Zeitschrift für Kristallographie - New Crystal Structures

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Volume 236, Issue 6

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Zeitschrift für Kristallographie - New Crystal Structures

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Frontmatter

November 2, 2021

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New Crystal Structures
Open Access
Redetermination of the crystal structure of 3-bromonitrobenzene at 200 K, C₆H₄BrNO₂ – temperature effects on cell constants

July 30, 2021

Pholani Manana, Eric C. Hosten, Richard Betz

Page range: 1131-1133

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C 6 H 4 BrNO 2 , orthorhombic, Pna 2 1 (no. 33), a = 21.3992(17) Å, b = 5.9311(4) Å, c = 5.2923(4) Å, V = 671.70(9) Å 3 , Z = 4, R gt ( F ) = 0.0284, wR ref ( F 2 ) = 0.0708, T = 200(2) K.
Open Access
Crystal structure of (E)-ethyl 2-((4-oxo-4H-chromen-3-yl)methyleneaminooxy)acetate, C₁₄H₁₃NO₅

July 29, 2021

Miri Yoo, Dongsoo Koh

Page range: 1135-1137

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C 14 H 13 NO 5 , monoclinic, P 2 1 (no. 4), a = 4.6967(7) Å, b = 10.7175(16) Å, c = 12.945(2) Å, β = 94.827(8)°, V = 649.30(17) Å 3 , Z = 2, R gt ( F ) = 0.0577, wR ref ( F 2 ) = 0.1302, T = 223(2) K.
Open Access
Crystal structure of (8R,10R,14R, Z)-2-((3–Fluoropyridin-4-yl) methylene)-12-hydroxy-4,4,8,10,14-pentamethyl-17-((R)-2,6, 6-trimethyltetrahydro-2H-pyran-2-yl) hexadecahydro-3H-cyclopenta[a] phenanthren-3-one, C₃₆H₅₂FNO₃

July 30, 2021

Mei Zhang, Qing-Guo Meng, Gui-Ge Hou, Sheng Jiang, Yong-Sheng Jin, Yue Gao

Page range: 1139-1142

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C 36 H 52 FNO 3 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 7.8016(7) Å, b = 13.1609(10) Å, c = 30.536(2) Å, V = 3135.3(4) Å 3 , Z = 4, R gt ( F ) = 0.0657, wR ref ( F 2 ) = 0.1435, T = 100 K.
Open Access
Crystal structure of [6,6′-((1E,1′E)-(propane-1,3- diylbis(azaneylylidene))bis(methaneylylidene)) bis(3-chlorophenol)-κ⁴N,N′,O,O′] copper(II), C₁₇H₁₄Cl₂CuN₂O₂

August 3, 2021

Baiying Wei, Chenzhong Cao

Page range: 1143-1144

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C 17 H 14 Cl 2 CuN 2 O 2 , monoclinic, C 2/ c (no. 15), a = 22.743(4) Å, b = 8.0434(15) Å, c = 8.9388(17) Å, V = 1630.8(5) Å 3 , Z = 4, R gt ( F ) = 0.0376, wR ref ( F 2 ) = 0.0997, T = 296(2) K.
Open Access
The crystal structure of 6-amino-2-carboxypyridin-1-ium bromide, C₆H₇BrN₂O₂

August 2, 2021

Mengbing Cui, Yan Zeng, Yong Li, Heng Chen

Page range: 1145-1146

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C 6 H 7 BrN 2 O 2 , monoclinic, C 2/ c (no. 15), a = 23.7470(19) Å, b = 5.4355(4) Å, c = 15.3336(11) Å, β = 127.291(2)°, V = 1574.6(2) Å 3 , Z = 8, R gt ( F ) = 0.0292, wR ref ( F 2 ) = 0.0756, T = 150(2) K.
Open Access
Redetermination of the crystal structure of bis[N,N′-ethylenebis(acetylacetoniminato)nickel(II)] sodium perchlorate, C₂₄H₃₆ClN₄NaNi₂O₈

August 9, 2021

Lucky Dey, Saswata Rabi, Zinnat A. Begum, Tsugiko Takase, Ismail M.M. Rahman, Edward R.T. Tiekink, Tapashi Ghosh Roy

Page range: 1147-1150

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C 24 H 36 ClN 4 NaNi 2 O 8 , monoclinic, C 2/ c (no. 15), a = 19.5909(11) Å, b = 10.8023(6) Å, c = 14.5722(8) Å, β = 112.032(1)°, V = 2858.7(3) Å 3 , Z = 4, R gt ( F ) = 0.0260, wR ref ( F 2 ) = 0.0701, T = 93(2) K.
Open Access
The crystal structure of 3-methyl-2,6-dinitrophenol, C₇H₆N₂O₅

August 2, 2021

He Jiayuan, Liu Yunzhang, Zhang Kaiyue, Chen Lizhen, Wang Jianlong

Page range: 1151-1153

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C 7 H 6 N 2 O 5 , monoclinic, P 2 1 / n (no. 14), a = 9.5931(16) Å, b = 17.332(3) Å, c = 9.8989(14) Å, β = 94.902(5)°, V = 1639.9(4) Å 3 , Z = 8, R gt ( F ) = 0.0619, wR ref ( F 2 ) = 0.1784, T = 170 K.
Open Access
The crystal structure of 5-chloro-2-(quinolin-8-yl)isoindoline-1,3-dione, C₁₇H₉ClN₂O₂

August 6, 2021

Wei Zhang, Yu Zhang, Song-Hao Feng, Jing-Jing Wang

Page range: 1155-1156

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C 17 H 9 ClN 2 O 2 , triclinic, P 1 ‾ $P‾{1}$ (no. 2), a = 7.8944(4) Å, b = 8.0678(5) Å, c = 12.6285(9) Å, α = 74.627(6)°, β = 78.654(5)°, γ = 63.569(5)°, V = 691.58(8) Å 3 , Z = 2, R gt ( F ) = 0.0431, wR ref ( F 2 ) = 0.1309, T = 293(2) K.
Open Access
Crystal structure of trans-tetraaqua-bis{2-carboxy-4-((5-carboxypyridin-3-yl)oxy)benzoato-κ¹ N}cobalt(II) dihydrate C₂₈H₂₈O₂₀N₂Co

September 22, 2021

Xigang Du

Page range: 1157-1159

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C 28 H 28 O 20 N 2 Co, triclinic, P 1 ‾ $P‾{1}$ (no. 2), a = 7.7951(3) Å, b = 9.3511(4) Å, c = 11.3352(4) Å, β = 105.499(4)°, Z = 1, V = 762.19(6) Å 3 , R gt ( F ) = 0.0339, wR ref ( F 2 ) = 0.0798, T = 293.0 K.
Open Access
Crystal structure of 3-allyl-4-(2-bromoethyl)-5-(4-methoxyphenyl)-2-(p-tolyl)furan, C₂₃H₂₃BrO₂

