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Zeitschrift für Kristallographie - New Crystal Structures

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Frontmatter

26. Oktober 2019

Seiten: i-vii

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Open Access
Crystal structure of [aqua[2,2′-(1,2-phenylene)bis(1H-imidazole-4-carboxylato-5-carboxy)-κ⁴N³,N³′,O⁴,O⁴′] zinc(II)] monohydrate, C₁₆H₁₀N₄O₉Zn⋅H₂O

17. August 2019

Wen-Bin Wang, Xin-Chang Shi, Ying-Ying Li, Fang-Rong Cheng

Seiten: 1133-1135

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C 16 H 12 N 4 O 10 Zn, monoclinic, C 2/ c (no. 15), a = 18.6618(10) Å, b = 13.5466(6) Å, c = 14.7722(8) Å, β = 108.481(2)°, V = 3541.9(3) Å 3 , Z = 8, R gt ( F ) = 0.0392, wR ref ( F 2 ) = 0.1061, T = 293(2) K.
Open Access
Crystal structure of ethyl 3-(4-methoxyphenyl)-5-methylcarbamoyl-1H-pyrazole-4-carboxylate, C₁₅H₁₇N₃O₄

9. September 2019

Fatin Nur Ain Abdul Rashid, Mohd Fazli Mohammat, Suhana Arshad, Zurina Shaameri, Ahmad Sazali Hamzah

Seiten: 1137-1139

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C 15 H 17 N 3 O 4 , triclinic, P 1̄ (no. 2), a = 10.5986(5) Å, b = 11.5298(5) Å, c = 13.5386(6) Å, α = 102.694(1)°, β = 102.999(1)°, γ = 108.918(1)°, V = 1446.03(11) Å 3 , Z = 4, R gt ( F ) = 0.0525, wR ref ( F 2 ) = 0.1526, T = 100(1) K.
Open Access
7-(4-Fluorobenzylidene)-3-(4-fluorophenyl)-N-phenyl-3,3a,4,5,6,7-hexahydro-2H-indazole-2-carbothioamide–dimethylformamide (2/1), C₂₇H₂₃F₂N₃S, 0.5(C₃H₇NO)

17. August 2019

Obaid Fahad Aldosari, Bakr F. Abdel-Wahab, Mohammad Hayal Alotaibi, Amany S. Hegazy, Benson M. Kariuki, Gamal A. El-Hiti

Seiten: 1141-1143

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C 27 H 23 F 2 N 3 S, 0.5(C 3 H 7 NO), monoclinic, C 2/ c (no. 15), a = 25.1579(10) Å, b = 9.9356(4) Å, c = 20.1799(7) Å, β = 91.741(4)°, V = 5041.8(3) Å 3 , Z = 8, R gt ( F ) = 0.0508, wR ref ( F 2 ) = 0.1385, T = 296(2) K.
Open Access
Crystal structure of 4,4′-(hydrazonomethylene)diphenol dihydrate, C₁₃H₁₆N₂O₄

23. August 2019

Xia Li, Shangjun Liu

Seiten: 1145-1146

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C 13 H 16 N 2 O 4 , monoclinic, P 2 1 / c (no. 14), a = 13.312(2) Å, b = 8.8222(13) Å, c = 12.4784(18) Å, β = 115.350(2)°, V = 1324.4(3) Å 3 , Z = 4, R gt ( F ) = 0.0372, wR ref ( F 2 ) = 0.0739, T = 293 K.
Open Access
Crystal structure of 4-methoxyphenyl-3-phenylpropiolate, C₁₆H₁₂O₃

9. September 2019

Jun Pan, Guo-Kai Jia, Fang Liu, Xiao-Ming Chen, Xing-Yu Zhang

Seiten: 1147-1148

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C 16 H 12 O 3 , orthorhombic, Pbca (no. 19), a = 3.9935(16) Å, b = 16.629(7) Å, c = 19.406(8) Å, V = 1288.7(9) Å 3 , Z = 4, R gt ( F ) = 0.0387, wR ref ( F 2 ) = 0.1084, T = 296(2) K.
Open Access
Crystal Structure of tris(tetrakis{1-vinyl-1H-imidazole-κN}copper(II)) bis[tri-μ₂-bromido-tetrabromido-bis(1-vinyl-1H-imidazole-κN)tetracopper(I)], C₈₀H₉₆N₃₂Cu₁₁Br₁₄

25. September 2019

Fu-Jie Liu, Guo-Xi Wang

Seiten: 1149-1151

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C 80 H 96 N 32 Cu 11 Br 14 , triclinic, P 1̄ (no. 2), a = 11.370(2) Å, b = 14.287(3) Å, c = 17.621(3) Å, α = 85.929(2)°, β = 88.392(2)°, γ = 74.464(2)°, V = 2750.9(8) Å 3 , Z = 1, R gt ( F ) = 0.0432, wR ref ( F 2 ) = 0.0859, T = 296(2) K.
Open Access
Crystal structure of (E)-2-(3,6-bis(diethylamino)-9H-xanthen-9-yl)-N′-(quinoxalin-2-ylmethylene)benzohydrazide, C₃₇H₃₆N₆O₂

9. September 2019

Jun-Ying Song, Zi-Chuang Wang, Zhen-Qiang Zhang

Seiten: 1153-1155

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C 37 H 36 N 6 O 2 , monoclinic, P 2 1 / c (no. 14), a = 9.18664(12) Å, b = 14.50209(16) Å, c = 23.1787(3) Å, β = 94.0829(12)°, Z = 4, V = 3080.16(7) Å 3 , R gt ( F ) = 0.0398, wR ref ( F 2 ) = 0.1041, T = 113.5(4) K.
Open Access
Crystal structure of 4-(1-phenylimidazo[1,5-a]pyridin-3-yl)benzoic acid (C₂₀H₁₄N₂O₂)

27. September 2019

Adeleke A. Adesola, Sizwe J. Zamisa, Bernard Omondi

Seiten: 1157-1159

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C 20 H 14 N 2 O 2 , monoclinic, C 2/ c (no. 15), a = 17.8410(5) Å, b = 15.3081(4) Å, c = 11.3881(3) Å, β = 104.280(1)°, V = 3014.12(14) Å 3 , Z = 8, R gt ( F ) = 0.0364, wR ref ( F 2 ) = 0.0997, T = 100(2) K.
Open Access
Crystal structure of 3-fluoro-3-methyl-1-((2-nitrophenyl)sulfonyl)-5,5-diphenylpiperidine, C₂₄H₂₃FN₂O₄S

