Zeitschrift für Kristallographie - New Crystal Structures

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Zeitschrift für Kristallographie - New Crystal Structures

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Zeitschrift für Kristallographie - New Crystal Structures

Contents

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Frontmatter

December 26, 2022

Page range: i-vi

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New Crystal Structures
Open Access
Crystal structure of undecacalcium decaarsenide, Ca₁₁As₁₀

October 11, 2022

Andrea V. Hoffmann, Viktor Hlukhyy, Thomas F. Fässler

Page range: 1-3

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Ca 11 As 10 , tetragonal, I 4/ mmm (no. 139), a = 11.2532(1) Å, c = 16.2351(4) Å, and V = 2055.92(6) Å 3 , Z = 4, R gt ( F ) = 0.0347, wR ref ( F 2 ) = 0.0931, T = 150 K.
Open Access
Crystal structure of catena-poly[diiodido-(μ₂-1,5-dimethyl-2-phenyl-4-((pyridin-4- ylmethylene)amino)-1,2-dihydro-3H -pyrazol-3-one-κ² N: O)zinc(II)], C₁₇H₁₆I₂N₄OZn

November 1, 2022

Ben Li, Yujiao Huang, Weicheng Qian, Haixia Pang, Qiang Tang

Page range: 5-7

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C 17 H 16 I 2 N 4 OZn, monoclinic, P 2 1 / n , a = 7.4827(5) Å, b = 14.9521(10) Å, c = 18.2838(13) Å, β = 99.251(1)°, V = 2019.0(2) Å 3 , Z = 4, R gt ( F ) = 0.0404, wR ref ( F 2 ) = 0.787, T = 298 K.
Open Access
The crystal structure of 5,10,15,20-tetrakis(4-(tert-butyl)phenyl)porphyrin-21,23-diido-κ⁴ N ⁴-naphthalocyanido-κ⁴ N ⁴-neodymium(IV) - chloroform (1/6) C₁₁₄H₉₀N₁₂Cl₁₈Nd

November 1, 2022

Yang Liguo, Wang Xin, Fu Jiaqi, Ji Xinyu

Page range: 9-12

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C 114 H 90 N 12 Cl 18 Nd, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 17.3389(7) Å, b = 18.7671(5) Å, c = 19.1454(8) Å, α = 79.600(3)°, β = 68.752(4)°, γ = 68.572(3)°, V = 5396.7(4) Å 3 , Z = 2, R gt ( F ) = 0.0722, wR ref ( F 2 ) = 0.1979, T = 298 K.
Open Access
The crystal structure of 1-(4-bromophenyl)-3-(2-chlorobenzyl)urea, C₁₄H₁₂BrClN₂O

November 4, 2022

Zhihong Zhu, Lilei Zhang

Page range: 13-14

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C 14 H 12 BrClN 2 O, monoclinic, P 2 1 / c (no. 14), a = 13.4072(6) Å, b = 8.6103(5) Å, c = 12.3824(6) Å, β = 100.475(4), V = 1405.60(12) Å 3 , Z = 4, R gt ( F ) = 0.0499, wR ref ( F 2 ) = 0.1215, T = 173 K.
Open Access
Crystal structure of bis[benzyl(methyl)carbamodithioato-κ ² S,S′]-di-n-butyltin(IV), C₂₆H₃₈N₂S₄Sn

October 24, 2022

Nurul Amalina Abd Aziz, Normah Awang, Kok Meng Chan, Nurul Farahana Kamaludin, Nur Najmi Mohamad Anuar, Nur Atiyah Nadhrah Jamaludin, Yee Seng Tan, Edward R. T. Tiekink

Page range: 15-18

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C 26 H 38 N 2 S 4 Sn, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 9.6272(1) Å, b = 12.1043(2) Å, c = 13.3584(2) Å, α = 82.296(1)°, β = 86.611(1)°, γ = 66.912(1)°, V = 1419.02(4) Å 3 , Z = 2, R gt ( F ) = 0.0235, wR ref ( F 2 ) = 0.0612, T = 100 K.
Open Access
Crystal structure of (E)-3-(2-(4-(diethylamino)-2-hydroxystyryl)-3,3-dimethyl-3H-indol-1-ium-1-yl)propane-1-sulfonate – methanol (1/2), C₂₅H₃₂N₂O₄S⋅2CH₃OH

