Volume 234, Issue 4

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Zeitschrift für Kristallographie - New Crystal Structures

Contents

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Frontmatter

June 22, 2019

Page range: i-viii

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Open Access
Crystal structure of (E)-2-(1-((2-aminophenyl)imino)ethyl)-5-fluorophenol, C₁₄H₁₃FN₂O

March 14, 2019

Ling Bai, Yong Hong, Wei Liu, Jie Wu

Page range: 593-594

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C 14 H 13 FN 2 O, orthorhombic, Pna 2 1 (no. 33), a = 7.1841(6) Å, b = 23.3361(17) Å, c = 7.1672(5) Å, V = 1201.57(16) Å 3 , Z = 4, R gt ( F ) = 0.0437, wR ref ( F 2 ) = 0.1112, T = 293(2) K.
Open Access
Crystal structure of (E)-2-(1-((2-aminophenyl)imino)ethyl)-4,6-dichlorophenol, C₁₄H₁₂Cl₂N₂O

March 11, 2019

Heyun Zong, Yong Hong, Wei Liu, Jie Wu

Page range: 595-596

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C 14 H 12 Cl 2 N 2 O, monoclinic, P 2 1 / c (no. 14), a = 3.9631(3) Å, b = 24.119(2) Å, c = 13.6138(11) Å, β = 91.185(3)°, V = 1301.01(18) Å 3 , Z = 4, R gt ( F ) = 0.0586, wR ref ( F 2 ) = 0.1171, T = 293(2) K.
Open Access
The crystal structure of (E)-1-(4-methoxyphenyl)-3-(2-nitrophenyl)triaz-1-ene C₈H₈N₂O₄

April 22, 2019

Dong-Mei Gao, Lu Liu, Meng Tang, Chunting He, Zhen-Ting Du

Page range: 597-598

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C 8 H 8 N 2 O 4 , monoclinic, C 2/ c (no. 15) , a = 27.748(5) Å, b = 5.6488(10) Å, c = 16.437(3) Å, β = 93.393(3)°, V = 2571.87 Å 3 , Z = 8, R gt ( F ) = 0.0330, wR ref ( F 2 ) = 0.0963, T = 296(2) K.
Open Access
Crystal structure of (E)-2-(((6-bromopyridin-2-yl)methylene)amino)-3′,6′-bis(ethylamino)-2′,7′-dimethylspiro[isoindoline-1,9′-xanthen]-3-one—methanol (1:1), C₃₂H₃₀N₅O₂Br ⋅ CH₄O

March 28, 2019

Ai-Ping Xing, Dai Zeng

Page range: 599-601

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C 33 H 34 N 5 O 3 Br, triclinic, P 1̄ (no. 2), a = 9.1179(2) Å, b = 9.3291(3) Å, c = 18.4706(6) Å, α = 91.187(3)°, β = 95.764(2)°, γ = 102.256(2)°, Z = 2, V = 1526.15(8) Å 3 , R gt ( F ) = 0.0357, wR ref ( F 2 ) = 0.0954, T = 105.7(5) K.
Open Access
Crystal structure of 2,4-pentanedione bis(2,4-dinitrophenylhydrazone), C₁₇H₁₆N₈O₈

March 15, 2019

Ekemini D. Akpan, Sizwe J. Zamisa, Bernard Omondi

Page range: 603-604

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C 17 H 16 N 8 O 8 , orthorhombic, Pna 2 1 (no. 33), a = 13.2406(3) Å, b = 21.0883(5) Å, c = 7.1364(2) Å, V = 1992.64(9) Å 3 , Z = 4, R gt ( F ) = 0.0285, wR ref ( F 2 ) = 0.0802, T = 173(2) K.
Open Access
Crystal structure of sodium morpholine-4-carbodithioate, (C₅H₁₂NNaO₃S₂)

March 26, 2019

Nolwazi Solomane, Peter A. Ajibade, Bernard Omondi

Page range: 605-607

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C 5 H 12 NNaO 3 S 2 , monoclinic, P 2 1 / c (no. 14), a = 28.8222(3) Å, b = 5.6782(3) Å, c = 12.3810(9) Å, β = 102.074(2)°, V = 1987.43(17) Å 3 , Z = 8, R gt ( F ) = 0.0269, wR ref ( F 2 ) = 0.0591, T = 100(2) K.
Open Access
Crystal structure of 1,1′-(hexane-1,6-diyl)bis(3-ethyl-1H-imidazol-3-ium) bis(hexafluorido phosphate), C₁₆H₂₈F₁₂N₄P₂

