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Zeitschrift für Kristallographie - New Crystal Structures

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Volume 238, Issue 4

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Zeitschrift für Kristallographie - New Crystal Structures

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Zeitschrift für Kristallographie - New Crystal Structures

Contents

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Frontmatter

July 5, 2023

Page range: i-vii

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New Crystal Structures
Open Access
Crystal structure of a polymorph of potassium picrate, C₆H₂KN₃O₇

May 24, 2023

Xinyao Luo, Cuilian Chen, Zunjian Hu, Fei Wang, Shanhu Sun, Zhirong Suo, Li Su

Page range: 593-594

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C 6 H 2 KN 3 O 7 , monoclinic, P 2 1 / m (no. 11), a = 4.1681(2) Å, b = 10.6704(6) Å, c = 10.2381(6) Å, β = 95.134(2)°, V = 453.52(4) Å 3 , Z = 2, R gt ( F ) = 0.0404, wR ref ( F 2 ) = 0.0967, T = 295 K.
Open Access
The crystal structure of (1E,2E)-1,2-bis(quinolin-2-ylmethylene)hydrazine, C₂₀H₁₄N₄

May 5, 2023

Fuguang Liao, Shuhao Yuan, Weifeng Nie, Zirong Yi, Qian Zhang, Shiyu Yan, Ying Cui

Page range: 595-596

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C 20 H 14 N 4 , monoclinic, P 2 1 / c (no. 14), a = 13.4569(16) Å, b = 4.7592(5) Å, c = 11.9902(13) Å, β = 94.914(2)°, V = 765.08(15) Å 3 , Z = 2, R gt ( F ) = 0.0333, wR ref ( F 2 ) = 0.0935, T = 296(2) K.
Open Access
5-Amino-2-chloro-4-fluoro-N-(N-isopropyl-N-methylsulfamoyl) benzamide, C₁₁H₁₅O₃ClFN₃S

April 20, 2023

Wang Jie, Shu-Zhen Xiao, Huang Cong, Ya-Qiang Liu, Da-Yong Peng

Page range: 597-598

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C 11 H 15 O 3 ClFN 3 S, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 7.8107(11) Å, b = 9.1644(13) Å, c = 11.3521(15) Å, α = 67.543(2)°, β = 72.776 ( 2 ) ∘ $72.776{(2)}^{\circ }$ , γ = 88.529 ( 2 ) ∘ $88.529{(2)}^{\circ }$ , V = 713.76(17) Å 3 , Z = 2, R g t ${R}_{\mathit{g}\mathit{t}}$ ( F ) = 0.0385, w R r e f $w{R}_{\mathit{r}\mathit{e}\mathit{f}}$ ( F 2 ) = 0.1338, T = 296(2) K.
Open Access
Crystal structure of trans-N ¹,N ⁸-bis(2-cyanoethyl)-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane, C₂₂H₄₂N₆

May 5, 2023

Saswata Rabi, Lucky Dey, Ismail M. M. Rahman, Edward R. T. Tiekink, Tapashi Ghosh Roy

Page range: 599-601

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C 22 H 42 N 6 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 8.3115(2) Å, b = 8.8263(2) Å, c = 9.7688(2) Å, α = 111.490 ( 2 ) ° $111.490(2){}^{\circ}$ , β = 115.056 ( 2 ) ° $115.056(2){}^{\circ}$ , γ = 93.681 ( 2 ) ° $93.681(2){}^{\circ}$ , V = 583.25(3) Å 3 , Z = 1, R gt ( F ) = 0.0465, wR ref ( F 2 ) = 0.1351, T = 294 K.
Open Access
The crystal structure of [N-{[2-(oxy)-4-methoxyphenyl](phenyl)methylidene}alaninato]-diphenyl-silicon(IV) – chloroform (1/1), C₂₉H₂₅NO₄Si·CHCl₃

April 28, 2023

Uwe Böhme, Sabine Fels

Page range: 603-605

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C 29 H 25 NO 4 Si·CHCl 3 , monoclinic, P 2 1 / c (no. 14), a = 17.1316(8) Å, b = 10.1173(3) Å, c = 18.2252(8) Å, β = 117.195 ( 3 ) ° $117.195(3){}^{\circ}$ , V = 2809.7(2) Å 3 , Z = 4, R gt ( F ) = 0.0431, wR ref ( F 2 ) = 0.1050, T = 153 K.
Open Access
Crystal structure of tetracarbonyl-{μ-[N-(diphenylphosphanyl)-N,P,P-triphenylphosphinous amide]}-bis[μ-(phenylmethanethiolato)]diiron (Fe–Fe), C₄₈H₃₉Fe₂NO₄P₂S₂

June 6, 2023

Xin-Ping Gao, Shuang Lü, Qian-Li Li

Page range: 607-609

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C 48 H 39 Fe 2 NO 4 P 2 S 2 , orthorhombic, P 2 1 (no. 4), a = 11.4073(11) Å, b = 16.9013(14) Å, c = 11.8261(12) Å, α = 90°, β = 108.297(4)°, γ = 90°, V = 2164.8(4) Å 3 , Z = 2, R gt ( F ) = 0.0355, w R ref ( F 2 ) = 0.0740, T = 298(2) K.
Open Access
Crystal structure of baryte from Mine du Pradet (France)

April 26, 2023

Christian Paulsen, Valérie Galéa-Clolus, Rainer Pöttgen

Page range: 611-613

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BaSO 4 , orthorhombic, Pnma (no. 62), a = 8.8806(8) Å, b = 5.4539(5) Å, c = 7.1570(7) Å, V = 346.64(6) Å 3 , Z = 4, R gt ( F 2 ) = 0.0141, wR ref ( F 2 ) = 0.0329, T = 293 K.
Open Access
The crystal structure of [(2,2′-bipyridine-6-carboxylato-κ³ N,N,O)-(6-phenylpyridine-2-carboxylate-κ² N,O)copper(II)] monohydrate, C₂₃H₁₇N₃O₅Cu

April 27, 2023

Zhao Zeng-Bing, Li Xue-Ping, Yang Shu-Cheng, Yang Bing-Qi, Wang Ze-Tao, Cheng Lan-Xing, Tai Xi-Shi

Page range: 615-617

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C 23 H 17 N 3 O 5 Cu, monoclinic, P 2 1 / n (no. 14), a = 11.49510(10) Å, b = 8.69660(10) Å, c = 21.1454(2) Å, β = 105.433(1)°, V = 2037.65(4) Å 3 , Z = 4, R gt ( F ) = 0.0298, w R ref ( F 2 ) = 0.0862, T = 294 K.
Open Access
Crystal structure of bis(μ-benzeneselenolato)-(μ-[N-benzyl-N-(diphenylphosphanyl)-P,P-diphenylphosphinous amide])-tetracarbonyl diiron (Fe–Fe), C₄₇H₃₇Fe₂NO₄P₂Se₂