14. Juni 2019

Zedong Cai, Xie Huang, Wei He

Seiten: 1161-1162

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C 24 H 23 FN 2 O 4 S, orthorhombic, Pbca (no. 19), a = 14.3646(18) Å, b = 15.5927(19) Å, c = 19.645(3) Å, V = 4400.1(10) Å 3 , Z = 8, R gt ( F ) = 0.0349, wR ref ( F 2 ) = 0.0982, T = 296(2) K.
Open Access
Crystal structure of dimethyl 3,12-dibenzyl-6,10-diphenyl-3,12-diazapentacyclo [6.3.1.0^2.7.0^4.11.0^5.9]-dodecane-7,11-dicarboxylate — acetone (2/1), C₄₀H₃₈N₂O₂ ⋅ 0.5C₃H₆O

2. August 2019

Ya-Nan Wang, Yan Wu, Ye Tian

Seiten: 1163-1166

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C 83 H 82 N 4 O 5 , monoclinic, P 2 1 / c (no. 14), a = 21.705(8) Å, b = 18.455(6) Å, c = 17.774(7) Å, β = 112.216(6)°, V = 6591(4) Å 3 , Z = 4, R gt ( F ) = 0.0647, wR ref ( F 2 ) = 0.1531, T = 128 K.
Open Access
Crystal structure of poly[(μ₂-2-(1H-1,2,4-triazol-1-yl)benzoato-κ⁴O:O′:N:N′)silver(I)] monohydrate, C₉H₈AgO₃N₃

2. August 2019

Kai-Hui Li, Peng Zhang

Seiten: 1167-1168

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C 9 H 8 AgO 3 N 3 , monoclinic, P 2 1 / n (no. 14), a = 6.5358(3) Å, b = 6.0583(4) Å, c = 24.9951(11) Å, β = 92.040(4)°, V = 989.08(8) Å 3 , Z = 4, R gt ( F ) = 0.0297, wR ref ( F 2 ) = 0.0552, T = 288.74(10) K.
Open Access
Crystal structure of poly[(μ₂-9H-carbazole-3,6-dicarboxylate-κ⁴O¹,O²:O³,O⁴)(μ₂-1,3-di(pyridin-4-yl)propane-κ²N:N^′)cadmium(II)]monohydrate, C₂₇H₂₃N₃O₅Cd

29. August 2019

Daguang Wang, Wei Li, Yabin Sun

Seiten: 1169-1171

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C 27 H 23 N 3 O 5 Cd, monoclinic, P 2 1 / n (no. 14), a = 9.6161(7) Å, b = 16.5427(11) Å, c = 15.8900(11) Å, β = 105.653(1)°, V = 2434.0(3) Å 3 , Z = 4, R gt ( F ) = 0.0327, wR ref ( F 2 ) = 0.0828, T = 152(2) K.
Open Access
The synthesis and crystal structure of bis(2-(benzo[d]thiazol-2-yl)-5-methylbenzen-1-ido-κ²C,N)-(N,N′-diethyldithiocarbamato-κ²S,S′)iridium(III), C₃₃H₃₀N₃S₄Ir

18. Juli 2019

Lianqing Chen, Zhongda Wu, Jing Yang, Shijuan Zhang

Seiten: 1173-1176

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C 33 H 30 N 3 S 4 Ir, monoclinic, P 2 1 / c (no. 14), a = 11.6429(10) Å, b = 10.9111(10) Å, c = 24.234(2) Å, β = 93.2890(10)°, V = 3073.6(5) Å 3 , Z = 4, R gt ( F ) = 0.0198, wR ref ( F 2 ) = 0.0507, T = 273(2) K.
Open Access
The crystal structure of 5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-(trifluoromethylsulfonyl)-1H-pyrazole-3-carboxamide, C₁₂H₆N₄Cl₂F₆O₃S

24. Juni 2019

Lianqing Chen, Lijun Tian

Seiten: 1177-1179

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C 12 H 6 N 4 Cl 2 F 6 O 3 S, orthorhombic, Pna 2 1 (no. 33), a = 18.7340(10) Å, b = 9.4010(10) Å, c = 19.2330(10) Å, V = 3387.3(4) Å 3 , Z = 8, R gt ( F ) = 0.0449, wR ref ( F 2 ) = 0.1074, T = 100.15 K.
Open Access
Synthesis and crystal structure of poly[(μ₂-nitrato-κ⁴O,O′:O′,O′′)-nitrato-κO-(μ₂-1,4-bis((1H-imidazol-1-yl)methyl)benzene-κ²N:N′)cadmium(II)], C₁₄H₁₄N₆O₆Cd

19. Juni 2019

Bin Xu, Qing-Lin Yang, Meng Yun, Xiao-Yu Zhang, Yan-Fang Wu, Xiu-Yan Dong

Seiten: 1181-1182

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C 14 H 14 CdN 6 O 6 , monoclinic, P 2 1 / c (no. 14), a = 11.2983(5) Å, b = 9.2539(4) Å, c = 17.0604(7) Å, β = 105.398(1)°, Z = 4, V = 1719.69(13) Å 3 , R gt ( F ) = 0.0321, wR ref ( F 2 ) = 0.1060, T = 193(2) K.
Open Access
Crystal structure of ethyl (Z)-(4-oxo-4-phenylbut-2-en-2-yl)glycinate, C₁₄H₁₇NO₃

17. August 2019

A.S. Safavora, Ivan Brito, Jonathan Cisterna, Alejandro Cárdenas, E.Z. Huseynov, A.N. Khalilov, F.N. Naghiyev, R.K. Askerov, A.M. Maharramov

Seiten: 1183-1185

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C 14 H 17 NO 3 , monoclinic, P 2 1 / n (no. 14), a = 11.1445(7) Å, b = 8.5442(5) Å, c = 14.2503(8) Å, β = 97.5684(11)°, V = 1345.10(14) Å 3 , Z = 4, R gt ( F ) = 0.0668, wR ref ( F 2 ) = 0.1680, T = 296(2) K.
Open Access
Halogen bonds in the crystal structure of 5-bromo-3,4′-bipyridine – 1,4-diiodotetrafluorobenzene (2/1), C₂₆H₁₄Br₂F₄I₂N₄

