Zeitschrift für Kristallographie - New Crystal Structures

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Zeitschrift für Kristallographie - New Crystal Structures

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Zeitschrift für Kristallographie - New Crystal Structures

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Frontmatter

28. April 2023

Seiten: i-vi

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New Crystal Structures
Open Access
Crystal structure of phenyl(3,3-dichloro-1,3-dihydro-2H-pyrrolo[2,3-b]pyridin-2-one)methanone, C₇H₄Cl₂N₂O

29. März 2023

Su-Fen Bai, Shan-Shan Li, Jia-Xuan Liu, Chun-Yu Tian, Xiao-Long Li, Xiao-Jin La

Seiten: 411-412

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C 7 H 4 Cl 2 N 2 O, monoclinic, P 2 1 / c (no. 14), a = 6.215(2) Å, b = 16.544(5) Å, c = 8.561(3) Å, β = 108.707(4)°, V = 833.8(5) Å 3 , Z = 4, R gt ( F ) = 0.0339, wR ref ( F 2 ) = 0.1265, T = 296 K.
Open Access
Crystal structure of poly[diaqua-bis(μ ₂-1,4-diaminobutane-N:N′)cobalt(II)] dichloride, C₈H₂₈Cl₂CoN₄O₂

24. Februar 2023

Shin Jiehye, Kang Jaeun, Junghwan Do

Seiten: 413-415

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C 8 H 28 Cl 2 CoN 4 O 2 , orthorhombic, Fddd (no. 70), a = 10.116(2) Å, b = 13.532(3) Å, c = 23.507(5) Å, V = 3217.8(11) Å 3 , Z = 8, R gt ( F ) = 0.0361, wR ref ( F 2 ) = 0.1069, T = 100.5 K.
Open Access
Synthesis and crystal structure of (4aR,7S)-7-hydroxy-7-isopropyl-1,1-dimethyldecahydro-2H,6H-8a,4a-(epoxymethano)phenanthren-12-one, C₂₀H₃₂O₃

24. Februar 2023

Ren-Song Chen, Jing-Jie Zhang, Yi Zhang, Chuan-Yan Xu, Jiang-Hai Ye

Seiten: 417-419

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C 20 H 32 O 3 , monoclinic, P 2 1 (no. 4), a = 7.8981(17) Å, b = 10.302(2) Å, c = 11.028(3) Å, β = 90.020(2)°, V = 897.3(3) Å 3 , Z = 2, R gt ( F ) = 0.0603, wR ref ( F 2 ) = 0.1342, T = 273(2) K.
Open Access
The crystal structure of 1-(2-chlorobenzyl)-3-(3,5-dichlorophenyl)urea, C₁₄H₁₁Cl₃N₂O

24. Februar 2023

Yingju Li, Zhimao Yang

Seiten: 421-423

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C 14 H 11 Cl 3 N 2 O, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 8.3600(4) Å, b = 12.0085(8) Å, c = 14.3665(6) Å, V = 1442.27(13) Å 3 , Z = 4, R gt ( F ) = 0.0460, w R ref ( F 2 ) = 0.0944, T = 293 K.
Open Access
Crystal structure of tetrapropylammonium-1,3,5-thiadiazole-5-amido-2-carbamate – 1,2,4-thiadiazole-3,5-diamine – water (1/1/1), C₁₇H₃₇N₉O₃S₂

6. März 2023

Huawei Tang, Qianqian Han, Lijuan Liu

Seiten: 425-427

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C 17 H 37 N 9 O 3 S 2 , monoclinic, P 2 1 / c (no. 14), a = 8.8492(13) Å, b = 17.285(3) Å, c = 16.810(3) Å, β = 93.493(2)°, V = 2566.4(7) Å 3 , Z = 4, R gt ( F ) = 0.0395, wR ref ( F 2 ) = 0.1277, T = 296(2) K.
Open Access
Tetrabutylammonium 1,3,5-thiadiazole-5-amido-2-carbamate—1,2,4-thiadiazole-3,5-diamine— water (1/1/1), C₂₁H₄₅N₉O₃S₂

6. März 2023

Huawei Tang, Qianqian Han, Lijuan Liu

Seiten: 429-431

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C 21 H 45 N 9 O 3 S 2 , orthorhombic, Pbca (no. 61), a = 9.5299(6) Å, b = 16.5181(9) Å, c = 36.886(2) Å, β = 90°, V = 5806.4(6) Å 3 , Z = 8, R gt ( F ) = 0.0568, wR ref ( F 2 ) = 0.1420, T = 296(2) K.
Open Access
The crystal structure of ((E)-2,4-dichloro-6-(((2-hydroxy-5-nitrophenyl)imino)methyl)phenolato-κ ³ N,O,O′)tris(pyridine-κN)manganese(II), C₂₈H₂₁Cl₂MnN₅O₄

