Volume 237, Issue 4

Published by

Become an author with De Gruyter Brill

Submit Manuscript Author Information

This issue is in the journal

Zeitschrift für Kristallographie - New Crystal Structures

Contents

Publicly Available
Frontmatter

June 28, 2022

Page range: i-viii

Download PDF
New Crystal Structures
Open Access
Crystal structure of N-((3s,5s,7s)-adamantan-1-yl)-2-(3-benzoylphenyl)propanamide, C₂₆H₂₉NO₂

April 20, 2022

Li-Na Gao, Ye Gu, Feng Jin, Duo Hao, Xin-Ru Zhang

Page range: 497-499

Download PDF

C 26 H 29 NO 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 10.8490(8) Å, b = 13.2892(9) Å, c = 14.7199(10) Å, α = 89.161(3)°, β = 79.991(2)°, γ = 85.746(2)°, V = 2084.2(3) Å 3 , Z = 4, R gt ( F ) = 0.0641, wR ref ( F 2 ) = 0.1449, T = 170 K.
Open Access
The crystal structure of bis(μ₂-5-chloro-2-oxido-N-(1-oxidopropylidene)benzohydrazonato-κ⁵ N,O,O′:N′,O′′)-octakis(pyridine-κ¹ N)trinickel(II) C₆₀H₅₆Cl₂N₁₂Ni₃O₆

April 25, 2022

Wang Xin, Yang Liguo, Dong Yizhuo, Ye Yanlin, Wang Yifan

Page range: 501-504

Download PDF

C 60 H 56 Cl 2 N 12 Ni 3 O 6 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 12.684(5) Å, b = 12.827(5) Å, c = 19.100(7) Å, α = 84.641(4)°, β = 81.178(4)°, γ = 85.471(4)°, V = 3050.7(19) Å 3 , Z = 2, R gt ( F ) = 0.0267, wR ref ( F 2 ) = 0.0735, T = 298 K.
Open Access
The crystal structure of 3-(4-chlorophenyl)-1,5-di-p-tolylpentane-1,5-dione, C₂₅H₂₃ClO₂

April 15, 2022

Jun Zheng, Sen Liu, Yaru Zhang, Xianqiang Huang

Page range: 505-507

Download PDF

C 25 H 23 ClO 2 , orthorhombic, P 2 1 2 1 2 1 , a = 5.5648(5) Å, b = 17.6062(15) Å, c = 21.5033(19) Å, V = 2106.8(3) Å 3 , Z = 4, R gt ( F ) = 0.0529, wR ref ( F 2 ) = 0.1371, T = 298 K.
Open Access
The crystal structure of 2,4,4-triphenyl-4H-benzo[b][1,4]oxaphosphinin-4-ium bromide – dichloromethane (1/1), C₂₇H₂₂BrCl₂OP

April 20, 2022

Fen Liu, Longgen Sun, Haiyang Huang

Page range: 509-511

Download PDF

C 27 H 22 BrCl 2 OP, monoclinic, P 2 1 / c (no. 14), a = 9.0066(2) Å, b = 15.4924(4) Å, c = 18.5110(4) Å, β = 95.487(2)°, V = 2571.06(11) Å 3 , Z = 4, R gt ( F ) = 0.0509, wR ref ( F 2 ) = 0.1494, T = 296 K.
Open Access
The crystal structure of 2-(3,6-di-tert-butyl-1,8-diiodo-9H-carbazol-9-yl)acetonitrile, C₂₂H₂₄I₂N₂

April 15, 2022

Lin-Li Tang, Fei Zeng

Page range: 513-515

Download PDF

C 22 H 24 I 2 N 2 , orthorhombic, Pbca (no. 33), a = 21.069(4) Å, b = 8.7963(17) Å, c = 23.757(5) Å, V = 4402.8(15) Å 3 , Z = 8, R gt ( F ) = 0.0530, w R ref ( F 2 ) = 0.1569, T = 296(2) K. CCDC no.: 2153325
Open Access
Crystal structure of 3-phenylpropyl 2-(6-methoxynaphthalen-2-yl)propanoate, C₂₃H₂₄O₃

April 20, 2022

Li-li Wang, De-dong Xue

Page range: 517-519

Download PDF

C 23 H 24 O 3 , orthorhombic, P 2 1 2 1 2 1 (no 19), a = 5.7576(2) Å, b = 7.7223(4) Å, c = 41.6710(16) Å, V = 1852.77(14) Å 3 , Z = 4, R gt ( F ) = 0.0442, wR ref ( F 2 ) = 0.1068, T = 170 K.
Open Access
The crystal structure of (4-fluorophenyl)(5-(hydroxymethyl)furan-2-yl)methanol, C₁₂H₁₁FO₃

April 20, 2022

Yanrong Gao, Hui Ran, Wenqiang Tang

Page range: 521-523

Download PDF

C 12 H 11 FO 3 , monoclinic, P 2 1 / c (no. 14), a = 12.0648(9) Å, b = 8.3896(5) Å, c = 10.5727(9) Å, β = 104.204(8)°, V = 1037.44(14) Å 3 , Z = 4, R gt ( F ) = 0.0614, wR ref ( F 2 ) = 0.1516, T = 293 K.
Open Access
Crystal structure of the dihydrate of tetraethylammonium 1,3,5-thiadiazole-5-amido-2-carbamate, C₁₁H₂₇N₅O₄S

April 20, 2022

Xiaoke Tan, Xin Zhu

Page range: 525-526

Download PDF

C 11 H 27 N 5 O 4 S, triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 7.8359 (2) Å, b = 8.6966 (3) Å, c = 12.9907(4) Å, α = 92.047 (2)°, β = 92.041 (2)°, γ = 96.087 (2)°, V = 879.02 (5) Å 3 , Z = 2, R gt ( F ) = 0.0412, wR ref ( F 2 ) = 0.1265, T = 298 K.
Open Access
Crystal structure of (Z)-4-[(p-tolylamino)(furan-2-yl)methylene]-3-phenyl-1-1-p-tolyl-1H-phenyl-1H-pyrazol-5(4H)-one, C₂₈H₂₃N₃O₂

April 15, 2022

Wei Wei, Qiong Wu, Tong-Yin Jin, Ya-Zhai Zhang, Zhao-Kun Xuan, Heng-Qiang Zhang

Page range: 527-529

Download PDF

C 28 H 23 N 3 O 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 7.6590(7) Å, b = 11.8598(12) Å, c = 12.4954(14) Å, α = 92.027(9)°, β = 99.837(9)°, γ = 93.597(8)°, V = 1114.9(2) Å 3 , Z = 2, R gt ( F ) = 0.0508, wR ref ( F 2 ) = 0.1317, T = 293(2) K.
Open Access
The crystal structure of (E)-3-(2-chlorophenyl)-1-ferrocenylprop-2-en-1-one, C₁₉H₁₅ClFeO

April 12, 2022

Lilei Zhang, Mengru Xie

Page range: 531-533

Download PDF

C 19 H 15 ClFeO, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 10.2693(5) Å, b = 11.2568(6) Å, c = 20.8930(10) Å, α = 80.350(2)°, β = 76.9640(10)°, γ = 86.921(2)°, V = 2319.4(2) Å 3 , Z = 6, R gt ( F ) = 0.0534, wR ref ( F 2 ) = 0.0968, T = 170 K.
Open Access
The pseudosymmetric crystal structure of 3-((1R,2S)-1-methylpyrrolidin-1-ium-2-yl)pyridin-1-ium hexachloridostannate(IV), C₁₀H₁₆N₂SnCl₆