July 29, 2021

Xue-Li Xu, Jihong Li

Page range: 1161-1163

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C 23 H 23 BrO 2 , monoclinic, P 2 1 / c (no. 14), a = 24.193(4) Å, b = 5.8614(10) Å, c = 13.873(3) Å, β = 93.168(3) ∘ , V = 1964.3(6) Å 3 , Z = 4, R gt ( F ) = 0.0316, wR ref ( F 2 ) = 0.0915, T = 296(2) K.
Open Access
The crystal structure of 6,6′-(((2-(dimethylamino)ethyl)azanediyl)bis(methylene))bis(benzo[d][1,3]dioxol-5-ol ato-κ⁴N,N′,O,O′)-(pyridine-2,6-dicarboxylato-N,O,O′)-titanium(IV)-dichloromethane(1/1), C₂₇H₂₅N₃O₁₀Ti

August 16, 2021

Shanjia Li, Peng Wang, Mingyu Ji, Mingjun Yang, Xiuying Pu, Tiankun Zhao

Page range: 1165-1167

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C 27 H 25 N 3 O 10 Ti, monoclinic, P 2 1 / n (no. 14), a = 11.3366(11) Å, b = 11.0253(11) Å, c = 23.7160(2) Å, β = 100.839(2)°, V = 2911.4(5) Å 3 , Z = 4, R gt ( F ) = 0.0615, wR ref ( F 2 ) = 0.1411, T = 296(2) K.
Open Access
Crystal structure of (((1E,1′E)-1,2-phenylenebis(methaneylylidene))bis(hydrazin-1-yl-2-ylidene))bis(aminomethaniminium) dinitrate C₁₀H₁₆N₁₀O₆

August 5, 2021

Ze-Sen Jin, E. Liu, Xiao-Jing Liu, Zhuang-Yu Li, Fang-fang Jian, Tongling Liang

Page range: 1169-1170

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C 10 H 16 N 10 O 6 , monoclinic, C 2 /c (no. 15), a = 12.5131(7) Å, b = 16.4675(9) Å, c = 8.1488(4) Å, β = 107.361(5)°, V = 1602.64(15) Å 3 , Z = 4, R gt ( F ) = 0.0380, wR ref ( F 2 ) = 0.1180, T = 170(1) K.
Open Access
Crystal structure of catena-poly[triaqua-(μ ₂-1,3-di(1H-imidazol-1-yl)propane-κ ² N:N′)-(4,4′-(1H-1,2,4-triazole-3,5-diyl)dibenzoato-κ ¹ O)nickel(II)]N,N′-dimethylformamide (1/1), C₂₈H₃₅N₈O₈Ni

August 16, 2021

Fei Xi, Yan-Hong Gao, Bo Tang, Hong-Guang Ge, Qin Wang, Jiu-Fu Lu

Page range: 1171-1173

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C 28 H 35 N 8 O 8 Ni, monoclinic, P 2 1 / c (no. 14), a = 14.7476(15) Å, b = 19.6335(19) Å, c = 10.8116(11) Å, β = 104.334(2)°, V = 3033.0(5) Å 3 , Z = 4, R gt ( F ) = 0.0548, wR ref ( F 2 ) = 0.0961, T = 293(2) K.
Open Access
The crystal structure of 3,3′-[1,4-phenylenebis(methylene)]bis(1-ethenyl-1H-imidazol-3-ium) dichloride – dichloromethane – water (1/1/1), C₁₉H₂₄Cl₄N₄O₁

August 13, 2021

Wenqi Song, Miaoxiu Yang, Liwei Qian, Zongcheng Miao

Page range: 1175-1177

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C 19 H 24 Cl 4 N 4 O 1 , triclinic, P 1 ‾ $P‾{1}$ (no. 2), a = 8.5930(4) Å, b = 12.0814(5) Å, c = 12.2430(5) Å, α = 69.805(2)°, β = 75.2820(10)°, γ = 86.733(2)°, V = 1153.07(9) Å 3 , Z = 2, R gt ( F ) = 0.0411, wR ref ( F 2 ) = 0.1053, T = 296 K.
Open Access
Crystal structure of 1,1′-(methane-1,1-diyl)bis(3-propyl-1H-imidazol-3-ium) bis(hexafluoridophosphate), C₁₃H₂₂F₁₂N₄P₂

August 13, 2021

Xin-Ting Liu, Xu-Liang Nie, Shi-Shun Chen, Su-Qin Wu, Wan-Ming Xiong

Page range: 1179-1182

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C 13 H 22 F 12 N 4 P 2 , monoclinic, P 2 1 / c (no. 14), a = 25.252(3) Å, b = 8.3297(9) Å, c = 23.268(2) Å, β = 116.271(1)°, V = 4388.7(8) Å 3 , Z = 8, R gt ( F ) = 0.0661, wR ref ( F 2 ) = 0.2191, T = 296(2) K.
Open Access
Crystal structure of dichlorido-bis(4-chlorophenyl-κC ¹)tin(IV), C₁₂H₈Cl₄Sn

August 2, 2021

Kong Mun Lo, See Mun Lee, Edward R. T. Tiekink

Page range: 1183-1185

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C 12 H 8 Cl 4 Sn, monoclinic, P 2 1 / c (no. 14), a = 13.4238(1) Å, b = 18.2079(2) Å, c = 5.7617(1) Å, β = 95.506(1)°, V = 1401.77(3) Å 3 , Z = 4, R gt ( F ) = 0.0272, wR ref ( F 2 ) = 0.0798, T = 100 K.
Open Access
Synthesis and crystal structure of 4-acetylpyrene, C₁₈H₁₂O

August 2, 2021

Zhang Ran, Wang Hui, Miao Bao-Xi, Zhang Li-Fang

Page range: 1187-1190

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C 18 H 12 O, triclinic, P 1 ‾ $P‾{1}$ (no. 2), a = 10.132(2) Å, b = 10.654(2) Å, c = 11.730(2) Å, α = 90.31(3)°, β = 102.38(3)°, γ = 104.81(3)°, V = 1193.2(4) Å 3 , Z = 4, R gt ( F ) = 0.0403, wR ref ( F 2 ) = 0.1037, T = 293(2) K.
Open Access
Crystal structure of 2,2′-(butane-1,4-diylbis(azanylylidene))bis(methanylylidene))bis(4-methoxyphenol), C₂₀H₂₄N₂O₄