November 1, 2022

Wen-Ze Zhao

Page range: 19-21

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C 27 H 40 N 2 O 6 S, monoclinic, P 2 1 / c (no. 14), a = 11.2654(15) Å, b = 21.630(3) Å, c = 12.2868(17) Å, β = 111.422(3)°, V = 2787.1(7) Å 3 , Z = 4, R gt ( F ) = 0.0493, w R ref ( F 2 ) = 0.1313, T = 198(2) K.
Open Access
Synthesis and crystal structure of {(N′,N″-(((ethane-1,2-diylbis(oxy))bis(2,1-phenylene))-bis(methaneylylidene))bis(2-hydroxybenzohydrazonato)-κ⁶ N ² O ⁴}copper(II), C₃₀H₂₄CuN₄O₆

November 1, 2022

Jie-Qiong Cai

Page range: 23-25

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C 30 H 24 CuN 4 O 6 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 10.8014(2) Å, b = 10.8211(2) Å, c = 13.4530(3) Å, α = 100.308(1)°, β = 113.075(1)°, γ = 99.989(1)°, Z = 2, V = 1370.76(5) Å 3 , R gt ( F ) = 0.0365, wR ref ( F 2 ) = 0.0937, T = 297 K.
Open Access
The crystal structure of ((E)-2,4-dibromo-6-(((5-(nitro)-2-oxidophenyl)imino)methyl)phenolato-κ ³ N,O,O′)tris(pyridine-κN)manganese(II), C₂₈H₂₁Br₂MnN₅O₄

October 28, 2022

Ting Li, Keying Qiu, Yuxing Tan, Wujiu Jiang

Page range: 27-29

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C 28 H 21 Br 2 MnN 5 O 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.9193(14) Å, b = 9.2271(15) Å, c = 17.933(3) Å, α = 103.574(2)°, β = 91.518(2)°, γ = 98.762(2)°, V = 1415.0(4) Å 3 , Z = 2, R gt ( F ) = 0.0347, wR ref ( F 2 ) = 0.0864, T = 296(2) K.
Open Access
Synthesis and crystal structure of 1-((3R,10S,13R,17S)-10,13-dimethyl-3-(p-tolylamino)hexadecahydro-1H-cyclopenta-[a]phenanthren-17-yl)ethan-1-one, C₂₈H₄₁NO

November 1, 2022

Hua Huang, Wen-Wen Zhang, Jiang-Hai Ye, Juan Zou, Kang He

Page range: 31-33

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C 28 H 41 NO, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 10.5758(10) Å, b = 12.3659(9) Å, c = 18.0301(16) Å, V = 2358.0(4) Å 3 , Z = 4, R gt ( F ) = 0.0524, wR ref ( F 2 ) = 0.1220, T = 273(2) K.
Open Access
The crystal structure of 3-nitrobenzene-1,2-dicarboxylic acid—pyrazine-2-carboxamide(1/1), C₁₃H₁₀N₄O₇

November 1, 2022

Cheng-Jun Jiang, Die Cheng, Ying-Fan Xia, Jia-rong Zhang, Shu-ting Lin

Page range: 35-37

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C 13 H 10 N 4 O 7 , monoclinic, P 2 1 / n (no. 14), a = 10.7017(7) Å, b = 7.1240(5) Å, c = 19.0878(13) Å, β = 99.280(3)°, V = 1436.19(17) Å 3 , Z = 4, R gt ( F ) = 0.0586, wR ref ( F 2 ) = 0.1746, T = 296.15 K.
Open Access
Crystal structure of poly[tetrakis(μ₃-2-aminonicotinato-κ³N,O,O′)-(μ₂-oxalato-κ⁴ O,O′:O″,O′″)-(μ₄-oxalato-κ⁶ N:N′:O,O′:O″,O′″)dicopper(I)-disamarium(III)], [SmCu(C₆N₂H₅O₂)₂(C₂O₄)]_n