April 18, 2022

Marie Barbara Wolke, Guido J. Reiss

Page range: 535-538

Download PDF

C 10 H 16 N 2 SnCl 6 , monoclinic, I 2 (no. 5), a = 14.0477(4) Å, b = 8.9140(2) Å, c = 27.6199(6) Å, β = 93.060(2)°, Z = 8, V = 3453.67(15) Å 3 , R gt ( F ) = 0.0395, wR ref = 0.0858, T = 290 K.
Open Access
Crystal structure of (2-(1-hydroxyheptyl)octahydro-8aH-chromene-5,8,8a-triol), C₁₆H₃₀O₅

April 20, 2022

Guangdi Wang, Shihao Qian, Sun Yan, Tingchi Wen

Page range: 539-541

Download PDF

C 16 H 30 O 5 , monoclinic, P 2 1 (no. 4), a = 5.6814(5) Å, b = 13.0181(12) Å, c = 22.833(2) Å, β = 96.473(2)°, V = 1677.9(3) Å 3 , Z = 4, R gt ( F ) = 0.0508, wR ref ( F 2 ) = 0.1346, T = 296(2) K.
Open Access
The crystal structure of N-cyclohexyl-3-hydroxy-4-methoxybenzamide, C₁₄H₁₉NO₃

April 13, 2022

Jingxiao Zhang, Xiaoxiao Zhao, Chenyu Cai

Page range: 543-545

Download PDF

C 14 H 19 NO 3 , monoclinic, Cc (no. 9), a = 11.1235(5) Å, b = 15.3724(5) Å, c = 8.1110(3) Å, β = 109.3980(10)°, V = 1308.21(9) Å 3 , Z = 4, R gt ( F ) = 0.0300, wR ref ( F 2 ) = 0.0703, T = 170 K.
Open Access
Crystal structure of 1-(4-hydroxybenzyl)-4-methoxy-9,10-dihydrophenanthrene-2,7-diol from Arundina graminifolia, C₂₂H₂₀O₄

April 12, 2022

Mei-Feng Liu, Xing-Yu Zhang, Yi-Mei Du, Yan Chen

Page range: 547-549

Download PDF

C 22 H 20 O 4 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 11.355(5) Å, b = 15.084(7) Å, c = 20.078(9) Å, V = 3439(3) Å 3 , Z = 4, R gt ( F ) = 0.0382, wR ref ( F 2 ) = 0.0994, T = 296(2) K.
Open Access
The crystal structure of N-cyclopentyl-3-hydroxy-4-methoxybenzamide, C₁₃H₁₇NO₃

April 12, 2022

Jingxiao Zhang, Shubin Guo, Yongnan Guo, Yanliang Yang

Page range: 551-553

Download PDF

C 13 H 17 NO 3 , monoclinic, Cc (no. 9), a = 11.6502(8) Å, b = 13.8752(8) Å, c = 7.9644(5) Å, β = 106.051(2)°, V = 1237.25(14) Å 3 , Z = 4, R gt ( F ) = 0.0427, wR ref ( F 2 ) = 0.1023, T = 170 K.
Open Access
The crystal structure of 2,5,5-triphenyl-3,5-dihydro-4H-imidazol-4-one, C₂₁H₁₆N₂O

April 29, 2022

De-Xing Wang, Peng Cao

Page range: 555-556

Download PDF

C 21 H 16 N 2 O, monoclinic, P 2 1 / c (no. 14), a = 13.8987(3) Å, b = 15.0321(5) Å, c = 8.1727(2) Å, β = 99.337(2)°, V = 1684.87(8) Å 3 , Z = 4, R gt ( F ) = 0.0411, wR ref ( F 2 ) = 0.1137, T = 293(2) K.
Open Access
Crystal structure of 1H-1,2,3-Triazolo[4,5-b]-pyridin-4-ium nitrate, C₅H₅N₅O₃

April 29, 2022

Meng-Shu Zhou, Hong-Ru Fu

Page range: 557-558

Download PDF

C 5 H 5 N 5 O 3 , orthorhombic, Pnma (no. 62), a = 13.4643(13) Å, b = 6.2866(10) Å, c = 9.1138(9) Å, V = 771.43(16) Å 3 , Z = 4, R gt ( F ) = 0.0517, wR ref ( F 2 ) = 0.1317, T = 293 K.
Open Access
Crystal structure of (Z)-4-(((4-bromophenyl)amino)(furan-2-yl)methylene)-2,5-diphenyl-2,4-dihydro-3H-pyrazol-3-one, C₂₆H₁₈BrN₃O₂

May 5, 2022

Zhang Li, Qiong Wu, Ya-Zhai Zhang, Wei-Ya Zhang, Hong-Li Chen, Heng-Qiang Zhang

Page range: 559-561

Download PDF

C 26 H 18 BrN 3 O 2 , monoclinic, P 2 1 / n (no. 14), a = 9.5191(14) Å, b = 23.056(3) Å, c = 10.0556(15) Å, β = 95.470(3)°, V = 2196.9(6) Å 3 , Z = 4, R gt ( F ) = 0.0640, wR ref ( F 2 ) = 0.1645, T = 296(2) K.
Open Access
Crystal structure of 2-(4-methoxyphenyl)-3-methyl-1,8-naphthyridine, C₁₆H₁₄N₂O

May 5, 2022

Xin-Sheng Xiao, Guo-Kai Jia

Page range: 563-564

Download PDF

C 16 H 14 N 2 O, monoclinic, P 2 1 / c (no. 14), a = 6.903(2) Å, b = 7.217(2) Å, c = 26.071(8) Å, β = 93.023(4)°, V = 1296.9(7) Å 3 , Z = 4, R gt ( F ) = 0.0474, wR ref ( F 2 ) = 0.1423, T = 296(2) K.
Open Access
The crystal structure of 3-([1,1′-biphenyl]-2-yl)-1,2-diphenylbenzo[b]phosphole-1-oxide, C₃₂H₂₃OP

April 29, 2022

Chengxiong Yuan, Mingqing Huang, Fen Liu, Haiyang Huang

Page range: 565-567

Download PDF

C 32 H 23 OP, monoclinic, P 2 1 / n (no. 14), a = 9.1869(11) Å, b = 27.940(3) Å, c = 9.6992(11) Å, β = 107.422(2)°, V = 2375.4(5) Å 3 , Z = 4, R gt ( F ) = 0.0486, w R ref ( F 2 ) = 0.1255, T = 296 K.
Open Access
The crystal structure of ammonium (E)-4-((4-carboxyphenyl)diazenyl)benzoate, C₁₄H₁₃N₃O₄

May 5, 2022

Wang Jian-Ge, Wang Hua-Rui

Page range: 569-570

Download PDF

C 14 H 13 N 3 O 4 , monoclinic, I 2/ a (no. 15), a = 11.4188(4) Å, b = 3.7968(2) Å, c = 30.2320(18) Å, β = 96.037(6) ∘ , V = 1303.44(11) Å 3 , Z = 4, R gt ( F ) = 0.0656, w R ref ( F 2 ) = 0.2073, T = 293(2) K.
Open Access
Crystal structure of bis(5-amino-1,2,4-triazol-4-ium-3-yl)methane sulfate, C₅H₁₀N₈O₄S

