Tongling Liang

Page range: 911-912

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C 22 H 28 Cl 2 N 4 Ni, monoclinic, P 2 1 / c (no. 14), a = 9.7332(19) Å, b = 14.886(3) Å, c = 18.623(5) Å, β = 117.45(2)°, V = 2394.5(10) Å 3 , Z = 4, R gt ( F ) = 0.0450, wR ref ( F 2 ) = 0.1466, T = 293.0 K.
Open Access
The crystal structure of 2-(2,3-dimethoxyphenyl)-3-hydroxy-4H-chromen-4-one, C₁₇H₁₄O₅

April 9, 2020

Dongsoo Koh

Page range: 913-914

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C 17 H 14 O 5 , monoclinic, P 2 1 / c (no. 14), a = 11.7580(7) Å, b = 8.3745(5) Å, c = 13.8754(8) Å, β = 92.622(2)°, V = 1364.84(14) Å 3 , Z = 4, R gt ( F ) = 0.0423, wR ref ( F 2 ) = 0.1163, T = 223(2) K.
Open Access
The crystal structure of 5-(2-(4-fluorophenyl)hydrazono)-4-methyl-2-((3-(5-methyl-1-(4-methylphenyl)-1H-1,2,3-triazol-4-yl)-1-phenyl-1H-pyrazol-4-yl)methylene) hydrazono)-2,5-dihydrothiazole dimethylformamide monosolvate, C₃₀H₂₅FN₁₀S⋅C₃H₇NO

April 16, 2020

Abdullah A. Alotaibi, Bakr F. Abdel-Wahab, Amany S. Hegazy, Benson M. Kariuki, Gamal A. El-Hiti

Page range: 915-917

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C 30 H 25 FN 10 S⋅C 3 H 7 NO, triclinic, P 1̄ (no. 2), a = 10.9189(6) Å, b = 12.3898(7) Å, c = 13.9206(7) Å, α = 199.412(4)°, β = 110.024(5)°, γ = 105.904(5)°, V = 1631.17(17) Å 3 , Z = 2, R gt ( F ) = 0.0536, wR ref ( F 2 ) = 0.1471, T = 296 K.
Open Access
The crystal structure of 1,8-bis(pyridin-4-ylethynyl)anthracene-1,2,4,5-tetrafluoro-3,6-diiodobenzene (2/1), C₆₂H₃₂F₄I₂N₄

April 17, 2020

Lingfan Zhang, Man-Hua Ding

Page range: 919-921

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C 62 H 32 F 4 I 2 N 4 , triclinic, P 1̄ (no. 2), a = 10.201(9) Å, b = 10.897(9) Å, c = 13.499(12) Å, α = 106.740(9)°, β = 98.981(9)°, γ = 115.198(9)°, V = 1231.1(18) Å 3 , Z = 2, R gt ( F ) = 0.0675, wR ref ( F 2 ) = 0.0645, T = 296(2) K.
Open Access
The crystal structure of 3,6-di-tert-butyl-1,8-diiodo-9-methyl-9H-carbazole, C₂₁H₂₅I₂N

April 16, 2020

Wei-Jun Zhang, Tao Zeng

Page range: 923-924

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C 21 H 25 I 2 N, monoclinic, P 2 1 / m (no. 11), a = 10.2277(18) Å, b = 7.6698(13) Å, c = 13.142(2) Å, β = 93.819(2)°, V = 1028.6(3) Å 3 , Z = 2, R gt ( F ) = 0.0261, wR ref ( F 2 ) = 0.0680, T = 296(2) K.
Open Access
The crystal structure of 8-((4-chlorophenylamino)methylene)-6,10-dioxaspiro[4.5]decane-7,9-dione, C₁₅H₁₄ClNO₄

