Zeitschrift für Kristallographie - New Crystal Structures

Issue Open Access

Volume 238, Issue 3

Published by

Become an author with De Gruyter Brill

Submit Manuscript Author Information

Zeitschrift für Kristallographie - New Crystal Structures

This issue is in the journal

Zeitschrift für Kristallographie - New Crystal Structures

Contents

Publicly Available
Frontmatter

April 28, 2023

Page range: i-vi

Download PDF
New Crystal Structures
Open Access
Crystal structure of phenyl(3,3-dichloro-1,3-dihydro-2H-pyrrolo[2,3-b]pyridin-2-one)methanone, C₇H₄Cl₂N₂O

March 29, 2023

Su-Fen Bai, Shan-Shan Li, Jia-Xuan Liu, Chun-Yu Tian, Xiao-Long Li, Xiao-Jin La

Page range: 411-412

Download PDF

C 7 H 4 Cl 2 N 2 O, monoclinic, P 2 1 / c (no. 14), a = 6.215(2) Å, b = 16.544(5) Å, c = 8.561(3) Å, β = 108.707(4)°, V = 833.8(5) Å 3 , Z = 4, R gt ( F ) = 0.0339, wR ref ( F 2 ) = 0.1265, T = 296 K.
Open Access
Crystal structure of poly[diaqua-bis(μ ₂-1,4-diaminobutane-N:N′)cobalt(II)] dichloride, C₈H₂₈Cl₂CoN₄O₂

February 24, 2023

Shin Jiehye, Kang Jaeun, Junghwan Do

Page range: 413-415

Download PDF

C 8 H 28 Cl 2 CoN 4 O 2 , orthorhombic, Fddd (no. 70), a = 10.116(2) Å, b = 13.532(3) Å, c = 23.507(5) Å, V = 3217.8(11) Å 3 , Z = 8, R gt ( F ) = 0.0361, wR ref ( F 2 ) = 0.1069, T = 100.5 K.
Open Access
Synthesis and crystal structure of (4aR,7S)-7-hydroxy-7-isopropyl-1,1-dimethyldecahydro-2H,6H-8a,4a-(epoxymethano)phenanthren-12-one, C₂₀H₃₂O₃

February 24, 2023

Ren-Song Chen, Jing-Jie Zhang, Yi Zhang, Chuan-Yan Xu, Jiang-Hai Ye

Page range: 417-419

Download PDF

C 20 H 32 O 3 , monoclinic, P 2 1 (no. 4), a = 7.8981(17) Å, b = 10.302(2) Å, c = 11.028(3) Å, β = 90.020(2)°, V = 897.3(3) Å 3 , Z = 2, R gt ( F ) = 0.0603, wR ref ( F 2 ) = 0.1342, T = 273(2) K.
Open Access
The crystal structure of 1-(2-chlorobenzyl)-3-(3,5-dichlorophenyl)urea, C₁₄H₁₁Cl₃N₂O

February 24, 2023

Yingju Li, Zhimao Yang

Page range: 421-423

Download PDF

C 14 H 11 Cl 3 N 2 O, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 8.3600(4) Å, b = 12.0085(8) Å, c = 14.3665(6) Å, V = 1442.27(13) Å 3 , Z = 4, R gt ( F ) = 0.0460, w R ref ( F 2 ) = 0.0944, T = 293 K.
Open Access
Crystal structure of tetrapropylammonium-1,3,5-thiadiazole-5-amido-2-carbamate – 1,2,4-thiadiazole-3,5-diamine – water (1/1/1), C₁₇H₃₇N₉O₃S₂

March 6, 2023

Huawei Tang, Qianqian Han, Lijuan Liu

Page range: 425-427

Download PDF

C 17 H 37 N 9 O 3 S 2 , monoclinic, P 2 1 / c (no. 14), a = 8.8492(13) Å, b = 17.285(3) Å, c = 16.810(3) Å, β = 93.493(2)°, V = 2566.4(7) Å 3 , Z = 4, R gt ( F ) = 0.0395, wR ref ( F 2 ) = 0.1277, T = 296(2) K.
Open Access
Tetrabutylammonium 1,3,5-thiadiazole-5-amido-2-carbamate—1,2,4-thiadiazole-3,5-diamine— water (1/1/1), C₂₁H₄₅N₉O₃S₂

March 6, 2023

Huawei Tang, Qianqian Han, Lijuan Liu

Page range: 429-431

Download PDF

C 21 H 45 N 9 O 3 S 2 , orthorhombic, Pbca (no. 61), a = 9.5299(6) Å, b = 16.5181(9) Å, c = 36.886(2) Å, β = 90°, V = 5806.4(6) Å 3 , Z = 8, R gt ( F ) = 0.0568, wR ref ( F 2 ) = 0.1420, T = 296(2) K.
Open Access
The crystal structure of ((E)-2,4-dichloro-6-(((2-hydroxy-5-nitrophenyl)imino)methyl)phenolato-κ ³ N,O,O′)tris(pyridine-κN)manganese(II), C₂₈H₂₁Cl₂MnN₅O₄