August 9, 2021

Daniel M. Orang’o, Martin O. Onani, Paul K. Tarus, Samuel T. Lutta, Roger A. Lalancette

Page range: 1191-1193

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C 20 H 24 N 2 O 4 , monoclinic, P 2 1 / n (no. 14), a = 11.0474(3) Å, b = 6.0853(2) Å, c = 13.9881(4) Å, β = 104.271(2)°, V = 911.36(5) Å 3 , Z = 2, R gt ( F ) = 0.0290, wR ref ( F 2 ) = 0.0728, T = 100(2) K.
Open Access
The crystal structure of (E)-2-(((5-((triphenylstannyl)thio)-1,3,4-thiadiazol-2-yl)imino)methyl)phenol, C₂₇H₂₁N₃OS₂Sn

August 18, 2021

Junshan Sun

Page range: 1195-1197

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C 27 H 21 N 3 OS 2 Sn, triclinic, P 1 ‾ $P‾{1}$ (no. 2), a = 11.064(3) Å, b = 11.538(3) Å, c = 12.257(3) Å, V = 1258.2(6) Å 3 , Z = 2, R gt ( F ) = 0.0316, wR ref ( F 2 ) = 0.0664, T = 298 K.
Open Access
Crystal structure of diaqua-bis(μ₂-6-phenylpyridine-2-carboxylate-κ³N,O:O)-bis(6-phenylpyridine-2-carboxylato-κ²N,O)lead(II) – N,N-dimethylformamide – water (1/2/4), C₅₄H₅₈N₆O₁₆Pb₂

August 13, 2021

Xi-Shi Tai, Lei Liang, Xiang-Tao Li, Shu-Hua Cao, Li-Hua Wang

Page range: 1199-1201

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C 54 H 58 N 6 O 16 Pb 2 , triclinic, P 1 ‾ $P‾{1}$ (no. 2), a = 9.4690(6) Å, b = 12.9374(6) Å, c = 13.2303(7) Å, V = 1341.90(15) Å 3 , α = 63.395(5)°, β = 74.291(5)°, γ = 69.113(5)°, Z = 1, R gt ( F ) = 0.0284, wR ref ( F 2 ) = 0.0484, T = 150 K.
Open Access
Crystal structure of methyl 4-acetoxy-3-methoxybenzoate, C₁₁H₁₂O₅

August 13, 2021

Pan-Lei Xiao, Xiu-Ying Song, Chen-Yu Yang, Xu-Liang Nie, Yi-Hua Wang

Page range: 1203-1205

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C 11 H 12 O 5 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 5.5523(7) Å, b = 12.7610(17) Å, c = 15.374(2) Å, V = 1089.3(2) Å 3 , Z = 4, R gt ( F ) = 0.0273, wR ref ( F 2 ) = 0.0787, T = 296(2) K.
Open Access
Crystal structure of 2,2′-(propane-1,3-dilylbis(azaneylylidene))bis(methanylylidene)bis(4-methylphenol), C₁₉H₂₂N₂O₂

August 31, 2021

Daniel M. Orang’o, Martin O. Onani, Paul K. Tarus, Samuel T. Lutta, Roger A. Lalancette

Page range: 1207-1209

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C 19 H 22 N 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 19.3063(4) Å, b = 5.83200(10) Å, c = 14.7996(3) Å, β = 92.715(1)°, V = 1664.48(6) Å 3 , Z = 4, R gt ( F ) = 0.0423, wR ref ( F 2 ) = 0.1102, T = 100(2) K.
Open Access
Crystal structure of dichlorido-bis(4-methylphenyl-κC¹)tin(IV), C₁₄H₁₄Cl₂Sn

August 2, 2021

Kong Mun Lo, See Mun Lee, Edward R. T. Tiekink

Page range: 1211-1213

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C 14 H 14 Cl 2 Sn, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 8.2912(1) Å, b = 9.6221(1) Å, c = 18.5616(2) Å, V = 1480.82(3) Å 3 , Z = 4, R gt ( F ) = 0.0142, wR ref ( F 2 ) = 0.0347, T = 100 K.
Open Access
Crystal structure of methyl (E)-3-(4-acetoxyphenyl)acrylate, C₁₂H₁₂O₄

August 31, 2021

Jia Gu, Xiu-Ying Song, Gui-Shu Wang, Jun Peng, Xu-Liang Nie

Page range: 1215-1217

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C 12 H 12 O 4 , monoclinic, P 2 1 / c (no. 14), a = 16.071(6) Å, b = 9.424(4) Å, c = 7.640(3) Å, β = 101.861(5)°, V = 1132.4(8) Å 3 , Z = 4, R gt ( F ) = 0.0366, wR ref ( F 2 ) = 0.1043, T = 296(2) K.
Open Access
The crystal structure of bis(benzoato-κ² O,O′)-(2,9-dimethyl-1,10-phenanthroline-κ² N,N′)-copper(II), C₂₈H₂₂CuN₂O₄

August 18, 2021

Fei Yang, Pengju Liu, Libing Guo, Dong Xian

Page range: 1219-1221

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C 28 H 22 CuN 2 O 4 , monoclinic, C 2/ c (no. 15), a = 17.2971(3) Å, b = 14.4409(3) Å, c = 9.5617(2) Å, β = 90.580(2)°, V = 2388.25(8) Å 3 , Z = 4, R gt ( F ) = 0.0536, wR ref ( F 2 ) = 0.1406, T = 293 K.
Open Access
Crystal structure of (8R,10R,14R,Z)-12-hydroxy-2-((6-methoxypyridin-2-yl)methylene)-4,4,8,10,14-pentamethyl-17-((R)-2,6,6-trimethyltetrahydro-2H-pyran-2-yl)hexadecahydro-3H-cyclopenta[a]phenanthren-3-one–water (2/1), C₃₇H₅₆NO_4.5

September 7, 2021

Qin Luo, Qing-Guo Meng, Gui-Ge Hou, Sheng Jiang, Yong-Sheng Jin, Yue Gao

Page range: 1223-1226

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C 37 H 56 NO 4.5 , tetragonal, P 4 1 2 1 2/ c (no. 92), a = 10.4368(10) Å, b = 10.4268(10) Å, c = 61.5166(11) Å, V = 6700.80(18) Å 3 , Z = 8, R gt ( F ) = 0.0557, wR ref ( F 2 ) = 0.1350, T = 100 K.
Open Access
Crystal structure of dimethyl-bis(4-bromophenyl-κC¹)tin(IV), C₁₄H₁₄Br₂Sn