25. Juli 2019

Weizhou Wang

Seiten: 1187-1188

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C 26 H 14 Br 2 F 4 I 2 N 4 , triclinic, P 1̄ (no. 2), a = 8.7472(4) Å, b = 8.7822(4) Å, c = 9.4065(4) Å, α = 102.745(4)°, β = 105.489(4)°, γ = 91.949(4)°, V = 675.88(5) Å 3 , Z = 1, R gt ( F ) = 0.0336, wR ref ( F 2 ) = 0.0813, T = 290 K.
Open Access
Crystal structure of bis(2,2′-bipyridine-κ²N,N′)-tetrakis(μ₂-3-(phenylsulfonamido)propanoato-κ²O:O′)-bis(3-(phenylsulfonamido)propanoato-κ²O,O′)digadolinium(III) – 2,2′-bipyridine (1/1), C₈₄H₈₄Gd₂N₁₂O₂₄S₆

13. August 2019

Tao-Li Deng, Zheng-Jun Liu, Xiao-Miao Chen, Xue-Mei Liu

Seiten: 1189-1191

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C 84 H 84 Gd 2 N 12 O 24 S 6 , triclinic, P 1̄, a = 9.733(2) Å, b = 11.3610(8) Å, c = 21.4970(3) Å, α = 89.635(3)°, β = 82.334(3)°, γ = 69.794(3)°, V = 2208.8(5) Å 3 , Z = 1, R gt ( F ) = 0.0467, wR ref ( F 2 ) = 0.0925, T = 293(2) K.
Open Access
Crystal structure of poly[aqua(μ₂-2-amino-1,4-benzenedisulfonato-κ²O:O′)bis(μ₂-pyrazin-κ²N:N′)silver(I)], C₁₄H₁₆Ag₂N₅O₈S₂

17. August 2019

Jia-Wei Li, Jin-Ke Jiang, Hui Jiang

Seiten: 1193-1194

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C 14 H 16 Ag 2 N 5 O 8 S 2 , triclinic, P 1̄ (no. 2), a = 7.1305(7) Å, b = 7.3558(6) Å, c = 9.8517(10) Å, α = 73.816(9)°, β = 82.648(8)°, γ = 88.080(7)°, V = 492.17(8) Å 3 , Z = 1, R gt ( F ) = 0.0491, wR ref ( F 2 ) = 0.1515, T = 293(2) K.
Open Access
The crystal structure of 1,6-di-tert-butyl-1,1,3,3,4,4,6,6-octamethyl-2,2,5,5-tetrakis (trimethylsilyl)hexasilane, C₂₈H₇₈Si₁₀

18. Juli 2019

Xu-Qiong Xiao, Jun-Ting Xu, Yinan Wu, Qiong-Yan Wang

Seiten: 1195-1198

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C 28 H 78 Si 10 , monoclinic, Pn (no. 7), a = 21.413(4) Å, b = 9.8568(17) Å, c = 22.074(4) Å, β = 93.426(4)°, V = 4650.6(14) Å 3 , Z = 4, R gt ( F ) = 0.0613, wR ref ( F 2 ) = 0.1750, T = 296(2) K.
Open Access
Crystal structure of discandium triruthenium tetrasilicide, Sc₂Ru₃Si₄

20. Juli 2019

Soshi Ibuka, Yoshitaka Matsushita, Motoharu Imai

Seiten: 1199-1200

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Sc 2 Ru 3 Si 4 , monoclinic, C 2/ c (no. 15), a = 19.0663(5) Å, b = 5.27810(10) Å, c = 13.3458(4) Å, β = 127.7710(10)°, V = 1061.62(5) Å 3 , Z = 8, R gt ( F ) = 0.0209, wR ref ( F 2 ) = 0.0530, T = 293(2) K.
Open Access
Crystal structure of poly[(μ₂-4-amino-1,5-naphthalenedisulfonato-κ⁴O,N:O′, N′)bis(μ₂-hexamethylenetetramino-κ²N;N′)silver(I)], {C₂₂H₃₀Ag₂N₉O₆S₂}_n

23. August 2019

Jin-Ke Jiang, Gang-Mei Li, Jian-Nan Sun, Ge-Shuang Ju, Jing-Jie Du, Xin Jin

Seiten: 1201-1202

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C 22 H 30 Ag 2 N 9 O 6 S 2 , monoclinic, P 2 1 /c (no. 14), a = 10.4629(10) Å, b = 10.9785(8) Å, c = 12.3483(15) Å, β = 109.766(12)°, V = 1334.8(2) Å 3 , Z = 2, R gt ( F ) = 0.0662, wR ref ( F 2 ) = 0.1356, T = 293(2) K.
Open Access
Crystal structure of diaqua[5,5′-dicarboxy-2,2′-(propane-1,3-diyl)bis(1H-imidazole-4-carboxylato-κ⁴O,O′,N,N′)]zinc(II) dihydrate, C₁₃H₁₈N₄O₁₂Zn

2. August 2019

Xiao-Fei Li, Li-Gang Ma, Wen-Feng Guo, Wen-Feng Zhao

Seiten: 1203-1205

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C 13 H 18 N 4 O 12 Zn, triclinic, P 1̄ (no. 2), a = 9.0311(3) Å, b = 9.4464(3) Å, c = 12.6951(5) Å, α = 109.2790(11)°, β = 92.6348(12)°, γ = 116.2514(10)°, V = 892.97(5) Å 3 , Z = 2, R gt ( F ) = 0.0263, wR ref ( F 2 ) = 0.0712, T = 293(2) K.
Open Access
The crystal structure of poly [(μ₃-N¹,N⁴-bis(pyridin-3-yl)cyclohexane-1,4-dicarboxamide-κ³-O:N:N′)-(p-toluenesulfonato-κ²O,O′)silver(I)], C₂₅H₂₇Ag₁N₄O₅S

23. August 2019

Qiang Zhang, Wen-Lin Shuai, Tao Yang

Seiten: 1207-1209

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(C 25 H 27 AgN 4 O 5 S) n , monoclinic, P 2 1 / c (no. 14), a =8.4459(2) Å, b = 23.8845(5) Å, c = 13.0653(3) Å, β =105.096(2)°, V = 2544.66(10) Å 3 , Z = 4, R gt ( F ) = 0.0315, wR ref ( F 2 ) = 0.0689, T = 293(2) K.
Open Access
The crystal structure of 1,2-bis(3-bromophenoxy) ethane, C₁₄H₁₂Br₂O₂