April 23, 2020

Yun-Chen Zhang, Wu-Lan Zeng

Page range: 925-927

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C 15 H 14 ClNO 4 , monoclinic, P 2 1 / n (no. 14), a = 14.188(3) Å, b = 5.6930(11) Å, c = 17.444(4) Å, β = 95.60(3)°, V = 1402.3(5) Å 3 , Z = 4, R gt ( F ) = 0.0719, wR ref ( F 2 ) = 0.2214, T = 293(2) K.
Open Access
The crystal structure of catena-poly[oktaaqua-bis(μ₂-4,4′-ethene-1,2-diyldipyridine-κ²N:N′)-(μ₂-3,3′-(1-oxidodiazene-1,2-diyl)diphthalato-κ²O:O′)dicobalt(II)] dihydrate, C₂₈H₃₆N₄O₁₉Co₂

April 30, 2020

Xun Feng, Nan Chen, Zhengtao Zhang, Jingjing Yu, Yiming Zhang

Page range: 929-931

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C 28 H 36 N 4 O 19 Co 2 , triclinic, P 1̄ (no. 2), a = 7.4890(5) Å, b = 8.8913(4) Å, c = 13.5918(7) Å, α = 88.027(4)°, β = 89.819(5)°, γ = 69.729(5)°, V = 848.44(9) Å 3 , Z = 1, R gt ( F ) = 0.0435, wR ref ( F 2 ) = 0.1015, T = 293(2) K.
Open Access
Crystal structure of (E)-1-(2-cyano-3-oxo-1-phenylprop-1-en-1-yl)-3,7-diphenylindolizine-6-carbonitrile, C₃₁H₁₉N₃O

April 10, 2020

Feng Wang, Lun-Hua Shen, Jin-Ke Jiang, Nian-gen Chen

Page range: 933-934

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C 31 H 19 N 3 O, triclinic, P 1̄ (no. 2), a = 8.672(5) Å, b = 10.725(6) Å, c = 13.886(8) Å, α = 97.550(9)°, β = 101.415(9)°, γ = 109.603(9)°, V = 1164.9(12) Å 3 , Z = 2, R gt ( F ) = 0.0439, wR ref ( F 2 ) = 0.1288, T = 296 K.
Open Access
Crystal structure of 1,1′-bis(diphenylphosphino)ferrocene-(1,1′-bis(diphenylphosphino)ferrocene-κ²P,P′)-(O-isobutyl sulfurodithioito-κ²S,S′)copper(I), C₃₉H₃₇CuFeOP₂S₂

April 17, 2020

Zhuang-yu Li, Xiao-jing Liu, E. Liu, Fang-fang Jian, Tongling Liang

Page range: 935-937

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C 39 H 37 CuFeOP 2 S 2 , triclinic, P 1̄ (no. 2), a = 9.6132(10) Å, b = 11.5667(12) Å, c = 16.8739(18) Å, α = 99.732(2)°, β = 96.342(2)°, γ = 93.446(2)°, V = 1832.0(3) Å 3 , Z = 2, R gt ( F ) = 0.0455, wR ref ( F 2 ) = 0.1212, T = 293.0 K.
Open Access
Crystal structure of poly[(5-bimethylamino-1-naphthalenesulfonato-κO)-(μ₃-hexamethylenetetramino-κ³N:N′:N′′)silver(I)] dihydrate, C₃₆H₅₂Ag₂N₁₀O₈S₂

April 10, 2020

Jin-Ke Jiang, Gang Yang, Li-Ying Sun, Chun-Yan Wang, Feng Wang

Page range: 939-941

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abstract C 36 H 52 Ag 2 N 10 O 8 S 2 , orthorhombic, Pna 2 1 (no. 33), a = 11.7911(16) Å, b = 31.310(5) Å, c = 10.6883(11) Å, V = 3945.9(9) Å 3 , Z = 4, R gt ( F ) = 0.0353, wR ref ( F 2 ) = 0.0784, T = 293(2) K.
Open Access
Crystal structure of poly[μ₂-diaqua-(μ₂-2-amino-4,5-dicyano-κ²N:N′-imidazol-1-ide)sodium(I)], C₅H₆N₅O₂Na