May 15, 2023

Shu-Fen Bai, Shuang Lü, Qian-Li Li

Page range: 619-621

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C 47 H 37 Fe 2 NO 4 P 2 Se 2 , monoclinic, P 2 1 / n (no. 14), a = 12.8144(11) Å, b = 17.9714(15) Å, c = 19.1077(17) Å, β = 104.329(4)°, V = 4263.5(6) Å 3 , Z = 4, R gt ( F ) = 0.0420, w R ref ( F 2 ) = 0.0968, T = 298(2) K.
Open Access
The crystal structure of diaqua-methanol-κ¹ O- (3-thiophenecarboxylato-κO)-(2,2′-dipyridyl-κ² N,N′)manganese(II) 3-thiophenecarboxylate, C₂₁H₂₂N₂O₇S₂Mn

May 12, 2023

Zheng Shi, Zhongyu Zhang, Bing Han, Yunyun Li

Page range: 623-625

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C 21 H 22 N 2 O 7 S 2 Mn, monoclinic, P 2 1 / c (no. 14), a = 14.544(6) Å, b = 9.636(4) Å, c = 17.087(7) Å, β = 96.664 ( 6 ) ° $96.664(6){}^{\circ}$ , V = 2378.5(17) Å 3 , Z = 4, R g t ${R}_{\mathit{g}\mathit{t}}$ ( F ) = 0.0349, w R r e f $w{R}_{\mathit{r}\mathit{e}\mathit{f}}$ ( F 2 ) = 0.1036, T = 273.15 K.
Open Access
Crystal structure of catena-poly[tetrakis(butyl)-μ₂-2-((oxido(phenyl)methylene)hydrazineylidene)propanoato-κ⁴ O:O,O′,N-μ₂-2-((oxido(phenyl)methylene)hydrazineylidene)propanoato-κ⁴ O,N,O′:N′-ditin(IV)], C₃₄H₅₀N₆O₆Sn₂

May 15, 2023

Zhongjun Gao, Haifeng Zhang

Page range: 627-629

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C 34 H 50 N 6 O 6 Sn 2 , triclinic, P 1 ‾ $\overline{1}$ , a = 12.110(2) Å, b = 12.406(2) Å, c = 13.744(3) Å, α = 79.547 ( 2 ) ° $79.547(2){}^{\circ}$ , β = 82.072 ( 2 ) ° $82.072(2){}^{\circ}$ , γ = 87.257 ( 2 ) ° $87.257(2){}^{\circ}$ , V = 2010.7(7) Å 3 , Z = 2, R gt ( F ) = 0.0471, wR ref ( F 2 ) = 0.1392, T = 298 K.
Open Access
Crystal structure of 4-chloro-N′-[(1E)-(2-nitrophenyl)methylidene]benzohydrazide, C₁₄H₁₀ClN₃O₃

April 27, 2023

Lamya H. Al-Wahaibi, Olivier Blacque, Edward R. T. Tiekink, Ali A. El-Emam

Page range: 631-633

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C 14 H 10 ClN 3 O 3 , triclinic, P 1 (no. 1), a = 4.8813(2) Å, b = 6.7806(2) Å, c = 10.3135(2) Å, α = 98.101 ( 2 ) ∘ $98.101{\left(2\right)}^{\circ }$ , β = 94.174 ( 2 ) ∘ $94.174{\left(2\right)}^{\circ }$ , γ = 97.612 ( 3 ) ∘ $97.612{\left(3\right)}^{\circ }$ , V = 333.515(18) Å 3 , Z = 1, R g t ${R}_{gt}$ (F) = 0.0270, w R r e f $w{R}_{ref}$ (F 2 ) = 0.0743, T = 160 K.
Open Access
The crystal structure of 3-(1′-deoxy-3′,5′-O-dibenzy-β-d-ribosyl)adenine dichloromethane solvate, C₄₉H₅₂Cl₂N₁₀O₆

May 16, 2023

Pingqiao Wang, Yunlong Zhu, Haixin Ding, Haiyang Huang

Page range: 635-637

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C 49 H 52 Cl 2 N 10 O 6 , monoclinic, P 2 1 (no. 4), a = 12.2875(14) Å, b = 8.3031(10) Å, c = 13.1242(15) Å, β = 100.0640 ( 10 ) ∘ $100.0640{(10)}^{\circ }$ , V = 1318.4(3) Å 3 , Z = 1, R g t ${R}_{\mathrm{g}\mathrm{t}}$ ( F ) = 0.0736, w R r e f $w{R}_{\mathrm{r}\mathrm{e}\mathrm{f}}$ ( F 2 ) = 0.1545, T = 296 K.
Open Access
The crystal structure of (Z)-4-amino-N′-(1-(o-tolyl)ethylidene)benzohydrazide, C₁₆H₁₇N₃O

May 1, 2023

Ai-Li Qiao, Zheng-Feng Guo

Page range: 639-640

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C 16 H 17 N 3 O, monoclinic, P 2 1 / n (no. 14), a = 8.2818(6) Å, b = 17.0495(10) Å, c = 10.2429(7) Å, β = 98.980(6)°, V = 1428.58(17) Å 3 , Z = 4, R gt ( F ) = 0.0629, wR ref ( F 2 ) = 0.1461, T = 293 K.
Open Access
The co-crystal structure of etoricoxib–phthalic acid (1/1), C₁₈H₁₅ClN₂O₂S·C₈H₆O₄

April 28, 2023

Yu-Heng Ma, Miao-Miao Zhu, Chun-Ni Zhang, Xiao-Sa Tang, Wei-Guo Zhang, Wen-Jing Ma

Page range: 641-643

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C 18 H 15 ClN 2 O 2 S·C 8 H 6 O 4 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 8.4340(17) Å, b = 12.172(2) Å, c = 12.816(3) Å, α = 89.98 ( 3 ) ° $89.98(3){}^{\circ}$ , β = 77.41 ( 3 ) ° $77.41(3){}^{\circ}$ , γ = 72.52 ( 3 ) ° $72.52(3){}^{\circ}$ , V = 1221.7(5) Å 3 , Z = 2, R gt ( F ) = 0.0482, wR ref ( F 2 ) = 0.1344, T = 293 K.
Open Access
Crystal structure of (glycinto-κ ² O,N ^′)-[5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ ⁴ N,N ^′,N ^″,N ^‴]nickel(II) perchlorate monohydrate C₁₈H₄₂ClN₅NiO₇