20. Juli 2019

Ming-Gang Teng, Yu-Mei Qin, Dan Long, Jian-Xin Cao, Chun-Shen Zhao

Seiten: 1211-1212

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C 14 H 12 Br 2 O 2 , monoclinic, C 2/ c (no. 15), a = 27.323(3) Å, b = 5.8516(6) Å, c = 8.9145(10) Å, β = 103.596(3)°, V = 1385.4(3) Å 3 , Z = 4, R gt ( F ) = 0.0378, wR ref ( F 2 ) = 0.1019, T = 296(2) K.
Open Access
The crystal structure of 4-(pyren-1-yl)butyl-3-nitrobenzoate, C₂₇H₂₁NO₄

30. Juli 2019

Claudio Barrientos, Patricia Barahona, Juan Luis Guevara, J. Arturo Squella, Silvana Moris

Seiten: 1213-1214

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C 27 H 21 NO 4 , triclinic, P 1̄ (no. 2), a = 8.1182(5) Å, b = 9.0097(5) Å, c = 14.8013(10) Å, α = 72.603(2)°, β = 82.642(2)°, γ = 79.351(3)°, V = 1012.23(11) Å 3 , Z = 2, R gt ( F ) = 0.0367, wR ref ( F 2 ) = 0.1018, T = 150 K.
Open Access
Crystal structure of bis[(2-(4-chlorophenyl)-5-methyl-1,3-dioxane-5-carboxylato-κ¹O) (5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ⁴N,N′,N′′,N′′′)]nickel(II), C₄₀H₆₀Cl₂N₄NiO₈

23. August 2019

Yang Liao, Rong-Ling Yan

Seiten: 1215-1216

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C 40 H 60 Cl 2 N 4 NiO 8 , triclinic, P 1̄ (no. 2), a = 8.2372(8) Å, b = 9.7100(10) Å, c = 13.7518(14) Å, α = 100.060(1)°, β = 101.854(1)°, γ = 91.675(1)°, V = 1057.48(18) Å 3 , Z = 1, R gt ( F ) = 0.0311, wR ref ( F 2 ) = 0.0761, T = 296(2) K.
Open Access
The crystal structure of 1,5-dinitro-2,3,4-trichlorobenzene, C₆H₁Cl₃N₂O₄

2. August 2019

Wang Peilan, Wang Jianlong, Chen Lizhen, Zhao Zihao, Cao Cai

Seiten: 1217-1218

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C 6 H 1 Cl 3 N 2 O 4 , monoclinic, P 2 1 /c (no. 14), a = 5.3193(2) Å, b = 11.3307(4) Å, c = 15.1131(5) Å, β = 93.329(1)°, V = 909.35(6) Å 3 , Z = 4, R gt ( F ) = 0.0264, wR ref ( F 2 ) = 0.1098, T = 100 K.
Open Access
The crystal structure of the solid solution of 3,5-dinitropyrazole and 4-chlorine-3,5-dinitropyrazole, C₃H_1.24Cl_0.76N₄O₄

11. September 2019

Wang Jianlong, Liu Yunzhang, Chen Lizhen, Li Zhihua, Hu Wanghua

Seiten: 1219-1220

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C 3 H 1.24 Cl 0.76 N 4 O 4 , monoclinic, P 2 1 / c (no. 14), a = 11.3953(11) Å, b = 5.9373(4) Å, c = 9.7498(9) Å, β = 96.630(4)°, V = 655.23(10) Å 3 , Z = 4, R gt ( F ) = 0.0446, wR ref ( F 2 ) = 0.1068, T = 173(2) K.
Open Access
The cocrystal structure of 4-nitropyrazole — acetic acid (1/1), C₅H₇N₃O₄

2. August 2019

Liu Yunzhang, Chen Lizhen, Wang Jianlong, Zhang Luyao, Ruan Jian

Seiten: 1221-1222

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C 5 H 7 N 3 O 4 , monoclinic, P 1̄ (no. 2), a = 5.1166(12) Å, b = 8.711(2) Å, c = 8.744(2) Å, α = 103.169(7)°, β = 90.454(6)°, γ = 96.121(7)°, V = 377.08(16) Å 3 , Z = 2, R gt ( F ) = 0.0619, wR ref ( F 2 ) = 0.1241, T = 173(2) K.
Open Access
The crystal structure of propan-2-one O-(2,4,6-trinitrophenyl) oxime, C₉H₈N₄O₇

2. August 2019

Chen Lizhen, Liu Yunzhang, Wang Jianlong, Chen Jun, Pan Hongxia

Seiten: 1223-1224

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C 9 H 8 N 4 O 7 , orthorhombic, Aea 2 (no. 41; old symbol Aba 2), a = 21.0595(11) Å, b = 14.8565(8) Å, c = 7.6437(4) Å, V = 2391.5(2) Å 3 , Z = 8, R gt ( F ) = 0.0397, wR ref ( F 2 ) = 0.0825, T = 173(2) K.
Open Access
The crystal structure of ethyl 2-(3-(2-ethoxy-2-oxoethyl)benzo[d] thiazol-2(3H)-ylidene)acetate, C₁₅H₁₇NO₄S

2. August 2019

Deng-Ze Wu

Seiten: 1225-1226

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C 15 H 17 NO 4 S, orthorhombic, Pbca (no. 61), a = 9.9890(11) Å, b = 14.4529(16) Å, c = 21.635(2) Å, V = 3123.4(6) Å 3 , Z = 8, R gt ( F ) = 0.0565, wR ref ( F 2 ) = 0.1656, T = 293(2) K.
Open Access
Crystal structure of (acetic acid-κ¹O)-bis(μ₂-2-chlorobenzoato-κ²O:O′)-(2-chlorobenzoato-κ¹O)-(μ²-hydroxy-κ²O:O)-bis(1,10-phenanthroline-κ²N,N′)dimanganese(II) — methanol (1/1), C₄₈H₃₇Cl₃Mn₂N₄O₁₀

9. September 2019

Feng Li

Seiten: 1227-1229

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C 48 H 37 Cl 3 Mn 2 N 4 O 10 , monoclinic, P 2 1 / n (no. 14), a = 12.759(3) Å, b = 19.347(5) Å, c = 18.945(5) Å, β = 97.321(5)°, V = 4638(2) Å 3 , Z = 4, R gt ( F ) = 0.0432, wR ref ( F 2 ) = 0.1196, T = 298(2) K.
Open Access
Crystal structure of 3-methyl-2-phenyl-1,8-naphthyridine, C₁₅H₁₂N₂