May 5, 2022

Guo-Tao Zhang, Hua Wang, Hong-Ya Li, Biao Yan

Page range: 571-572

Download PDF

C 5 H 10 N 8 O 4 S, Orthorhombic, Pba 2 (no. 32), a = 7.7320(11) Å, b = 12.8686(19) Å, c = 5.0657(8) Å, β = 90°, V = 504.04(13) Å 3 , Z = 2, R gt ( F ) = 0.0298, w R ref ( F 2 ) = 0.0748, T = 296(2) K.
Open Access
The crystal structure of phenantroline-κ² N,N′-bis(6-phenylpyridine-2-carboxylato-κ² N,O)copper(II), C₃₆H₂₄N₄O₄Cu

April 29, 2022

Zhao Mei-Li, Tai Xi-Shi

Page range: 573-575

Download PDF

C 36 H 24 N 4 O 4 Cu, monoclinic, I 1 2 / a 1 (no. 15), a = 16.5119(17) Å, b = 11.0747(7) Å, c = 17.6272(17) Å, β = 117.916(13)°, V = 2848.3(5) Å 3 , Z = 4, R gt ( F ) = 0.0335, wR ref ( F 2 ) = 0.0759, T = 200 K.
Open Access
The crystal structure of tris(6-methylpyridin-2-yl)phosphine oxide, C₁₈H₁₈N₃OP

May 10, 2022

Gui-Ling Wu

Page range: 577-578

Download PDF

C 18 H 18 N 3 OP, monoclinic, P 2 1 / n (no. 14), a = 13.3987(17) Å, b = 8.7084(11) Å, c = 14.5063(18) Å, β = 95.849(2)° V = 1683.8(4) Å 3 , Z = 4, R gt ( F ) = 0.0423, w R ref ( F 2 ) = 0.1311, T = 296(2) K.
Open Access
The crystal structure of N-(2′-hydroxymethyl-5′-phenyl-3′,4′-dihydro-[1,1′:3′,1″-terphenyl]- 1′(2′H)-yl)-P,P-diphenylphosphinic amide, C₃₇H₃₄NO₂P

May 5, 2022

Jinzhen Jian, Jianghai Ye, Guoyong Luo, Tianqiong Lang

Page range: 579-581

Download PDF

C 37 H 34 NO 2 P, monoclinic, P 2 1 / c (no. 14), a = 9.3479(3) Å, b = 23.0805(8) Å, c = 13.7819(5) Å, β = 102.462(10)°, V = 2903.44(17) Å 3 , Z = 4, R gt ( F ) = 0.0458, wR ref ( F 2 ) = 0.1309, T = 300(2) K.
Open Access
Crystal structure of (E)-4-(6-(4-(2-(pyridin-4-yl)vinyl)phenoxy)pyrimidin-4-yl)morpholine, C₂₁H₂₀N₄O₂

May 5, 2022

Su-Fen Bai, Jia-Xuan Liu, Shan-Shan Li, Chun-Yu Tian, Xiao-Jin La

Page range: 583-585

Download PDF

C 21 H 20 N 4 O 2 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 5.874(3) Å, b = 16.526(7) Å, c = 20.147(8) Å, α = 67.140(5)°, β = 83.287(6)°, γ = 86.910(6)°, V = 1789.7(14) Å 3 , Z = 4, R gt ( F ) = 0.0614, w R ref ( F 2 ) = 0.1675, T = 296 K.
Open Access
Crystal structure of 5-(adamantan-1-yl)-3-[(4-trifluoromethylanilino)methyl]-2,3-dihydro-1,3,4-oxadiazole-2-thione, C₂₀H₂₂F₃N₃OS

May 5, 2022

Lamya H. Al-Wahaibi, Hazem A. Ghabbour, Fatmah A. M. Al-Omary, Edward R. T. Tiekink, Ali A. El-Emam

Page range: 587-591

Download PDF

C 20 H 22 F 3 N 3 OS, triclinic, P 1 (no. 1), a = 6.9678(8) Å, b = 10.7614(14) Å, c = 13.0503(14) Å, α = 76.870(3)°, β = 88.004(4)°, γ = 87.275(4)°, V = 951.60(19) Å 3 , Z = 2, R gt ( F ) = 0.0629, wR ref ( F 2 ) = 0.1626, T = 100 K.
Open Access
Crystal structure of 2,2-dichloro-1-(4-chloro-1H-indol-1-yl)ethan-1-one, C₁₀H₆Cl₃NO

May 6, 2022

Zhao-Yu Ma, Wan Lu, Yu-Chao Guo, Ying-Jiao Li

Page range: 593-594

Download PDF

C 10 H 6 Cl 3 NO, monoclinic, P 2 1 / n (no. 14), a = 9.7097(10) Å, b = 10.6037(11) Å, c = 10.1735(10) Å, β = 96.580(4)°, V = 1040.55(18) Å 3 , Z = 4, R gt ( F ) = 0.0214, wR ref ( F 2 ) = 0.0574, T = 101 K.
Open Access
The crystal structure of 4-(((3-bromo-5-(trifluoromethyl)pyridin-2-yl)oxy)methyl)benzonitrile, C₂₈H₁₆Br₂F₆N₄O₂

May 5, 2022

Zhi-Qiang Lu

Page range: 595-597

Download PDF

C 28 H 16 Br 2 F 6 N 4 O 2 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 8.0085(4) Å, b = 13.6578(7) Å, c = 14.1964(6) Å, α = 96.950(4)°, β = 105.376(4)°, γ = 106.772(5)°, V = 1400.32(12) Å 3 , Z = 2, R gt ( F ) = 0.0570, wR ref ( F 2 ) = 0.1268, T = 293(2) K.
Open Access
The crystal structure of 1H-benzimidazole-2-carboxamide, C₈H₇N₃O

May 6, 2022

Hang Ma, Qiang Tian, Banglong Wan

Page range: 599-600

Download PDF

C 8 H 7 N 3 O, orthorhombic, Pccn (no. 56), a = 9.9071(14) Å, b = 11.1950(19) Å, c = 13.315(2) Å, V = 1476.8(4) Å 3 , Z = 8, R gt ( F ) = 0.0356, wR ref ( F 2 ) = 0.1034, T = 100(2) K, β = 90 ° .
Open Access
The crystal structure of Histidinium hydrogensquarate, C₁₀H₁₁N₃O₆

May 5, 2022

Tsonko Kolev, Martina I. Peeva, Ivan P. Bogdanov, Iliyan V. Ognyanov, Atanas G. Atanasov, Nikolay T. Tzvetkov

Page range: 601-603

Download PDF

C 10 H 11 N 3 O 6 , monoclinic, P 2 1 / c (no. 14), a = 7.4928(12) Å, b = 14.860(3) Å, c = 11.0593(18) Å, β = 109.465(5)°, V = 1161.0(4) Å 3 , Z = 4, R gt ( F ) = 0.0439, w R ref ( F 2 ) = 0.1060, T = 300.0(2) K.
Open Access
The crystal structure of 3-amino-5-carboxypyridin-1-ium iodide, C₆H₇IN₂O₂