February 22, 2023

Ting Li, Xiyuan Xiao, Yuxing Tan, Weiwei Fu

Page range: 433-435

Download PDF

C 28 H 21 Cl 2 MnN 5 O 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.9699(9) Å, b = 9.1185(9) Å, c = 17.6902(17) Å, α = 103.776(1)°, β = 92.407(1)°, γ = 99.761(1)°, V = 1379.8(2) Å 3 , Z = 2, R gt ( F ) = 0.0388, wR ref ( F 2 ) = 0.0920, T = 296 K.
Open Access
The crystal structure of aqua-bis{2-bromo-6-((2-(2-phenylacetyl)hydrazineylidene)methyl)phenolato-κ³ N,O,O′}-dimethylformamide-κ¹ O-erbium(III) chloride – dimethylformamide – water (1/2/1), C₃₉H₄₉N₇O₉Br₂ClEr

February 22, 2023

Li-Hua Wang, Hao-Wen Tai, Gui-Quan Song, Xi-Shi Tai

Page range: 437-439

Download PDF

C 39 H 49 N 7 O 9 Br 2 ClEr, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 12.3164(9) Å, b = 12.7581(9) Å, c = 14.5023(11) Å, α = 70.873(2)°, β = 80.281(2)°, γ = 65.810(2)°, V = 1962.4(3) Å 3 , Z = 1, R gt ( F ) = 0.0383, wR ref ( F 2 ) = 0.0765, T = 296.15 K.
Open Access
Crystal structure of (diaqua-bis(phenanthroline-K ² N,N′)-tetrakis(m ₂-3,4,5,6-tetrafluorophthalato-K ⁴ O,O:O′:O″;K ² O:O′)dierbium (III) phenanthroline (1/2), C₈₀H₃₈Er₂F₁₆N₈O₁₈

March 27, 2023

Jun-Ya Song, Xiao-Yu Zhang, Chun-Li Zhang, Bei-Bei Zhao, Shi-Jie Huang, Xinfang Liu

Page range: 441-443

Download PDF

C 80 H 38 Er 2 F 16 N 8 O 18 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 11.4228(4) Å, b = 12.6712(3) Å, c = 13.2663(4) Å, α = 102.660(2)°, β = 98.047(3)°, γ = 105.509(3)°, V = 1764.54(10) Å 3 , Z = 1, R gt ( F ) = 0.0311, wR ref ( F 2 ) = 0.0668, T = 293(2) K.
Open Access
Crystal structure of (E)-7-methoxy-2-(4-methoxy-2-(trifluoromethyl)benzylidene)-3,4-dihydronaphthalen-1(2H)-one, C₂₀H₁₇F₃O₃

February 22, 2023

Shuai Lai, Yun Hou, Feng-Lan Zhao, Qing-Guo Meng

Page range: 445-447

Download PDF

C 20 H 17 F 3 O 3 , monoclinic, P 2 1 / c (no. 14), a = 9.0684(4) Å, b = 13.1942(6) Å, c = 13.7883(7) Å, β = 96.250(5)°, V = 1639.97(13) Å 3 , Z = 4, R gt ( F ) = 0.0415, wR ref ( F 2 ) = 0.1125, T = 100 K.
Open Access
The crystal structure of 4–(4,4,5,5–tetramethyl–1,3,2–dioxaborolan–2–yl)morpholine, C₁₀H₂₀BNO₃

February 22, 2023

Marcus Herbig, Uwe Böhme

Page range: 449-450

Download PDF

C 10 H 20 BNO 3 , monoclinic, P 2 1 / c (no. 14), a = 11.0681(8) Å, b = 6.1883(3) Å, c = 18.1603(13) Å, β = 105.111(6)°, V = 1200.84(14) Å 3 , Z = 4, R gt ( F ) = 0.0338, wR ref ( F 2 ) = 0.0861, T = 153 K.
Open Access
The crystal structure of catena–poly[aqua(1-naphthoato-κ ² O,O′)-(μ-1-naphthoato-κ ⁴ O:O,O′:O′)lead(II)], C₂₂H₁₆O₅Pb

February 22, 2023

Jiahong Li, Zheyu Deng, Biao Li, Jiaqi Ou, Xiaoming Zhu

Page range: 451-453

Download PDF

C 22 H 16 O 5 Pb, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 7.3395(8) Å, b = 10.7768(11) Å, c = 23.034(3) Å, V = 1821.9(3) Å 3 , Z = 4, R gt ( F ) = 0.0327, w R ref ( F 2 ) = 0.0735, T = 296(2) K.
Open Access
The crystal structure of 1-(4-chlorophenyl)-3-cycloheptylurea, C₁₄H₁₉ClN₂O

February 28, 2023

Qianqian Tang, Hanqi Dai, Guangfu Zhou, Yuanjiang Wu, Wei Wang, Yang Zhao

Page range: 455-457

Download PDF

C 14 H 19 ClN 2 O, monoclinic, P 2 1 / c (no. 14), a = 12.8823(9) Å, b = 9.1617(6) Å, c = 11.7421(9) Å, β = 98.377(7)°, V = 1371.06(17) Å 3 , Z = 4, R gt (F) = 0.0678, wR ref (F 2 ) = 0.1912, T = 293 K.
Open Access
The crystal structure of 4-(pyren-1-yl)butyl-4-nitrobenzoate, C₂₇H₂₁NO₄