7. August 2019

Yuan Wen, Xin-Sheng Xiao, Guo-Kai Jia

Seiten: 1231-1232

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C 15 H 12 N 2 , monoclinic, P 2 1 / c (no. 14), a = 7.323(4) Å, b = 6.975(3) Å, c = 22.411(11) Å, β = 93.195(5)°, V = 1143.0(10) Å 3 , Z = 4, R gt ( F ) = 0.0457, wR ref ( F 2 ) = 0.1324, T = 296(2) K.
Open Access
Crystal structure of chlorido-(5-acetyl-2-(5-methylpyridin-2-yl)benzen-1-ido-κ²C,N)-pyridine-κN-palladium(II), C₁₉H₁₇ClN₂OPd

17. September 2019

Xin-Hua Lou

Seiten: 1233-1235

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C 19 H 17 ClN 2 OPd, monoclinic, P 2 1 / c (no. 14), a = 9.0720(8) Å, b = 10.9390(10) Å, c = 17.9604(7) Å, β = 97.054(6)°, V = 1768.9(2) Å 3 , Z = 4, R gt ( F ) = 0.0389, wR ref ( F 2 ) = 0.0816, T = 293(2) K.
Open Access
Crystal structure of (4-methyl-benzoato-κ²O,O′)-(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ⁴N,N′,N′′,N′′′)nickel(II) perchlorate monohydrate, C₂₄H₄₅ClN₄NiO₇

11. September 2019

Xiao-Ming Chen

Seiten: 1237-1239

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C 24 H 45 ClN 4 NiO 7 , monoclinic, P 2 1 / n (no. 14), a = 10.4947(11) Å, b = 14.3956(13) Å, c = 19.7182(18) Å, β = 93.212(6)°, V = 2974.3(5) Å 3 , Z = 4, R gt ( F ) = 0.0426, wR ref ( F 2 ) = 0.1389, T = 296(2) K.
Open Access
Crystal structure of (1,4,7,10,13,16-hexaoxacyclooctadecane-κ⁶O₆) 1,2,3,4,5-pentamethyl-cyclopenta-2,4-dien-1-yl(potassium, rubidium) — ammonia (1/2), [K_0.3Rb_0.7(18-crown-6)]Cp*⋅2 NH₃, C₂₂H₄₅K_0.3N₂O₆Rb_0.7

11. September 2019

Thomas Henneberger, Wilhelm Klein, Thomas F. Fässler

Seiten: 1241-1243

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C 22 H 45 K 0.26 N 2 O 6 Rb 0.74 , orthorhombic, Pbca (no. 61), a = 10.1587(8) Å, b = 16.2842(15) Å, c = 32.862(3) Å, V = 5436.2(8) Å 3 , Z = 8, R gt ( F ) = 0.0386, wR ref ( F 2 ) = 0.0616, T = 120(2) K.
Open Access
Crystal structure of (3E,5E)-1-((4-fluorophenyl)sulfonyl)-3,5-bis(3-nitrobenzylidene)piperidin-4-one — dichloromethane (2/1), C₅₁H₃₈Cl₂F₂N₆O₁₄S₂

9. September 2019

Qin Zhao, Dong Lin, Yun Hou, Gui-Ge Hou

Seiten: 1245-1247

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C 51 H 38 Cl 2 F 2 N 6 O 14 S 2 , triclinic, P 1̄ (no. 2), a = 11.8987(6) Å, b = 14.0939(8) Å, c = 16.1915(9) Å, α = 67.590(5)°, β = 75.402(5)°, γ = 77.522(4)°, V = 2407.3(2) Å 3 , Z = 2, R gt ( F ) = 0.0584, wR ref ( F 2 ) = 0.1645, T = 100.0(1) K.
Open Access
Crystal structure of (E)-N′-((1,6-dihydropyren-1-yl)methylene)isonicotinohydrazide — methanol (1/1), C₂₄H₁₉N₃O₂

2. August 2019

Lili Wang

Seiten: 1249-1250

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C 24 H 19 N 3 O 2 , monoclinic, P 2 1 / c (no. 14), a = 11.0629(2) Å, b = 10.4583(2) Å, c = 16.0432(3) Å, β = 92.373(2)°, V = 1854.59(7) Å 3 , Z = 4, R gt ( F ) = 0.0435, wR ref ( F 2 ) = 0.1269, T = 116.2(3) K.
Open Access
Crystal structure of poly[aqua(μ₂-2-amino-1,4-benzenedisulfonato-κ³N,O:O′)-(μ₄-hexamethylenetetramino-κ⁴N:N′:N′′:N′′′)disilver(I)] monohydrate, C₁₂H₂₁Ag₂N₅O₈S₂

23. August 2019

Jin-Ke Jiang, Xi-Xi Li, Hui Jiang, Xian-Wu Dong

Seiten: 1251-1252

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C 12 H 21 Ag 2 N 5 O 8 S 2 , triclinic, P 1 (no. 1), a = 6.3703(5) Å, b = 6.4191(5) Å, c = 12.3215(7) Å, α = 87.841(5)°, β = 75.119(6)°, γ = 87.489(6)°, V = 486.30(6) Å 3 , Z = 1, R gt ( F ) = 0.0444, wR ref ( F 2 ) = 0.1289, T = 293(2) K.
Open Access
Crystal structure of bis(acridin-10-ium) 2,5-dihydroxyterephthalate — 2,5-dihydroxyterephthalic acid (1/1), C₂₁H₁₅NO₆

17. September 2019

Xin-Hong Chang

Seiten: 1253-1254

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C 21 H 15 NO 6 , triclinic, P 1̄ (no. 2), a = 9.3591(4) Å, b = 9.4371(5) Å, c = 10.1106(5) Å, α = 102.581(4)°, β = 92.929(4)°, γ = 102.573(4)°, V = 846.09(7) Å 3 , Z = 2, R gt ( F ) = 0.0452, wR ref ( F 2 ) = 0.1135, T = 288.7(3) K.
Open Access
The crystal structure of 1,12-diazaperylene, C₁₈H₁₀N₂

23. August 2019

Matthias Kirste, Thomas Brietzke, Hans-Jürgen Holdt, Uwe Schilde

Seiten: 1255-1257

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C 18 H 10 N 2 , monoclinic, P 2 1 / c (no. 14), a = 7.9297(9) Å, b = 11.4021(14) Å, c = 13.3572(15) Å, β = 105.363(8)°, V = 1164.5(2) Å 3 , Z = 4, R gt ( F ) = 0.0325, wR ref ( F 2 ) = 0.0774, T = 210(2) K.
Open Access
Crystal structure of 1-(5-(4-chlorophenyl)-3-(2-fluorophenyl)-4,5-dihydro-1H-pyrazol-1-yl)ethan-1-one, C₁₇H₁₄N₂OFCl