22. Februar 2023

Ting Li, Xiyuan Xiao, Yuxing Tan, Weiwei Fu

Seiten: 433-435

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C 28 H 21 Cl 2 MnN 5 O 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.9699(9) Å, b = 9.1185(9) Å, c = 17.6902(17) Å, α = 103.776(1)°, β = 92.407(1)°, γ = 99.761(1)°, V = 1379.8(2) Å 3 , Z = 2, R gt ( F ) = 0.0388, wR ref ( F 2 ) = 0.0920, T = 296 K.
Open Access
The crystal structure of aqua-bis{2-bromo-6-((2-(2-phenylacetyl)hydrazineylidene)methyl)phenolato-κ³ N,O,O′}-dimethylformamide-κ¹ O-erbium(III) chloride – dimethylformamide – water (1/2/1), C₃₉H₄₉N₇O₉Br₂ClEr

22. Februar 2023

Li-Hua Wang, Hao-Wen Tai, Gui-Quan Song, Xi-Shi Tai

Seiten: 437-439

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C 39 H 49 N 7 O 9 Br 2 ClEr, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 12.3164(9) Å, b = 12.7581(9) Å, c = 14.5023(11) Å, α = 70.873(2)°, β = 80.281(2)°, γ = 65.810(2)°, V = 1962.4(3) Å 3 , Z = 1, R gt ( F ) = 0.0383, wR ref ( F 2 ) = 0.0765, T = 296.15 K.
Open Access
Crystal structure of (diaqua-bis(phenanthroline-K ² N,N′)-tetrakis(m ₂-3,4,5,6-tetrafluorophthalato-K ⁴ O,O:O′:O″;K ² O:O′)dierbium (III) phenanthroline (1/2), C₈₀H₃₈Er₂F₁₆N₈O₁₈

27. März 2023

Jun-Ya Song, Xiao-Yu Zhang, Chun-Li Zhang, Bei-Bei Zhao, Shi-Jie Huang, Xinfang Liu

Seiten: 441-443

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C 80 H 38 Er 2 F 16 N 8 O 18 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 11.4228(4) Å, b = 12.6712(3) Å, c = 13.2663(4) Å, α = 102.660(2)°, β = 98.047(3)°, γ = 105.509(3)°, V = 1764.54(10) Å 3 , Z = 1, R gt ( F ) = 0.0311, wR ref ( F 2 ) = 0.0668, T = 293(2) K.
Open Access
Crystal structure of (E)-7-methoxy-2-(4-methoxy-2-(trifluoromethyl)benzylidene)-3,4-dihydronaphthalen-1(2H)-one, C₂₀H₁₇F₃O₃

22. Februar 2023

Shuai Lai, Yun Hou, Feng-Lan Zhao, Qing-Guo Meng

Seiten: 445-447

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C 20 H 17 F 3 O 3 , monoclinic, P 2 1 / c (no. 14), a = 9.0684(4) Å, b = 13.1942(6) Å, c = 13.7883(7) Å, β = 96.250(5)°, V = 1639.97(13) Å 3 , Z = 4, R gt ( F ) = 0.0415, wR ref ( F 2 ) = 0.1125, T = 100 K.
Open Access
The crystal structure of 4–(4,4,5,5–tetramethyl–1,3,2–dioxaborolan–2–yl)morpholine, C₁₀H₂₀BNO₃

22. Februar 2023

Marcus Herbig, Uwe Böhme

Seiten: 449-450

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C 10 H 20 BNO 3 , monoclinic, P 2 1 / c (no. 14), a = 11.0681(8) Å, b = 6.1883(3) Å, c = 18.1603(13) Å, β = 105.111(6)°, V = 1200.84(14) Å 3 , Z = 4, R gt ( F ) = 0.0338, wR ref ( F 2 ) = 0.0861, T = 153 K.
Open Access
The crystal structure of catena–poly[aqua(1-naphthoato-κ ² O,O′)-(μ-1-naphthoato-κ ⁴ O:O,O′:O′)lead(II)], C₂₂H₁₆O₅Pb

22. Februar 2023

Jiahong Li, Zheyu Deng, Biao Li, Jiaqi Ou, Xiaoming Zhu

Seiten: 451-453

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C 22 H 16 O 5 Pb, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 7.3395(8) Å, b = 10.7768(11) Å, c = 23.034(3) Å, V = 1821.9(3) Å 3 , Z = 4, R gt ( F ) = 0.0327, w R ref ( F 2 ) = 0.0735, T = 296(2) K.
Open Access
The crystal structure of 1-(4-chlorophenyl)-3-cycloheptylurea, C₁₄H₁₉ClN₂O

28. Februar 2023

Qianqian Tang, Hanqi Dai, Guangfu Zhou, Yuanjiang Wu, Wei Wang, Yang Zhao

Seiten: 455-457

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C 14 H 19 ClN 2 O, monoclinic, P 2 1 / c (no. 14), a = 12.8823(9) Å, b = 9.1617(6) Å, c = 11.7421(9) Å, β = 98.377(7)°, V = 1371.06(17) Å 3 , Z = 4, R gt (F) = 0.0678, wR ref (F 2 ) = 0.1912, T = 293 K.
Open Access
The crystal structure of 4-(pyren-1-yl)butyl-4-nitrobenzoate, C₂₇H₂₁NO₄