February 28, 2023

Claudio Barrientos, Juan Arturo Squella, Silvana Moris

Page range: 459-461

Download PDF

C 27 H 21 NO 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 7.3476(2) Å, b = 7.4894(2) Å, c = 20.5137(5) Å, α = 89.33000(10)°, β = 79.7070(10)°, γ = 67.5220(10)°, V = 1024.31(5) Å 3 , Z = 2, R gt ( F ) = 0.0536, w R ref ( F 2 ) = 0.1792, T = 296.15 K.
Open Access
Crystal structure of cyclo-(bis(µ₂-3,3′-(1H-imidazole-3-ium-1,3-diyl)dipropionato-κ⁴ O,O′:O″,O″′)-dinitrato-κ² O,O′-tetraoxido-diuranium(VI) C₁₈H₂₂N₆O₁₈U₂

February 20, 2023

Yuning Meng, Bin Cai

Page range: 463-464

Download PDF

C 18 H 22 N 6 O 18 U 2 , monoclinic, P 2/ c (no. 13), a = 10.894(2) Å, b = 7.9674(16) Å, c = 16.787(3) Å, β = 100.823(2)°, V = 1399.1(5) Å 3 , Z = 2, R gt ( F ) = 0.0307, w R ref ( F 2 ) = 0.0728, T = 296(2) K.
Open Access
The crystal structure of catena-[nitrato-κ ² O,O′-(μ ₃-3-iodobenzene-1,2-dicarboxylato-κ ⁴ O:O′:O″,O‴)-(2,2′:6′,2″-terpyridine-κ ³ N,N′,N″)lanthanum(III)], C₂₃H₁₄IN₄O₇La

March 16, 2023

Bin Cai, Yuning Meng

Page range: 465-466

Download PDF

C 23 H 14 IN 4 O 7 La, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.2438(3) Å, b = 12.3786(5) Å, c = 12.6230(5) Å, α = 111.802(1)°, β = 91.144(1)°, γ = 100.6470(10)°, V = 1169.86(8) Å 3 , Z = 2, R gt ( F ) = 0.0313, w R ref ( F 2 ) = 0.1051, T = 296 K.
Open Access
Redetermination of crystal structure of [bis(pyridin-2-ylmethyl)amine-κ ³ N,Nʹ,Nʺ]chloridopalladium(II) chloride monohydrate

February 20, 2023

Kwang Ha

Page range: 467-469

Download PDF

C 12 H 13 Cl 2 N 3 Pd·H 2 O, triclinic, P 1̄ (no. 2), a = 7.0698(4) Å, b = 8.5546(6) Å, c = 12.8539(9) Å, α = 106.541(2)°, β = 102.510(2)°, γ = 91.572(2)°, V = 724.23(8) Å 3 , Z = 2, R gt ( F ) = 0.0199, wR ref ( F 2 ) = 0.0438, T = 223 K.
Open Access
Crystal structure of catena-poly[triaqua-[bis(m₂-4-(1H-1,2,4-triazol-1-yl)benzoato-k²O:O')-(4-(1H-1,2,4-triazol-1-yl)benzoato-k¹O)-praseodymium (III) monohydrate], C₂₇H₂₆N₉O₁₀Pr

March 30, 2023

Li Liu, Huan-Mei Guo, Li-Li Liu, Xin-Ru Qian

Page range: 471-473

Download PDF

C 27 H 26 N 9 O 10 Pr, monoclinic, P 2 1 / c , a = 13.2280(12) Å, b = 5.5628(5) Å, c = 41.140(3) Å, β = 105.109(2)°, V = 2922.6(4) Å 3 , Z = 4, R gt ( F ) = 0.0426, w R ref ( F 2 ) = 0.0803, T = 298.15 K.
Open Access
Crystal structure of trans-diaqua-bis(methyl methylcarbamohydrazonothioato-κ² N,N′) nickel(II) iodide semihydrate, C₆H₂₂N₆O₂NiS₂I₂·0.5H₂O

March 14, 2023

Svetlana Belošević, Vukadin M. Leovac, Mirjana M. Radanović, Milica G. Bogdanović, Nikola D. Radnović, Marko V. Rodić

Page range: 475-477

Download PDF

C 6 H 23 I 2 N 6 NiO 2.50 S 2 , monoclinic, C 2/ c (no. 15), a = 8.2282(4) Å, b = 21.9200(7) Å, c = 11.4906(4) Å, β = 109.451(4)°, V = 1954.19(14) Å 3 , Z = 4, R gt ( F ) = 0.0322, wR ref ( F 2 ) = 0.1113, T = 295.
Open Access
The crystal structure of 2-(2-fluoro-4-methyl-5-((2,2,2-trifluoroethyl)thio)phenyl)isoindolin-1-one, C₁₇H₁₃F₄NOS