March 26, 2019

Zhao Wen, Chen Jing, Xiong Wan-Ming, Lan Ying-Dong, Nie Xu-Liang

Page range: 609-611

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C 16 H 28 N 4 2(F 6 P), monoclinic, P 2 1 / n (no. 14), a = 8.7921(12) Å, b = 16.173(2) Å, c = 9.1376(12) Å, β = 111.13(10)°, V = 1211.1(3) Å 3 , Z = 2, R gt ( F ) = 0.0475, wR ref ( F 2 ) = 0.1262, T = 296(2) K.
Open Access
Crystal structure of 5-(4-chlorophenyl)-3-(4-fluorophenyl)-1-phenyl-4,5-dihydro-1H-pyrazole, C₂₁H₁₆ClFN₂

May 8, 2019

Zhenpeng Shen, E. Liu, Xinzhe Tian, Fangfang Jian

Page range: 613-615

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C 21 H 16 ClFN 2 , monoclinic, P 2 1 / c (no. 14), a = 20.286(4) Å, b = 5.3827(11) Å, c = 16.254(3) Å, β = 104.95(3)°, Z = 4, V = 1714.7(7) Å 3 , R gt ( F ) = 0.0548, wR ref ( F 2 ) = 0.1199, T = 293(2) K.
Open Access
Crystal structure of catena-poly[diaqua-bis(3-carboxy-5-methoxybenzoato-κO)-(1,2-bis(imidazol-1-yl)ethane-κ²N:N′)cobalt(II)], C₂₆H₂₈CoN₄O₁₂, [Co(C₉H₆O₅)₂(H₂O)₂(C₈H₁₀N₄)]

March 26, 2019

Min-Le Han

Page range: 617-618

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C 26 H 28 CoN 4 O 12 , triclinic, P 1̄ (no. 2), a = 6.5186(10) Å, b = 9.4111(14) Å, c = 12.1777(18) Å, α = 79.365(2)°, β = 77.535(2)°, γ = 89.226(2)°, V = 716.66(19) Å 3 , Z = 1, R gt ( F ) = 0.0304, wR ref ( F 2 ) = 0.0778, T = 296.15 K.
Open Access
The crystal structure of 3-cyclohexyl-1,5-dioxaspiro[5.5]undecane-2,4-dione, C₁₅H₂₂O₄

March 13, 2019

Zeng Wu-Lan, Xin Wan

Page range: 619-620

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C 15 H 22 O 4 , monoclinic, P 2 1 / c (no. 14), a = 12.7370(5) Å, b = 11.4565(7) Å, c = 10.0430(6) Å, β = 103.340(1)°, V = 1425.95(13) Å 3 , Z = 4, R gt ( F ) = 0.0508, wR ref ( F 2 ) = 0.1406, T = 296(2) K.
Open Access
Crystal structure of (2,4-dimethoxybenzyl)triphenylphosphonium trifluoroacetate — trifluoroacetic acid (1/1), C₃₁H₂₇F₆O₆P

March 13, 2019

Jireh B.M. Smit, Charlene Marais, Frederick P. Malan, Barend C.B. Bezuidenhout

Page range: 621-623

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C 31 H 27 F 6 O 6 P, triclinic, P 1̄ (no. 2), a = 8.0017(2) Å, b = 11.1702(3) Å, c = 17.8353(4) Å, α = 104.9000(10)°, β = 96.5360(10)°, γ = 97.7380(10)°, V = 1508.05(7) Å 3 , Z = 2, R gt ( F ) = 0.0354, wR ref ( F 2 ) = 0.0896, T = 150(2) K.
Open Access
Crystal structure of 4-tert-butyl-1-(2,6-dimethylphenyl)-1H-1,2,3-triazole, C₁₄H₁₉N₃

March 26, 2019

Iliya B. Yerima, Sizwe J. Zamisa, Muhammad D. Bala

Page range: 625-627

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C 14 H 19 N 3 , orthorhombic, Pca 2 1 (no. 29), a = 22.2821(8) Å, b = 10.8464(4) Å, c = 10.8509(4) Å, V = 2622.5(2) Å 3 , Z = 8, R gt ( F ) = 0.0318, wR ref ( F 2 ) = 0.0865, T = 100(2) K.
Open Access
Crystal structure of 1,1′-methylenebis(4-tert-butylpyridinium) tetrachloridocobaltate(II) – dichloromethane (1:1), C₂₀H₃₀Cl₆CoN₂