April 25, 2023

Zu-Jiao Zhang, Guang-Chuan Ou

Page range: 645-647

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C 18 H 42 ClN 5 NiO 7 , orthorhombic, Pca 2 1 (no. 29), a = 14.270(3) Å, b = 9.918(2) Å, c = 17.603(4) Å, V = 2491.4(10) Å 3 , Z = 4, R gt ( F ) = 0.0382, wR ref ( F 2 ) = 0.0861, T = 173(2) K.
Open Access
The crystal structure of catena-poly[bis(1-ethylimidazole-k¹ N)-(μ ₂-benzene-1-carboxyl-3,5-dicarboxylato-κ ² O, O′)zinc(II)], C₁₉H₂₀N₄O₆Zn

May 15, 2023

Ya-Fei Guo, Bao-Kuan Chen

Page range: 649-651

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C 19 H 20 N 4 O 6 Zn, monoclinic, P 2 1 / n (no. 14), a = 11.7411(7) Å, b = 13.7831(9) Å, c = 13.5425(10) Å, β = 97.564 ( 2 ) ∘ $97.564{(2)}^{\circ }$ , V = 2172.5(3) Å 3 , Z = 4, R gt ( F ) = 0.0645, wR ref ( F 2 ) = 0.1643, T = 298 K.
Open Access
Crystal structure of 3-(thiazol-2-ylcarbamoyl)-7-oxabicyclo[2.2.1]heptane-2-carboxylic acid, C₁₁H₁₂N₂O₄S

June 8, 2023

Jinqing Song, Beibei Cui, Xia Mi, Jingyu Zhang

Page range: 653-654

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C 11 H 12 N 2 O 4 S 1 , orthorhombic, Pbca (no. 61), a = 11.08447(14) Å, b = 10.71473(16) Å, c = 19.5463(3) Å, V = 2321.46(6) Å 3 , Z = 8, R gt ( F ) = 0.0450, wR ref ( F 2 ) = 0.1275, T = 293(2) K.
Open Access
Rietveld structure analysis of keatite, a rare, metastable SiO₂ polymorph

May 10, 2023

Isabel Grosskreuz, Bernd Marler

Page range: 655-657

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O 24 Si 12 , tetragonal, P 4 3 2 1 2 (no. 96), a = 7.4462(1) Å, c = 8.5838(4) Å, V = 475.93(3) Å 3 , Z = 1, R(F) = 0.037, T = 293 K.
Open Access
Crystal structure of catena-poly[(μ₂-isophthalato-k³ O,O′:O″)(4-(4-pyridyl)-2,5-dipyrazylpyridine-k³ N,N′,N″)cobalt(II)] trihydrate C₂₆H₂₂N₆O₇Co₁

June 8, 2023

Chao-Jun He, Zhou-Qin Wang, Yu-Fang Wang

Page range: 659-661

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C 26 H 22 N 6 O 7 Co, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 9.0033(4) Å, b = 10.1338(5) Å, c = 15.5122(8) Å, α = 96.164(4)°, β = 100.835 ( 4 ) ∘ $100.835{(4)}^{\circ }$ , γ = 113.867 ( 5 ) ∘ $113.867{(5)}^{\circ }$ , V = 1244.20(11) Å 3 , Z = 2, R gt ( F ) = 0.0473, wR ref ( F 2 ) = 0.1023, T = 293(2) K.
Open Access
Crystal structure of 3,5–di-O-benzoyl-1,2-O-isopropylidene-α–D-ribose, C₂₂H₂₂O₇

May 23, 2023

Binbin Wu, Guangying Chen, Haixin Ding

Page range: 663-665

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C 22 H 22 O 7 , orthorhombic, C 222 1 (no. 20), a = 8.891(2) Å, b = 17.938(5) Å, c = 25.996(6) Å, V = 4146.0(18) Å 3 , Z = 8, R gt ( F ) = 0.0461, wR ref ( F 2 ) = 0.1189, T = 296 K.
Open Access
The crystal structure of fac-tricarbonyl(6-bromo-2,2-bipyridine-κ² N,N)-(nitrato-κO)rhenium(I), C₁₃H₇BrN₃O₆Re

May 9, 2023

Marcus Mkhatshwa, Frederick P. Malan, Katlego Makgopa, Amanda-Lee E. Manicum

Page range: 667-669

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C 13 H 7 BrN 3 O 6 Re, monoclinic, P 2 1 / n (no. 14), a = 7.2645(1) Å, b = 10.0607(1) Å, c = 20.7717(2) Å, β = 97.1800(10)°, V = 1506.22(3) Å 3 , Z = 4, R gt ( F ) = 0.0359, wR ref ( F 2 ) = 0.0810, T = 150 K.
Open Access
The crystal structure of (E)-N′-(4-hydroxy-3-methoxybenzylidene)-2-naphthohydrazide monohydrate, C₁₉H₁₈N₂O₄

June 5, 2023

Sheng-Ting Zhang, Fei Zou, Ni Lai, Lin Yuan, Zhong-Yan Li

Page range: 671-672

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C 19 H 18 N 2 O 4 , monoclinic, P 2 1 / n (no. 14), a = 8.375(2) Å, b = 22.018(6) Å, c = 9.237(3) Å, β = 106.271 ( 3 ) ∘ $106.271{(3)}^{\circ }$ , V = 1635.1(8) Å 3 , Z = 4, R g t ${R}_{gt}$ ( F ) = 0.0427, w R r e f ${wR}_{ref}$ ( F 2 ) = 0.1185, T = 296(2) K.
Open Access
The crystal structure of 5,5′-diselanediyl-bis(2-hydroxybenzaldehyde), C₁₄H₁₀O₄Se₂

May 24, 2023

Lin Tingting, Peng Qiuling, Lv Meiyun, Guo Mengping

Page range: 673-674

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C 14 H 10 O 4 Se 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 6.6836(11) Å, b = 8.9933(11) Å, c = 11.5062(19) Å, α = 77.128(12)°, β = 87.684(14)°, γ = 89.975(12)°, V = 673.65(18) Å 3 , Z = 2, R gt ( F ) = 0.0564, w R ref ( F 2 ) = 0.1512, T = 293 K.
Open Access
The crystal structure of catena-poly[diaqua-m₂-dicyanido-κ² C:N-dicyanido-κ¹ C-bis(4-(pyridin-4-yl)benzaldehyde-κ¹N)iron(II)-platinum(II), C₂₈H₂₂N₆O₄PtFe