November 1, 2022

Wei-Wei Zhou, Wang Zhao, Jing Wang, Ming-Jun Song

Page range: 39-41

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[SmCu(C 6 N 2 H 5 O 2 ) 2 (C 2 O 4 )] n , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 9.457(6) Å, b = 9.482(4) Å, c = 11.013(4) Å, α = 75.87(4)°, β = 89.853(12)°, γ = 62.786(11)°, V = 844.8(7) Å 3 , Z = 2, R gt ( F ) = 0.0292, wR ref ( F 2 ) = 0.0691, T = 296 K.
Open Access
The crystal structure of 2,3,4-trihydroxybenzoic- acid—pyrazine-2-carboxamide—water (1/1/1), C₁₂H₁₃N₃O₇

November 1, 2022

Cheng-Jun Jiang, Zhi-Hua Wang, Ying-Fan Xia, Chao-Feng Li, Shu-ting Lin, Jia-rong Zhang

Page range: 43-44

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C 12 H 13 N 3 O 7 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 6.9878(9) Å, b = 7.0956(8) Å, c = 13.8113(15) Å, α = 88.745(5)°, β = 87.764(5)°, γ = 75.785(5)°, V = 663.27(14) Å 3 , Z = 2, R gt ( F ) = 0.0455, wR ref ( F 2 ) = 0.1264, T = 296.15 K.
Open Access
Crystal structure of N-ethyl-4-[3-(trifluoromethyl)-phenyl]piperazine-1-carbothioamide, C₁₄H₁₈F₃N₃S

October 28, 2022

Lamya H. Al-Wahaibi, Olivier Blacque, Nora H. Al-Shaalan, Edward R. T. Tiekink, Ali A. El-Emam

Page range: 45-47

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C 14 H 18 F 3 N 3 S, monoclinic, P 2 1 / c (no. 14), a = 4.61919(4) Å, b = 29.1507(3) Å, c = 11.27803(10) Å, β = 94.4768(8)°, V = 1513.99(3) Å 3 , Z = 4, R gt ( F ) = 0.0588, wR ref ( F 2 ) = 0.1579, T = 160 K.
Open Access
The crystal structure of 3-anilino-1,4-diphenyl-4H-1,2,4-triazol-1-ium iodide, C₂₀H₁₇N₄I

November 1, 2022

Hon Man Lee, Hsiu-Yu Hung

Page range: 49-50

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C 20 H 17 N 4 I, monoclinic, P 2 1 / n (no. 14), a = 7.304(3) Å, b = 14.830(7) Å, c = 16.482(7) Å, β = 98.202(12)°, V = 1767.2(14) Å 3 , Z = 4, R gt ( F ) = 0.0568, wR ref ( F 2 ) = 0.1359, T = 150 K.
Open Access
The crystal structure of (tris(2-benzimidazolylmethyl)amine)-benzoato-copper(II) perchlorate monohydrate, CuC₃₁H₂₈N₇O₇Cl

October 28, 2022

Ji Li, Mingzhi Miao

Page range: 51-53

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CuC 31 H 28 N 7 O 7 Cl, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 10.1386(6) Å, b = 12.1155(8) Å, c = 14.1972(8) Å, α = 100.297(2)°, β = 98.411(2)°, γ = 112.744(2)°, V = 1536.78(16) Å 3 , Z = 2, R gt ( F ) = 0.0613, wR ref ( F 2 ) = 0.1519, T = 250(2) K.
Open Access
Crystal structure of [2-hydroxy-3-methyl-benzoato-k¹ O-triphenyltin(IV)], C₂₆H₂₂O₃Sn