April 24, 2020

Xue Mei, Wang Jianlong, Yan Sheng, Yang Kaixin, Gao Pengxiang, Duan Jiale

Page range: 943-944

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C 5 H 6 N 5 O 2 Na, triclinic, P 1̄ (no. 2), a = 7.0140(10) Å, b = 7.4328(13) Å, c = 8.9483(16) Å, α = 103.303(7)°, β = 103.719(6)°, γ = 103.634(6)°, V = 419.73(12) Å 3 , Z = 2, R gt ( F ) = 0.0622, wR ref ( F 2 ) = 0.1795, T = 170(2) K.
Open Access
Crystal structure of (1,3-propanediamine-κ²N,N′)(N-(3-aminopropyl)-α-methyl aspartato-κ⁴N,N′,O,O′)cobalt(III) chloride, C₁₁H₂₄ClCoN₄O₄

April 24, 2020

Jiehye Shin, Jaeun Kang, Kang Min Ok, Junghwan Do

Page range: 945-946

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C 11 H 24 ClCoN 4 O 4 , monoclinic, P 2 1 / c (no. 14), a = 11.4214(1) Å, b = 9.8842(1) Å, c = 13.6893(1) Å, β = 106.436(1)°, V = 1482.25(2) Å 3 , Z = 4, R gt ( F ) = 0.0238, wR ref ( F 2 ) = 0.0616, T = 296(2) K.
Open Access
Crystal structure and anti-inflammatory activity of (3E,5E)-3,5-bis(4-fluorobenzylidene)-1-((4-fluorophenyl)sulfonyl)piperidin-4-one-dichloromethane (1/1), C₂₆H₂₀Cl₂F₃NO₃S

April 30, 2020

Wei-Bin Yan, Yong-Jun Liu, Gui-Ge Hou, Wei Cong, Qing-Guo Meng

Page range: 947-949

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C 26 H 20 Cl 2 F 3 NO 3 S, triclinic, P 1̄ (no. 2), a = 8.5616(4) Å, b = 11.6052(6) Å, c = 14.1451(8) Å, α = 66.617(6)°, β = 82.391(4)°, γ = 69.072(4)°, V = 1204.85(12) Å 3 , Z = 2, R gt ( F ) = 0.0460, wR ref ( F 2 ) = 0.1206, T = 100.00(10) K.
Open Access
Crystal structure of (S)-(+)-1-cyclohexylethylaminium chloride, C₈H₁₈NCl

April 29, 2020

Ann-Kathrin Scherer, Walter Frank

Page range: 951-953

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C 8 H 18 NCl, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 5.5244(3) Å, b = 11.0915(6) Å, c = 16.0339(12) Å, V = 982.46(11) Å 3 , Z = 4, R gt ( F ) = 0.0295, wR ref ( F 2 ) = 0.0785, T = 233(2) K.
Open Access
The crystal structure of tris(nitrato-κ²O,O′)-bis(4,4,5,5-tetramethyl-2-(o-pyridyl)imidazoline-1-oxyl 3-oxide-κ²N,O)yttrium(III), C₂₄H₃₂N₉O₁₃Y

April 29, 2020

Dongjiao Li

Page range: 955-957

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C 24 H 32 N 9 O 13 Y, monoclinic, P 2 1 / n (no. 14), a = 12.237(3) Å, b = 11.058(3) Å, c = 23.235(6) Å, β = 98.486(4)°, V = 3109.6(14) Å 3 , Z = 4, R gt ( F ) = 0.0455, wR ref ( F 2 ) = 0.0903, T = 293 K.
Open Access
Hydrogen bonding versus packing effects in the crystal structure of 3-((1R,2S)-1-methylpyrrolidin-1-ium-2-yl)pyridin-1-ium tetraiodidozincate(II), C₁₀H₁₆I₄ZnN₂