28. Februar 2023

Claudio Barrientos, Juan Arturo Squella, Silvana Moris

Seiten: 459-461

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C 27 H 21 NO 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 7.3476(2) Å, b = 7.4894(2) Å, c = 20.5137(5) Å, α = 89.33000(10)°, β = 79.7070(10)°, γ = 67.5220(10)°, V = 1024.31(5) Å 3 , Z = 2, R gt ( F ) = 0.0536, w R ref ( F 2 ) = 0.1792, T = 296.15 K.
Open Access
Crystal structure of cyclo-(bis(µ₂-3,3′-(1H-imidazole-3-ium-1,3-diyl)dipropionato-κ⁴ O,O′:O″,O″′)-dinitrato-κ² O,O′-tetraoxido-diuranium(VI) C₁₈H₂₂N₆O₁₈U₂

20. Februar 2023

Yuning Meng, Bin Cai

Seiten: 463-464

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C 18 H 22 N 6 O 18 U 2 , monoclinic, P 2/ c (no. 13), a = 10.894(2) Å, b = 7.9674(16) Å, c = 16.787(3) Å, β = 100.823(2)°, V = 1399.1(5) Å 3 , Z = 2, R gt ( F ) = 0.0307, w R ref ( F 2 ) = 0.0728, T = 296(2) K.
Open Access
The crystal structure of catena-[nitrato-κ ² O,O′-(μ ₃-3-iodobenzene-1,2-dicarboxylato-κ ⁴ O:O′:O″,O‴)-(2,2′:6′,2″-terpyridine-κ ³ N,N′,N″)lanthanum(III)], C₂₃H₁₄IN₄O₇La

16. März 2023

Bin Cai, Yuning Meng

Seiten: 465-466

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C 23 H 14 IN 4 O 7 La, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.2438(3) Å, b = 12.3786(5) Å, c = 12.6230(5) Å, α = 111.802(1)°, β = 91.144(1)°, γ = 100.6470(10)°, V = 1169.86(8) Å 3 , Z = 2, R gt ( F ) = 0.0313, w R ref ( F 2 ) = 0.1051, T = 296 K.
Open Access
Redetermination of crystal structure of [bis(pyridin-2-ylmethyl)amine-κ ³ N,Nʹ,Nʺ]chloridopalladium(II) chloride monohydrate

20. Februar 2023

Kwang Ha

Seiten: 467-469

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C 12 H 13 Cl 2 N 3 Pd·H 2 O, triclinic, P 1̄ (no. 2), a = 7.0698(4) Å, b = 8.5546(6) Å, c = 12.8539(9) Å, α = 106.541(2)°, β = 102.510(2)°, γ = 91.572(2)°, V = 724.23(8) Å 3 , Z = 2, R gt ( F ) = 0.0199, wR ref ( F 2 ) = 0.0438, T = 223 K.
Open Access
Crystal structure of catena-poly[triaqua-[bis(m₂-4-(1H-1,2,4-triazol-1-yl)benzoato-k²O:O')-(4-(1H-1,2,4-triazol-1-yl)benzoato-k¹O)-praseodymium (III) monohydrate], C₂₇H₂₆N₉O₁₀Pr

30. März 2023

Li Liu, Huan-Mei Guo, Li-Li Liu, Xin-Ru Qian

Seiten: 471-473

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C 27 H 26 N 9 O 10 Pr, monoclinic, P 2 1 / c , a = 13.2280(12) Å, b = 5.5628(5) Å, c = 41.140(3) Å, β = 105.109(2)°, V = 2922.6(4) Å 3 , Z = 4, R gt ( F ) = 0.0426, w R ref ( F 2 ) = 0.0803, T = 298.15 K.
Open Access
Crystal structure of trans-diaqua-bis(methyl methylcarbamohydrazonothioato-κ² N,N′) nickel(II) iodide semihydrate, C₆H₂₂N₆O₂NiS₂I₂·0.5H₂O

14. März 2023

Svetlana Belošević, Vukadin M. Leovac, Mirjana M. Radanović, Milica G. Bogdanović, Nikola D. Radnović, Marko V. Rodić

Seiten: 475-477

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C 6 H 23 I 2 N 6 NiO 2.50 S 2 , monoclinic, C 2/ c (no. 15), a = 8.2282(4) Å, b = 21.9200(7) Å, c = 11.4906(4) Å, β = 109.451(4)°, V = 1954.19(14) Å 3 , Z = 4, R gt ( F ) = 0.0322, wR ref ( F 2 ) = 0.1113, T = 295.
Open Access
The crystal structure of 2-(2-fluoro-4-methyl-5-((2,2,2-trifluoroethyl)thio)phenyl)isoindolin-1-one, C₁₇H₁₃F₄NOS