August 13, 2021

See Mun Lee, Kong Mun Lo, Edward R. T. Tiekink

Page range: 1227-1229

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C 14 H 14 Br 2 Sn, monoclinic, P 2 1 / c (no. 14), a = 12.9848(2) Å, b = 18.9911(2) Å, c = 6.0550(1) Å, β = 99.136(1)°, V = 1474.19(4) Å 3 , Z = 4, R gt ( F ) = 0.0193, wR ref ( F 2 ) = 0.0490, T = 100 K.
Open Access
The crystal structure of the cocrystal di-μ₂-chlorido-octamethyl-di-μ₃-oxido-bis(2,3,4,5-tetrafluorobenzoato-κ² O,O′)tetratin(IV) ─ octamethyl-di-μ₃-oxido-bis(μ₂-2,3,4,5-tetrafluorobenzoato-κ² O:O′)-bis(μ₂-2,3,4,5-tetrafluorobenzoato-κ² O:O;O′)tetratin(IV) C₅₈H₅₄Cl₂F₂₄O₁₆Sn₈

October 1, 2021

Junshan Sun

Page range: 1231-1233

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C 58 H 54 Cl 2 F 24 O 16 Sn 8 , triclinic, P 1 ‾ $P‾{1}$ (no. 2), a = 7.609(4) Å, b = 13.938(6) Å, c = 19.190(9) Å, α = 77.599(7)°, β = 89.846(7)°, γ = 79.841(7)°, V = 1955.2(15) Å 3 , Z = 1, R gt ( F ) = 0.0578, wR ref ( F 2 ) = 0.1660, T = 298 K.
Open Access
Crystal structure of 3-iodo-N ²-(2-methyl-1-(methylsulfonyl)propan-2-yl)-N ¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide, C₂₃H₂₂F₇I₁N₂O₄S₁

September 6, 2021

Juan Luo, Jie Wang, Gao-Yan Qiu, Wan-Ming Xiong, Da-Yong Peng

Page range: 1235-1238

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8[C 23 H 22 F 7 I 1 N 2 O 4 S 1 ], monoclinic, Cc (no. 9), a = 19.762(3) Å, b = 24.690(4) Å, c = 12.106(2) Å, β = 113.696(2)°, V = 5408.8(15) Å 3 , Z = 1, R gt ( F ) = 0.0488, wR ref ( F 2 ) = 0.1411, T = 296(2) K.
Open Access
Crystal structure of 1-(2-(4-bromophenyl)-2,3-dihydro-1H-benzo[e]indol-1-yl)-naphthalen-2-ol – dichloromethane – dimethyl sulfoxide (1/1/1), C₂₈H₁₈BrNO·CH₂Cl₂·C₂H₆SO

October 1, 2021

Lei Zhu, Jiao Wang, Jingzhe Zhao, Shaobin Miao

Page range: 1239-1241

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C 28 H 18 BrNO, triclinic, P 1 ‾ $P‾{1}$ (no. 2), a = 11.7627(7) Å, b = 11.8731(9) Å, c = 11.9240(7) Å, α = 76.952(3)°, β = 85.718(6)°, γ = 60.534(3)°, V = 1411.16(16) Å 3 , Z = 2, R gt ( F ) = 0.0497, wR ref ( F 2 ) = 0.1365, T = 273 K.
Open Access
Crystal structure of [meso-5,7,7,12,14,14,-hexamethyl-1,4,8,11-tetraazacyclotetradecane]nickel(II) diperchlorate – dimethylsulphoxide (1/2), C₂₀H₄₈Cl₂N₄NiO₁₀S₂

August 13, 2021

Saswata Rabi, Lucky Dey, Debashis Palit, Benu Kumar Dey, Ismail M. M. Rahman, Edward R. T. Tiekink, Tapashi Ghosh Roy

Page range: 1243-1245

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C 20 H 48 Cl 2 N 4 NiO 10 S 2 , monoclinic, P 2 1 / n (no. 14), a = 8.657(2) Å, b = 15.233(4) Å, c = 11.956(3) Å, β = 102.737(2)°, V = 1537.9(7) Å 3 , Z = 2, R gt ( F ) = 0.0237, wR ref ( F 2 ) = 0.0655, T = 93(2) K.
Open Access
Crystal structure of 1,1′-(1,3-phenylenebis(methylene))bis(pyridin-1-ium) bis(1,2-dicyanoethene-1,2-dithiolato-κ² S:S) palladium(II), C₂₆H₁₈N₆PdS₄

October 1, 2021

Xue-Guo Liu, Hui-Yan Pan

Page range: 1247-1249

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C 26 H 18 N 6 PdS 4 , monoclinic, C 2/ c (no. 15), a = 16.658(2) Å, b = 10.398(3) Å, c = 17.284(2) Å, β = 116.928(3)°, V = 2669.2(9) Å 3 , Z = 4, R gt ( F ) = 0.0330, wR ref ( F 2 ) = 0.0912, T = 293(2) K.
Open Access
The crystal structure of bis(6-phenylpyridine-2-carboxylato-κ² N,O)copper(II), C₂₄H₁₆N₂O₄Cu

September 22, 2021

Wang Li-Hua, Liang Lei, Li Xiang-Tao, Cao Shu-Hua, Tai Xi-Shi

Page range: 1251-1253

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C 24 H 16 N 2 O 4 Cu, triclinic, P 1 ‾ $P‾{1}$ (no. 2), a = 11.2454(6) Å, b = 13.5960(7) Å, c = 14.0076(8) Å, V = 1958.9(2) Å 3 , α = 79.019(5)°, β = 71.729(5)°, γ = 76.126(5)°, Z = 4, R gt ( F ) = 0.0438, wR ref ( F 2 ) = 0.1030, T = 150 K.
Open Access
Crystal structure of dichlorido-bis(4-chlorophenyl-κC)-bis(triphenylarsine oxide-κO)tin(IV), C₄₈H₃₈As₂Cl₄O₂Sn

August 11, 2021

See Mun Lee, Kong Mun Lo, Edward R. T. Tiekink

Page range: 1255-1257

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C 48 H 38 As 2 Cl 4 O 2 Sn, monoclinic, P 2 1 / n (no. 14), a = 10.8019(1) Å, b = 14.6976(1) Å, c = 13.6266(1) Å, β = 90.983(1)°, V = 2163.07(3) Å 3 , Z = 2, R gt ( F ) = 0.0199, wR ref ( F 2 ) = 0.0514, T = 100 K.
Open Access
Crystal structure of (4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane-κ ⁸ N ₂, O ₆) potassium cyclopentadienide, [K([2.2.2]crypt)]Cp, C₂₃H₄₁KN₂O₆