May 31, 2023

Jitao Lu, Xiaolin Wu, Youwei Zhang, Yufang Xiao

Page range: 675-677

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(C 28 H 22 N 6 O 4 PtFe) n , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 7.9137(6) Å, b = 8.5766(13) Å, c = 10.970(3) Å, α = 70.266 ( 19 ) ° $70.266(19){}^{\circ}$ , β = 81.258 ( 14 ) ° $81.258(14){}^{\circ}$ , γ = 78.728 ( 11 ) ° $78.728(11){}^{\circ}$ , V = 684.3(2) Å 3 , Z = 1, R gt ( F ) = 0.0408, wR ref ( F 2 ) = 0.0657, T = 293 K.
Open Access
Redetermination of the crystal structure of 5,14-dihydro-6,17-dimethyl-8,15-diphenyldibenzo(b,i)(1,4,8,11)tetra-azacyclotetradecine, C₃₂H₂₈N₄

May 1, 2023

Lucky Dey, Saswata Rabi, Debashis Palit, Ismail M. M. Rahman, Edward R. T. Tiekink, Tapashi Ghosh Roy

Page range: 679-682

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C 32 H 28 N 4 , monoclinic, P 2 1 / c (no. 14), a = 17.7218(4) Å, b = 20.7769(5) Å, c = 14.9434(3) Å, β = 113.598 ( 3 ) ° $113.598(3){}^{\circ}$ , V = 5042.1(2) Å 3 , Z = 8, R gt ( F ) = 0.0519, wR ref ( F 2 ) = 0.1544, T = 294 K.
Open Access
Crystal structure of poly[(μ₃-2-(3,5-dicarboxyphenyl) benzimidazole-6-carboxylato-κ⁴O:O:O′:O″)lead(II)] monohydrate, C₁₆H₁₀N₂O₇Pb

June 20, 2023

Yujie Zhang, Shushu Xiong, Yongke He

Page range: 683-684

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C 16 H 10 N 2 O 7 Pb, tetragonal, I 4 1 / a (no. 88), a = 15.1344(2) Å, b = 15.1344(2) Å, c = 26.5431(6) Å, V = 6079.7(2) Å 3 , Z = 16, R gt ( F ) = 0.0419, wR ref ( F 2 ) = 0.0991, T = 150 K.
Open Access
The crystal structure of fac-tricarbonyl(2-pyridin-2-yl-quinoline-κ² N,N′)-(pyrazole-κN)rhenium(I)nitrate, C₂₀H₁₄N₄O₃ReNO₃

May 9, 2023

Sibusiso A. Sithole, Federick P. Malan, David R. Katerere, Amanda-Lee E. Manicum

Page range: 685-687

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C 20 H 14 N 4 O 3 ${\mathrm{C}}_{20}{\mathrm{H}}_{14}{\mathrm{N}}_{4}{\mathrm{O}}_{3}$ Re N O 3 ${\mathrm{N}\mathrm{O}}_{3}$ , monoclinic, P 2 1 ${2}_{1}$ / c (no. 14), a = 12.9572 (2), b = 9.1568 (2), c = 17.3658 (3) Å, β = 97.267 ( 2 ) ° $97.267(2){}^{\circ}$ , V = 2043.84 (7)  Å 3 ${\mathrm{\mathring{\text{A}}}}^{3}$ , Z = 4, R g t ${R}_{gt}$ ( F ) = 0.0231, w R r e f $w{R}_{ref}$ ( F 2 ${F}^{2}$ ) = 0.0514, T = 154 K
Open Access
Crystal structure of dibromo-dicarbonyl-bis(tricyclohexylphosphine)-osmium(II) dichloromethane solvate, C₃₈H₆₆Br₂O₂OsP₂

May 15, 2023

Jubrey M. Monareng, Hadley S. Clayton

Page range: 689-692

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C 38 H 66 Br 2 O 2 OsP 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 10.4091(2) Å, b = 10.6868(2) Å, c = 21.3533(4) Å, α = 84.658(1)°, β = 89.764(1)°, γ = 64.918(1)°, V = 2140.36(7) Å 3 , Z = 2, R gt ( F ) = 0.0248, w R ref ( F 2 ) = 0.0578, T = 173(2) K.
Open Access
Crystal structure of poly[bis(μ ₂-2,6-bis(1-imidazoly)pyridine-κ ² N:N′)copper(II)] diperchlorate dihydrate, C₂₂H₂₂Cl₂CuN₁₀O₁₀

June 5, 2023

Sujuan Kan, Yawei Ma, Chunjie Chen, Jun Qian

Page range: 693-695

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C 22 H 22 Cl 2 CuN 10 O 10 , monoclinic, P 2 1 / c (no. 14), a = 6.8548(14) Å, b = 12.482(3) Å, c = 17.162(4) Å, β = 112.54(3)°, V = 1356.2(6) Å 3 , Z = 2, R gt ( F ) = 0.0575, w R ref ( F 2 ) = 0.1726, T = 293 K.
Open Access
The crystal structure of fac-tricarbonyl(N-benzoyl-N,N-cyclohexylmethylcarbamimidothioato-κ² S,O)-(pyridine-κN)rhenium(I), C₂₃H₂₄N₃O₄ReS

May 11, 2023

Luleka Makhakhayi, Frederick P. Malan, Vuyelwa J. Tembu, Comfort M. Nkambule, Amanda-Lee E. Manicum

Page range: 697-699

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C 23 H 24 N 3 O 4 ReS, orthorhombic, Pbca (no. 61), a = 15.1264(4) Å, b = 15.1167(5) Å, c = 20.1500 Å, V = 4607.5(2) Å 3 , Z = 8, T = 150(2) K, R gt ( F ) = 0.0416, w R ref ( F 2 ) = 0.0691.
Open Access
Crystal structure of (E)-7-fluoro-2-(4-fluorobenzylidene)-3,4-dihydronaphthalen-1(2H)-one, C₁₇H₁₂F₂O

May 31, 2023

Pan-Pan Wei, Qing-Guo Meng, Bao-Gang Wang, Gui-Ge Hou, Ya-Bin Song

Page range: 701-703

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C 17 H 12 F 2 O, triclinic, P 1¯ (no. 2), a = 7.9570(14) Å, b = 8.9872(19) Å, c = 9.3974(16) Å, α = 94.467(16)°, β = 96.737(14)°, γ = 103.162(16)°, V = 646.0(2) Å 3 , Z = 2, R gt ( F ) = 0.0417, wR ref ( F 2 ) = 0.1112, T = 293 K.
Open Access
Synthesis and crystal structure of 1-((3R,10S,13S, 17S)-3-((2-methoxyphenyl)amino)-10,13-dimethylhexadecahydro-1H-cyclopenta[α]phenanthren-17-yl)ethan-1-one, C₂₈H₄₁NO₂