March 1, 2023

Jing Zhang, Lixin Zhang

Page range: 479-481

Download PDF

C 17 H 13 F 4 NOS, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 6.1249(7) Å, b = 9.9306(10) Å, c = 13.1754(13) Å, α = 83.116(8)°, β = 80.305(9)°, γ = 73.204(9)°, V = 754.08 Å 3 , Z = 2, R gt ( F ) = 0.0460, wR ref ( F 2 ) = 0.1078, T = 150 K.
Open Access
The crystal structure of di-μ-1-naphthylacetato-κ ³ O,O′:O;κ ³ O:O,O′-bis[(1-naphthylacetato-κ ² O,O′)(2,2′-bipyridine-κ ² N,N′)lead(II)] monohydrate, C₆₈H₅₄N₄O₉Pb₂

March 28, 2023

Zheyu Deng, Jiahong Li, Xinbo Hou, Na Luo, Xiaoming Zhu

Page range: 483-485

Download PDF

C 68 H 54 N 4 O 9 P b 2 ${\mathrm{C}}_{68}{\mathrm{H}}_{54}{\mathrm{N}}_{4}{\mathrm{O}}_{9}{\mathrm{P}\mathrm{b}}_{2}$ , monoclinic, C 2/ c (no. 15), a = 15.7286(14) Å, b = 16.3623(14) Å, c = 22.500(2) Å, β = 97.369 ( 1 ) ° $97.369(1){}^{\circ}$ , V = 5742.7(9) Å 3 ${\mathrm{\mathring{\text{A}}}}^{3}$ , Z = 4, R g t ${R}_{gt}$ ( F ) = 0.0203, w R r e f ${R}_{ref}$ ( F 2 ${F}^{2}$ ) = 0.0488, T = 296(2) K.
Open Access
Crystal structure of tetrapropylammonium guanidinium 4,4′-sulfonyldibenzoate monohydrate, C₂₇H₄₄N₄O₇S

March 28, 2023

Na Lin, Ruiqin Sun, Xiaofang Li

Page range: 487-489

Download PDF

C 27 H 44 N 4 O 7 S, monoclinic, P 2 1 / n (no. 14), a = 10.216(3) Å, b = 18.133(5) Å, c = 17.036(5) Å, β = 98.371(3)°, V = 3122.2(16) Å 3 , Z = 4, R gt ( F ) = 0.0435, wR ref ( F 2 ) = 0.1333, T = 296(2) K.
Open Access
Crystal structure of bis(tetrapropylammonium) terephthalate – 1-(diaminomethylene)thiourea – water (1/2/4) C₁₈H₄₀N₅O₄S

March 23, 2023

Mengfei Li, Fangfang Geng, Honglei Zhu

Page range: 491-493

Download PDF

C 18 H 40 N 5 O 4 S, monoclinic, P 2 1 / n (no. 14), a = 8.4254(9) Å, b = 8.4254(9) Å, c = 16.1470(17) Å, β = 98.302(2)°, V = 2411.9(4) Å 3 , Z = 4, R gt ( F ) = 0.0409, w R ref ( F 2 ) = 0.1162, T = 296(2) K.
Open Access
Crystal structure of (E)-7-fluoro-2-(4-morpholinobenzylidene)-3,4-dihydronaphthalen-1(2H)-one, C₂₁H₂₀FNO₂

March 14, 2023

Han-Lin Luo, Wen-Xuan Li, Xian-Yong Bai, Qing-Guo Meng, Yun Hou

Page range: 495-497

Download PDF

C 21 H 20 F N O 2 ${\mathrm{C}}_{21}{\mathrm{H}}_{20}\mathrm{F}\mathrm{N}{\mathrm{O}}_{2}$ , triclinic, P 1̄ (no. 2), a = 9.2201(7) Å, b = 9.3195(8) Å, c = 11.4012(9) Å, α = 103.880 ( 7 ) ° $103.880(7){}^{\circ}$ , β = 100.987 ( 7 ) ° $100.987(7){}^{\circ}$ , γ = 115.090 ( 7 ) ° $115.090(7){}^{\circ}$ , V = 1796.31(20) Å 3 ${\mathrm{\mathring{\text{A}}}}^{3}$ , Z = 2, R g t ${R}_{gt}$ (F) = 0.0421, w R r e f $w{R}_{ref}$ ( F 2 ${\mathrm{F}}^{2}$ ) = 0.1136, T = 293 K.
Open Access
The crystal structure of poly[diaqua-bis(μ ₃-5-bromobenzene-1,3-dicarboxylato-κ ³ O,O,O′)-(μ ₂-1,3-bis-(4-pyridyl)-propane-κ ² N,N′)-dizinc(II))] – 5-bromobenzene-1,3-dicarboxylic acid [2/1], C₃₇H₂₉Br₃N₂O₁₄Zn₂

March 30, 2023

Xiao-Ming Shi, Yu-Jia Fu

Page range: 499-501

Download PDF

C 37 H 29 Br 3 N 2 O 14 Zn 2 , monoclinic, P 2 1 / m (no. 11), a = 8.2047(6) Å, b = 28.6129(13) Å, c = 8.8721(7) Å, β = 112.069(9)°, V = 1930.2(3) Å 3 , Z = 2, R gt ( F ) = 0.0588, w R ref ( F 2 ) = 0.1547, T = 200 K.
Open Access
The crystal structure of 2-bromo-1,3-phenylene bis(4-methylbenzenesulfonate), C₂₀H₁₇BrO₆S₂