1. März 2023

Jing Zhang, Lixin Zhang

Seiten: 479-481

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C 17 H 13 F 4 NOS, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 6.1249(7) Å, b = 9.9306(10) Å, c = 13.1754(13) Å, α = 83.116(8)°, β = 80.305(9)°, γ = 73.204(9)°, V = 754.08 Å 3 , Z = 2, R gt ( F ) = 0.0460, wR ref ( F 2 ) = 0.1078, T = 150 K.
Open Access
The crystal structure of di-μ-1-naphthylacetato-κ ³ O,O′:O;κ ³ O:O,O′-bis[(1-naphthylacetato-κ ² O,O′)(2,2′-bipyridine-κ ² N,N′)lead(II)] monohydrate, C₆₈H₅₄N₄O₉Pb₂

28. März 2023

Zheyu Deng, Jiahong Li, Xinbo Hou, Na Luo, Xiaoming Zhu

Seiten: 483-485

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C 68 H 54 N 4 O 9 P b 2 ${\mathrm{C}}_{68}{\mathrm{H}}_{54}{\mathrm{N}}_{4}{\mathrm{O}}_{9}{\mathrm{P}\mathrm{b}}_{2}$ , monoclinic, C 2/ c (no. 15), a = 15.7286(14) Å, b = 16.3623(14) Å, c = 22.500(2) Å, β = 97.369 ( 1 ) ° $97.369(1){}^{\circ}$ , V = 5742.7(9) Å 3 ${\mathrm{\mathring{\text{A}}}}^{3}$ , Z = 4, R g t ${R}_{gt}$ ( F ) = 0.0203, w R r e f ${R}_{ref}$ ( F 2 ${F}^{2}$ ) = 0.0488, T = 296(2) K.
Open Access
Crystal structure of tetrapropylammonium guanidinium 4,4′-sulfonyldibenzoate monohydrate, C₂₇H₄₄N₄O₇S

28. März 2023

Na Lin, Ruiqin Sun, Xiaofang Li

Seiten: 487-489

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C 27 H 44 N 4 O 7 S, monoclinic, P 2 1 / n (no. 14), a = 10.216(3) Å, b = 18.133(5) Å, c = 17.036(5) Å, β = 98.371(3)°, V = 3122.2(16) Å 3 , Z = 4, R gt ( F ) = 0.0435, wR ref ( F 2 ) = 0.1333, T = 296(2) K.
Open Access
Crystal structure of bis(tetrapropylammonium) terephthalate – 1-(diaminomethylene)thiourea – water (1/2/4) C₁₈H₄₀N₅O₄S

23. März 2023

Mengfei Li, Fangfang Geng, Honglei Zhu

Seiten: 491-493

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C 18 H 40 N 5 O 4 S, monoclinic, P 2 1 / n (no. 14), a = 8.4254(9) Å, b = 8.4254(9) Å, c = 16.1470(17) Å, β = 98.302(2)°, V = 2411.9(4) Å 3 , Z = 4, R gt ( F ) = 0.0409, w R ref ( F 2 ) = 0.1162, T = 296(2) K.
Open Access
Crystal structure of (E)-7-fluoro-2-(4-morpholinobenzylidene)-3,4-dihydronaphthalen-1(2H)-one, C₂₁H₂₀FNO₂

14. März 2023

Han-Lin Luo, Wen-Xuan Li, Xian-Yong Bai, Qing-Guo Meng, Yun Hou

Seiten: 495-497

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C 21 H 20 F N O 2 ${\mathrm{C}}_{21}{\mathrm{H}}_{20}\mathrm{F}\mathrm{N}{\mathrm{O}}_{2}$ , triclinic, P 1̄ (no. 2), a = 9.2201(7) Å, b = 9.3195(8) Å, c = 11.4012(9) Å, α = 103.880 ( 7 ) ° $103.880(7){}^{\circ}$ , β = 100.987 ( 7 ) ° $100.987(7){}^{\circ}$ , γ = 115.090 ( 7 ) ° $115.090(7){}^{\circ}$ , V = 1796.31(20) Å 3 ${\mathrm{\mathring{\text{A}}}}^{3}$ , Z = 2, R g t ${R}_{gt}$ (F) = 0.0421, w R r e f $w{R}_{ref}$ ( F 2 ${\mathrm{F}}^{2}$ ) = 0.1136, T = 293 K.
Open Access
The crystal structure of poly[diaqua-bis(μ ₃-5-bromobenzene-1,3-dicarboxylato-κ ³ O,O,O′)-(μ ₂-1,3-bis-(4-pyridyl)-propane-κ ² N,N′)-dizinc(II))] – 5-bromobenzene-1,3-dicarboxylic acid [2/1], C₃₇H₂₉Br₃N₂O₁₄Zn₂