August 31, 2021

Christina Fischer, Wilhelm Klein, Thomas F. Fässler

Page range: 1259-1261

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C 23 H 41 KN 2 O 6 , monoclinic, P 2 1 / c (no. 14), a = 10.9817(6) Å, b = 23.8330(15) Å, c = 9.7379(7) Å, β = 94.705(5)°, V = 2540.1(3) Å 3 , Z = 4, R gt ( F ) = 0.0327, wR ref ( F 2 ) = 0.0682, T = 120 K.
Open Access
The crystal structure of bis(2-oxidopyridin-1-ium-3-carboxylato-κ²O,O′)-(phenantroline-κ²N,N′)manganese(II) - methanol (1/3), C₂₇H₂₈N₄O₉Mn

September 29, 2021

Xiaoxia Men, Zhongyu Zhang, Xiaoli Li, Weiqin Sun

Page range: 1263-1265

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C 27 H 28 N 4 O 9 Mn, monoclinic, P 2 1 / n (no. 14), a = 10.0269(7) Å, b = 14.1702(10) Å, c = 20.0750(14) Å, β = 100.298(1)°, V = 2806.4(3) Å 3 , Z = 4, R gt ( F ) = 0.0403, wR ref ( F 2 ) = 0.0985, T = 296.15 K.
Open Access
Crystal structure of 4-(dimethylamino)pyridinium dibromido-tris(4-chlorophenyl-κC)stannate(IV), C₂₅H₂₃Br₂Cl₃N₂Sn

August 16, 2021

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 1267-1269

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C 25 H 23 Br 2 Cl 3 N 2 Sn, monoclinic, P 2 1 / c (no. 14), a = 10.9372(1) Å, b = 23.1045(1) Å, c = 11.1856(1) Å, β = 106.942(1)°, V = 2703.91(4) Å 3 , Z = 4, R gt ( F ) = 0.0167, wR ref ( F 2 ) = 0.0393, T = 100 K.
Open Access
Crystal structure of (3E,5E)-1-(4-cyanobenzenesulfonyl)-3,5-bis(3-fluorobenzylidene)piperidin-4-one-dichloromethane (1/1), C₂₇H₂₀Cl₂F₂N₂O₃S

September 10, 2021

Zhong-Fei Gao, Lei Wang, Gui-Ge Hou, Chun-Hua Wang

Page range: 1271-1274

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C 27 H 20 Cl 2 F 2 N 2 O 3 S, triclinic, P 1 ‾ $P‾{1}$ (no. 2), a = 8.7887(4) Å, b = 11.2517(6) Å, c = 13.7609(7) Å, α = 74.962(4)°, β = 81.084(4)°, γ = 71.259(4)°, V = 1240.68(11) Å 3 , Z = 2, R gt ( F ) = 0.0582, wR ref ( F 2 ) = 0.1543, T = 100.0(1) K.
Open Access
Crystal structure of (3E,5E)-3,5-bis(4-fluorobenzylidene)-1-((4-trifluoromethyl)benzenesulfonyl)piperidin-4-one, C₂₆H₁₈F₅NO₃S

September 2, 2021

Zhong-Fei Gao, Lei Wang, Gui-Ge Hou, Xiao-Fan Zhang

Page range: 1275-1278

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C 26 H 18 F 5 NO 3 S, triclinic, P 1 ‾ $P‾{1}$ (no. 2), a = 7.8831(4) Å, b = 11.9591(7) Å, c = 13.3258(7) Å, α = 69.072(5)°, β = 88.556(4)°, γ = 73.730(5)°, V = 1122.48(11) Å 3 , Z = 2, R gt ( F ) = 0.0507, wR ref ( F 2 ) = 0.1216, T = 100.0(1) K.
Open Access
Crystal structure of chlorido-(4-methyl-2-((phenylimino)methyl)phenolato-κ² N,O)-(pyridine-κ¹ N)platinum(II), C₁₉H₁₇ClN₂OPt

September 8, 2021

Arshad Khan, Rabia Usman, Moamen S. Refat, Abeer M. Alosaimi, Mohammed T. Alghamdi, Faiz-Ur Rahman

Page range: 1279-1281

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C 10 H 8 BrN 3 , orthorhombic, P 1 ‾ $P‾{1}$ (no. 2), a = 12.114(7) Å, b = 12.254(8) Å, c = 13.186(8) Å, α = 71.659(10)°, β = 84.744(10)°, γ = 89.725(10)°, V = 1850(2) Å 3 , Z = 4, R gt ( F ) = 0.0511, wR ref ( F 2 ) = 0.1644, T = 293 K.
Open Access
Crystal structure of (4-methylbenzyl)(triphenyl)phosphonium chloride dihydrate, C₂₆H₂₈ClO₂P

August 16, 2021

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 1283-1285

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C 26 H 28 ClO 2 P, monoclinic, P 2 1 / c (no. 14), a = 11.6061(2) Å, b = 19.7791(4) Å, c = 11.1982(3) Å, β = 116.278(3)°, V = 2304.98(10) Å 3 , Z = 4, R gt ( F ) = 0.0373, wR ref ( F 2 ) = 0.1034, T = 100 K.
Open Access
The crystal structure of poly[μ₂-chlorido-(μ₂-1,2-bis(4-pyridyl)ethane-κ²N:N′silver(I)], C₁₂H₁₂AgClN₂

September 2, 2021

Jianghua Fang, Minjie Hu, Ying Li, Weihong Xu

Page range: 1287-1289

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C 12 H 12 AgClN 2 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 9.007(2) Å, b = 9.493(2) Å, c = 13.642(3) Å, V = 1166.5(4) Å 3 , Z = 4, R gt ( F ) = 0.0160, wR ref ( F 2 ) = 0.0370, T = 295 K.
Open Access
Crystal structure of poly[(μ₄-benzene-1,2,4,5-tetracarboxylato)-bis(μ₂-adipohydrazide)dicadmium], C₁₁H₁₅N₄O₆Cd

September 8, 2021

Yuhong Long, Xiaoyu Hu, Jingwen Ran

Page range: 1291-1293

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C 11 H 15 CdN 4 O 6 , monoclinic, P 2 1 / n (no. 14), a = 11.1387(15) Å, b = 10.3933(14) Å, c = 12.2891(17) Å, β = 105.319(2)°, Z = 4, V = 1372.1(3) Å 3 , R gt ( F ) = 0.0286, wR ref ( F 2 ) = 0.0477, T = 296(2) K.
Open Access
The crystal structure of (E)-N′-(butan-2-ylidene)isonicotinohydrazide 0.5 hydrate C₁₀H₁₃N₃O·0.5H₂O