March 13, 2019

Gwaza E. Ayom, Sizwe J. Zamisa, Werner E. Van Zyl

Page range: 629-631

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C 20 H 30 Cl 6 CoN 2 , orthorhombic, Pbca (no. 61), a = 20.756(1) Å, b = 9.3427(5) Å, c = 27.6827(12) Å, V = 5368.1(5) Å 3 , Z = 8, R gt ( F ) = 0.0235, wR ref ( F 2 ) = 0.0593, T = 100(2) K.
Open Access
Crystal structure of (4,4′-(ethane-1,2-diylbis((nitrilo)(2-furylmethylylidene)))bis(3-methyl-1-phenyl-1H-pyrazol-5-olato-κ⁴N,N′,O,O′))-nickel(II)), C₃₂H₂₆N₆NiO₄

March 19, 2019

Wei Wei, Qiong Wu, Heng-Qiang Zhang, Tong-Yin Jin, Hong-Li Chen

Page range: 633-634

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C 32 H 26 N 6 NiO 4 , monoclinic, C 2/ c (no. 15), a = 22.270(4) Å, b = 16.814(2) Å, c = 8.1486(9) Å, β = 111.222(3)°, V = 2835.0(9) Å 3 , Z = 4, R gt ( F ) = 0.0481, wR ref ( F 2 ) = 0.1440, T = 295(2) K.
Open Access
Synthesis and crystal structure of bis{((E)-((4-((E)-1-(benzyloxyimino)ethyl)phenyl)imino)methyl)-2-phenolato-κ²N,O}copper(II), C₄₄H₃₈CuN₄O₄

May 14, 2019

Jing Huang, Jin-Xia Ma, Ping Wei, Ji-Xing Zhao

Page range: 635-637

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C 44 H 38 CuN 4 O 4 , monoclinic, P 2 1 / n (no. 14), a = 8.0172(13) Å, b = 10.9003(17) Å, c = 42.154(8) Å, β = 94.749(6)°, Z = 4, V = 3671.2(11) Å 3 , R gt ( F ) = 0.0483, wR ref ( F 2 ) = 0.1072, T = 173(2)K.
Open Access
Crystal structure of catena-poly[diaqua-bis(3,5-dichloropyridine-4-carboxylato-κ¹O)-bis(μ₂-4,4′-bipyridine-κ²N:N′)cobalt(II)], C₂₂H₁₆Cl₄CoN₄O₆

March 14, 2019

Xiao-Ling Li, Kai-Xin Feng, Ling-Yun Xin

Page range: 639-640

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C 22 H 16 Cl 4 CoN 4 O 6 , orthorhombic, P 2 1 2 1 2 (no. 18), a = 10.1837(5) Å, b = 11.2878(6) Å, c = 11.3984(4) Å, V = 1310.26(11) Å 3 , Z = 2, R gt ( F ) = 0.0400, wR ref ( F 2 ) = 0.0910, T = 290(2) K.
Open Access
The crystal structure of 2-(4-chloro-2,6-dinitrophenyl)-1-(4-chloro-3,5-dinitrophenyl)diazene 1-oxide, C₁₂H₄Cl₂N₆O₉

March 14, 2019

Junyan Cao, Jianlong Wang, Min Li, Ke Zhang, Shuai Li, Zhen Wan

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C 12 H 4 Cl 2 N 6 O 9 , monoclinic, C 2/ c (no. 15), a = 50.136(3) Å, b = 8.1074(5) Å, c = 15.9816(11) Å, β = 91.927(2)°, V = 6492.4(7) Å 3 , Z = 16, R gt ( F ) = 0.0427, wR ref ( F 2 ) = 0.0969, T = 173(2) K.
Open Access
The crystal structure of 3-(1H-benzo[d]imidazol-2-yl)-7-chloro-1-cyclopropyl-6-fluoro-1,4-dihydroquinolin — dimethylsulfoxide (1/1), C₂₁H₁₉ClFN₃O₂S

March 11, 2019

Anas J. Rasras, Mutasem Sinnokrot, Murad A. AlDamen, Monther A. Khanfar, Raed A. Al-Qawasmeh