30. März 2023

Xiao-Ming Shi, Yu-Jia Fu

Seiten: 499-501

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C 37 H 29 Br 3 N 2 O 14 Zn 2 , monoclinic, P 2 1 / m (no. 11), a = 8.2047(6) Å, b = 28.6129(13) Å, c = 8.8721(7) Å, β = 112.069(9)°, V = 1930.2(3) Å 3 , Z = 2, R gt ( F ) = 0.0588, w R ref ( F 2 ) = 0.1547, T = 200 K.
Open Access
The crystal structure of 2-bromo-1,3-phenylene bis(4-methylbenzenesulfonate), C₂₀H₁₇BrO₆S₂

6. März 2023

Jue-Yuan Chen, Long-Sheng Zou, Ni Lai, Zi-Yi Yin, Lin Yuan, Zhong-Yan Li

Seiten: 503-505

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C 20 H 17 BrO 6 S 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.173(2) Å, b = 8.256(2) Å, c = 16.514(5) Å, α = 89.947(3)°, β = 83.105(3)°, γ = 72.077(3)°, V = 1051.8(5) Å 3 , Z = 2, R gt ( F ) = 0.0334, w R ref ( F 2 ) = 0.0889, T = 296(2) K.
Open Access
Crystal structure of europium dichromium icosaaluminum, EuCr₂Al₂₀

8. März 2023

Aylin Koldemir, Steffen Klenner, Rainer Pöttgen

Seiten: 507-509

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EuCr 2 Al 20 , cubic, F d 3 ‾ m $Fd\overline{3}m$ (no. 227), a = 14.5245(7) Å, V = 3064.1(3) Å 3 , Z = 8, R gt ( F ) = 0.0351, wR ref ( F 2 ) = 0.0402, T = 293 K.
Open Access
The crystal structure of N′¹,N′³-di((E)-benzylidene) isophthalohydrazide dihydrate, C ₂₂ H ₂₂ N ₄ O ₄

20. März 2023

Ni Lai, Sheng-Ting Zhang, Fei Zou, Lin Yuan, Zhong-Yan Li

Seiten: 511-512

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C 22 H 22 N 4 O 4 ${\mathrm{C}}_{22}{\mathrm{H}}_{22}{\mathrm{N}}_{4}{\mathrm{O}}_{4}$ , monoclinic, C 2/ c (no. 15), a = 34.315(13) Å, b = 6.701(3) Å, c = 9.105(3) Å, β = 98.510 ( 4 ) ° $98.510(4){}^{\circ}$ , V = 2070.7(13) Å 3 ${\mathrm{\mathring{\text{A}}}}^{3}$ , Z = 4, R g t ${R}_{gt}$ ( F ) = 0.0461, w R r e f $w{R}_{ref}$ ( F 2 ${F}^{2}$ ) = 0.1413, T = 296(2) K.
Open Access
Crystal structure of 7α,11α-dihydroxy-15-oxo-ent-kauran-16-en-19,6β-olide, C₂₀H₂₆O₅

23. März 2023

Lu Zhang, Hang Yuan, Jiang-Hai Ye, Kang He, Chun-Hua Lai, Juan Zou

Seiten: 513-515

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C 20 H 26 O 5 , monoclinic, P 2 1 2 1 2 1 (no. 19), a = 7.5455(15) Å, b = 12.735(3) Å, c = 18.333(4) Å, V = 1761.6(6) Å 3 , Z = 4, R g t ${R}_{gt}$ ( F ) = 0.0529, w R r e f $w{R}_{ref}$ ( F 2 ) = 0.1407, T = 273(2) K.
Open Access
Crystal structure of 4-chloro-N′-[(1E)-pyridin-3-ylmethylidene]benzohydrazide, C₁₃H₁₀ClN₃O

8. März 2023

Lamya H. Al-Wahaibi, Olivier Blacque, Edward R. T. Tiekink, Ali A. El-Emam

Seiten: 517-520

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C 13 H 10 ClN 3 O, monoclinic, P 2 1 / c (no. 14), a = 19.0933(2) Å, b = 23.0910(3) Å, c = 10.6831(2) Å, β = 90.064(1)°, V = 4710.00(12) Å 3 , Z = 16, R gt ( F ) = 0.0411, wR ref ( F 2 ) = 0.1081, T = 160 K.
Open Access
The crystal structure of (Z)-3-(1-(2-((E)-4-isopropylbenzylidene)hydrazinyl)ethylidene) chroman-2,4-dione, C₂₁H₂₀N₂O₃

13. April 2023

Vidoslav S. Dekić, Biljana R. Dekić, Dragana M. Sejmanović, Suzana Janićević, Biljana Krüger, Volker Kahlenberg, Marko V. Rodić

Seiten: 521-524

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C 21 H 20 N 2 O 3 , monoclinic, P 2 1 / c (no. 14), a = 6.8892(3) Å, b = 21.8269(13) Å, c = 35.1144(19) Å, β = 90.344(5)°, V = 5280.1(5) Å 3 , Z = 12, R gt ( F ) = 0.0672, wR ref ( F 2 ) = 0.1460, T = 170(2) K.
Open Access
Crystal structure of E-7-fluoro-2-(2-(trifluoromethyl)benzylidene)-3,4-dihydronaphthalen-1(2H)-one, C₁₈H₁₂F₄O