May 12, 2022

Mengbing Cui, Yong Li, Heng Chen, Hui Wang, Yan Zeng

Page range: 605-606

Download PDF

C 6 H 7 BrN 2 O 2 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 7.4522(4) Å, b = 7.4741(5) Å, c = 8.3144(5) Å, α = 90.036(3)°, β = 99.808(3)°, γ = 117.724(2)°, V = 402.25(4) Å 3 , Z = 2, R gt ( F ) = 0.0156, w R ref ( F 2 ) = 0.0367, T = 150.0 K.
Open Access
Crystal structure of (E)-amino(2-(3-ethoxy-4-hydroxybenzylidene)hydrazineyl)methaniminium nitrate hemihydrate C₁₀H₁₆N₅O_5.5

May 12, 2022

Ze-Sen Jin, E. Liu, Xiao-Jing Liu, Fang-Fang Jian, Tongling Liang

Page range: 607-609

Download PDF

C 10 H 16 N 5 O 5.5 , monoclinic, C 2/ c (no. 15), a = 17.7836(8) Å, b = 9.4796(4) Å, c = 15.8740(8) Å, β = 97.093(5)°, V = 2655.6(2) Å 3 , Z = 8, R gt ( F ) = 0.0469, wR ref ( F 2 ) = 0.1289, T = 170 K.
Open Access
Crystal structure of 1,2-bis(4,5-dinitro-1H-imidazol-1-yl)ethane, C₈H₆N₈O₈

May 6, 2022

Wang Yong, Wu Bingheng, Yuan Jun, Cao Duanlin, Wang Jianlong, Chen Lizhen

Page range: 611-612

Download PDF

C 8 H 6 N 8 O 8 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 6.7563(9) Å, b = 7.2512(12) Å, c = 25.884(3) Å, V = 1268.1(3) Å 3 , β = 90°, Z = 4, R gt ( F ) = 0.0473, w R ref ( F 2 ) = 0.1170, T = 170 K.
Open Access
The crystal structure of diaqua-bis(pyrazolo[1,5-a]pyrimidine-3-carboxylato-κ²N,O)manganese(II), C₁₄H₁₂N₆O₆Mn

May 5, 2022

Dong-Feng Hong, Meng-Fei Li, Tian-Tian Chu

Page range: 613-614

Download PDF

C 14 H 12 N 6 O 6 Mn, monoclinic, P 2 1 / n (no. 14), a = 7.0839(3) Å, b = 13.1211(4) Å, c = 8.9854(3) Å, β = 112.359(5) ∘ , V = 772.39(5) Å 3 , Z = 2, R gt ( F ) = 0.0274, wR ref ( F 2 ) = 0.0725, T = 293 K.
Open Access
The crystal structure of catena-poly[aqua-2,2′bipyridine-κ²N,N′-(μ₂-5-ethoxyisophthalato-κ ⁴O,O′:Oʺ,O′ʺ)cadmium(II)] monohydrate, C₂₀H₂₀CdN₂O₇

May 5, 2022

Lilei Zhang, Deming Chang, Mengdan Dun

Page range: 615-617

Download PDF

C 20 H 20 CdN 2 O 7 , monoclinic, P 2 1 / c (no. 14), a = 9.0154(3) Å, b = 17.7168(8) Å, c = 12.8449(5) Å, β = 98.537(4)°, V = 2028.91(14) Å 3 , Z = 4, R gt ( F ) = 0.0320, w R ref ( F 2 ) = 0.0715, T = 288.32(10) K.
Open Access
The crystal structure of (1S,3R)-1-(4-isopropylphenyl)-3-(methoxycarbonyl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-2-iumchloride monohydrate, C₂₂H₂₇ClN₂O₃

May 5, 2022

Jingxiao Zhang, Miao Gu, Xinyu Bai

Page range: 619-621

Download PDF

C 22 H 27 ClN 2 O 3 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 8.6797(3) Å, b = 9.8809(3) Å, c = 24.7824(8) Å, V = 2125.42(12) Å 3 , Z = 4, R gt ( F ) = 0.0478, wR ref ( F 2 ) = 0.1082, T = 170 K.
Open Access
Crystal structure of 1-isopropyl-3-(prop-1-en-2-yl)-1H-pyrazolo[3,4-d]pyrimidin-4-amine, C₁₁H₁₅N₅

May 17, 2022

Yanjiao Wang, Xiaoqin Tang, Bin Liu

Page range: 623-625

Download PDF

C 11 H 15 N 5 , monoclinic, P 2 1 / c (no. 14), a = 9.5677(16) Å, b = 8.1755(15) Å, c = 14.846(3) Å, β = 93.783(4)°, V = 1158.7(4) Å 3 , Z = 4, R gt ( F ) = 0.0473, wR ref ( F 2 ) = 0.1425, T = 173 K.
Open Access
The crystal structure of (2,2′-bipyridine-κ²N,N′)- bis(6-phenylpyridine-2-carboxylate-κ²N,O)manganese(II)] monohydrate, C₃₄H₂₆N₄O₅Mn

May 12, 2022

Xi-Shi Tai, Li-Hua Wang

Page range: 627-630

Download PDF

C 34 H 26 N 4 O 5 Mn, monoclinic, C2/c (no. 15), a = 29.4330(18) Å, b = 10.4120(6) Å, c = 20.0207(12) Å, β = 107.246(6)°, V = 5859.6(6) Å 3 , Z = 8, R gt ( F ) = 0.0380, wR ref ( F 2 ) = 0.0865, T = 200 K.
Open Access
Crystal structure of the cocrystal 1,3,5,7-tetranitro-1,3,5,7-tetrazoctane ─ 2,3-dihydroindole (1/1), C₁₂H₁₇N₉O₈

May 13, 2022

Penghua Liu, Jiangtao Xing, Zhiqiang Wang, Baomin Wang

Page range: 631-633

Download PDF

C 12 H 17 N 9 O 8 , orthorhombic, Pna 2 1 (no. 33), a = 11.376(4) Å, b = 7.966(2) Å, c = 19.076(6) Å, V = 1728.6(9) Å 3 , Z = 4, R gt ( F ) = 0.0373, wR ref ( F 2 ) = 0.0908, T = 296 K.
Open Access
Crystal structure of 3-acetyl-6-hydroxy-2H-chromen-2-one monohydrate, C₁₁H₁₀O₅

May 13, 2022

Zhi-Qiang Xiong, Ling Yang, Shu-Zhen Xiao, Chen-Yu Yang, Xu-Liang Nie

Page range: 635-637

Download PDF

[C 11 H 10 O 5 ], monoclinic, P 2 1 / n , a = 7.041(3) Å, b = 9.339(4) Å, c = 15.614(6) Å, β = 103.03°, V = 1000.2(7) Å 3 , Z = 4, R gt ( F ) = 0.0337, w R ref ( F 2 ) = 0.0994, T = 296(2) K.
Open Access
Crystal structure of 6,9-diamino-2-ethoxyacridinium 3,5-dinitrobenozate — dimethylsulfoxide — water (1/1/1), C₂₄H₂₇N₅O₉S