November 1, 2022

Shaoliang Zhang, Shanshan Li

Page range: 55-56

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C 26 H 22 O 3 Sn, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 10.8480(9) Å, b = 11.3511(11) Å, c = 11.4109(12) Å, α = 114.431(3)°, β = 96.994(2)°, γ = 108.207(3)°, V = 1162.94(19) Å 3 , Z = 2, R gt ( F ) = 0.0357, wR ref ( F 2 ) = 0.0667, T = 298 K.
Open Access
Crystal structure of diaqua-bis(4-(hydroxymethyl)-benzoato-k¹ O)zinc(II), C₁₆H₁₈O₈Zn

November 1, 2022

Yujiao Huang, Ben Li, Siyi Miao, Linhui Luo, Haixia Pang, Qiang Tang

Page range: 57-59

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C 16 H 18 O 8 Zn, monoclinic, I 2/ a (no. 15), a = 12.152(2) Å, b = 5.0051(8) Å, c = 27.273(5) Å, β = 101.536(7)°, V = 1625.3(5) Å 3 , Z = 4, R gt ( F ) = 0.052, w R ref ( F 2 ) = 0.143, T = 296 K.
Open Access
The crystal structure of dicarbonyl-(N-nitroso-N-oxido-phenylamine-κ ² O,O)-rhodium(I), C₈H₅N₂O₄Rh

November 10, 2022

Mohammed A. Elmakki, Wesley Abdul Gafoor, Orbett T. Alexander, Johan A. Venter, Andreas Roodt

Page range: 61-63

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C 8 H 5 N 2 O 4 Rh, monoclinic, P 2 1 / c (no. 14), a = 14.1998(9) Å, b = 3.6516(2) Å, c = 17.7458(11) Å, β = 92.801(2)°, V = 919.06(10) Å 3 , Z = 4, R gt ( F ) = 0.0281, wR ref ( F 2 ) = 0.0702, T = 100 K.
Open Access
The crystal structure of oxalic acid – 2-ethoxybenzamide (2/1), C₂₀H₂₄N₂O₈

December 1, 2022

Ying-Fan Xia, Shu-Ting Lin, Jia-Rong Zhang, Cheng-Jun Jiang

Page range: 65-67

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C 20 H 24 N 2 O 8 , monoclinic, P 2 1 / n (no. 14), a = 3.8981(3) Å, b = 16.0675(11) Å, c = 16.2908(10) Å, β = 94.537(3)°, V = 1017.14(12) Å 3 , Z = 2, R gt ( F ) = 0.0634, wR ref ( F 2 ) = 0.1746, T = 170 K.
Open Access
The crystal structure of ethyl 7-ethyl-5-methyl-4,7-dihydrotetrazolo[1,5-a]pyrimidine-6-carboxylate, C₁₀H₁₅N₅O₂

November 10, 2022

Wenxiang Wang, Jiahui Mou, Yue Sun

Page range: 69-70

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C 10 H 15 N 5 O 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.0501(16) Å, b = 8.6163(17) Å, c = 9.6654(19) Å, α = 69.74(3)°, β = 75.79(3)°, γ = 87.43(3)°, V = 609.1(2) Å 3 , Z = 2, R gt ( F ) = 0.0593, w R ref ( F 2 ) = 0.1821, T = 293 K.
Open Access
Crystal structure of poly[(N,N-dimethylacetamide-κO) (μ₄-2-nitroisophthalato-κ ⁴ O:O′:O″:O′″)manganese(II)], C₁₁H₁₀N₂O₇Mn

November 16, 2022

Xiao-Ming Shi, Yu-Jia Fu, Zhi-Chao Zhang

Page range: 71-73

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C 11 H 10 N 2 O 7 Mn, monoclinic, P 2 1 / c (no. 14), a = 8.1501(5) Å, b = 10.8198(7) Å, c = 15.2391(9) Å, β = 91.921(5)°, V = 1343.07(14) Å 3 , Z = 4, R gt ( F ) = 0.0363, wR ref ( F 2 ) = 0.0783, T = 293 K.
Open Access
Crystal structure of 14-O-acetyldelcosine, C₂₆H₄₁NO₈