23. März 2023

Juan Zhang, Yun Hou, Feng-Lan Zhao, Qing-Guo Meng

Seiten: 525-527

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C 18 H 12 F 4 O, triclinic, P 1̄ (no. 2), a = 7.9400(8) Å, b = 8.1071(9) Å, c = 13.3238(15) Å, α = 89.394 ( 9 ) ° $89.394\left(9\right)^{\circ} $ , β = 76.343 ( 9 ) ° $76.343\left(9\right)^{\circ} $ , γ $$ = 63.411 ( 11 ) ° $\text{63.411}\left(11\right)^{\circ} $ , V = 740.79(15) Å 3 , Z = 2, R g t ${R}_{\mathit{g}\mathit{t}}$ ( F ) = 0.0472, w R r e f $w{R}_{\mathit{r}\mathit{e}\mathit{f}}$ ( F 2 ) = 0.1244, T = 293 K.
Open Access
Crystal structure of bis(6-aminopyridine-2-carboxylato–k²O,N)-bis(N,N-dimethylformamide-k¹ O)zinc(II), C₁₈H₂₄N₆O₆Zn

5. April 2023

Dong-feng Hong, Jia-Qi Ye, Wen-Bo Guo

Seiten: 529-531

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C 18 H 24 N 6 O 6 Zn, monoclinic, P 2 1 / n (no. 14), a = 10.1669(6) Å, b = 8.0831(4) Å, c = 13.1012(8) Å, β = 91.221 ( 5 ) ° $91.221(5){}^{\circ}$ , Z = 2, V = 1076.41(11) Å 3 , R gt (F) = 0.0396, w R ref (F 2 ) = 0.0987, T = 273 K.
Open Access
Crystal structure of 5-(adamantan-1-yl)-3-[(4-{[2-(trifluoromethyl)phenyl]-methyl}piperazin-1-yl)methyl]-1,3,4-oxadiazole-2(3H)-thione, C₂₅H₃₁F₃N₄OS

20. März 2023

Lamya H. Al-Wahaibi, Mohammed S. M. Abdelbaky, Santiago Garcia-Granda, Edward R. T. Tiekink, Ali A. El-Emam

Seiten: 533-535

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C 25 H 31 F 3 N 4 OS, monoclinic, P 2 1 / c (no. 14), a = 6.7323(1) Å, b = 15.4999(2) Å, c = 23.7905(4) Å, β = 93.037(2)°, V = 2479.05(6) Å 3 , Z = 4, R gt ( F ) = 0.0473, wR ref ( F 2 ) = 0.1394, T = 293 K.
Open Access
Crystal structure of tetrapropylammonium bicarbonate–1-(diaminomethylene)thiourea – water (2/2/1), C₃₀H₇₂N₁₀O₇S₂

4. April 2023

Lulu Zhang, Qianqian Han, Xin Zhu

Seiten: 537-539

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C 30 H 72 N 10 O 7 S 2 , triclinic, P 1̄ (no. 2), a = 8.75510(10) Å, b = 15.1170(2) Å, c = 16.8843(2) Å, α = 76.272 ( 1 ) ° $76.272(1){}^{\circ}$ , β = 78.397 ( 1 ) ° $78.397(1){}^{\circ}$ , γ = 88.277 ( 1 ) ° $88.277(1){}^{\circ}$ , V = 2126.09(5) Å 3 , Z = 2, R gt ( F ) = 0.0407, wR ref ( F 2 ) = 0.1282, T = 296(2) K.
Open Access
Crystal structure of tris(2,2′-bipyridine-κ² N,N′)iron(II) triiodide – dichloromethane (2/1), C₆₁H₅₀Cl₂Fe₂I₁₂N₁₂

23. März 2023

Chuanguo Cui, Jinxiao Zhang, Zhiyin Xiao

Seiten: 541-543

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C 61 H 50 Cl 2 Fe 2 I 12 N 12 , orthorhombic, Pbcn (no. 60), a = 13.0247(4) Å, b = 17.0204(5) Å, c = 34.1475(9) Å, β = 90, V = 7570.0(4) Å 3 , Z = 4, R gt ( F ) = 0.0694, wR ref ( F 2 ) = 0.1605, T = 293(2) K.
Open Access
Crystal structure of 2-amino-3-[2-(1,3,3-trimethyl-1,3-dihydro-indol-2-ylidene)-ethylideneamino]-but-2-enedinitrile, C₁₇H₁₇N₅

5. April 2023

Ze-Yi Lian, Wei-Na Wu

Seiten: 545-546

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C 17 H 17 N 5 , monoclinic, P 2 1 / c (no. 14), a = 9.4347(9) Å, b = 15.6392(15) Å, c = 11.0939(11) Å, β = 100.215 ( 2 ) ° $100.215(2){}^{\circ}$ , V = 1611.0(3) Å 3 , Z = 4, R gt ( F ) = 0.0392, wR ref ( F 2 ) = 0.1105, T = 296 K.
Open Access
The crystal structure of 1-(2-chlorophenyl)-3-cycloheptylurea, C₁₄H₁₉ClN₂O