9. September 2019

E. Liu, Zhuang-Yu Li, Fang-Fang Jian, Tongling Liang

Seiten: 1259-1260

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C 17 H 14 N 2 OFCl, triclinic, P 1̄ (no. 2), a = 8.2387(19) Å, b = 9.764(2) Å, c = 10.644(3) Å, α = 72.023(4)°, β = 72.770(4)°, γ = 78.581(4)°, V = 772.5(3) Å 3 , Z = 2, R gt ( F ) = 0.0444, wR ref ( F 2 ) = 0.1099, T = 294.15 K.
Open Access
Crystal structure of (4aR,6aR,6bR,10S,12aR)-10-acetoxy-1,2,3,4, 4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a, 12b,13,14b-icosahydro-2,2,4a,6b,9,9,12a-heptamethylpicene-6a-carboxylic acid, C₃₂H₅₀O₄

2. August 2019

Kang He, Tian-Tai Wu, Lin-Yan Shen, Lin-Lin Fan, Jiang-Hai Ye, Juan Zou

Seiten: 1261-1263

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C 32 H 50 O 4 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 14.090(3) Å, b = 15.642(3) Å, c = 25.956(6) Å, V = 5721(2) Å 3 , Z = 8, R gt ( F ) = 0.0679, wR ref ( F 2 ) = 0.1764, T = 250(2) K.
Open Access
The crystal structure of tetrachlorido-bis{1,3-bis(2,6-diisopropylphenyl)-1H-3λ⁴-imidazol-2-yl}-(μ₂-pyrimidine-κ²N:N′)dipalladium(IV) — dichloromethane (1/2), C₆₀H₈₀Cl₈N₆Pd₂

2. August 2019

Xiao-Yun Zhao, Lian-Hui Chen

Seiten: 1265-1268

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C 60 H 80 Cl 8 N 6 Pd 2 , triclinic, P 1̄ (no. 2), a = 10.8703(10) Å, b = 17.0284(15) Å, c = 18.9595(17) Å, α = 83.1960(10)°, β = 88.909(2)°, γ = 71.523(2)°, V = 3304.5(5) Å 3 , Z = 2, R gt ( F ) = 0.0488, wR ref ( F 2 ) = 0.1213, T = 130 K.
Open Access
The crystal structure of (E)-4-(7-methoxy-2-oxo-2H-chromen-8-yl)-2-methylbut-2-en-1-yl 4-nitrobenzoate, C₂₂H₁₉NO₇

25. Juli 2019

Xiang Yu, Lu Peng, Xin Wang, Ya-Fang Chen

Seiten: 1269-1270

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C 22 H 19 NO 7 , monoclinic, P 2 1 / n (no. 14), a = 7.5742(4) Å, b = 20.0688(12) Å, c = 13.2932(8) Å, β = 102.469(2)°, V = 1973.0(2) Å 3 , Z = 4, R gt ( F ) = 0.0726, wR ref ( F 2 ) = 0.1777, T = 198 K.
Open Access
Crystal structure of 3-methyl-N-(pyrimidin-5-ylmethyl)pyridin-2-amine, C₁₁H₁₂N₄

2. August 2019

Yun-Lian Shi, Xu-Liang Nie, Tao Huang, Jin-Hui Xie, Da-Yong Peng, Xu-Gen Shi, Bao-Tong Li

Seiten: 1271-1272

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[C 11 H 12 N 4 ], triclinic, P 1̄, a = 6.6939(10) Å, b = 8.8034(13) Å, c = 9.1140(13) Å, α = 97.749(2)°, β = 99.285(2)%, γ = 95.917(2)°, V = 520.90(13) Å 3 , Z = 2, R gt ( F ) = 0.0381, wR ref ( F 2 ) = 0.1030, T = 296(2) K.
Open Access
The crystal structure of 2,5-dichloroterephthalic acid dihydrate, C₈H₈Cl₂O₆

23. August 2019

Chao-Jun Du, Yuan-Liang Zhu, Yan Zeng

Seiten: 1273-1274

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C 8 H 8 Cl 2 O 6 , monoclinic, P 2 1 / c (no. 14), a = 10.6836(9) Å, b = 7.2382(6) Å, c = 6.8585(5) Å, β = 92.850(3)°, V = 529.71(7) Å 3 , Z = 2, R gt (F) = 0.0315, wR ref (F 2 ) = 0.0811, T = 150(2) K.
Open Access
The crystal structure of 2,4,6-tris[4-(1H-imidazol-1-yl)phenyl]-1,3,5-triazine — dimethylformamide (1/1), C₃₃H₂₈N₁₀O

11. September 2019

Hao Cui, Xin-Ting Yan, Wenya Chen, Tao Yang

Seiten: 1275-1278

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C 33 H 28 N 10 O, triclinic, P 1̄ (no. 2), a = 14.7148(9) Å, b = 15.5185(10) Å, c = 16.1128(9) Å, α = 113.219(6)°, β = 96.735(5)°, γ = 115.259(6)°, V = 2872.0(3) Å 3 , Z = 4, R gt ( F ) = 0.0426, wR ref ( F 2 ) = 0.1108, T = 150(2) K.
Open Access
Crystal structure of N-(adamantan-1-yl)-5-(dimethylamino)naphthalene-1-sulfonamide, C₂₂H₂₈N₂O₂S

11. September 2019

Jacques Joubert

Seiten: 1279-1281

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C 22 H 28 N 2 O 2 S, monoclinic, P 2 1 / n (no. 14), a = 9.2516(7) Å, b = 10.5122(8) Å, c = 19.7782(15) Å, β = 98.9530(10)°, V = 1900.1(2) Å 3 , Z = 4, R gt ( F ) = 0.0356, wR ref ( F 2 ) = 0.1004, T = 100(2) K.
Open Access
Crystal structure of poly[diaqua-(μ₄-4-(3,5-dicarboxy-κ¹O-phenoxy)phthalato-κ³O:O′:O′)cadmium(II)], C₁₆H₁₂CdO₁₁