May 23, 2023

Jiang-Hai Ye, Ren-Song Chen, Wen-Wen Zhang, Kang He, Juan Zou

Page range: 705-707

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C 28 H 41 NO 2 , monoclinic, C 2 (no. 5), a = 4.8622(5) Å, b = 6.7853(7) Å, c = 14.3349(17) Å, β = 96.556(3)°, V = 469.84(9) Å 3 , Z = 2, R gt ( F ) = 0.0482, w R ref ( F 2 ) = 0.1257, T = 284(2) K.
Open Access
The crystal structure of fac-tricarbonyl((pyridin-2-yl)methanamino-κ² N,N′)-((pyridin-2-yl)methanamino-κN)rhenium(I) nitrate, C₁₅H₁₆O₃N₄Re

May 23, 2023

Lesetja V. Ramoba, Orbett T. Alexander, Frederick P. Malan, Amanda-Lee E. Manicum

Page range: 709-711

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C 15 H 16 O 3 N 4 Re, triclinic, P 1̄ (no. 2), a = 7.4939(2) Å, b = 10.1316(2) Å, c = 13.8351(3) Å, α = 103.453(2)°, β = 101.992(2)°, γ = 107.880(2)°, V = 926.98(4) Å 3 , Z = 2, R gt ( F ) = 0.0341, wR ref ( F 2 ) = 0.0861, T = 150 K.
Open Access
The crystal structure of (1-(pyridin-2-yl)-N-(pyridin-2-ylmethyl)-N-((1-(4-vinylbenzyl)-1H-benzo[d]imidazol-2-yl)methyl)methanamine-κ ⁴ N,N′,N″,N‴)tris(nitrato-kO,O′)-erbium(III), C₂₉H₂₇ErN₈O₉

June 9, 2023

Hai-Ping Wang, Lu Chen, Jia-Jun Liang, Guo-Peng Huang

Page range: 713-715

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C 29 H 27 ErN 8 O 9 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.6681(2) Å, b = 13.0695(3) Å, c = 14.1408(4) Å, α = 80.130(2)°, β = 86.409(2)°, γ = 75.761(2)°, V = 1529.43(4) Å 3 , Z = 2, R gt ( F ) = 0.0382, w R ref ( F 2 ) = 0.1110, T = 295 K.
Open Access
Crystal structure of tetracene-5,12-dione, C₁₈H₁₀O₂

May 12, 2023

Xiaoxin Zheng, Jinke Jiang, Yang Liu

Page range: 717-718

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C 18 H 10 O 2 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 3.95660(10) Å, b = 12.2859(3) Å, c = 24.5014(6) Å, V = 1191.02(5) Å 3 , Z = 4, R g t ${R}_{gt}$ ( F ) = 0.0609, w R r e f $w{R}_{ref}$ ( F 2 ) = 0.1660, T = 302(2) K.
Open Access
Crystal structure of (3R,3aS,6R,6aR)-6-hexyl-3-methyltetrahydrofuro[3,4-b]furan-2,4-dione, C₁₃H₂₀O₄

May 15, 2023

Yu-Xi Huang, Zan-Hong Chen, Yu-Ting Liao, Jia-Yi Li, Mei-Ying Huang, Bo Ding, Hong-Bo Huang, Yi-Wen Tao

Page range: 719-721

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C 13 H 20 O 4 , monoclinic, P 2 1 (no. 4), a = 9.7071(4) Å, b = 7.9026(4) Å, c = 17.3139(7) Å, β = 101.617(4)°, V = 1300.97(10) Å 3 , Z = 4, R gt (F) = 0.0428, wR ref ( F 2 ) = 0.1145, T = 170 K.
Open Access
The crystal structure of N′¹,N′³-bis((E)-thiophen-2-ylmethylene)isophthalohydrazide monohydrate, C₁₈H₁₆N₄O₃S₂

May 9, 2023

Zi-Yi Yin, Fei Zou, Jue-Yuan Chen, Lin Yuan, Zhong-Yan Li

Page range: 723-724

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C 18 H 16 N 4 O 3 S 2 , monoclinic, C 2/ c (no. 15), a = 19.694(4) Å, b = 11.450(2) Å, c = 8.3382(16) Å, β = 91.820 ( 2 ) ∘ $91.820{(2)}^{\circ }$ , V = 1879.3(6) Å 3 , Z = 4, R g t ${R}_{gt}$ ( F ) = 0.0408, w R r e f $w{R}_{ref}$ ( F 2 ) = 0.1206, T = 296(2) K.
Open Access
Crystal structure of methyl ((4-aminobenzyl)sulfonyl)-L-prolinate, C₁₃H₁₈N₂O₄S

May 11, 2023

Zhen Wang, Feng-Lan Zhao, Gui-Ge Hou, Qing-Guo Meng

Page range: 725-727

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C 13 H 18 N 2 O 4 S, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 6.8619(2) Å, b = 12.0735(4) Å, c = 16.6591(5) Å, V = 1380.16(7) Å 3 , Z = 4, R gt ( F ) = 0.0236, wR ref ( F 2 ) = 0.0604, T = 150 K.
Open Access
Crystal structure of (E)-3-(3-methoxybenzylidene)benzofuran-2(3H)-one, C₁₆H₁₂O₃

May 15, 2023

Liang Liang Zheng, Xiong Li Liu, Zhang Chao Dong, Yang Shi, Bo Wen Pan, Ting Ting Feng

Page range: 729-731

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C 16 H 12 O 3 , monoclinic, P 2 1 / c (no. 14), a = 10.9636(14) Å, b = 12.1767(12) Å, c = 10.1557(13) Å, β = 116.588(16)°, V = 1212.4(3) Å 3 , Z = 4, R gt ( F ) = 0.0366, wR ref ( F 2 ) = 0.1019, T = 250.00(10) K.
Open Access
Synthesis and crystal structure (E)-1-(4-bromo-2-hydroxyphenyl)-3-(dimethylamino)prop-2-en-1-one, C₁₁H₁₂BrNO₂

May 16, 2023

Zhang-Chao Dong, Liang-Liang Zheng, Bo-Wen Pan, Yang Shi, Ying Zhou

Page range: 733-734

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C 11 H 12 BrNO 2 , monoclinic, P 2 1 / n (no. 14), a = 7.5143(12) Å, b = 11.8968(15) Å, c = 12.9852(13) Å, β = 105.575(14)°, V = 1118.2(3) Å 3 , Z = 4, R gt ( F ) = 0.0607, w R ref ( F 2 ) = 0.1615, T = 293.00(10) K.
Open Access
Synthesis and crystal structure of (S,E)-4-hydroxy-3-(2-((4aR,6aS,7R,10aS,10bR)-3,3,6a,10b-tetramethyl-8-methylenedecahydro-1H-naphtho[2,1-d][1,3]dioxin-7-yl)ethylidene)dihydrofuran-2(3H)-one, C₂₃H₃₄O₅