March 6, 2023

Jue-Yuan Chen, Long-Sheng Zou, Ni Lai, Zi-Yi Yin, Lin Yuan, Zhong-Yan Li

Page range: 503-505

Download PDF

C 20 H 17 BrO 6 S 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.173(2) Å, b = 8.256(2) Å, c = 16.514(5) Å, α = 89.947(3)°, β = 83.105(3)°, γ = 72.077(3)°, V = 1051.8(5) Å 3 , Z = 2, R gt ( F ) = 0.0334, w R ref ( F 2 ) = 0.0889, T = 296(2) K.
Open Access
Crystal structure of europium dichromium icosaaluminum, EuCr₂Al₂₀

March 8, 2023

Aylin Koldemir, Steffen Klenner, Rainer Pöttgen

Page range: 507-509

Download PDF

EuCr 2 Al 20 , cubic, F d 3 ‾ m $Fd\overline{3}m$ (no. 227), a = 14.5245(7) Å, V = 3064.1(3) Å 3 , Z = 8, R gt ( F ) = 0.0351, wR ref ( F 2 ) = 0.0402, T = 293 K.
Open Access
The crystal structure of N′¹,N′³-di((E)-benzylidene) isophthalohydrazide dihydrate, C ₂₂ H ₂₂ N ₄ O ₄

March 20, 2023

Ni Lai, Sheng-Ting Zhang, Fei Zou, Lin Yuan, Zhong-Yan Li

Page range: 511-512

Download PDF

C 22 H 22 N 4 O 4 ${\mathrm{C}}_{22}{\mathrm{H}}_{22}{\mathrm{N}}_{4}{\mathrm{O}}_{4}$ , monoclinic, C 2/ c (no. 15), a = 34.315(13) Å, b = 6.701(3) Å, c = 9.105(3) Å, β = 98.510 ( 4 ) ° $98.510(4){}^{\circ}$ , V = 2070.7(13) Å 3 ${\mathrm{\mathring{\text{A}}}}^{3}$ , Z = 4, R g t ${R}_{gt}$ ( F ) = 0.0461, w R r e f $w{R}_{ref}$ ( F 2 ${F}^{2}$ ) = 0.1413, T = 296(2) K.
Open Access
Crystal structure of 7α,11α-dihydroxy-15-oxo-ent-kauran-16-en-19,6β-olide, C₂₀H₂₆O₅

March 23, 2023

Lu Zhang, Hang Yuan, Jiang-Hai Ye, Kang He, Chun-Hua Lai, Juan Zou

Page range: 513-515

Download PDF

C 20 H 26 O 5 , monoclinic, P 2 1 2 1 2 1 (no. 19), a = 7.5455(15) Å, b = 12.735(3) Å, c = 18.333(4) Å, V = 1761.6(6) Å 3 , Z = 4, R g t ${R}_{gt}$ ( F ) = 0.0529, w R r e f $w{R}_{ref}$ ( F 2 ) = 0.1407, T = 273(2) K.
Open Access
Crystal structure of 4-chloro-N′-[(1E)-pyridin-3-ylmethylidene]benzohydrazide, C₁₃H₁₀ClN₃O

March 8, 2023

Lamya H. Al-Wahaibi, Olivier Blacque, Edward R. T. Tiekink, Ali A. El-Emam

Page range: 517-520

Download PDF

C 13 H 10 ClN 3 O, monoclinic, P 2 1 / c (no. 14), a = 19.0933(2) Å, b = 23.0910(3) Å, c = 10.6831(2) Å, β = 90.064(1)°, V = 4710.00(12) Å 3 , Z = 16, R gt ( F ) = 0.0411, wR ref ( F 2 ) = 0.1081, T = 160 K.
Open Access
The crystal structure of (Z)-3-(1-(2-((E)-4-isopropylbenzylidene)hydrazinyl)ethylidene) chroman-2,4-dione, C₂₁H₂₀N₂O₃

April 13, 2023

Vidoslav S. Dekić, Biljana R. Dekić, Dragana M. Sejmanović, Suzana Janićević, Biljana Krüger, Volker Kahlenberg, Marko V. Rodić

Page range: 521-524

Download PDF

C 21 H 20 N 2 O 3 , monoclinic, P 2 1 / c (no. 14), a = 6.8892(3) Å, b = 21.8269(13) Å, c = 35.1144(19) Å, β = 90.344(5)°, V = 5280.1(5) Å 3 , Z = 12, R gt ( F ) = 0.0672, wR ref ( F 2 ) = 0.1460, T = 170(2) K.
Open Access
Crystal structure of E-7-fluoro-2-(2-(trifluoromethyl)benzylidene)-3,4-dihydronaphthalen-1(2H)-one, C₁₈H₁₂F₄O