Page range: 645-647

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C 21 H 19 ClFN 3 O 2 S, monoclinic, P 2 1 / n (no. 14), a = 10.1495(4) Å, b = 8.9769(5) Å, c = 22.1431(10) Å, β = 99.901(4)°, V = 1987.43(16) Å 3 , Z = 4, R gt ( F ) = 0.0473, wR ref ( F 2 ) = 0.1418, T = 293(2) K.
Open Access
The crystal structure of dichlorido-bis(1-butyl-1H-imidazole-κN)zinc(II), C₁₄H₂₄Cl₂ZnN₄

April 22, 2019

Zongmu Li

Page range: 649-651

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C 14 H 24 Cl 2 ZnN 4 , orthorhombic, Pbca (no. 61), a = 13.3238(11) Å, b = 15.9366(13) Å, c = 18.0943(16) Å, V = 3842.1(6) Å 3 , Z = 8, R gt ( F ) = 0.0393, wR ref ( F 2 ) = 0.1053, T = 298(2) K.
Open Access
(Z)-N-tert-butyl-1-(2-(3,5-dichlorobenzamido)phenyl) methanimine oxide, C₁₈H₁₈Cl₂N₂O₂

March 15, 2019

Xia Mi, Jingyu Zhang, Jing Yang

Page range: 653-654

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C 18 H 18 Cl 2 N 2 O 2 , monoclinic, P 2 1 / n (no. 14), a = 8.5266(3) Å, b = 17.9521(7) Å, c = 11.8709(4) Å, β = 97.288(3)°, V = 1802.41(10) Å 3 , Z = 4, R gt ( F ) = 0.0515, wR ref ( F 2 ) = 0.1497, T = 293(2) K.
Open Access
Crystal structure of diaqua-bis(3-carboxy-5-bromoisophthalato-κO)-bis(1-(3-(1H-benzo[d]imidazol-1-yl)propyl)-1H-benzo[d]imidazol-3-ium-κN)nickel(II) bis(3-carboxy-5-bromoisophthalate), C₆₆H₅₄Br₄N₈NiO₁₈

April 22, 2019

Min-Le Han

Page range: 655-657

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C 66 H 54 Br 4 N 8 NiO 18 , triclinic, P 1̄ (no. 2), a = 8.821(2) Å, b = 14.6587(14) Å, c = 14.8211(14) Å, α = 119.608(1)°, β = 95.365(1)°, γ = 99.249(1)°, V = 1610.8(5) Å 3 , Z = 1, R gt ( F ) = 0.0345, wR ref ( F 2 ) = 0.0815, T = 296(2) K.
Open Access
Crystal structure of poly[aqua(μ₂-5-methoxyisophthalato-κ²O,O′:O′′)-(1,2-bis(imidazol-1′-yl)ethane-κ²N:N′)cobalt(II), C₃₄H₃₆Co₂N₈O₁₂

March 15, 2019

Xun-Li Ling, Yue-Min Wei, Bi-Gang Zhang, Min-Le Han

Page range: 659-661

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C 34 H 36 Co 2 N 8 O 12 , triclinic, P 1̄ (no. 2), a = 8.5834(8) Å, b = 10.2975(10) Å, c = 22.727(2) Å, α = 78.325(1)°, β = 82.934(1)°, γ = 69.214(1)°, V = 1836.3(3) Å 3 , Z = 2, R gt ( F ) = 0.0319, wR ref ( F 2 ) = 0.0761, T = 296 K.
Open Access
Crystal structure of poly[diaqua-bis(μ₂-1-(4-(1H-imidazol-1-yl)benzyl)-1H-1,2,4-triazole-κ²N:N′)manganese(II)] terephthalate tetrahydrate, MnC₃₂H₃₈N₁₀O₁₀

March 26, 2019

Xia Zhu

Page range: 663-664

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MnC 32 H 38 N 10 O 10 , triclinic, P 1̄ (no. 2), a = 8.508(2) Å, b = 8.659(3) Å, c = 12.755(4) Å, α = 71.120(10)°, β = 84.432(16)°, γ = 88.133(16)°, V = 885.0(5) Å 3 , Z = 1, R gt ( F ) = 0.0371, wR ref ( F 2 ) = 0.1040, T = 223(2) K.
Open Access
Crystal structure of the fluorescent fipronil derivative 5,5′-(methylenebis(azanediyl))bis(1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-((trifluoromethyl)sulfinyl)-1H-pyrazole-3-carbonitrile), C₂₅H₆N₈O₂Cl₄F₁₂S₂