May 17, 2022

Artur Mirocki

Page range: 639-641

Download PDF

C 24 H 27 N 5 O 9 S, triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 7.5749(4) Å, b = 10.0368(5) Å, c = 17.9111(10) Å, α = 87.224(4)°, β = 83.678(4)°, γ = 85.414(4)°, V = 1348.04(12) Å 3 , Z = 2, R gt ( F ) = 0.0562, w R ref ( F 2 ) = 0.1477, T = 295(2) K.
Open Access
The crystal structure of 4,4′-bipyridinium bis-(2-hydroxy-3-methoxybenzoate), 2(C₈H_7.68O₄)·C₁₀H_8.64N₂

May 13, 2022

Devin J. Angevine, Jason B. Benedict

Page range: 643-645

Download PDF

C 26 H 24 N 2 O 8 , monoclinic, P 2 1 / c (no. 14), a = 6.9170(9) Å, b = 26.012(3) Å, c = 12.7449(17) Å, β = 91.896(4)°, V = 2291.9(5) Å 3 , Z = 4, R gt ( F ) = 0.0471, wR ref ( F 2 ) = 0.1320, T = 90 K.
Open Access
Crystal structure of (Z)-4-(((4-fluorophenyl)amino)(furan-2-yl)methylene)-5-methyl-2-phenyl-2,4-dihydro-3H-pyrazol-3-one

May 20, 2022

Qiong Wu, Li Zhang, Jun-Jie Gao, Liu Yang, Heng-Qiang Zhang, Li-Li Fan, Ya-Zhai Zhang

Page range: 647-649

Download PDF

C 22 H 16 FN 3 O 2 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 8.7335(18) Å, b = 9.967(2) Å, c = 11.968(3) Å, α = 70.677(4)°, β = 86.259(4)°, γ = 65.759(4) Å, V = 893.4(3) Å 3 , Z = 2, R gt ( F ) = 0.0543, wR ref ( F 2 ) = 0.1677, T = 296(2) K.
Open Access
The crystal structure of bis(4-chloro-2-(((2-chloroethyl)imino)methyl)phenolato-κ²N,O)-oxidovanadium(IV), C₁₈H₁₆Cl₄N₂O₃V

May 20, 2022

Wei Wei, Ya-Zhai Zhang, Heng-Qiang Zhang, Qi-Ying Zhang, Zhao-Kun Xuan, Hong-Li Chen

Page range: 651-653

Download PDF

C 18 H 16 Cl 4 N 2 O 3 V, orthorhombic, Pbca (no. 61), a = 7.8555(3) Å, b = 21.6645(7) Å, c = 23.7584(8) Å, V = 4043.3(2) Å 3 , Z = 8, R gt ( F ) = 0.0296, wR ref ( F 2 ) = 0.0799, T = 296(2) K.
Open Access
The crystal structure of 17-(bromoethynyl)-17-hydroxy-10, 13-dimethyl- 1,2,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-3H-cyclopenta[a]phenanthren-3-one, C₂₁H₂₇BrO₂

May 20, 2022

Xiao-Liang Ji, Feng Xie, Yi-Biao Li

Page range: 655-657

Download PDF

C 21 H 27 BrO 2 , monoclinic, P 2 1 (no. 4), a = 6.6220(14) Å, b = 11.7640(2) Å, c = 11.8485(2) Å, β = 95.0757(19)° V = 919.39(3) Å 3 , Z = 2, R gt ( F ) = 0.0264, wR ref ( F 2 ) = 0.0695, T = 150 K, Flack-parameter = 0.007(13).
Open Access
The crystal structure of 4-((6-fluoropyridin-2-yloxy)methyl)benzonitrile, C₁₃H₉FN₂O

May 20, 2022

Zhi-Qiang Lu

Page range: 659-660

Download PDF

C 13 H 9 FN 2 O, triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 7.4664(8) Å, b = 8.2700(7) Å, c = 10.0709(11) Å, α = 76.991(8)°, β = 88.403(9)°, γ = 63.619(10)° V = 540.93(10) Å 3 , Z = 2, R gt (F) = 0.0534, w R ref (F 2 ) = 0.1644, T = 293(2) K.
Open Access
Crystal structure of (Z)-2-(1-bromo-2-phenylvinyl)-5-ethyl-2-methyl-1,3-dioxane-5-carboxylic acid, C₁₅H₁₇Br₁O₄

May 20, 2022

Guo-Kai Jia, Xian-You Yuan

Page range: 661-662

Download PDF

C 15 H 17 Br 1 O 4 , monoclinic, P 2 1 / n (no. 14), a = 7.1178(16) Å, b = 8.752(2) Å, c = 24.554(6) Å, β = 94.761(3)°, V = 1524.3(6) Å 3 , Z = 4, R gt ( F ) = 0.0275, w R ref ( F 2 ) = 0.0694, T = 296(2) K.
Open Access
Crystal structure of catena-poly[tribenzyl-κ¹C-(μ₂-6-oxidopyridin-1-ium-3-carboxylato-κ²O:O’)tin(IV)-dichloromethane-methanol (1/1/1), C₂₉H₃₁Cl₂NO₄Sn

May 20, 2022

Zhongjun Gao, Haifeng Zhang

Page range: 663-665

Download PDF

C 29 H 31 Cl 2 NO 4 Sn, monoclinic, P 2 1 / n (no. 14), a = 10.638(4) Å, b = 17.168(7) Å, c = 18.399(5) Å, β = 120.573(16)°, V = 2893.1(18) Å 3 , Z = 4, R gt ( F ) = 0.0314, wR ref ( F 2 ) = 0.0875, T = 298 K.
Open Access
Crystal structure of bis{2-(tert-butyl)-6-((E)-((4-((E)-1-(methoxyimino)ethyl)phenyl)imino)methyl)phenolato-κ²N,O}zinc(II), C₄₀H₄₆N₄O₄Zn

May 17, 2022

Ji-Xing Zhao, Lei-Fang Wu, Da-Qun Chen

Page range: 667-669

Download PDF

C 40 H 46 N 4 O 4 Zn, monoclinic, P 2 1 / n (no. 14), a = 12.0198(4) Å, b = 28.0212(9) Å, c = 12.0655(4) Å, β = 110.727(2)°, V = 3800.8(2) Å 3 , Z = 4, R gt ( F ) = 0.0442, wR ref ( F 2 ) = 0.1076, T = 173(2) K.
Open Access
Crystal structure of diaqua-bis(μ₂-2-carboxy-3,4,5,6-tetrafluorobenzoato-κ²O:O′)-bis(phenanthroline-κ²N,N′)-bis(μ₂-3,4,5,6-tetrafluorophthalato-κ³O:O,O′)dieuropium(III) – phenanthroline (1/2), C₄₀H₁₉EuF₈N₄O₉

May 20, 2022

Xiao-Yu Zhang, Xin-Fang Liu, Bei-Bei Zhao, Shi-Jie Huang

Page range: 671-674

Download PDF

C 40 H 19 EuF 8 N 4 O 9 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 11.3326(4) Å, b = 12.7652(4) Å, c = 13.2629(4) Å, α = 102.266(2)°, β = 97.689(2)°, γ = 105.630(3)°, V = 1767.93(10) Å 3 , Z = 2, R gt ( F ) = 0.0329, wR ref ( F 2 ) = 0.0648, T = 293(2) K.
Open Access
The crystal structure of diaqua-bis(6-phenylpyridine-2-carboxylato-κ²N,O) manganese(II) — water — dimethylformamide (1/2/1), C₂₇H₃₁N₃O₉Mn