November 21, 2022

Huan-Ni Liu, Yi-Kun Hao, Neng-Hua Chen, Lai-Ming Li

Page range: 75-77

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C 26 H 41 NO 8 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 8.24370(10) Å, b = 13.1867(2) Å, c = 22.8490(4) Å, V = 2483.85(6) Å 3 , Z = 4, R gt ( F ) = 0.0357, wR ref ( F 2 ) = 0.0975, T = 169.99(10) K.
Open Access
The crystal structure of poly[(1,10-phenanthroline-κ² N,N′)-(μ ₄-2-chlorobenzene-1,3-dicarboxylato-κ⁵ O:O′:O″:O‴) cadmium(II)] monohydrate, C₂₀H₁₃CdClN₂O₅

November 24, 2022

Guang Huang

Page range: 79-81

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C 20 H 13 CdClN 2 O 5 , monoclinic, P 2 1 / n (no. 14), a = 11.4994(9) Å, b = 13.1171(10) Å, c = 13.0233(10) Å, β = 109.126(8)°, V = 1856.0(3) Å 3 , Z = 4, R gt ( F ) = 0.0341, wR ref ( F 2 ) = 0.0779, T = 293 K.
Open Access
Crystal structure of propane-1,3-diylbis(diphenylphosphine sulfide) ethanol solvate, C₂₇H₂₆P₂S₂

November 21, 2022

Kgaugelo C. Tapala, Hadley S. Clayton

Page range: 83-85

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C 27 H 26 P 2 S 2 , tetragonal, I 4 (no. 79), a = 16.9196(12) Å, c = 9.4187(8) Å, V = 2696.3(4) Å 3 , Z = 4, R gt ( F ) = 0.0341, wR ref ( F 2 ) = 0.0726, T = 173(2) K.
Open Access
Crystal structure of bis{[(4-diethylamino-2-hydroxy-benzylidene)-hydrazinocarbonylmethyl]-trimethylammonium} tetrabromozincate, C₃₂H₅₄N₈O₄ZnBr₄

November 25, 2022

Shi-Lin Zhang

Page range: 87-89

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C 32 H 54 N 8 O 4 ZnBr 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.250(5) Å, b = 12.289(10) Å, c = 20.954(14) Å, α = 82.36(2)°, β = 81.977(14)°, γ = 86.96(2)°, V = 2084(2) Å 3 , Z = 2, R gt ( F ) = 0.0525, w R ref ( F 2 ) = 0.1419, T = 150(2) K.
Open Access
Synthesis and crystal structure of dimethyl 2,2′-(2,5-bis(4-hydroxyphenyl)-2,5-dihydrofuran-3,4-diyl)dibenzoate, C₃₄H₃₀O₇

November 18, 2022

Yun-Yee Low, Siew-Huah Lim

Page range: 91-93

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C 34 H 30 O 7 , monoclinic, C 2/ c (no. 15), a = 29.4446(6) Å, b = 12.4393(3) Å, c = 14.9807(3) Å, β = 90.390(1)°, V = 5486.9(2) Å 3 , Z = 8, R gt ( F ) = 0.0408, w R ref ( F 2 ) = 0.1023, T = 100 K.
Open Access
Synthesis and crystal structure of 2-(2-oxo-2-phenylethyl)-4H-chromen-4-one, C₁₇H₁₂O₃

November 22, 2022

Feng Liu, Yi Liu, Yang Chen, Xiaolong Yan, Tao Xiao

Page range: 95-96

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C 17 H 12 O 3 , monoclinic, P 2 1 / c (no. 14), a = 9.2911(15) Å, b = 17.525(3) Å, c = 8.5586(15) Å, β = 109.358(7)° V = 1314.8(4) Å 3 , Z = 4, R gt ( F ) = 0.0550, w R ref ( F 2 ) = 0.1789, T = 296(2) K.
Open Access
The crystal structure of tetra(imidazole-κ¹ N)zinc(II) μ₂-oxido-hexaoxido-divanadium(VI) C₁₂H₁₆N₈O₆V₂Zn