August 31, 2021

Itumeleng B. Setshedi, Andreas Lemmerer, Mark G. Smith

Page range: 1295-1296

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C 10 H 13 N 3 O·0.5H 2 O, orthorhombic, Aba2 (no. 41), a = 19.9676(19) Å, b = 8.4674(7) Å, c = 12.4082(10) Å, V = 2097.9(3) Å 3 , Z = 8, R gt ( F ) = 0.0299, wR ref ( F 2 ) = 0.0849, T = 173 K. CCDC no.: 2086756
Open Access
The crystal structure of bis(6-phenylpyridine-2-carboxylate-κ² N,O)-(2,2′-bipyridine-κ² N,N′)zinc(II) monohydrate, C₃₄H₂₆N₄O₅Zn

September 8, 2021

Li-Hua Wang, Zi-Jian Wang, Jian Ouyang, Xi-Shi Tai

Page range: 1297-1299

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C 34 H 26 N 4 O 5 Zn, monoclinic, C 2/ c (no. 15), a = 29.3891(18) Å, b = 10.3260(5) Å, c = 19.9101(11) Å, V = 5783.1(6) Å 3 , Z = 8, R gt ( F ) = 0.0334, wR ref ( F 2 ) = 0.0759, T = 199.99(10) K.
Open Access
The crystal structure of (1R ^*,2S ^*)-1,2-bis(2-fluorophenyl)-3,8-dimethoxyacenaphthene-1,2-diol, C₂₆H₂₀F₂O₄

September 6, 2021

Hiroaki Iitsuka, Kun Li, Miyuki Kobayashi, Kikuko Iida, Keiichi Noguchi, Noriyuki Yonezawa, Akiko Okamoto

Page range: 1301-1304

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C 26 H 20 F 2 O 4 , monoclinic, P 2 1 / n (no. 14), a = 10.3707(2) Å, b = 12.0232(2) Å, c = 15.7744(3) Å, β = 90.907(1)°, V = 1966.65(6) Å 3 , Z = 4, R gt ( F ) = 0.0371, wR ref ( F 2 ) = 0.1013, T = 193.15 K.
Open Access
Crystal structure of catena-poly[(μ₂-1-((2-ethyl-4-methyl-1H-imidazol-1-yl)methyl)-1H-benzotriazole-κ²N:N′)-(nitrato-κ²O,O′)silver (I)], C₁₃H₁₅Ag₁N₆O₃

September 16, 2021

Yan Chen

Page range: 1305-1307

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C 13 H 15 Ag 1 N 6 O 3 , monoclinic, P 2 1 / c (no. 14), a = 9.0684(6) Å, b = 21.5490(10) Å, c = 9.1728(7) Å, β = 118.101(10)°, Z = 4, V = 1581.2(2) Å 3 , R gt ( F ) = 0.0425, wR ref ( F 2 ) = 0.0877, T = 293(2) K.
Open Access
The crystal structure of [(phenantroline-κ² N,N′)-bis(6-phenylpyridine-2-carboxylate-κ² N,O)cobalt(II)]monohydrate, C₃₆H₂₆N₄O₅Co

September 9, 2021

Xi-Shi Tai, Zi-Jian Wang, Jian Ouyang, Yun-Fei Li, Wei Zhang, Wen-Lei Jia, Li-Hua Wang

Page range: 1309-1311

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C 36 H 26 N 4 O 5 Co, triclinic, P 2 1 2 1 2 1 (no. 19), a = 10.6380(5) Å, b = 10.6639(5) Å, c = 26.5443(15) Å, V = 3011.2(3) Å 3 , Z = 4, R gt ( F ) = 0.0330, wR ref ( F 2 ) = 0.0681, T = 200 K.
Open Access
Crystal structure of (1E)-N′-[(1E)-1-(4-chlorophenyl)ethylidene]-2-[1-(4-chlorophenyl)ethylidene]hydrazine-1-carbohydrazonamide, C₁₇H₁₇Cl₂N₅

September 22, 2021

Zeliha Atioğlu

Page range: 1313-1316

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C 17 H 17 Cl 2 N 5 , monoclinic, P 2 1 / c (no. 14), a = 14.603(2) Å, b = 24.059(4) Å, c = 10.1380(16) Å, β = 93.141(3) ∘ , V = 3556.4(10) Å 3 , Z = 8, R gt (F) = 0.0512, wR ref ( F 2 ) = 0.1416, T = 296(2) K.
Open Access
The crystal structure of (E)-2-((tert-butylimino)methyl)-4-chlorophenol, C₁₁H₁₄ClNO

September 23, 2021

Lin Yuan, Yuan-Da Li, Xu Fan, Zhong-Yan Li

Page range: 1317-1318

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C 11 H 14 ClNO, monoclinic, P 2 1 / c (no. 14), a = 9.072(3) Å, b = 5.882(2) Å, c = 21.258(7) Å, β = 100.351°, V = 1115.9(7) Å 3 , Z = 4, R gt ( F ) = 0.0391, w R ref ( F 2 ) = 0.1167, T = 296(2) K.
Open Access
Crystal structure of all-cis-2,4,6-trihydroxycyclohexane- 1,3,5-triaminium chloride sulfate, C₆H₁₈ClN₃O₇S

September 22, 2021

Vyara Velcheva, Kaspar Hegetschweiler, Galina Gencheva

Page range: 1319-1321

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C 6 H 18 ClN 3 O 7 S, trigonal, P 31 c (no. 159), a = 8.3990(14) Å, b = 8.3990(14) ∘ , c = 9.6208(17) Å, V = 587.76(17) Å 3 , Z = 2, R gt ( F ) = 0.0497, w R ref ( F 2 ) = 0.1404, T = 300.15 K.
Open Access
Crystal structure of dichlorido-bis(dimethyl sulfoxide-κO)bis(4-methylphenyl-κC ¹)tin(IV), C₁₈H₂₆Cl₂O₂S₂Sn

September 8, 2021

Kong Mun Lo, See Mun Lee, Edward R. T. Tiekink

Page range: 1323-1325

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C 18 H 26 Cl 2 O 2 S 2 Sn, monoclinic, P 2 1 / n (no. 14), a = 8.3295(1) Å, b = 10.5647(1) Å, c = 12.0078(1) Å, β = 96.612(1)°, V = 1049.642(18) Å 3 , Z = 2, R gt ( F ) = 0.0174, wR ref ( F 2 ) = 0.0455, T = 100 K.
Open Access
Crystal structure of dichlorido-bis(4-chlorophenyl-κC ¹)(2,2′-bipyridyl-κ ² N,N′)tin(IV), C₂₂H₁₆Cl₄N₂Sn