30. März 2023

Yuanci Li, Zhiqiang Feng, Hongjuan Tong

Seiten: 547-549

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C 14 H 19 ClN 2 O, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 8.9579(3) Å, b = 12.2172(4) Å, c = 12.5669(5) Å, V = 1375.33(8) Å 3 , Z = 4, R gt ( F ) = 0.0541, w R ref ( F 2 ) = 0.1449, T = 193 K.
Open Access
Crystal structure of potassium bis(pentaselenido-κ ² Se ¹,Se ⁵)palladate(II), K₂[Pd(Se₅)₂]

27. März 2023

Kang-Woo Kim

Seiten: 551-553

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K 2 PdSe 10 , orthorhombic, Pcma (no. 55), a = 8.293(3) Å, b = 10.987(3) Å, c = 16.432(5) Å, V = 1497.1(8) Å 3 , Z = 4, R gt ( F ) = 0.0349, wR ref ( F 2 ) = 0.0688, T = 173(2) K.
Open Access
The crystal structure of 5,10-bis(2-methoxyethyl)-5,10-dihydro-[1,2,3,4]tetrathiocino[5,6-b:8, 7-b′]diindole, C₂₂H₂₂N₂O₂S₄

23. März 2023

Ming Ni, Penghui Ni

Seiten: 555-557

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C 22 H 22 N 2 O 2 S 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.4865(14) Å, b = 11.756(2) Å, c = 12.863(2) Å, α = 69.693(2)°, β = 70.812(2)°, γ = 72.170(2)°, V = 1109.6(3) Å 3 , Z = 2, R gt ( F ) = 0.0280, wR ref ( F 2 ) = 0.0753, T = 296(2) K.
Open Access
The crystal structure of 4-(4-iodophenyl)-5H-1,2,3-dithiazole-5-thione, C₈H₄INS₃

23. März 2023

Huiyang Liao, Penghui Ni

Seiten: 559-561

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C 8 H 4 INS 3 , monoclinic, P 2 1 / c (no. 14), a = 11.8060(19) Å, b = 7.8961(14) Å, c = 11.972(2) Å, β = 110.981 ( 2 ) ° $110.981(2){}^{\circ}$ , V = 1042.1(3) Å 3 , Z = 4, R gt ( F ) = 0.0279, wR ref ( F 2 ) = 0.0739, T = 296(2) K.
Open Access
Crystal structure of bis{μ₂-(4-acetyl-phenoxy)acetato-κ² O:O′}-bis{μ₂-(4-acetyl-phenoxy)acetato-κ³ O,O′:O)- bis{(4-acetyl-phenoxy)acetato-κ² O,O′}-bis(phenanthrolin-κ² N,N′)didysprosium(III) tetrahydrate, C₈₄H₇₈N₄O₂₈Dy₂

4. April 2023

Li–Hua Wang, Hao–Wen Tai, Mei–Li Zhao, Xi–Shi Tai

Seiten: 563-565

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C 84 H 78 N 4 O 28 Dy 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 12.3134(5) Å, b = 12.7705(5) Å, c = 14.5150(6) Å, α = 70.852(1)°, β = 80.298(1)°, γ = 65.726(1)°, V = 1964.05(14) Å 3 , Z = 1, R gt ( F ) = 0.0381, w R ref ( F 2 ) = 0.0682, T = 296.15 K.
Open Access
Crystal structure of Eu₂Pd_3.37(1)Zn_13.63(1)

21. März 2023

Steffen Klenner, Theresa Block, Rainer Pöttgen

Seiten: 567-569

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Eu 2 Pd 3.37 Zn 13.63 , trigonal, R 3 ‾ m $R\overline{3}m$ (no. 166), a = 9.1693(7) Å, c = 13.2443(13) Å, V = 964.34(14) Å 3 , Z = 3, R gt ( F ) = 0.0268, wR ref ( F 2 ) = 0.0287, T = 293 K.
Open Access
Crystal structure of 2-methoxy-4-(methoxy-carbonyl)phenyl 2-chloro-4-fluorobenzoate, C₁₆H₁₂ClFO₅

19. April 2023

Xin-Ting Xiong, Pan-Lei Xiao, Xiao-Hui Ou-Yang, Xu-Liang Nie, Xiu-Ying Song

Seiten: 571-573

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C 16 H 12 ClFO 5 , monclinic, P 2 1 / c (no. 14), a = 14.7536(6) Å, b = 7.8281(3) Å, c = 14.0501(7) Å, β = 111.174 ( 5 ) ° $111.174(5){}^{\circ}$ , V = 1513.13(12) Å 3 , Z = 4, R gt ( F ) = 0.0367, wR ref ( F 2 ) = 0.0865, T = 296(2) K.
Open Access
Crystal structure of catena-poly[bis(μ₂-dicyanamide-κ² N:N′)-bis(4-vinylpyridine-κN)-copper(II)], C₁₈H₁₄CuN₈