14. September 2019

Tao Sun, Ke Li

Seiten: 1283-1284

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C 16 H 12 CdO 11 , monoclinic, P 2 1 / c (no. 14), a = 14.6977(6) Å, b = 5.9706(2) Å, c = 20.7220(10) Å, β = 109.802(5)°, V = 1710.91(13) Å 3 , Z = 4, R gt ( F ) = 0.0456, wR ref ( F 2 ) = 0.1583, T = 296(2) K.
Open Access
Crystal structure of poly[diaqua-bis(μ₂-3-((1H-imidazol-1-yl)methyl)benzoato-κ²N:O)manganese(II)], C₂₂H₂₂MnN₄O₆

19. September 2019

Tian Zhang

Seiten: 1285-1286

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C 22 H 22 MnN 4 O 6 , monoclinic, P 2 1 /n, a = 11.9331(7) Å, b = 5.5962(3) Å, c = 16.0671(9) Å, β = 107.391(6)°, Z = 2, V = 1023.92(11) Å 3 , R gt (F) = 0.046, w R ref (F 2 ) = 0.055, T = 287 K.
Open Access
Crystal structure of 9-(3-phenoxyphenyl)-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dione, C₂₅H₂₃NO₃

13. August 2019

Qian Huang, Quan Yuan

Seiten: 1287-1288

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C 25 H 23 NO 3 , monoclinic, P 2 1 / c (no. 14), a = 10.972(6) Å, b = 7.392(4) Å, c = 25.804(10) Å, β = 109.349(18)°, V = 1974.6(17) Å 3 , Z = 4, R gt ( F ) = 0.0640, wR ref ( F 2 ) = 0.2381, T = 293(2) K.
Open Access
The crystal structure of poly[(μ₃-2,4,6-tris[4-(1H-imidazol-1-yl)phenyl]-1,3,5-triazine-k³N:N′:N′′)-(nitrato-k²O,O)-(nitrato-k¹O)zinc(II)] - N,N-dimethylacetamide (1/2), C₃₈H₃₉N₁₃O₈Zn

11. September 2019

Hao Cui, Si-Si Qiu, Tao Yang

Seiten: 1289-1292

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C 38 H 39 N 13 O 8 Zn, monoclinic, P 2 1 / c (no. 14), a = 13.0155(7) Å, b = 32.7011(14) Å, c = 9.8464(4) Å, β = 110.228(1)°, V = 3932.4(3) Å 3 , Z = 4, R gt ( F ) = 0.0476, wR ref ( F 2 ) = 0.1358, T = 150(2) K.
Open Access
Crystal structure of poly[(μ₇-4-(3,5-dicarboxylatophenoxy)phthalato)-(1,10-phenanthroline-κ²N,N′)dizinc(II)], C₂₈H₁₄N₂O₉Zn₂

23. August 2019

Tao Sun, Ke Li

Seiten: 1293-1294

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C 28 H 14 N 2 O 9 Zn 2 , triclinic, P 1̄ (no. 2), a = 9.6870(5) Å, b = 10.1849(9) Å, c = 12.7338(9) Å, α = 95.202(6)°, β = 107.027(5)°, γ = 91.896(5)°, V = 1193.97(14) Å 3 , Z = 2, R gt ( F ) = 0.0516, wR ref ( F 2 ) = 0.1267, T = 293(2) K.
Open Access
The crystal structure of methyl 2-(benzylamino)-5-(benzyloxy)benzoate, C₂₂H₂₁NO₃

1. August 2019

Yu-Mei Qin, Xue Zou, Dan Long, Chun Ji, Chun-Shen Zhao

Seiten: 1295-1296

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C 22 H 21 NO 3 , triclinic, P 1̄ (no. 2), a = 5.757(3) Å, b = 12.106(5) Å, c = 13.139(6) Å, α = 93.725(12)°, β = 92.508(15)°, γ = 92.508(15)° V = 891.3(7) Å 3 , Z = 2, R gt ( F ) = 0.0474, wR ref ( F 2 ) = 0.1429, T = 296(2) K.
Open Access
Crystal structure of (1,4,8,11-tetraazacyclotetradecane)palladium(II) tetracyanoplatinate(II), C₁₄H₂₄N₈PdPt

1. August 2019

Kwang Ha

Seiten: 1297-1298

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C 14 H 24 N 8 PdPt, monoclinic, P 2 1 / c (no. 14), a = 9.0747(3) Å, b = 8.3376(3) Å, c = 14.4578(6) Å, β = 123.8260(10)°, V = 908.73(6) Å 3 , Z = 2, R gt ( F ) = 0.0115, wR ref ( F 2 ) = 0.0235, T = 223 K.
Open Access
Crystal structure of (pyridine-2-carboxylato-κ²N,O)-[2-(2-pyridyl)phenyl-κ²N,C¹]palladium(II), C₁₇H₁₂N₂O₂Pd

25. Juli 2019

Kwang Ha

Seiten: 1299-1300

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C 17 H 12 N 2 O 2 Pd, orthorhombic, Pna 2 1 (no. 33), a = 20.6775(12) Å, b = 11.7539(7) Å, c = 5.4868(3) Å, V = 1333.52(13) Å 3 , Z = 4, R gt ( F ) = 0.0154, wR ref ( F 2 ) = 0.0373, T = 223(2) K.
Open Access
Crystal structure of (cyclohexane-1,4-diammonium) 4-[(4-carboxylatophenyl)disulfanyl]benzoate dimethylsulphoxide hydrate (1/1/1/1), [C₆H₁₆N₂]²⁺[C₁₄H₈O₄S₂]²⁻⋅C₂H₆OS⋅H₂O

21. September 2019

Sang Loon Tan, Edward R. T. Tiekink

Seiten: 1301-1304

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C 22 H 32 N 2 O 6 S 3 , triclinic, P 1̄ (no. 2), a = 6.1543(1) Å, b = 14.4991(2) Å, c = 15.3859(3) Å, α = 64.545(2)°, β = 81.828(1)°, γ = 89.505(1)°, V = 1224.93(4) Å 3 , Z = 2, R gt ( F ) = 0.0290, wR ref ( F 2 ) = 0.0787, T = 100 K.
Open Access
Crystal structure of the 2:1 co-crystal 2-[(2-carboxyphenyl)disulfanyl]benzoic acid – 3-bromobenzoic acid, 2(C₁₄H₁₀O₄S₂)⋅C₇H₅BrO₂