June 1, 2023

Shi-Qing Li, Jian Zhou, Zhang-Chao Dong, Bo Wen Pan, Yang Shi, Ying Zhou

Page range: 735-737

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C 23 H 34 O 5 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 11.1838(3) Å, b = 11.7824(3) Å, c = 16.3160(5) Å, V = 2149.99(10) Å 3 , Z = 4, R g t ${R}_{\mathrm{g}\mathrm{t}}$ ( F ) = 0.0399, w R r e f $w{R}_{\mathrm{r}\mathrm{e}\mathrm{f}}$ ( F 2 ) = 0.1097, T = 293 K.
Open Access
The crystal structure of N,N′-(1,2-phenylene)bis (2-((2-oxopropyl)selanyl)benzamide), C₂₆H₂₄N₂O₄Se₂

May 31, 2023

Shuxiao Feng, Xuan Zhong, Kaiyan Qi, Yafei Guo, Junling Wang, Guangna Gu, Junying Ma

Page range: 739-741

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C 26 H 24 N 2 O 4 Se 2 , monoclinic, C 2/ c (no. 15), a = 22.9092(7) Å, b = 5.8900(2) Å, c = 36.6209(9) Å, β = 91.983(3)°, V = 4938.5(3) Å 3 , Z = 8, R gt ( F ) = 0.0419, wR ref ( F 2 ) = 0.1162, T = 293 K.
Open Access
The crystal structure of 1-ethyl-2-nitro-imidazole oxide, C₅H₇N₃O₃

May 11, 2023

Yuan Jun, Wu Bingheng, Wang Yong, Wang Jianlong, Cao Duanlin, Chen Lizhen

Page range: 743-744

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C 5 H 7 N 3 O 3 , monoclinic, P 2 1 / n (no. 14), a = 8.7821(7) Å, b = 7.1320(5) Å, c = 11.6293(10) Å, β = 104.718 ( 3 ) ∘ $104.718{(3)}^{\circ }$ , V = 704.49(10) Å 3 , Z = 4, R g t ${R}_{gt}$ ( F ) = 0.0468, w R r e f $w{R}_{ref}$ ( F 2 ) = 0.1125, T = 170.0 K.
Open Access
The crystal structure of 2-(2-fluorophenyl)naphtho[2,1-d]thiazole, C₁₇H₁₀FNS

May 18, 2023

Xiaoming Zhu, Hongsheng Jin

Page range: 745-746

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C 17 H 10 FNS, monoclinic, P 2 1 / n (no. 14), a = 6.1859(2) Å, b = 10.7071(2) Å, c = 19.4475(4) Å, β = 95.794(2)°, V = 1281.49(5) Å 3 , Z = 4, R gt ( F ) = 0.0476, wR ref ( F 2 ) = 0.1333, T = 296 (2) K.
Open Access
Crystal structure of (E)-2,4-di-tert-butyl-6-(((2-fluorophenyl)imino) methyl)phenol, C₂₁H₂₆FNO

June 12, 2023

Wen-Ze Zhao, Huan Tian

Page range: 747-748

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C 21 H 26 FNO, orthorhombic, Pna 2 1 (no. 33), a = 12.329(3) Å, b = 9.048(3) Å, c = 16.881(5) Å, β = 90°, V = 1883.2(9) Å 3 , Z = 4, R gt ( F ) = 0.0500, wR ref ( F 2 ) = 0.1184, T = 273(2) K.
Open Access
Synthesis and crystal structure of 3-methyl-2-(methylthio)-4H-chromen-4-one, C₁₂H₁₂O₂S

May 24, 2023

Feng Liu, Yuming Zhang, Zhimeng Zhao, Yi Liu, Yang Chen, Tao Xiao

Page range: 749-750

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C 12 H 12 O 2 S, monoclinic, P 2 1 / c (no. 14), a = 7.4771(1) Å, b = 8.6860(1) Å, c = 16.0445(2) Å, β = 95.374 ( 1 ) ∘ $95.374{\left(1\right)}^{\circ }$ , V = 1037.45(2) Å 3 , Z = 4, R gt ( F ) = 0.0311, wR ref ( F 2 ) = 0.1156, T = 293(2) K.
Open Access
Crystal structure of dithieno[2,3-d:2′,3′-d′]benzo[1,2-b:4,5-b′]dithiophene-5,10-dione, C₁₄H₄O₂S₄

May 12, 2023

Yan Jia, Pengling Yu, Shihui Li, Yumei Zhao, Xiaoxin Zheng

Page range: 751-752

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C 14 H 4 O 2 S 4 , monoclinic, P 2 1 / n (no. 14), a = 3.85180(10) Å, b = 8.9728(2) Å, c = 18.0073(4) Å, β = 93.554(1)°, V = 621.16(3) Å 3 , Z = 2, R gt ( F ) = 0.0411, wR ref ( F 2 ) = 0.1091, T = 301(2) K.
Open Access
The crystal structure of dimethyl 2,2ʹ-((adamantane-1,3-diylbis(4,1-phenylene)) bis(oxy))diacetate, C₂₈H₃₂O₆

May 18, 2023

Xiao-Ming Chen, Fei Zeng

Page range: 753-755

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C 28 H 32 O 6 , orthorhombic, Pnma (no. 62), a = 7.752(2) Å, b = 29.959(8) Å, c = 10.176(3) Å, V = 2363.5(11) Å 3 , Z = 4, R gt ( F ) = 0.1145, w R ref ( F 2 ) = 0.1076, T = 296(2) K.
Open Access
The crystal structure of N-(6-chloro-2-methyl-2H-indazol-5-yl)acetamide, C₁₀H₁₀ClN₃O

June 1, 2023

Yi-Jing Du, Hong-Shun Sun, Jian-Qiang Wang, Cheng Guo

Page range: 757-758

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C 10 H 10 ClN 3 O, monoclinic, P 2 1 / c (no. 14), a = 4.7273(7) Å, b = 10.2148(16) Å, c = 21.283(3) Å, β = 91.458(4)°, V = 1027.4(3) Å 3 , Z = 4, R g t ${R}_{gt}$ ( F ) = 0.0623, w R r e f $w{R}_{ref}$ ( F 2 ) = 0.1287, T = 193 K.
Open Access
Crystal structure of triaqua-(5-bromoisophthalato-κ¹ O)-(2,2′-bipyridine-κ² N:N′)nickel(II) hydrate, C₁₈H₁₉BrN₂NiO₈

May 31, 2023

Zhen-Zhen Shi, Jun-Ling Chen

Page range: 759-761

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C 18 H 19 BrN 2 NiO 8 , monoclinic, P 2 1 / n (no. 14), a = 16.7861(4) Å, b = 7.0732(2) Å, c = 17.1041(4) Å, β = 102.674 ( 2 ) ° $102.674(2){}^{\circ}$ , V = 1981.31(9) Å 3 , Z = 4, R gt ( F ) = 0.0340, wR ref ( F 2 ) = 0.0670, T = 293(2) K.
Open Access
The crystal structure of 2-amino-4-carboxypyridin-1-ium perchlorate, C₆H₇ClN₂O₆