12. April 2023

Chong Tan, Tong Zhang, Xiaodong Yi

Seiten: 575-576

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C 18 H 14 CuN 8 , triclinic, P 1̄ (no. 2), a = 7.2431(5) Å, b = 7.3783(5) Å, c = 9.8740(6) Å, α = 110.174(6)°, β = 105.036(5)°, γ = 92.219(5)°, V = 473.55(6) Å 3 , Z = 1, R gt ( F ) = 0.0409, wR ref ( F 2 ) = 0.1272, T = 293(2) K.
Open Access
The crystal structure of iguratimod-dimethylformamide (1/1), C₁₇H₁₄N₂O₆S·C₃H₇NO

5. April 2023

Wen-Jing Ma, Hao Wang, Zhen-Yu Wang, Yu-Xuan Long, Xin-Qi Wang, Qian Ma, Cui-Ran Xu, Yu-Heng Ma

Seiten: 577-578

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C 17 H 14 N 2 O 6 S·C 3 H 7 NO, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 5.4146(4) Å, b = 11.7925(8) Å, c = 16.9527(12) Å, α = 85.238(2)°, β = 86.674(4)°, γ = 78.959(2)°, V = 1057.77(13) Å 3 , Z = 2, R gt ( F ) = 0.0418, wR ref ( F 2 ) = 0.1175, T = 296(2) K.
Open Access
Synthesis and crystal structure of 1-((3R,10S,13S,17S)-10,13-dimethyl-3-(m-tolylamino)hexadecahydro-1H-cyclopenta[α]phenanthren-17-yl)ethan-1-one, C₂₈H₄₁NO

13. April 2023

Jin-Feng Zhao, Wen-Wen Zhang, Jiang-Hai Ye, Kang He, Juan Zou

Seiten: 579-581

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C 28 H 41 NO, triclinic, P 1 $P1$ (no. 1), a = 6.3144(8) Å, b = 9.7315(13) Å, c = 10.5867(14) Å, α = 111.561(4)°, β = 96.486 ( 4 ) ∘ $96.486{(4)}^{\circ }$ , γ = 97.128(4)°, V = 591.41(14) Å 3 , Z = 1, R g t ${R}_{\mathit{g}\mathit{t}}$ ( F ) = 0.0579, w R r e f $w{R}_{\mathit{r}\mathit{e}\mathit{f}}$ ( F 2 ) = 0.1687, T = 273(2) K.
Open Access
The crystal structure of diaqua-bis(4-bromo-2-formylphenoxy)zinc(II), C₁₄H₁₂Br₂O₆Zn

13. April 2023

Fei Zou, Sheng-Ting Zhang, Jue-Yuan Chen, Lin Yuan

Seiten: 583-584

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C 14 H 12 Br 2 O 6 Zn, monoclinic, C 2/ c (no. 15), a = 29.43(2) Å, b = 4.774(4) Å, c = 11.658(9) Å, β = 103.194 ( 7 ) ∘ $103.194{(7)}^{\circ }$ , V = 1595(2) Å 3 , Z = 4, R g t ${R}_{gt}$ ( F ) = 0.0235, w R r e f $w{R}_{ref}$ ( F 2 ) = 0.0647, T = 296(2) K.
Open Access
The crystal structure of tetra(1-ethylimidazole-κ ¹ N)-[μ ₄-imidazole-4,5-dicarboxylato-κ ⁴ O, N, O′, N′]-trioxido-divanadium, C₂₅H₃₃N₁₀O₇V₂

14. April 2023

Na Li, Xiao-Jie Wang, Yu-Cai Qin, Jing-Yun Wang

Seiten: 585-587

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C 25 H 33 N 10 O 7 V 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 10.3933(4) Å, b = 12.5655(5) Å, c = 14.1841(5) Å, α = 65.373(1)°, β = 70.351 ( 1 ) ∘ $70.351{(1)}^{\circ }$ , γ = 88.052 ( 2 ) ∘ $88.052{(2)}^{\circ }$ , V = 1573.62(11) Å 3 , Z = 2, R gt ( F ) = 0.0362, wR ref ( F 2 ) = 0.0885, T = 173 K.
Open Access
The crystal structure of (E)-N′-(1-(4-fluorophenyl)propylidene)-2-hydroxybenzohydrazide, C₁₆H₁₅FN₂O₂

6. April 2023

Sha Yang, Jing Men, Wenqiang Tang

Seiten: 589-591

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C 16 H 15 FN 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 9.2751(7) Å, b = 13.1232(7) Å, c = 11.7155(8) Å, β = 90.011 ( 7 ) ∘ $90.011{(7)}^{\circ }$ , V = 1426.00(16) Å 3 , Z = 4, R g t ${R}_{\mathit{g}\mathit{t}}$ ( F ) = 0.0570, w R r e f $w{R}_{\mathit{r}\mathit{e}\mathit{f}}$ ( F 2 ) = 0.1462, T = 293 K.

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