March 23, 2023

Juan Zhang, Yun Hou, Feng-Lan Zhao, Qing-Guo Meng

Page range: 525-527

Download PDF

C 18 H 12 F 4 O, triclinic, P 1̄ (no. 2), a = 7.9400(8) Å, b = 8.1071(9) Å, c = 13.3238(15) Å, α = 89.394 ( 9 ) ° $89.394\left(9\right)^{\circ} $ , β = 76.343 ( 9 ) ° $76.343\left(9\right)^{\circ} $ , γ $$ = 63.411 ( 11 ) ° $\text{63.411}\left(11\right)^{\circ} $ , V = 740.79(15) Å 3 , Z = 2, R g t ${R}_{\mathit{g}\mathit{t}}$ ( F ) = 0.0472, w R r e f $w{R}_{\mathit{r}\mathit{e}\mathit{f}}$ ( F 2 ) = 0.1244, T = 293 K.
Open Access
Crystal structure of bis(6-aminopyridine-2-carboxylato–k²O,N)-bis(N,N-dimethylformamide-k¹ O)zinc(II), C₁₈H₂₄N₆O₆Zn

April 5, 2023

Dong-feng Hong, Jia-Qi Ye, Wen-Bo Guo

Page range: 529-531

Download PDF

C 18 H 24 N 6 O 6 Zn, monoclinic, P 2 1 / n (no. 14), a = 10.1669(6) Å, b = 8.0831(4) Å, c = 13.1012(8) Å, β = 91.221 ( 5 ) ° $91.221(5){}^{\circ}$ , Z = 2, V = 1076.41(11) Å 3 , R gt (F) = 0.0396, w R ref (F 2 ) = 0.0987, T = 273 K.
Open Access
Crystal structure of 5-(adamantan-1-yl)-3-[(4-{[2-(trifluoromethyl)phenyl]-methyl}piperazin-1-yl)methyl]-1,3,4-oxadiazole-2(3H)-thione, C₂₅H₃₁F₃N₄OS

March 20, 2023

Lamya H. Al-Wahaibi, Mohammed S. M. Abdelbaky, Santiago Garcia-Granda, Edward R. T. Tiekink, Ali A. El-Emam

Page range: 533-535

Download PDF

C 25 H 31 F 3 N 4 OS, monoclinic, P 2 1 / c (no. 14), a = 6.7323(1) Å, b = 15.4999(2) Å, c = 23.7905(4) Å, β = 93.037(2)°, V = 2479.05(6) Å 3 , Z = 4, R gt ( F ) = 0.0473, wR ref ( F 2 ) = 0.1394, T = 293 K.
Open Access
Crystal structure of tetrapropylammonium bicarbonate–1-(diaminomethylene)thiourea – water (2/2/1), C₃₀H₇₂N₁₀O₇S₂

April 4, 2023

Lulu Zhang, Qianqian Han, Xin Zhu

Page range: 537-539

Download PDF

C 30 H 72 N 10 O 7 S 2 , triclinic, P 1̄ (no. 2), a = 8.75510(10) Å, b = 15.1170(2) Å, c = 16.8843(2) Å, α = 76.272 ( 1 ) ° $76.272(1){}^{\circ}$ , β = 78.397 ( 1 ) ° $78.397(1){}^{\circ}$ , γ = 88.277 ( 1 ) ° $88.277(1){}^{\circ}$ , V = 2126.09(5) Å 3 , Z = 2, R gt ( F ) = 0.0407, wR ref ( F 2 ) = 0.1282, T = 296(2) K.
Open Access
Crystal structure of tris(2,2′-bipyridine-κ² N,N′)iron(II) triiodide – dichloromethane (2/1), C₆₁H₅₀Cl₂Fe₂I₁₂N₁₂

March 23, 2023

Chuanguo Cui, Jinxiao Zhang, Zhiyin Xiao

Page range: 541-543

Download PDF

C 61 H 50 Cl 2 Fe 2 I 12 N 12 , orthorhombic, Pbcn (no. 60), a = 13.0247(4) Å, b = 17.0204(5) Å, c = 34.1475(9) Å, β = 90, V = 7570.0(4) Å 3 , Z = 4, R gt ( F ) = 0.0694, wR ref ( F 2 ) = 0.1605, T = 293(2) K.
Open Access
Crystal structure of 2-amino-3-[2-(1,3,3-trimethyl-1,3-dihydro-indol-2-ylidene)-ethylideneamino]-but-2-enedinitrile, C₁₇H₁₇N₅

April 5, 2023

Ze-Yi Lian, Wei-Na Wu

Page range: 545-546

Download PDF

C 17 H 17 N 5 , monoclinic, P 2 1 / c (no. 14), a = 9.4347(9) Å, b = 15.6392(15) Å, c = 11.0939(11) Å, β = 100.215 ( 2 ) ° $100.215(2){}^{\circ}$ , V = 1611.0(3) Å 3 , Z = 4, R gt ( F ) = 0.0392, wR ref ( F 2 ) = 0.1105, T = 296 K.
Open Access
The crystal structure of 1-(2-chlorophenyl)-3-cycloheptylurea, C₁₄H₁₉ClN₂O