May 31, 2023

Tao Zhang, Yingchun Luo, Hailiang Hu

Page range: 763-764

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C 6 H 7 ClN 2 O 6 , triclinic, P 1̄ (no. 2), a = 5.3033(6) Å, b = 8.8875(10) Å, c = 10.3403(12) Å, α = 73.427 ( 10 ) ° $73.427(10){}^{\circ}$ , β = 85.158(10)°, γ = 73.284(10)°, V = 447.38(9) Å 3 , Z = 2, R gt ( F ) = 0.0370, wR ref ( F 2 ) = 0.0900, T = 292.99(10) K.
Open Access
The crystal structure of catena-poly[5-aminonicotinic acid-k¹ N-m₂-bromido-copper(I)], Cu(C₆N₂H₆O₂)Br

June 1, 2023

Nuo Chen, Qing-Hua Zheng, Wang Zhao, Wei-Wei Zhou

Page range: 765-766

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[Cu(C 6 N 2 H 6 O 2 )Br] n , monoclinic, P 2 1 / c (no. 14), a = 16.536(6) Å, b = 3.8463(14) Å, c = 14.403(6) Å, β = 115.009 ( 5 ) ∘ $115.009{(5)}^{\circ }$ , V = 830.2(6) Å 3 , Z = 4, R gt ( F ) = 0.0441, wR ref ( F 2 ) = 0.1054, T = 296 K.
Open Access
The crystal structure of 2,2-bis(3-methoxyphenyl)-1-tosyl-1,2-dihydro-2λ⁴,3λ⁴ -[1,3,2]diazaborolo[4,5,1-ij]quinoline - dichloromethane (1/1)

May 31, 2023

Siyi Ding

Page range: 767-769

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C 31 H 29 N 2 BO 4 Cl 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 1), a = 8.7365(3) Å, b = 11.9533(4) Å, c = 14.3566(5) Å, α = 85.7280(10)°, β = 74.8450(10)°, γ = 85.1990(10)°, V = 1439.88(9) Å 3 , Z = 2, R gt ( F ) = 0.0478, w R ref ( F 2 ) = 0.1176, T = 298 K.
Open Access
The crystal structure of catena-poly[bis(6-phenylpyridine-2-carboxylato-κ² N,O)-(μ₂-4,4′-bipyridne-κ² N:N)cadmium(II)], C₃₄H₂₄N₄O₄Cd

June 1, 2023

Liu Ping, Wang Li-Hua, Tai Xi-Shi

Page range: 771-773

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C 34 H 24 N 4 O 4 ${\mathrm{C}}_{34}{\mathrm{H}}_{24}{\mathrm{N}}_{4}{\mathrm{O}}_{4}$ Cd, monoclinic, C2 / c (no. 15), a = 17.5723(7) Å, b = 11.3574(4) Å, c = 15.8345(7) Å, β = 112.345 ( 5 ) ° $112.345(5){}^{\circ}$ , V = 2922.9(2)  Å 3 ${\mathrm{\mathring{\text{A}}}}^{3}$ , Z = 4, R g t ${R}_{gt}$ ( F ) = 0.0265, w R r e f $w{R}_{ref}$ ( F 2 ${F}^{2}$ ) = 0.0613, T = 200 K.
Open Access
The crystal structure of 5,7-dinitropyrazolo[5,1-b]quinazolin-9(4H)-one, C₁₀H₅N₅O₅

June 5, 2023

Shouwen Jin, Qiong Zhang, Yaoqi Zhen, Chengzhe Shi, Daqi Wang

Page range: 775-777

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C 10 H 5 N 5 O 5 , monoclinic, P 2 1 / c (no. 14), a = 10.9546(11) Å, b = 7.3433(8) Å, c = 13.2567(15) Å, β = 102.972 ( 5 ) ∘ $102.972{(5)}^{\circ }$ , V = 1039.19(19) Å 3 , Z = 4, R g t ${R}_{gt}$ ( F ) = 0.0630, w R r e f $w{R}_{ref}$ ( F 2 ) = 0.1622, T = 298 K.
Open Access
Crystal structure of rac-1,8-bis(2-carbamoylethyl)-5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane, C₂₂H₄₆N₆O₂

May 31, 2023

Pradip Paul, Sabina Yasmin, Saswata Rabi, Ismail M. M. Rahman, Edward R. T. Tiekink, Tapashi Ghosh Roy

Page range: 779-781

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C 22 H 46 N 6 O 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.5777(3) Å, b = 9.0205(4) Å, c = 9.9270(3) Å, α = 67.899 ( 3 ) ° $67.899(3){}^{\circ}$ , β = 71.106 ( 3 ) ° $71.106(3){}^{\circ}$ , γ = 63.774 ( 4 ) ° $63.774(4){}^{\circ}$ , V = 626.83(5) Å 3 , Z = 1, R g t ${R}_{\mathit{g}\mathit{t}}$ ( F ) = 0.0400, w R r e f $w{R}_{\mathit{r}\mathit{e}\mathit{f}}$ ( F 2 ) = 0.1162, T = 298(2) K.
Open Access
The crystal structure of (E)-N ^′-(2-bromobenzylidene)-2-naphthohydrazide, C₃₆H₂₆Br₂N₄O₂

June 1, 2023

Lin Yuan, Shao-Wen Deng, Fang Liu, Zhong-Yan Li

Page range: 783-785

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C 36 H 26 Br 2 N 4 O 2 , triclinic, P 1 (no. 1), a = 8.700(5) Å, b = 9.188(5) Å, c = 9.722(6) Å, α = 91.610(6)°, β = 91.436(6)°, γ = 100.925(6)°, V = 762.4(8) Å 3 , Z = 1, R g t ${R}_{\mathrm{g}\mathrm{t}}$ ( F ) = 0.0381, w R r e f $w{R}_{\mathrm{r}\mathrm{e}\mathrm{f}}$ ( F 2 ) = 0.1016, T = 296(2) K.
Open Access
The crystal structure of 5-nitronaphthoquinone, C₁₀H₅NO₄

May 31, 2023

Claudio Barrientos, Antonio Galdámez, Silvana Moris

Page range: 787-789

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C 10 H 5 NO 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 9.2564(8) Å, b = 11.0464(9) Å, c = 14.8016(12) Å, α = 110.132 ( 2 ) ∘ $110.132{(2)}^{\circ }$ , β = 106.157 ( 3 ) ∘ $106.157{(3)}^{\circ }$ , γ = 94.770 ( 3 ) ∘ $94.770{(3)}^{\circ }$ , V = 1337.7(2) Å 3 , Z = 6, R g t ${R}_{\mathit{g}\mathit{t}}$ ( F ) = 0.0567, w R r e f $w{R}_{\mathit{r}\mathit{e}\mathit{f}}$ ( F 2 ) = 0.1797, T = 296.15 K
Open Access
The crystal structure of (S, R _p)-4–benzhydrylideneamino-12-(4-tert-butyl oxazolin-2-yl)[2.2]paracyclophane, C₃₆H₃₆N₂O