May 20, 2022

Li-Hua Wang, Xi-Shi Tai

Page range: 675-677

Download PDF

C 27 H 31 N 3 O 9 Mn, monoclinic, P 2 1 / n (no. 14), a = 10.8917(9) Å, b = 11.2673(16) Å, c = 23.077(3) Å, β = 93.319(10)°, V = 2827.2(6) Å 3 , Z = 4, R gt ( F ) = 0.0735, wR ref ( F 2 ) = 0.1938, T = 250 K.
Open Access
The crystal structure of bis(pyrazolo[1,5-a]pyrimidine-3-carboxylato-κ²N,O)-copper(ii), C₁₄H₈N₆O₄Cu

May 20, 2022

Dong-Feng Hong, Ye Chen, Wen-Li Zhu

Page range: 679-680

Download PDF

C 14 H 8 N 6 O 4 Cu, monoclinic, C 2/ c (no. 15), a = 15.6054(8) Å, b = 7.0441(3) Å, c = 12.6301(6) Å, β = 108.550(5)°, V = 1316.24(11) Å 3 , Z = 4, R gt ( F ) = 0.0317, wR ref ( F 2 ) = 0.0778, T = 293 K.
Open Access
Crystal structure of poly[(μ₂-1-(1-imidazolyl)-4-(imidazol-1-ylmethyl)benzene-κ²N:N′)-(μ₃-pyridazine-4,5-dicarboxylate-κ³O:O′:N)]copper(II) hydrate, C₁₉H₁₆CuN₆O₅

May 20, 2022

Guang-Zhen Liu, Xiu-Jin Wang, Wen-Hui Wei

Page range: 681-683

Download PDF

C 19 H 16 CuN 6 O 5 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 9.0143(3) Å, b = 9.2122(3) Å, c = 11.8205(4) Å, α = 82.900(3)°, β = 74.593(3)°, γ = 83.612(3), V = 935.90(5) Å 3 , Z = 2, R gt ( F ) = 0.0284, wR ref ( F 2 ) = 0.0684, T = 293 K.
Open Access
Crystal structure of acrinidinium tetrafluorohydrogenphthalate, C₂₁H₁₁F₄NO₄

May 20, 2022

Xin-Fang Liu, Jun-Ya Song, Bei-Bei Zhao, Shi-Jie Huang

Page range: 685-687

Download PDF

C 21 H 11 F 4 NO 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 9.5000(4) Å, b = 13.9989(7) Å, c = 14.1423(5) Å, α = 91.355(4)°, β = 108.542(4)°, γ = 98.958(4)°, V = 1756.02(14) Å 3 , Z = 4, R gt ( F ) = 0.0494, wR ref ( F 2 ) = 0.1157, T = 293(2) K.
Open Access
Crystal structure of 2-(1H-pyrazol-3-yl-κN)pyridine-κN-bis(2-(2,4-difluorophenyl)pyridinato-κ²C,N)iridium(III) sesquihydrate, C₃₀H₁₈F₄IrN₅·1.5[H₂O]

May 25, 2022

Aqilah Abdul Latiff, Yan Yi Chong, Wun Fui Mark-Lee, Mohammad B. Kassim

Page range: 689-692

Download PDF

C 30 H 18 F 4 IrN 5 ·1.5[H 2 O], tetragonal, I 4 1 / a (no. 88), a = 37.5562(5) Å, b = 37.5562(5) Å, c = 9.2031(2) Å, V = 12980.7(4) Å 3 , Z = 16, R gt ( F ) = 0.0312, wR ref ( F 2 ) = 0.1166, T = 300(2) K.
Open Access
Crystal structure of 2-(2-hydroxy-5-nitrophenyl)-5-methyl-1,3-dioxane-5-carboxylic acid, C₁₂H₁₃N₁O₇

May 24, 2022

Guo-Kai Jia, Xian-You Yuan

Page range: 693-694

Download PDF

C 12 H 13 N 1 O 7 , monoclinic, P 2 1 / c (no. 14), a = 11.416(7) Å, b = 13.860(8) Å, c = 8.215(5) Å, β = 99.607(6)°, V = 1281.6(13) Å 3 , Z = 4, R gt ( F ) = 0.0433, wR ref ( F 2 ) = 0.1274, T = 293(2) K.
Open Access
The crystal structure of 1,2-bis(pyridinium-4-yl)ethane diperchlorate, C₁₂H₁₄N₂·2ClO₄ – a second polymorph

May 25, 2022

Qi-Ming Qiu, Jian-Biao Song, Li Yan, Ai-Guo Dong, Chuan-Tao Li, Zhi-Yuan Zheng

Page range: 695-696

Download PDF

C 12 H 14 N 2 ·2ClO 4 , monoclinic, P 2 1 / c (no. 14), a = 5.3170(4) Å, b = 12.8711(8) Å, c = 11.6788(7) Å, β = 100.888(2)°, V = 784.86(9) Å 3 , Z = 2, R gt ( F ) = 0.0434, wR ref ( F 2 ) = 0.1211, T = 298 K.
Open Access
The crystal structure of [(1,10-phenantroline-κ²N,N′)-bis(6-phenylpyridine-2-carboxylato-κ²N,O)manganese(II)] monohydrate, C₃₆H₂₆N₄O₅Mn

May 25, 2022

Zhang Hua-Xiang, Tai Xi-Shi

Page range: 697-699

Download PDF

C 36 H 26 N 4 O 5 Mn, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 10.7134(7) Å, b = 10.7573(10) Å, c = 26.6304(18) Å, β = 90°, V = 3069.1(4) Å 3 , Z = 4, R gt ( F ) = 0.0454, wR ref ( F 2 ) = 0.0890, T = 220 K.
Open Access
Crystal structure of 1,2-bis(2,2,3,3,5,5,5-heptamethyl-1,1,4,4- tetrakis(trimethylsilyl)pentasilan-1-yl)ditellane, C₃₈H₁₁₄Si₁₈Te₂

May 25, 2022

Fan Qi, Xu-Qiong Xiao

Page range: 701-703

Download PDF

C 38 H 114 Si 18 Te 2 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 9.0857(18) Å, b = 9.7412(19) Å, c = 24.213(5) Å, α = 94.25(3)°, β = 95.26(3)°, γ = 117.58(3)°, V = 1874.9(6) Å 3 , Z = 1, R gt ( F ) = 0.0425, wR ref ( F 2 ) = 0.1580, T = 296(2) K.
Open Access
Crystal structure of 1,2-bis(2,4-dinitro-1H-imidazol-1-yl)ethane – dimethylformamide (1/1), C₁₁H₁₃N₉O₉

May 26, 2022

Yuan Jun, Wu Bingheng, Wang Yong, Wang Jianlong, Cao Duanlin, Chen Lizhen

Page range: 705-706

Download PDF

C 11 H 13 N 9 O 9 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.6588(3) Å, b = 8.7538(3) Å, c = 11.7312(4) Å, α = 78.230(1)°, β = 82.060(1)°, γ = 76.031(1)° V = 841.05(5) Å 3 , Z = 2, R gt ( F ) = 0.0376, wR ref ( F 2 ) = 0.1006, T = 150.0 K.
Open Access
Crystal structure of (Z)-3-((tert-butylamino) methylene)-2-(2-hydroxynaphthalen-1-yl) chroman-4-one, C₂₄H₂₃NO₃