March 30, 2023

Yuanci Li, Zhiqiang Feng, Hongjuan Tong

Page range: 547-549

Download PDF

C 14 H 19 ClN 2 O, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 8.9579(3) Å, b = 12.2172(4) Å, c = 12.5669(5) Å, V = 1375.33(8) Å 3 , Z = 4, R gt ( F ) = 0.0541, w R ref ( F 2 ) = 0.1449, T = 193 K.
Open Access
Crystal structure of potassium bis(pentaselenido-κ ² Se ¹,Se ⁵)palladate(II), K₂[Pd(Se₅)₂]

March 27, 2023

Kang-Woo Kim

Page range: 551-553

Download PDF

K 2 PdSe 10 , orthorhombic, Pcma (no. 55), a = 8.293(3) Å, b = 10.987(3) Å, c = 16.432(5) Å, V = 1497.1(8) Å 3 , Z = 4, R gt ( F ) = 0.0349, wR ref ( F 2 ) = 0.0688, T = 173(2) K.
Open Access
The crystal structure of 5,10-bis(2-methoxyethyl)-5,10-dihydro-[1,2,3,4]tetrathiocino[5,6-b:8, 7-b′]diindole, C₂₂H₂₂N₂O₂S₄

March 23, 2023

Ming Ni, Penghui Ni

Page range: 555-557

Download PDF

C 22 H 22 N 2 O 2 S 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.4865(14) Å, b = 11.756(2) Å, c = 12.863(2) Å, α = 69.693(2)°, β = 70.812(2)°, γ = 72.170(2)°, V = 1109.6(3) Å 3 , Z = 2, R gt ( F ) = 0.0280, wR ref ( F 2 ) = 0.0753, T = 296(2) K.
Open Access
The crystal structure of 4-(4-iodophenyl)-5H-1,2,3-dithiazole-5-thione, C₈H₄INS₃

March 23, 2023

Huiyang Liao, Penghui Ni

Page range: 559-561

Download PDF

C 8 H 4 INS 3 , monoclinic, P 2 1 / c (no. 14), a = 11.8060(19) Å, b = 7.8961(14) Å, c = 11.972(2) Å, β = 110.981 ( 2 ) ° $110.981(2){}^{\circ}$ , V = 1042.1(3) Å 3 , Z = 4, R gt ( F ) = 0.0279, wR ref ( F 2 ) = 0.0739, T = 296(2) K.
Open Access
Crystal structure of bis{μ₂-(4-acetyl-phenoxy)acetato-κ² O:O′}-bis{μ₂-(4-acetyl-phenoxy)acetato-κ³ O,O′:O)- bis{(4-acetyl-phenoxy)acetato-κ² O,O′}-bis(phenanthrolin-κ² N,N′)didysprosium(III) tetrahydrate, C₈₄H₇₈N₄O₂₈Dy₂

April 4, 2023

Li–Hua Wang, Hao–Wen Tai, Mei–Li Zhao, Xi–Shi Tai

Page range: 563-565

Download PDF

C 84 H 78 N 4 O 28 Dy 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 12.3134(5) Å, b = 12.7705(5) Å, c = 14.5150(6) Å, α = 70.852(1)°, β = 80.298(1)°, γ = 65.726(1)°, V = 1964.05(14) Å 3 , Z = 1, R gt ( F ) = 0.0381, w R ref ( F 2 ) = 0.0682, T = 296.15 K.
Open Access
Crystal structure of Eu₂Pd_3.37(1)Zn_13.63(1)

March 21, 2023

Steffen Klenner, Theresa Block, Rainer Pöttgen

Page range: 567-569

Download PDF

Eu 2 Pd 3.37 Zn 13.63 , trigonal, R 3 ‾ m $R\overline{3}m$ (no. 166), a = 9.1693(7) Å, c = 13.2443(13) Å, V = 964.34(14) Å 3 , Z = 3, R gt ( F ) = 0.0268, wR ref ( F 2 ) = 0.0287, T = 293 K.
Open Access
Crystal structure of 2-methoxy-4-(methoxy-carbonyl)phenyl 2-chloro-4-fluorobenzoate, C₁₆H₁₂ClFO₅

April 19, 2023

Xin-Ting Xiong, Pan-Lei Xiao, Xiao-Hui Ou-Yang, Xu-Liang Nie, Xiu-Ying Song

Page range: 571-573

Download PDF

C 16 H 12 ClFO 5 , monclinic, P 2 1 / c (no. 14), a = 14.7536(6) Å, b = 7.8281(3) Å, c = 14.0501(7) Å, β = 111.174 ( 5 ) ° $111.174(5){}^{\circ}$ , V = 1513.13(12) Å 3 , Z = 4, R gt ( F ) = 0.0367, wR ref ( F 2 ) = 0.0865, T = 296(2) K.
Open Access
Crystal structure of catena-poly[bis(μ₂-dicyanamide-κ² N:N′)-bis(4-vinylpyridine-κN)-copper(II)], C₁₈H₁₄CuN₈