21. September 2019

Sang Loon Tan, Edward R.T. Tiekink

Seiten: 1305-1308

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C 35 H 25 BrO 10 S 4 , triclinic, P 1̄ (no. 2), a = 7.9533(2) Å, b = 10.27180(10) Å, c = 20.6598(4) Å, α = 103.462(1)°, β = 95.933(2)°, γ = 96.008(1)°, V = 1618.11(5) Å 3 , Z = 2, R gt ( F ) = 0.0624, wR ref ( F 2 ) = 0.1759, T = 100(2) K.
Open Access
Crystal structure of chlorido-dimethyl-(phenylpiperazine-1-carbodithioato-κ²S,S′)tin(IV), C₁₃H₁₉ClN₂S₂Sn

9. September 2019

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Seiten: 1309-1311

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C 13 H 19 ClN 2 S 2 Sn, triclinic, P 1̄ (no. 2), a = 6.5837(2) Å, b = 9.9458(2) Å, c = 12.8720(3) Å, α = 85.344(2)°, β = 79.508(2)°, γ = 83.832(2)°, V = 822.33(4) Å 3 , Z = 2, R gt ( F ) = 0.0176, wR ref ( F 2 ) = 0.0461, T = 100 K.
Open Access
Crystal structure of (N-n-butyl, N-methyl-dithiocarbamato-κ² S,S′)-chlorido-dimethyl-tin(IV), C₈H₁₈ClNS₂Sn

10. September 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Seiten: 1313-1315

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C 8 H 18 ClNS 2 Sn, triclinic, P 1̄ (no. 2), a = 6.4399(2) Å, b = 9.6430(3) Å, c = 11.6944(1) Å, α = 91.966(2)°, β = 101.821(2)°, γ = 105.391(3)°, V = 682.30(3) Å 3 , Z = 2, R gt ( F ) = 0.0227, wR ref ( F 2 ) = 0.0609, T = 100 K.
Open Access
Crystal structure of (2,2′-bipyridyl)bis(4-bromobenzyl)dibromidotin(IV), C₂₄H₂₀Br₄N₂Sn

9. September 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Seiten: 1317-1319

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C 24 H 20 Br 4 N 2 Sn, monoclinic, P 2 1 / n (no. 14), a = 9.3186(1) Å, b = 16.2615(1) Å, c = 16.8482(1) Å, β = 100.748(1)°, V = 2508.29(4) Å 3 , Z = 4, R gt ( F ) = 0.0254, wR ref ( F 2 ) = 0.0688, T = 100(2) K.
Open Access
Crystal structure of (2,2′-bipyridyl)bis(4-chlorobenzyl)dichloridotin(IV), C₂₄H₂₀Cl₄N₂Sn

9. September 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Seiten: 1321-1323

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C 24 H 20 Cl 4 N 2 Sn, monoclinic, P 2 1 / n (no. 14), a = 7.7944(1) Å, b = 21.1245(2) Å, c = 14.7611(1) Å, β = 95.077(1)°, V = 2420.92(4) Å 3 , Z = 4, R gt ( F ) = 0.0229, wR ref ( F 2 ) = 0.0603, T = 100(2) K.
Open Access
Crystal structure of N-methyl-N-phenyl(methylsulfanyl)carbothioamide, C₉H₁₁NS₂

12. September 2019

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Seiten: 1325-1327

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C 9 H 11 NS 2 , monoclinic, P 2 1 / n (no. 14), a = 5.6183(1) Å, b = 18.2426(3) Å, c = 9.5185(2) Å, β = 96.835(2)°, V = 968.64(3) Å 3 , Z = 4, R gt ( F ) = 0.0303, wR ref ( F 2 ) = 0.0826, T = 100(2) K.
Open Access
Crystal structure of 4-phenylpiperazin-1-ium (4-phenylpiperazin-1-yl)carbothioylsulfanide, [C₁₀H₁₅N₂][C₁₁H₁₃N₂S₂]

11. September 2019

Kong Mun Lo, See Mun Lee, Edward R.T. Tiekink

Seiten: 1329-1331

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[C 21 H 28 N 4 S 2 ], monoclinic, P 2 1 / c (no. 14), a = 16.1880(2) Å, b = 6.8168(1) Å, c = 19.7605(2) Å, β = 106.412(1)°, V = 2091.73(5) Å 3 , Z = 4, R gt ( F ) = 0.0281, wR ref ( F 2 ) = 0.0740, T = 100(2) K.
Open Access
Crystal structure of catena-{di-aqua-sodium [n-butyl(methyl)carbamothioyl]sulfanide}_n, [C₆H₁₆NNaO₂S₂]_n

17. September 2019

Kong Mun Lo, See Mun Lee, Nordiyana Binti Zaldi, Rusnah Syahila Duali Hussen, Edward R.T. Tiekink

Seiten: 1333-1335

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[C 6 H 16 NNaO 2 S 2 ] n , monoclinic, P 2 1 / c (no. 14), a = 16.3469(2) Å, b = 5.7512(1) Å, c = 11.8647(1) Å, β = 91.046(1)°, V = 1115.27(3) Å 3 , Z = 4, R gt ( F ) = 0.0212, wR ref ( F 2 ) = 0.0562, T = 100(2) K.
Open Access
Crystal structure of (2-([1,1-bis(hydroxymethyl)-2-oxyethyl]iminomethyl)-5-(n-decyl)phenolato)-dimethyl-tin(IV), C₂₃H₃₉NO₅Sn

13. September 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Seiten: 1337-1340

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C 23 H 39 NO 5 Sn, triclinic, P 1̄ (no. 2), a = 6.0101(2) Å, b = 9.2999(2) Å, c = 22.3110(6) Å, α = 91.482(2)°, β = 90.594(3)°, γ = 102.631(2)°, V = 1216.28(6) Å 3 , Z = 2, R gt ( F ) = 0.0425, wR ref ( F 2 ) = 0.1158, T = 100(2) K.
Open Access
Crystal structure of 4-chloro-N′-[(1E)-(3-ethoxy-2-hydroxyphenyl)methylidene]benzohydrazide – a Z′ = 3 structure, C₁₆H₁₅ClN₂O₃

10. September 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Seiten: 1341-1344

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C 16 H 15 ClN 2 O 3 , orthorhombic, Pbca (no. 61), a = 18.7178(2) Å, b = 15.2296(2) Å, c = 32.0558(3) Å, V = 9137.97(18) Å 3 , Z = 24, R gt ( F ) = 0.0407, wR ref ( F 2 ) = 0.1099, T = 100(2) K.

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