November 17, 2022

Yueyang Huo, Shiqi Fu, Yanqi Shi, Yingying Duan, Meiyu Zhang

Page range: 97-99

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C 12 H 16 N 8 O 6 V 2 Zn, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 9.5397(4) Å, b = 10.2457(4) Å, c = 11.0920(4) Å, α = 92.848(1)°, β = 110.314(1)°, γ = 94.421(1)°, V = 1010.29(7) Å 3 , Z = 2, R gt ( F ) = 0.0358, wR ref ( F 2 ) = 0.0932, T = 293 K.
Open Access
Crystal structure of S-2-(1-(5-methylpyridin-2-ylamino)octyl)-3-hydroxynaphthalene-1,4-dione, C₂₄H₂₈N₂O₃

November 16, 2022

Qing-Gang Chen, Wei Wan, Guo-Ying Peng, Chang-gan Huang

Page range: 101-103

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[C 24 H 28 N 2 O 3 ], monoclinic, P 12 1 / n , a = 12.8878(5) Å, b = 27.5641(11) Å, c = 13.0517(6) Å, β = 111.908(2) ∘ , V = 4301.7(3) Å 3 , Z = 4, R gt ( F ) = 0.0576, wR ref ( F 2 ) = 0.1749, T = 296(2) K.
Open Access
Crystal structure of bis(μ₂-5-chloro-2-oxido-N-(1-oxido-2-oxo-2-phenylethylidene)-benzohydrazonato-κ⁵ N,O,O′:N′,O′′)-oktakis(pyridine-κ¹ N)trinickel(II) – methanol – pyridine (1/1/1) C₇₆H₆₅N₁₃C_l2Ni₃O₉

November 18, 2022

Zhou Zhongyuan, Yang Liguo, Zou Kun, Fu Jiaqi, Ji Xinyu

Page range: 105-108

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C 76 H 65 N 13 Cl 2 Ni 3 O 9 , monoclinic, P 2 1 / n , a = 15.937(4) Å, b = 16.805(4) Å, c = 27.463(7) Å, β = 94.613(3)°, V = 7332(3) Å 3 , Z = 4, R gt ( F ) = 0.0490, wR ref ( F 2 ) = 0.1596, T = 298 K.
Open Access
The crystal structure of methyl 3,5-diaminobenzoate, C₈H₁₀N₂O₂

December 14, 2022

John M. Gardiner, James Raftery, Ian G. Beadham, Jannat N. Azarah, Mohammed Y. Abu-Foul, Adel M. Awadallah, Rami Y. Morjan

Page range: 109-110

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C 8 H 10 N 2 O 2 , orthorhombic, Pbca (no. 61), a = 11.0571(2) Å, b = 8.1172(2) Å, c = 17.6080(4) Å, V = 1580.37(6) Å 3 , Z = 8, R gt ( F ) = 0.0324, wR ref ( F 2 ) = 0.0872, T = 100(2) K.
Open Access
Crystal structure of 10-(9H-carbazol-9-yl)-5H-dibenzo[a,d][7]annelen-5-one, C₂₇H₁₇NO

December 14, 2022

Yunlu Li, Xinzhong Wang

Page range: 111-112

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C 27 H 17 NO, monoclinic, P 2 1 (no. 4), a = 9.8945(6) Å, b = 8.1838(5) Å, c = 12.2042(7) Å, β = 107.539(6)°, V = 942.29(10) Å 3 , Z = 2, R gt ( F ) = 0.0306, wR ref ( F 2 ) = 0.0698, T = 149.99(10)
Open Access
Crystal structure of ethyl 1-(2-hydroxyethyl)-4-((4-methoxyphenyl)amino)-5-oxo-2,5-dihydro-1H-pyrrole-3-carboxylate, C₁₆H₂₀N₂O₅

December 13, 2022

Fatin Nur Ain Abdul Rashid, Muhamad Zulfaqar Bacho, Alexandra M. Z. Slawin, Mohd Abdul Fatah Abdul Manan, Saiful Azmi Johari, Mohd Fazli Mohammat