April 12, 2023

Chong Tan, Tong Zhang, Xiaodong Yi

Page range: 575-576

Download PDF

C 18 H 14 CuN 8 , triclinic, P 1̄ (no. 2), a = 7.2431(5) Å, b = 7.3783(5) Å, c = 9.8740(6) Å, α = 110.174(6)°, β = 105.036(5)°, γ = 92.219(5)°, V = 473.55(6) Å 3 , Z = 1, R gt ( F ) = 0.0409, wR ref ( F 2 ) = 0.1272, T = 293(2) K.
Open Access
The crystal structure of iguratimod-dimethylformamide (1/1), C₁₇H₁₄N₂O₆S·C₃H₇NO

April 5, 2023

Wen-Jing Ma, Hao Wang, Zhen-Yu Wang, Yu-Xuan Long, Xin-Qi Wang, Qian Ma, Cui-Ran Xu, Yu-Heng Ma

Page range: 577-578

Download PDF

C 17 H 14 N 2 O 6 S·C 3 H 7 NO, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 5.4146(4) Å, b = 11.7925(8) Å, c = 16.9527(12) Å, α = 85.238(2)°, β = 86.674(4)°, γ = 78.959(2)°, V = 1057.77(13) Å 3 , Z = 2, R gt ( F ) = 0.0418, wR ref ( F 2 ) = 0.1175, T = 296(2) K.
Open Access
Synthesis and crystal structure of 1-((3R,10S,13S,17S)-10,13-dimethyl-3-(m-tolylamino)hexadecahydro-1H-cyclopenta[α]phenanthren-17-yl)ethan-1-one, C₂₈H₄₁NO

April 13, 2023

Jin-Feng Zhao, Wen-Wen Zhang, Jiang-Hai Ye, Kang He, Juan Zou

Page range: 579-581

Download PDF

C 28 H 41 NO, triclinic, P 1 $P1$ (no. 1), a = 6.3144(8) Å, b = 9.7315(13) Å, c = 10.5867(14) Å, α = 111.561(4)°, β = 96.486 ( 4 ) ∘ $96.486{(4)}^{\circ }$ , γ = 97.128(4)°, V = 591.41(14) Å 3 , Z = 1, R g t ${R}_{\mathit{g}\mathit{t}}$ ( F ) = 0.0579, w R r e f $w{R}_{\mathit{r}\mathit{e}\mathit{f}}$ ( F 2 ) = 0.1687, T = 273(2) K.
Open Access
The crystal structure of diaqua-bis(4-bromo-2-formylphenoxy)zinc(II), C₁₄H₁₂Br₂O₆Zn

April 13, 2023

Fei Zou, Sheng-Ting Zhang, Jue-Yuan Chen, Lin Yuan

Page range: 583-584

Download PDF

C 14 H 12 Br 2 O 6 Zn, monoclinic, C 2/ c (no. 15), a = 29.43(2) Å, b = 4.774(4) Å, c = 11.658(9) Å, β = 103.194 ( 7 ) ∘ $103.194{(7)}^{\circ }$ , V = 1595(2) Å 3 , Z = 4, R g t ${R}_{gt}$ ( F ) = 0.0235, w R r e f $w{R}_{ref}$ ( F 2 ) = 0.0647, T = 296(2) K.
Open Access
The crystal structure of tetra(1-ethylimidazole-κ ¹ N)-[μ ₄-imidazole-4,5-dicarboxylato-κ ⁴ O, N, O′, N′]-trioxido-divanadium, C₂₅H₃₃N₁₀O₇V₂

April 14, 2023

Na Li, Xiao-Jie Wang, Yu-Cai Qin, Jing-Yun Wang

Page range: 585-587

Download PDF

C 25 H 33 N 10 O 7 V 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 10.3933(4) Å, b = 12.5655(5) Å, c = 14.1841(5) Å, α = 65.373(1)°, β = 70.351 ( 1 ) ∘ $70.351{(1)}^{\circ }$ , γ = 88.052 ( 2 ) ∘ $88.052{(2)}^{\circ }$ , V = 1573.62(11) Å 3 , Z = 2, R gt ( F ) = 0.0362, wR ref ( F 2 ) = 0.0885, T = 173 K.
Open Access
The crystal structure of (E)-N′-(1-(4-fluorophenyl)propylidene)-2-hydroxybenzohydrazide, C₁₆H₁₅FN₂O₂

April 6, 2023

Sha Yang, Jing Men, Wenqiang Tang

Page range: 589-591

Download PDF

C 16 H 15 FN 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 9.2751(7) Å, b = 13.1232(7) Å, c = 11.7155(8) Å, β = 90.011 ( 7 ) ∘ $90.011{(7)}^{\circ }$ , V = 1426.00(16) Å 3 , Z = 4, R g t ${R}_{\mathit{g}\mathit{t}}$ ( F ) = 0.0570, w R r e f $w{R}_{\mathit{r}\mathit{e}\mathit{f}}$ ( F 2 ) = 0.1462, T = 293 K.

Issues in this Volume

Search the content of this journal

This issue

All issues

Issues in this Volume

Institutional Access

How does access work?

Downloaded on 16.11.2025 from https://www.degruyterbrill.com/journal/key/ncrs/238/3/html