September 8, 2021

Kong Mun Lo, See Mun Lee, Edward R. T. Tiekink

Page range: 1327-1329

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C 22 H 16 Cl 4 N 2 Sn, monoclinic, P 2 1 / n (no. 14), a = 10.0393(1) Å, b = 14.4490(2) Å, c = 14.1502(2) Å, β = 92.846(1)°, V = 2050.07(5) Å 3 , Z = 4, R gt ( F ) = 0.0224, wR ref ( F 2 ) = 0.0590, T = 100 K.
Open Access
Redetermination of the crystal structure of (E)-5-bromo-2-hydroxybenzaldehyde oxime, C₇H₆BrNO₂

September 23, 2021

Lin Yuan, Hong‑Yu Zhu, Jin‑Hao Kuang, Zhong‑Yan Li

Page range: 1331-1332

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C 11 H 14 ClNO, monoclinic, P 2 1 / c (no. 14), a = 14.48(2) Å, b = 3.956(6) Å, c = 13.765(19) Å, β = 99.266(15) ∘ , V = 778.4(19) Å 3 , Z = 4, R gt ( F ) = 0.0236, wR ref ( F 2 ) = 0.0584, T = 296(2) K.
Open Access
The crystal structure of (E)-amino(2-(4-methylbenzylidene)hydrazineyl)methaniminium 4-methylbenzoate, C₉H₁₃N₄ ⁺C₈H₇O₂ ⁻

September 22, 2021

Zeliha Atioğlu, Hüseyin Kekeçmuhammed

Page range: 1333-1335

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Monoclinic, P 2 1 / c (no. 14), a = 14.187(15) Å, b = 10.585(11) Å, c = 11.952(13) Å, β = 113.851(16) ∘ , V = 1642(3) Å 3 , Z = 4, R gt ( F ) = 0.0479, w R ref ( F 2 ) = 0.1408, T = 296(2) K.
Open Access
Crystal structure of 2-chloro-3-(isopentylamino)naphthalene-1,4-dione, C₁₅H₁₆ClNO₂

September 29, 2021

Zu-Shuai Deng, Peng Luo, Wei-Gao Pan

Page range: 1337-1339

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C 15 H 16 ClNO 2 , triclinic, P 1 ‾ $‾{1}$ (no. 2), a = 7.4339(12) Å, b = 8.2564(14) Å, c = 12.184(2) Å, α = 108.804(6) ∘ , β = 93.672(5) ∘ , γ = 94.373(6) ∘ , V = 702.8(2) Å 3 , Z = 2, R gt ( F ) = 0.0650, w R ref ( F 2 ) = 0.1974, T = 273 K.
Open Access
The crystal structure of bis(2-acetyl-5-methoxyphenyl)carbonate 1.5 hydrate, C₁₉H₁₈O₇

September 29, 2021

Juan Liu, Sai Chen, Honglei Li

Page range: 1341-1343

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C 19 H 18 O 7 , orthorhombic, P 2 1 2 1 2 (no. 18), a = 12.467(3) Å, b = 39.168(8) Å, c = 7.6005(16) Å, V = 3711.4(14) Å 3 , Z = 4, R gt ( F ) = 0.0440, wR ref ( F 2 ) = 0.1054, T = 296.15 K.
Open Access
The crystal structure of poly[(μ ₄-4,4′-(azanediylbis(methylene))dibenzoato-κ ⁴ O:N:O′:Oʺ)zinc(II)], C₁₆H₁₃NO₄Zn

September 23, 2021

Hai-Lin Chen, Dong-Mei Yao, Yan-Ping Wang, Ya-Xin Lao

Page range: 1345-1346

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C 16 H 13 NO 4 Zn, triclinic, P 1 ‾ $‾{1}$ (no. 2), a = 7.5223(6) Å, b = 8.0977(8) Å, c = 11.7739(11) Å, α = 76.410(8) ∘ , β = 75.495(8) ∘ , γ = 75.902(8) ∘ , V = 661.76(11) Å 3 , Z = 2, R gt ( F ) = 0.0532, w R ref ( F 2 ) = 0.1041, T = 293(2) K.
Open Access
The crystal structure of catena-poly[(1,10-phenanthroline-k²N,N′)-(μ₃-tetraoxidomoybdato(VI)-k³O:O′:O″)manganese(II)] C₁₂H₈N₂O₄MoMn

October 28, 2021

Qiu Ze-Hai, Zhang Zhu-Sen, Chen Wu-Hua

Page range: 1347-1349

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C 12 H 8 N 2 O 4 MoMn, monoclinic, P 2 1 / m (no. 11), a = 8.9812(5) Å, b = 6.5212(3) Å, c = 10.6167(6) Å, β = 100.120(6)°, V = 612.13(6) Å 3 , Z = 2, R gt ( F ) = 0.0391, wR ref ( F 2 ) = 0.0783, T = 293(2) K.
Open Access
Crystal structure of catena-poly[(4-hydroxyl-5-(methoylcarbonyl)thiophene-2-carboxylato-κ¹ O)-(μ₂-piperazine-1,4-diylbis(pyridin-4-ylmethanone)-κ² N:N′)silver(I)] monohydrate, C₂₃H₂₃AgN₄O₈S

September 22, 2021

Zhao-Hao Li, Gui-Xian Xie, Chen-Yang Li, Xiao-Ru Dou

Page range: 1351-1353

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C 23 H 23 AgN 4 O 8 S, monoclinic, P 2 1 / n (no. 14), a = 8.5356(4) Å, b = 27.9494(15) Å, c = 10.3796(6) Å, V = 2474.1(2) Å 3 , Z = 4, R gt ( F ) = 0.0347, w R ref ( F 2 ) = 0.0744, T = 289 K.
Open Access
Crystal structure of bis(4-bromo-2-(((3-bromopropyl)imino)methyl)phenolato-κ²N,O)-oxido-vanadium(IV), C₂₀H₂₀Br₄N₂O₃V

September 29, 2021

Wei Wei, Juan Xia, Wei-Ya Zhang, Heng-Qiang Zhang, Fu-Jian Fang, Yang Xin, Xiu-Jun Zheng

Page range: 1355-1357

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C 20 H 20 Br 4 N 2 O 3 V, monoclinic, P 2 1 / c (no. 14), a = 12.6011(10) Å, b = 16.5997(8) Å, c = 12.9206(12) Å, β = 119.006(11)°, V = 2363.7(4) Å 3 , Z = 4, R gt ( F ) = 0.0518, wR ref ( F 2 ) = 0.1062, T = 153(2) K.
Open Access
The crystal structure of (2a′S,2a1′S,3R,5a′S,7′R)-5-(furan-3-yl)-2a′,2a1′-dihydroxy-7′-methyldecahydro-2H-spiro[furan-3,6′-naphtho[1,8-bc]furan]-2,2′(2a′H)-dione, C₁₉H₂₂O₇