May 31, 2022

Tianhao Liu, Menglan Lv

Page range: 707-709

Download PDF

C 24 H 23 NO 3 , orthorhombic, Pna 2 1 , a = 8.2490(11) Å, b = 15.886(2) Å, c = 16.218(2) Å, β = 99.465(2)°, Z = 4, V = 2096.4(5) Å 3 , R gt ( F ) = 0.0545, wR ref ( F 2 ) = 0.1688, T = 273 K.
Open Access
Synthesis and crystal structure of (E)-1-(4-(((E)-3-(tert-butyl)-2-hydroxybenzylidene)amino)phenyl)ethan-1-one O-ethyl oxime, C₂₁H₂₆N₂O₂

May 31, 2022

Ji-Xing Zhao, Da-Qun Chen, Lei-Fang Wu

Page range: 711-713

Download PDF

C 21 H 26 N 2 O 2 , monoclinic, P 2 1 (no. 4), a = 7.1425(7) Å, b = 9.2733(8) Å, c = 14.3161(13) Å, β = 93.592(4)°, V = 946.36(15) Å 3 , Z = 2, R gt ( F ) = 0.0461, wR ref ( F 2 ) = 0.1148, T = 173(2) K.
Open Access
Crystal structure of the double salt bis(5-amino-1,2,4-triazol-4-ium-3-yl)methane hydrogen oxalate hemioxalate, C₈H₁₁N₈O₆

May 31, 2022

Guo-tao Zhang, Hua Wang, Hong-ya Li, Biao Yan

Page range: 715-717

Download PDF

C 8 H 11 N 8 O 6 , monoclinic, P 2 1 / n (no. 14), a = 5.6348(8) Å, b = 19.485(3) Å, c = 11.5316(17) Å, β = 101.013(2)°, V = 1242.8(3) Å 3 , Z = 4, R gt ( F ) = 0.0396, w R ref ( F 2 ) = 0.1039, T = 296(2) K.
Open Access
Hydrothermal synthesis and crystal structure of catena-poly[diaqua-bis(μ₂-4-[(4-pyridinylmethyl)amino]benzoato-κ²N:O)cobalt(II)]–1,2bi(4-pyridyl)ethene–water (1/1/1), C₅₀H₅₀N₈O₈Co

May 31, 2022

Liu Guang-Zhen, Ya-Di Li

Page range: 719-721

Download PDF

C 50 H 50 N 8 O 8 Co, triclinic, P 1 ‾ $\overline{1}$ , a = 9.2920(4) Å, b = 11.3648(5) Å, c = 11.9954(4) Å, α = 96.478(3)°, β = 104.766(3)°, γ = 103.901(4)°, V = 1168.40(8) Å 3 , Z = 1, R gt ( F ) = 0.0393, wR ref ( F 2 ) = 0.1431, T = 293(2) K.
Open Access
Crystal structure of 3-(3-bromophenyl)-1′,3′-dimethyl-2′H,3H,4H-spiro[furo[3, 2-c]chromene-2,5′-pyrimidine]-2′,4,4′,6′(1′H,3′H) tetraone, C₂₂H₁₅BrN₂O₆

May 31, 2022

Dong-Li Jiang, Lian-Lian Fan, Peng Yin, Di Liang, Rui Li

Page range: 723-724

Download PDF

C 22 H 15 BrN 2 O 6 , monoclinic, P 2 1 / c (No. 14), a = 5.1760 (5) Å, b = 17.5652(19) Å, c = 21.734(2) Å, β = 94.690(3) °, Z = 4, V = 1969.3(3) Å 3 , R gt ( F ) = 0.0569, wR ref ( F 2 ) = 0.1206, T = 170 K.
Open Access
The crystal structure of poly[aqua-(μ₂-4,4′- bis(imidazolyl)biphenyl-κ²N:N′)-(μ₂-3-nitrobenzene-1,2-dicarboxylato-κ²O:O′)]copper (II) hydrate, C₂₆H₂₁N₅O₈Cu

May 31, 2022

Gui-Lian Li, Meng-Ni Liu, Gao-Jing Du, Jin-Yuan Zhang

Page range: 725-727

Download PDF

C 26 H 21 N 5 O 8 Cu, monoclinic, P 2 1 / c (no. 14), a = 17.2262(10) Å, b = 7.3474(3) Å, c = 21.1086(11) Å, β = 111.498(6)°, V = 2485.8(2) Å 3 , Z = 4, R gt ( F ) = 0.0629, wR ref ( F 2 ) = 0.1433, T = 293(2) K.
Open Access
The crystal structure of bis(4-(6-carboxy-8-ethyl-3-fluoro-5-oxo-5,8-dihydro-1,8-naphthyridin-2- yl)piperazin-1-ium) adipate tetrahydrate, C₃₆H₅₂F₂N₈O₁₄

May 31, 2022

Cheng-Jun Jiang, Ying-Fan Xia

Page range: 729-731

Download PDF

C 36 H 52 F 2 N 8 O 14 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 6.9775(4) Å, b = 9.0785(6) Å, c = 16.8942(10) Å, β = 92.778(2)°, V = 990.91(11) Å 3 , Z = 1, R gt ( F ) = 0.0397, wR ref ( F 2 ) = 0.1088, T = 170 K.
Open Access
Synthesis and crystal structure of poly[aqua(μ₄-(1R,2S,4R)-4-hydroxy-1-((7-hydroxy-3-(4-hydroxy-3-sulfonatophenyl)-4-oxo-4H-chromen-8-yl)methyl)pyrrolidin-1-ium-2-carboxylate-κ⁴O:O′:O″:O‴)sodium(I)] monohydrate, C₂₁H₂₂NNaO₁₂S

June 8, 2022

Hai-Lin Chen, Xiu-Xiang Huang, Jian-Jing Lan, Dong-Mei Yao, Yan-Ping Wang, Qiu-Ping Liu

Page range: 733-735

Download PDF

C 21 H 22 NNaO 12 S, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 7.6850(1) Å, b = 10.8030(1) Å, c = 25.9262(2) Å, V = 2152.42(4) Å 3 , Z = 4, R gt ( F ) = 0.0309, wR ref ( F 2 ) = 0.0818, T = 100.0(4) K.
Open Access
Crystal structure of chlorido-(η⁶-toluene)(2,2′-bipyridine-κ²N,N′)ruthenium(II) hexafluorophosphate, C₁₇H₁₆ClN₂RuPF₆

June 10, 2022

Joel M. Gichumbi, Sizwe J. Zamisa, Holger B. Friedrich

Page range: 737-739

Download PDF

C 17 H 16 ClN 2 RuPF 6 , monoclinic, P 2 1 / c (no. 14), a = 14.4426(9) Å, b = 8.3311(5) Å, c = 16.413(1) Å, β = 109.2690°, V = 1864.2(2) Å 3 , Z = 4, R gt ( F ) = 0.0309, wR ref ( F 2 ) = 0.0697, T = 173 K.
Open Access
The crystal structure of (R)-6-hydroxy-8-methoxy-3-methylisochroman-1-one, C₁₁H₁₂O₄