Page range: 113-115

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C 16 H 20 N 2 O 5 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 7.9179(7) Å, b = 10.1982(9) Å, c = 10.4144(8) Å, α = 76.184(7)°, β = 87.090 (7)°, γ = 73.500(8)°, V = 782.86(12) Å 3 , Z = 2, R gt ( F ) = 0.0458, w R ref ( F 2 ) = 0.1333, T = 93 K.
Open Access
The crystal structure of 1-(4-bromophenyl)-3-cycloheptylurea, C₁₄H₁₉BrN₂O

December 14, 2022

Kai Gao, Su-E. Zha, Chang-Ying Liu, Qiao-Juan Wang, Er-Qiang Wang

Page range: 117-118

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C 14 H 19 BrN 2 O, monoclinic, P 2 1 / c (no. 14), a = 12.9782(8) Å, b = 9.1447(6) Å, c = 11.8842(8) Å, β = 98.214(6)°, V = 1395.97(16) Å 3 , Z = 4, R gt ( F ) = 0.0637, wR ref ( F 2 ) = 0.1876, T = 293 K.
Open Access
The crystal structure of 1,4-bis(1,2,3,4,5-pentamethylcyclopenta-2,4-dien-1-yl)-3,6-bis ((4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methylene)-1,4-dialuminacyclohexane – benzene (1/2), C₅₀H₇₂Al₂B₂O₄

December 14, 2022

Bing Wang, Bo-Han Hu, Di Wu

Page range: 119-121

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C 50 H 72 Al 2 B 2 O 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.7261(2) Å, b = 11.1827(3) Å, c = 13.8599(4) Å, α = 112.7800(10)°, β = 102.5410(10)°, γ = 93.8340(10)°, V = 1199.98(6) Å 3 , Z = 1, R gt ( F ) = 0.0365, wR ref ( F 2 ) = 0.1037, T = 170 K.
Open Access
Crystal structure of bis(μ ₃-diphenylphosphinato)-tetrakis(μ ₂-diphenylphosphinato)-bis(diphenylphosphinato)-bis(μ ₂-hydroxo)dicopper(II)-ditin(IV), C₁₀₄H₁₀₀O₁₈P₈Cu₂Sn₂

December 5, 2022

Sun Xiaolin, Guo Yuhua, Yu Youzhu

Page range: 123-125

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C 104 H 100 O 18 P 8 Cu 2 Sn 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 13.8254(6) Å, b = 14.1283(6) Å, c = 15.1940(7) Å, α = 112.571(1)°, β = 104.707(1)°, γ = 104.433(1)°, V = 2442.87(19) Å 3 , Z = 1, R gt ( F ) = 0.0256, wR ref ( F 2 ) = 0.0955, T = 296(2) K.
Open Access
Crystal structure of 3-((3,4-dichloroisothiazol-5-yl)methoxy)benzo[d] isothiazole 1,1-dioxide, C₁₁H₆Cl₂N₂O₃S₂

December 14, 2022

Huang Cong, Xiao Shu-Zhen, Zhong Liang, Chen Shang-Xing, Peng Da-Yong

Page range: 127-128

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C 11 H 6 Cl 2 N 2 O 3 S 2 , triclinic, P 1‾ (no. 2), a = 6.974(3) Å, b = 8.132(3) Å, c = 12.349(5) Å, α = 86.123(4)°, β = 78.299(4)°, γ = 85.715(4)°, V = 682.9(4) Å 3 , Z = 2, R gt ( F ) = 0.0410, wR ref ( F 2 ) = 0.1058, T = 296(2) K.
Open Access
Synthesis and crystal structure of 2-(2-(2-fluorophenyl)-2-oxoethyl)-4H-chromen-4-one, C₁₇H₁₁FO₃