May 5, 2020

Guido J. Reiss, Alena Sergeeva

Page range: 959-962

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C 10 H 16 I 4 ZnN 2 , monoclinic, P 2 1 (no. 4), a = 7.3340(1) Å, b = 14.4781(3) Å, c = 8.6768(2) Å, β = 94.919(2)°, V = 917.93(3) Å 3 , Z = 2, R gt ( F ) = 0.0165, wR ref ( F 2 ) = 0.0397, T = 110 K.
Open Access
Dimerization of 2-[(2-((2-aminophenyl)thio)phenyl)amino]-cyclohepta-2,4,6-trien-1-one through hydrogen bonding, C₁₉H₁₆N₂OS

May 5, 2020

Anna Hanft, Crispin Lichtenberg

Page range: 963-966

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C 19 H 16 N 2 OS, triclinic, P 1̄ (no. 2), a = 8.1510(3) Å, b = 8.8021(3) Å, c = 11.3953(5) Å, α = 72.546(2)°, β = 84.568(2)°, γ = 80.760(2)°, V = 768.86(5) Å 3 , Z = 2, R gt ( F ) = 0.0491, wR ref ( F 2 ) = 0.1494, T = 100 K.
Open Access
Crystal structure of 1-(4-chloro-phenyl)-7-ethoxyl-6,8-difluoro-4-oxo-1,4-dihydro-quinoline-3-carboxylic acid, C₁₈H₁₂ClF₂NO₄

April 24, 2020

Liu-Hong Zou, Xu-Liang Nie, Lei Zhao, Guo-Ping Huang, Jian-Ping Huang

Page range: 967-969

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C 18 H 12 ClF 2 NO 4 , monoclinic, P 2 1 / c (no. 14), a = 13.544(5) Å, b = 9.344(3) Å, c = 13.545(5) Å, β = 109.86°, V = 1612.4(10) Å 3 , Z = 4, R gt ( F ) = 0.0393, wR ref ( F 2 ) = 0.1058, T = 296(2) K.
Open Access
Crystal structure of 7-ethoxy-6,8-difluoro-4-oxo-1-pyridin-2-ylmethyl-1,4-dihydro-quinoline-3-carboxylic acid, C₁₈H₁₄F₂N₂O₄

April 24, 2020

Fang Shu-Fang, Gu Jia, Xiong Yuan-Zhen, Huang Guo-Ping, Huang Jian-Ping

Page range: 971-973

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C 18 H 14 F 2 N 2 O 4 , triclinic, P 1̄ (no. 2), a = 6.377(3) Å, b = 9.466(5) Å, c = 13.367(7) Å, α = 83.409(6)°, β = 83.283(6)°, γ = 83.728(6)°, V = 792.3(7) Å 3 , Z = 2, R gt ( F ) = 0.0587, wR ref ( F 2 ) = 0.1814, T = 296(2) K.
Open Access
Crystal structure of octahydro-7aR,8′R-dimethylspiro[isobenzofuran-4(1H), 4′ (3′H)-[1H-7,9a]methanocyclohepta[c]pyran]-1′,3, 9′ (3aH,4′aH)-trione, C₂₀H₂₆O₅

April 24, 2020

Kang He, Yu-Xue Wang, Jiang-Hai Ye, Juan Zou, Wei Zhao, Jing-Jie Zhang, Jin-Yi Zhang

Page range: 975-976

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C 20 H 26 O 5 , monoclinic, P 2 1 (no. 4), a = 7.0011(5) Å, b = 12.3136(9) Å, c = 10.4847(8) Å, β = 105.734(2)°, V = 870.01(11) Å 3 , Z = 2, R gt ( F ) = 0.0384, wR ref ( F 2 ) = 0.0925, T = 302(2) K.
Open Access
Crystal structure of bis(5-ethoxy-2-(((1-hydroxy-2-methyl-3-oxidopropan-2-yl)imino)methyl)phenolato-κ³N,O,O’)manganese(IV) – methanol (1/1), C₂₇H₃₈MnN₂O₉