March 26, 2019

Yanting Du, Quan Zhou, Yufeng Huang, Lianqing Chen

Page range: 665-667

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C 25 H 6 N 8 O 2 Cl 4 F 12 S 2 , monoclinic, C 2/ c (no. 15), a = 20.0584(9) Å, b = 16.1373(7) Å, c = 10.6232(5) Å, β = 93.238(4)°, V = 3433.1(3) Å 3 , Z = 8, R gt ( F ) = 0.0543, wR ref ( F 2 ) = 0.1427, T = 293(2) K.
Open Access
Crystal structure of the phosphorescent complex diethyldithiophosphonato-κ²S,S′-bis(2-phenylpyridinato-κ²C,N)iridium(III), C₂₆H₂₆N₂O₂PS₂Ir

March 11, 2019

Lianqing Chen, Zhongda Wu

Page range: 669-671

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C 26 H 26 N 2 O 2 PS 2 Ir, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 9.4097(6) Å, b = 13.2837(9) Å, c = 20.6400(14) Å, V = 2579.9(3) Å 3 , Z = 4, R gt ( F ) = 0.0202, wR ref ( F 2 ) = 0.0471, T = 293(2) K.
Open Access
The crystal structure of 4,10-diethoxy-6H,12H-6,12-epoxydibenzo[b,f][1,5]dioxocine, C₁₈H₁₈O₅

March 19, 2019

Wang Li-Hua, Lin Dan-Dan

Page range: 673-674

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C 18 H 18 O 5 , monoclinic, P 2 1 / c (no. 14), a = 9.762(2) Å, b = 11.832(2) Å, c = 13.376(3) Å, β = 102.81(3)°, V = 1506.5(6) Å 3 , Z = 4, R gt ( F ) = 0.0417, wR ref ( F 2 ) = 0.1380, T = 293(2) K.
Open Access
Crystal structure of dichlorido-bis(N-benzyl-2-(quinolin-8-yloxy)acetamide-κ²N,O)copper(II) — ethyl acetate (1/1), C₃₈H₃₆N₄O₆Cl₂Cu

April 22, 2019

Wan-Wan Wang, Xiao-Wei Deng, Wei-Na Wu

Page range: 675-676

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C 38 H 36 N 4 O 6 Cl 2 Cu, triclinic, P 1̄ (no. 2), a = 10.749(5) Å, b = 11.074(5) Å, c = 15.951(7) Å, α = 80.471(8)°, β = 80.987(8)°, γ = 77.283(8)°, V = 1812.3(14) Å 3 , Z = 2, R gt ( F ) = 0.0465, wR ref ( F 2 ) = 0.1279, T = 296(2) K.
Open Access
Synthesis and crystal structure of bis{4-methyl-2-((E)-((4-((E)-1-(benzyloxyimino)ethyl)phenyl)imino)methyl)phenolato-κ³N,O,O}copper(II), C₉₂H₈₄Cu₂N₈O₈

April 27, 2019

Jing Huang, Jin-Xia Ma, Ping Wei, Ji-Xing Zhao

Page range: 677-679

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C 92 H 84 Cu 2 N 8 O 8 , monoclinic, P 2 1 / c (no. 14), a = 18.315(2) Å, b = 12.1533(12) Å, c = 17.518(2) Å, β = 105.289(4)°, Z = 2, V = 3761.3(7) Å 3 , R gt ( F ) = 0.0658, wR ref ( F 2 ) = 0.1809, T = 173(2)K.
Open Access
The crystal structure of 1,3,5-trinitro-4,6-diazidobenzene, C₆HN₉O₆

May 8, 2019

Wang Peilan, Wang Jianlong, Chen Lizhen

Page range: 681-682

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C 6 HN 9 O 6 , orthorhombic, Pbca (no. 61), a = 10.5199(19) Å, b = 13.436(3) Å, c = 15.235(3) Å, V = 2153.4(7) Å 3 , Z = 8, R gt ( F ) = 0.0435, wR ref ( F 2 ) = 0.1355, T = 173 K.
Open Access
Crystal structure 1-cinnamyl-2-((Z)-styryl)-1H-benzo[d]imidazole — methanol (1/1), C₂₄H₂₀N₂ ⋅ CH₄O