October 18, 2021

Xin-Ke Xu, Can-Jie Li, Jin-Lin Tan, Hai-Yue Zhao, Qiang Lin, Yao-Lan Li, Yu-Bo Zhang, Guo-Cai Wang

Page range: 1359-1361

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C 19 H 22 O 7 , orthorhombic, P 2 1 (no. 4), a = 6.4154(1) Å, b = 7.8782(2) Å, c = 17.1555(4) Å, β = 91.021(2)°, V = 866.93(3) Å 3 , Z = 2, R gt ( F ) = 0.0326, wR ref ( F 2 ) = 0.1028, T = 150 K.
Open Access
The crystal structure of 3-bromopicolinic acid, C₆H₄BrNO₂

October 14, 2021

Guang Huang

Page range: 1363-1365

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C 6 H 4 BrNO 2 , orthorhombic, Pna 2 1 (no. 33), a = 14.3975(12) Å, b = 7.5773(7) Å, c = 12.2500(10) Å, β = 90°, V = 1336.4(2) Å 3 , Z = 8, R gt ( F ) = 0.0281, wR ref ( F 2 ) = 0.0536, T = 150(2) K.
Open Access
Crystal structure of 1,1′-(1,4-phenylenebis(methylene))bis(pyridin-1-ium) bis(1,2-dicyanoethene-1,2-dithiolato-κ² S,S) platinum(II), C₂₆H₁₈N₆PtS₄

October 27, 2021

Wei-Hong Yan, Xian-Cai Zeng

Page range: 1367-1369

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C 26 H 18 N 6 PtS 4 , triclinic, P 1 ‾ $P‾{1}$ (no. 2), a = 8.2661(5) Å, b = 9.1519(6) Å, c = 9.4673(6) Å, α = 70.473(1)°, β = 80.770(1)°, γ = 83.340(1)°, V = 664.77(7) Å 3 , Z = 1, R gt ( F ) = 0.0477, wR ref ( F 2 ) = 0.1168, T = 296(2) K.
Open Access
Synthesis and crystal structure of 5-(8-((3-carboxyazetidin-1-ium-1-yl)methyl)-7-hydroxy-4-oxo-4H-chromen-3-yl)-2-hydroxybenzenesulfonate monohydrate, C₂₀H₁₉NO₁₀S

October 15, 2021

Hai-Lin Chen, Xiu‑Xiang Huang, Dong‑Mei Yao, Yan‑Ping Wang, Xiao‑Bing Lu

Page range: 1371-1373

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C 20 H 19 NO 10 S, triclinic, P 1 ‾ $P‾{1}$ (no. 2), a = 8.3470(2) Å, b = 9.6701(2) Å, c = 12.9523(3) Å, α = 102.413(2)°, β = 103.199(2)°, γ = 97.753(2)°, V = 975.26(4) Å 3 , Z = 2, R gt ( F ) = 0.0439, wR ref ( F 2 ) = 0.1244, T = 100(1) K.
Open Access
The crystal structure of 3-amino-5-carboxypyridin-1-ium bromide, C₆H₇BrN₂O₂

October 18, 2021

Chao-Jun Du, De-Long Niu, Zhen-Li Yan, Shi-Li Zheng, Yan Zeng

Page range: 1375-1376

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C 6 H 7 BrN 2 O 2 , triclinic, P 1 ‾ $P‾{1}$ (no. 2), a = 7.3026(4) Å, b = 7.4618(4) Å, c = 7.8746(4) Å, α = 81.542(3)°, β = 89.459(3)°, γ = 61.718(3)°, V = 372.86(4) Å 3 , Z = 2, R gt ( F ) = 0.0209, wR ref ( F 2 ) = 0.0473, T = 150(2) K.
Open Access
The crystal structure of (2-hydroxy-5-methyl-phenyl)-(1H-pyrazol-4-yl)-methanone hemihydrate, C₁₁H_10.5N₂O_2.5

October 18, 2021

Li-Hua Wang, Xi-Shi Tai

Page range: 1377-1378

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C 11 H 10.5 N 2 O 2.5 , monoclinic, P 2 1 / c (no. 14), a = 4.9681(4) Å, b = 32.634(4) Å, c = 6.2373(10) Å, β = 96.244(10)°, V = 1005.3(2) Å 3 , Z = 4, R gt ( F ) = 0.0595, wR ref ( F 2 ) = 0.1112, T = 293(2) K.
Open Access
Crystal structure of tetraaqua-(2-(4-formylphenoxy)acetato-k¹O)cadmium(II), C₁₈H₂₂O₁₂Cd

October 20, 2021

Xi-Shi Tai, Li-Hua Wang

Page range: 1379-1380

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C 18 H 22 O 12 Cd, monoclinic, P 2 1 / c (no. 14), a = 13.3069(9) Å, b = 9.9041(6) Å, c = 8.1580(5) Å, β = 96.244(10)°, V = 1031.57(12) Å 3 , Z = 2, R gt ( F ) = 0.0216, wR ref ( F 2 ) = 0.0522, T = 200 K.
Open Access
Crystal structure of diethyl 6,12-dimethyl-3,9-di-p-tolyl-3,9-diazapentacyclo[6.4.0.0^2,7.0^4,11.0^5,10]dodecane-1,5-dicarboxylate, C₃₂H₃₈N₂O₄

October 22, 2021

Shuai Yang, Jin-Ling Dong, Jin-Ming Chen

Page range: 1381-1382

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C 15 H 14 N 2 O, triclinic, P 1 ‾ $P‾{1}$ (no. 2), a = 6.983(5) Å, b = 8.472(6) Å, c = 12.113(7) Å, β = 73.45°, V = 679.29(8) Å 3 , Z = 1, R gt ( F ) = 0.0566, wR ref ( F 2 ) = 0.1875, T = 296 K.
Open Access
Crystal structure of (E)-N′-(1-(3-chloro-4-fluorophenyl)ethylidene)-4-hydroxy – tetrahydrofuran (2/1), C₁₇H₁₆ClFN₂O_2.5

October 27, 2021

Xiaobo Bao, Chongchong Tian

Page range: 1383-1384

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C 17 H 16 ClFN 2 O 2.5 , monoclinic, P 2 1 / n (no. 14), a = 7.4495(6) Å, b = 16.5328(13) Å, c = 12.8519(10) Å, β = 91.329(1)°, V = 1582.4(2) Å 3 , Z = 4, R gt ( F ) = 0.0508, wR ref ( F 2 ) = 0.1461, T = 100(2) K.

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