June 7, 2023

Zhen Chen, Yanwen Sun, Chao Chen, Nuo Xu, Xiaozhong Wang, Sijun Li

Page range: 791-793

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C 36 H 36 N 2 ${\mathrm{C}}_{36}{\mathrm{H}}_{36}{\mathrm{N}}_{2}$ O, orthorhombic, P 2 1 2 1 2 1 ${2}_{1}{2}_{1}{2}_{1}$ (no. 19), a = 11.849(2) Å, b = 14.373(3) Å, c = 17.183(3) Å, V = 2926.4(10)  Å 3 ${\mathrm{\mathring{\text{A}}}}^{3}$ , Z = 4, R g t ${R}_{\mathrm{g}\mathrm{t}}$ ( F ) = 0.0514, w R r e f ${R}_{\mathrm{r}\mathrm{e}\mathrm{f}}$ ( F 2 ${F}^{2}$ ) = 0.1272, T = 296(2) K.
Open Access
Synthesis and crystal structure of 2-(2-oxo-2-(o-tolyl)ethyl)-4H-chromen-4-one, C₁₈H₁₄O₃

June 1, 2023

Yi Liu, Zhimeng Zhao, Yuming Zhang, Feng Liu, Yang Chen, Tao Xiao

Page range: 795-796

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C 18 H 14 O 3 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 7.75390(10) Å, b = 8.26060(10) Å, c = 11.6271(2) Å, α = 86.877 ( 1 ) ∘ $86.877{(1)}^{\circ }$ , β = 78.944 ( 1 ) ∘ $78.944{(1)}^{\circ }$ , γ = 68.908 ( 1 ) ∘ $68.908{(1)}^{\circ }$ , V = 681.861(18) Å 3 , Z = 2, R g t ${R}_{gt}$ ( F ) = 0.0518, w R r e f $\mathrm{w}{R}_{ref}$ ( F 2 ) = 0.1606, T = 293(2) K.
Open Access
Crystal structure of 2-(thiazol-2-yl)hexahydro-1H-4,7-epoxyisoindole-1,3(2H)-dione, C₁₁H₁₀N₂O₃S

June 5, 2023

Qinglong Wang, Xuehui Hou

Page range: 797-798

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C 11 H 10 N 2 O 3 S, monoclinic, Cm (no. 8), a = 10.8483(7) Å, b = 9.3377(8) Å, c = 5.4086(3) Å, β = 95.398(6)°, V = 545.45(7) Å 3 , Z = 2, R gt ( F ) = 0.0576, wR ref ( F 2 ) = 0.1429, T = 293(2) K.
Open Access
Crystal structure of N-(diaminomethylene)-1-(dimethylamino)-1-iminiomethanaminium dichloride, C₄H₁₃Cl₂N₅

June 7, 2023

Yu-Pei Xia

Page range: 799-800

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C 4 H 13 Cl 2 N 5 , monoclinic, P 2 1 (no. 4), a = 7.1868(6) Å, b = 5.8408(4) Å, c = 12.6534(11) Å, β = 105.134 ( 2 ) ∘ $105.134{(2)}^{\circ }$ , V = 512.73(7) Å 3 , Z = 2, R gt ( F ) = 0.0354, wR ref ( F 2 ) = 0.0961, T = 298 K.
Open Access
Crystal structure of poly[(μ₃-3, 5-dichloro-2-hydroxy-benzoato-κ⁴ Cl,O:O′:O″) silver(I)], C₇H₃AgCl₂O₃

June 5, 2023

Jin-Ke Jiang, Chun-Yan Niu

Page range: 801-802

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C 7 H 3 AgCl 2 O 3 , monoclinic, P 2 1 / c (no. 14), a = 13.1492(5) Å, b = 3.72760(10) Å, c = 16.5625(6) Å, β = 92.1810(10)°, V = 811.22(5) Å 3 , Z = 4, R gt (F) = 0.0229, w R ref ( F 2 ) = 0.0492, T = 301(2) K.
Open Access
The crystal structure of tetrakis(1-isopropylimidazole-κ¹ N)-[μ₂- imidazole-4,5-dicarboxylato-κ⁴ O,N,O′,N′)]- trioxido-divanadium, C₂₉H₄₁N₁₀O₇V₂

June 7, 2023

Xiang-Yu Ren, Xiao-Jie Wang, Yu-Cai Qin, Yue Tong

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C 29 H 41 N 10 O 7 V 2 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 11.3461(5) Å, b = 12.7013(5) Å, c = 14.0649(5) Å, α = 111.609 ( 1 ) ∘ $111.609{(1)}^{\circ }$ , β = 108.702 ( 1 ) ∘ $108.702{(1)}^{\circ }$ , γ = 93.957 ( 2 ) ∘ $93.957{(2)}^{\circ }$ , V = 1744.20(12) Å 3 , Z = 2, R gt ( F ) = 0.0439, wR ref ( F 2 ) = 0.1160, T = 173 K.
Open Access
Crystal structure of catena-[(μ₃-bromido)-(1H-1,2,4-triazol-1-yl)benzoato-κ¹ N)copper(I)], C₉H₇BrCuN₃O₂

June 7, 2023

Zhi-Min Yuan, Yu-Pei Xia

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C 9 H 7 BrCuN 3 O 2 , triclinic, P 1̄ (no. 2), a = 3.8736(3) Å, b = 7.5238(7) Å, c = 18.1555(19) Å, α = 84.581(1)°, β = 88.166 ( 2 ) ° $88.166(2){}^{\circ}$ , γ = 81.551(1)°, V = 520.96(8) Å 3 , Z = 2, R gt ( F ) = 0.0344, wR ref ( F 2 ) = 0.0845, T = 298(2) K.
Open Access
The crystal structure of (E)-4-fluoro-N′-(1-(2-hydroxyphenyl)propylidene)benzohydrazide, C₁₆H₁₅FN₂O₂

June 20, 2023

Xiaohua Li, Xin Zhao, Wenqiang Tang

Page range: 809-811

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C 16 H 15 FN 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 14.6825(16) Å, b = 11.7155(11) Å, c = 8.8285(7) Å, β = 102.753(10)°, V = 1481.2(2) Å 3 , Z = 4, R gt (F) = 0.0670 wR ref ( F 2 ) = 0.1669, T = 293 K.

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