December 2, 2022

Yi Liu, Feng Liu, Yang Chen, Xiaolong Yan, Tao Xiao

Page range: 129-131

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C 17 H 11 FO 3 , monoclinic, P 2 1 / c (no. 14), a = 9.1987(2) Å, b = 17.5458(3) Å, c = 8.5802(2) Å, β = 108.193(3)°, V = 1315.60(5) Å 3 , Z = 4, R gt ( F ) = 0.0346, wR ref ( F 2 ) = 0.1196, T = 293(2) K.
Open Access
The crystal structure of tris(carbonyl)-bis(carbonyl)-[μ-propane-1,2- dithiolato]-(benzyldiphenylphosphine)diiron (Fe—Fe), C₂₇H₂₃Fe₂O₅PS₂

December 14, 2022

Ming-Gang Wu, Xu-Feng Liu

Page range: 133-135

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C 27 H 23 Fe 2 O 5 PS 2 , monoclinic, P 2 1 / c (no. 14), a = 11.3170(5) Å, b = 16.1774(8) Å, c = 15.2170(7) Å, β = 92.933(1)°, V = 2782.3(2) Å 3 , Z = 4, R gt ( F ) = 0.0537, wR ref ( F 2 ) = 0.1636, T = 296(2) K.
Open Access
Crystal structure of 1-(2-(4-chlorophenethyl)-2-hydroxy-3,3-dimethylbutyl)-1H-1,2,4-triazol-4-ium nitrate, C₁₆H₂₃N₄O₄Cl

December 15, 2022

Hua Wang, Guo-tao Zhang, Hong-ya Li

Page range: 137-139

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C 16 H 23 N 4 O 4 Cl, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 7.609(2) Å, b = 9.287(3) Å, c = 13.511(4) Å, α = 90.530(7)°, β = 102.028(5)°, γ = 97.774(6)°, V = 924.4(5) Å 3 , Z = 2, R gt ( F ) = 0.0625, w R ref ( F 2 ) = 0.1634, T = 296(2) K.
Open Access
The crystal structure of 3,3′-disulfanediyldi(1H-1,2,4-triazol-5-amine) monohydrate, C₄H₈N₈OS₂

December 14, 2022

Giyosiddin Khayrullaev, Batirbay Torambetov, Shakhnoza Kadirova, Yevhenii Vaksler

Page range: 141-144

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C 4 H 8 N 8 OS 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 7.4377(5) Å, b = 7.5032(5) Å, c = 10.0964(6) Å, α = 91.481(5)°, β = 108.906(5)°, γ = 110.678(6)°, V = 492.41(6) Å 3 , Z = 2, R gt ( F ) = 0.0653, wR ref ( F 2 ) = 0.1888, T = 293 (2) K.
Open Access
The crystal structure of trans-[bis(4-methylpyridine-κN)bis(quinoline-2-carboxylato- κ ² N,O)cadmium(II)], C₃₂H₂₆CdN₄O₄

December 14, 2022

Boris-Marko Kukovec, Vesna Sokol, Zora Popović

Page range: 145-147

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C 32 H 26 CdN 4 O 4 , tetragonal, P 4 1 2 1 2 (no. 92), a = 13.7308(6) Å, c = 15.1806(7) Å, V = 2862.1(3) Å 3 , Z = 4, R gt ( F ) = 0.0359, wR ref ( F 2 ) = 0.0693, T = 296(2) K.
Open Access
The crystal structure of ethyl 2′-hydroxy-4′,6′-dimethoxy-3-(4-methoxynaphthalen-1-yl)-5-oxo-2,3,4,5-tetrahydro-[1,1′-biphenyl]-4-carboxylate, C₂₈H₂₈O₇

December 14, 2022

Soon Young Shin, Ha-Jin Lee, Dongsoo Koh

Page range: 149-151

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C 28 H 28 O 7 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 11.0746(18) Å, b = 11.4312(17) Å, c = 11.552(2) Å, α = 77.148(8)°, β = 62.164(8)°, γ = 67.858(8)°, V = 1195.9(4) Å 3 , Z = 2, R gt ( F ) = 0.0522, wR ref ( F 2 ) = 0.1862, T = 223(2) K .

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