June 9, 2022

Hong Li, Can–Kai Lin, Rong-Chun Huang, Kai-Xin Chen, Hai-Xuan Liang, Yan-Jia Cai, Zi-Feng Chen, Yi-Wen Tao, Bo Ding

Page range: 741-743

Download PDF

C 11 H 12 O 4 , monoclinic, P 2 1 (no. 4), a = 15.4586(2) Å, b = 7.80238(13) Å, c = 16.4003(2) Å, β = 91.0103(13)°, V = 1977.81(5) Å 3 , Z = 8, R gt ( F ) = 0.0413, wR ref ( F 2 ) = 0.1045, T = 180 K.
Open Access
Crystal structure of catena-poly[(5,5,7,12,12,14-hexamethyl -1,4,8,11-tetraazacyclotetradecane- κ⁴N,N′,Nʺ,N‴)nickel(II)-(μ₂-perchlorato-κ²O:O′)] 3,5-dicarboxybenzoate – methanol (1/2), C₂₇H₄₉ClN₄NiO₁₂

June 10, 2022

Qiong Wang, Guang-Chuan Ou

Page range: 745-747

Download PDF

C 27 H 49 ClN 4 NiO 12 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 11.180(2) Å, b = 12.320(3) Å, c = 12.754(3) Å, α = 98.263(2)°, β = 97.524(2)°, γ = 99.470(2)°, V = 1693.1(6) Å 3 , Z = 2, R gt ( F ) = 0.0423, w R ref ( F 2 ) = 0.1238, T = 296(2) K.
Open Access
The crystal structure of 4-(chloromethyl)benzonitrile, C₈H₆ClN

June 10, 2022

Mingzhi Miao, Ji Li

Page range: 749-750

Download PDF

C 8 H 6 ClN, orthorhombic, Pnma (no. 62), a = 20.3965(7) Å, b = 7.8164(3) Å, c = 4.5015(2) Å, V = 717.66(5) Å 3 , Z = 4, R gt ( F ) = 0.0265, wR ref ( F 2 ) = 0.0670, T = 100.0 K.
Open Access
The crystal structure of dimethylammonium 8-[(7,9-dioxo-6,10-dioxaspiro[4.5]decan-8-ylidene)methyl]-9-oxo-6,10-dioxaspiro[4.5]dec-7-en-7-olate, C₁₉H₂₅NO₈

June 10, 2022

Xia Wang, Yani Dong, Wulan Zeng, Xiaolong Zhang, Mengying Zhou, Keyu Chen

Page range: 751-753

Download PDF

C 19 H 25 NO 8 , monoclinic, P 2 1 / n (no. 14), a = 10.149(2) Å, b = 12.338(3) Å, c = 15.898(3) Å, β = 97.58(3)°, V = 1973.2(7) Å 3 , Z = 4, R gt ( F ) = 0.0581, wR ref ( F 2 ) = 0.1842, T = 293(2) K.
Open Access
Crystal structure of (2R,3S,4S,5R,6S)-2-(acetoxymethyl)-6-((1-acetyl-5-bromo-4-chloro-1H-indol-3-yl)oxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate hemihydrate C₂₄H₂₅BrClNO₁₁

June 13, 2022

Yucong Liu, Pingqiao Wang, Haixin Ding

Page range: 755-757

Download PDF

C 24 H 25 BrClNO 11 , monoclinic, C 2 (no. 5), a = 28.914(5) Å, b = 7.9349(14) Å, c = 13.062(2) Å, β = 114.867(3)°, V = 2718.9(8) Å 3 , Z = 4, R gt ( F ) = 0.0352, w R ref ( F 2 ) = 0.0888, T = 296.15 K.
Open Access
The crystal structure of the co-crystal tetrakis[2-(tris(4-methoxyphenyl)stannyl)ethyl]silane – tetrahydrofuran – toluene – tetrahydrofurane (1/1/1), C₁₀₃H₁₁₆O₁₃SiSn₄

June 10, 2022

Yilmaz Aksu, Elisabeth Irran, Sevil Aksu

Page range: 759-763

Download PDF

C 103 H 116 O 13 SiSn 4 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 14.8676(4) Å, b = 17.6664(4) Å, c = 20.8357(6) Å, α = 106.430(2)°, β = 107.192(2)°, γ = 100.898(2)°, V = 4787.5(2) Å 3 , Z = 2, R gt ( F ) = 0.0325, w R ref ( F 2 ) = 0.0845, T = 150 K.
Open Access
Crystal structure of methyl 3-(1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)propanoate, C₁₆H₁₃NO₄

June 10, 2022

Tiantian Wang, Yizi Su, Yunyun Feng, Xin Deng, Yuxing Tan

Page range: 765-766

Download PDF

C 16 H 13 NO 4 , monoclinic, P 2 1 / c (no. 14), a = 9.930(3) Å, b = 6.9807(18) Å, c = 18.954(5) Å, β = 93.080(4)°, V = 1311.9(6) Å 3 , Z = 4, R gt ( F ) = 0.0400, wR ref ( F 2 ) = 0.1142, T = 296 (2) K.
Open Access
Crystal structure of ethyl (Z)-3-amino-2-cyano-3-(2-oxo-2H-chromen-3-yl)acrylate, C₁₅H₁₂N₂O₄

June 10, 2022

Chun-Mei Guo, Sha Chen, Mei-Jun Chu, Min Wan, Xu-Liang Nie

Page range: 767-768

Download PDF

C 15 H 12 N 2 O 4 , monoclinic, P 2 1 / c (no. 14), a = 5.4588(5) Å, b = 29.629(3) Å, c = 8.1217(8) Å, β = 93.157(1)°, V = 1311.6(2) Å 3 , Z = 4, R gt ( F ) = 0.0346, w R ref ( F 2 ) = 0.0925, T = 296(2) K.
Open Access
Crystal structure of methyl 2-(1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)acetate, C₁₅H₁₁NO₄

June 13, 2022

Wei Peng, Jicai Yang, Yu Yue, Xin Deng, Wujiu Jiang

Page range: 769-771

Download PDF

C 15 H 11 NO 4 , monoclinic, P 2 1 / n (no. 14), a = 8.0909(6) Å, b = 24.4463(18) Å, c = 12.6980(10) Å, β = 96.6020(10)°, V = 2494.9(3) Å 3 , Z = 8, R gt ( F ) = 0.0470, wR ref ( F 2 ) = 0.1273, T = 296 (2) K.
Open Access
Crystal structure of catena-poly[diaqua-bis(μ₂-1,3-di(1H-imidazol-1-yl)propane-κ²N:N′)cobalt(II)] tetrafluoroterephthalate, C₂₆H₂₈N₈O₆F₄Co

June 13, 2022

Xiao-Zhou Huang, Jiu-Fu Lu

Page range: 773-774

Download PDF

C 26 H 28 N 8 O 6 F 4 Co, monoclinic, C 2/ m (no. 12), a = 15.7590(18) Å, b = 11.6981(15) Å, c = 9.1210(12) Å, β = 121.227(7)°, V = 1437.8(3) Å 3 , Z = 2, R gt ( F ) = 0.0323, wR ref ( F 2 ) = 0.0904, T = 293(2) K.

Issues in this Volume

Search the content of this journal

This issue

All issues

Issues in this Volume