April 24, 2020

Ge Yuan, Wang Dengwu, Huo Xiaoping, Yang Liguo, Zhang Cuihong

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C 27 H 38 MnN 2 O 9 , monoclinic, C 2/ c (no. 15), a = 14.9473(14) Å, b = 17.8744(16) Å, c = 12.5536(11) Å, β = 122.596(5)°, V = 2825.7(5) Å 3 , Z = 4, R gt ( F ) = 0.0423, wR ref ( F 2 ) = 0.1295, T = 298 K [1], [2], [3].
Open Access
Crystal structure of 8a,8a′′-oxybis(8aH-8,9-dioxa-3a¹λ⁴-aza-8aλ⁴-borabenzo[fg]tetracene), C₃₄H₂₂B₂N₂O₅

April 24, 2020

Siyi Ding, Qiang Ma, Huaping Ren, Zongcheng Miao

Page range: 979-980

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C 34 H 22 B 2 N 2 O 5 , monoclinic, P 2 1 / c (no. 14), a = 9.9886(3) Å, b = 17.8995(6) Å, c = 14.3437(5) Å, β = 98.141(3)°, V = 2538.68(15) Å 3 , Z = 4, R gt ( F ) = 0.0391, wR ref ( F 2 ) = 0.1022, T = 100 K.
Open Access
Crystal structure of bromido-triphenyl-(triphenylarsine oxide-κO)tin(IV), C₃₆H₃₀AsBrOSn

April 24, 2020

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

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C 36 H 30 AsBrOSn, triclinic, P 1̄ (no. 2), a = 9.8316(1) Å, b = 10.8781(2) Å, c = 14.9388(2) Å, α = 102.367(1)°, β = 93.369(1)°, γ = 103.134(1)°, V = 1510.07(4) Å 3 , Z = 2, R gt ( F ) = 0.0175, wR ref ( F 2 ) = 0.0469, T = 100 K.
Open Access
Crystal structure of catena-poly[chlorido-(μ₂-formato-κ²O:O′)-(1,10-phenathroline-κ²N,N′)copper(II)], C₂₆H₁₈Cl₂Cu₂N₄O₄

May 5, 2020

Xia Li, Shangjun Liu, Mingle Shen, Weihong Yan

Page range: 985-986

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C 26 H 18 Cl 2 Cu 2 N 4 O 4 , monoclinic, P 2 1 / c (no. 14), a = 9.5129(9) Å, b = 17.8130(17) Å, c = 15.2973(12) Å, β = 110.975(5)°, V = 2420.4(4) Å 3 , Z = 4, R gt ( F ) = 0.0269, wR ref ( F 2 ) = 0.0929, T = 293(2) K.
Open Access
The crystal structure of poly[(μ₁₀-5-carboxyisophthalato-κ¹⁰O)disodium], C₉H₄Na₂O₆

April 30, 2020

Ting-Ting Li, Yu-Cai Qin, Bao-Kuan Chen

Page range: 987-988

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C 9 H 4 Na 2 O 6 , monoclinic, C 2/ c (no. 15), a = 14.6828(15) Å, b = 9.8602(10) Å, c = 6.5024(7) Å, β = 101.360(4)°, V = 922.94(17) Å 3 , Z = 4, R gt ( F ) = 0.0337, wR ref ( F 2 ) = 0.0775, T = 173(2) K.
Open Access
The crystal structure of 3,5-difluoroisonicotinic acid, C₆H₃F₂NO₂

April 29, 2020

Yan Zeng, Chao-Jun Du

Page range: 989-990

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C 6 H 3 F 2 NO 2 , monoclinic, P 2 1 / n (no. 14), a = 6.8050(10) Å, b = 6.8443(9) Å, c = 12.7196(14) Å, β = 94.562(4)°, V = 590.54(13) Å 3 , Z = 4, R gt ( F ) = 0.0395, wR ref ( F 2 ) = 0.1038, T = 150(2) K.
Open Access
The crystal structure of ethyl-1-(N-(adamantan-1-yl)-carbamothioyl)piperidine-4-carboxylate, C₁₉H₃₀N₂O₂S

April 21, 2020

Ahmed Bari, Syed Saeed Ali, Abdulrahman M. Alghadeer, Turki Alturki, Eric C. Hosten

Page range: 991-992

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C 19 H 30 N 2 O 2 S, monoclinic, P 2 1 / n (no. 14), a = 6.4977(5) Å, b = 28.728(2) Å, c = 10.1806(8) Å, β = 101.549(3)°, V = 1861.9(2) Å 3 , Z = 4, R gt ( F ) = 0.0460, wR ref ( F 2 ) = 0.1213, T = 296 K.
Open Access
Crystal structure of 5-methyl-3-phenyl-1-tosyl-1,2,3,4-tetrahydropyridine, C₁₉H₂₁NO₂S

April 21, 2020

Huixia Liu, Xie Huang, Wei He

Page range: 993-994

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C 19 H 21 NO 2 S, orthorhombic, Pbca (no. 61), a = 16.792(5) Å, b = 9.153(3) Å, c = 22.809(6) Å, V = 3505.8(16) Å 3 , Z = 8, R gt ( F ) = 0.0622, wR ref ( F 2 ) = 0.1494, T = 296(2) K.
Open Access
Crystal structure of bis((3-chlorosalicylidene)-ethylenediaminato-κ⁴N,N′,O,O′)nickel (II), C₁₆H₁₂Cl₂NiN₂O₂

May 1, 2020

Jianchang Xiao, Cun Zhou, Hui Tan, Meifen Huang, Qiong Wu

Page range: 995-996

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C 16 H 12 Cl 2 NiN 2 O 2 , orthorhombic, Pbca (no. 61), a = 12.5166(12) Å, b = 12.5881(14) Å, c = 19.0086(19) Å, V = 2995.0(5) Å 3 , Z = 8, R gt ( F ) = 0.0435, wR 2 = 0.0826, T = 296.15.
Open Access
Crystal structure of (E)-N′-(2-chloro-6-hydroxybenzylidene)-4-hydroxybenzohydrazide — dihydrofuran-2(3H)-one (1/1), C₁₈H₁₇ClN₂O₅

April 24, 2020

Juan Chen, Zhe Liu, Haijun Yan

Page range: 997-998

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C 18 H 17 ClN 2 O 5 , monoclinic, P 2 1 / c (no. 14), a = 10.223(8) Å, b = 13.407(9) Å, c = 13.786(9) Å, β = 109.825(5)°, V = 1778(2) Å 3 , Z = 4, R gt ( F ) = 0.0912, wR ref ( F 2 ) = 0.1867, T = 293(2) K.
Open Access
Crystal structure of bis((3-bromosalicylidene)-ethylenediaminato-κ⁴N,N′,O,O′) nickel (II), C₁₆H₁₂Br₂NiN₂O₂

April 24, 2020

Jianchang Xiao, Cun Zhou, Xu Xindi, Hua Lei, Qiong Wu

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C 16 H 12 Br 2 NiN 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 11.7989(9) Å, b = 11.9007(7) Å, c = 12.7164(17) Å, β = 119.779(7)°, V = 1549.8(3) Å 3 , Z = 4, R gt ( F ) = 0.0324, wR ref ( F 2 ) = 0.0687, T = 173(2) K.
Open Access
Crystal structure of trimethylsulfoxonium tetrachloridocobaltate(II) [(CH₃)₃SO]₂CoCl₄

April 30, 2020

Xin Zhong, Junyan Zhou, Munan Hao

Page range: 1001-1002

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C 6 H 18 S 2 O 2 CoCl 4 , monoclinic, P 2 1 / c (no. 14), a = 8.4397(3) Å, b = 15.6692(5) Å, c = 12.5989(4) Å, β = 93.8580(10)°, V = 1662.35(10) Å 3 , Z = 4, R gt ( F ) = 0.0408, wR ref ( F 2 ) = 0.0965, T = 293(2) K.

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