March 14, 2019

Hong-Bo Tan, Zheng Huang

Page range: 683-684

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C 24 H 20 N 2 ⋅ CH 4 O, monoclinic, P 2 1 / n (no. 14), a = 12.764(3) Å, b = 8.744(2) Å, c = 18.733(5) Å, β = 93.944(5)°, V = 2085.8(9) Å 3 , Z = 4, R gt ( F ) = 0.0501, wR ref ( F 2 ) = 0.1447, T = 296(2) K.
Open Access
The crystal structure of poly[m₂-aqua-tetraaqua-bis(m₉-4-formylbenzene-1,3-disulfonato)tetrasodium(I) hydrate, C₁₄H₁₈O₁₉S₄Na₄

March 26, 2019

Tai Xi-Shi, Liu Li-Li, Zhou Xiao-Jing

Page range: 685-686

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C 14 H 18 O 19 S 4 Na 4 , triclinic, P 1̄ (no. 2), a = 7.0769(14) Å, b = 9.5622(19) Å, c = 10.952(2)) Å, α = 115.14(3)°, β = 90.46(3)°, γ = 106.53(3)°, V = 636.1(2) Å 3 , Z = 1, R gt ( F ) = 0.0448, wR ref ( F 2 ) = 0.1191, T = 293(2) K.
Open Access
Crystal structure of 2-((2,8-bis(trifluoromethyl)quinolin-4-yl)(hydroxy)methyl)piperidin-1-ium trifluoroacetate, [C₁₇H₁₇F₆N₂O][C₂F₃O₂]

March 16, 2019

James L. Wardell, Edward R.T. Tiekink

Page range: 687-689

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[C 17 H 17 F 6 N 2 O][C 2 F 3 O 2 ], triclinic, P 1̄ (no. 2), a = 7.9873(1) Å, b = 11.0534(2) Å, c = 13.2380(3) Å, α = 105.617(1)°, β = 102.189(1)°, γ = 106.075(1)°. V = 1028.76(3) Å 3 , Z = 2, R gt ( F ) = 0.0403, wR ref ( F 2 ) = 0.1086, T = 120(2) K.
Open Access
The crystal structure of bis(ferrocenecarboxylato-κ²O,O′)bis[4-(dimethylamino)pyridine-κN]copper(II) — acetonitrile(1/2), C₄₀H₄₄CuO₄Fe₂N₆

April 2, 2019

Su-Juan Wang, Dong-Jian Zhu, Ai-Shan Ren, Xiao-Wei Yan

Page range: 691-692

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C 40 H 44 CuO 4 Fe 2 N 6 , triclinic, P 1̄ (no. 2), a = 7.4758(4) Å, b = 7.7447(5) Å, c = 16.2929(10) Å, α = 87.111(2)°, β = 85.196(2)°, γ = 89.736(2)°, V = 938.82(10) Å 3 , Z = 1, R gt ( F ) = 0.0672, wR ref ( F 2 ) = 0.1316, T = 150(2) K.
Open Access
Crystal structure of poly[di-μ₂-aqua)-diaqua-bis(μ₆-4,4′,4′′-(benzene-1,3,5-triyltris(oxy))tribenzoato-κ⁶O¹:O²:O³:O³:O⁵:O⁶)tricadmium(II)] dihydrate, C₅₄H₄₂Cd₃O₂₄

March 21, 2019

Peng Zhang, Yan Su

Page range: 693-695

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C 54 H 42 Cd 3 O 24 , triclinic, P 1̄ (no. 2), a = 7.9122(5) Å, b = 9.0693(6) Å, c = 18.6637(11) Å, β = 100.765(6)°, V = 1241.99(15) Å 3 , Z = 1, R gt ( F ) = 0.0266, wR ref ( F 2 ) = 0.0646, T = 293(2) K.
Open Access
The crystal structure of dichlorido(1,3-bis(2,6-diisopropyl-phenyl)-1H-3λ⁴-imidazol-2-yl)(3-phenyl-pyridine-κN)palladium(IV), C₃₈H₄₅N₃Cl₂Pd

April 27, 2019

Zhen Bao, Ping Lin

Page range: 697-699

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C 38 H 45 N 3 Cl 2 Pd, monoclinic, P 2 1 / c (no. 14), a = 12.8249(8) Å, b = 16.0552(9) Å, c = 20.5611(10) Å, β = 115.396(3)°, V = 3824.5(4) Å 3 , Z = 4, R gt ( F ) = 0.0287, wR ref ( F 2 ) = 0.0879, T = 173(2) K.
Open Access
The crystal structure of 2-chloro-4-(prop-2-yn-1-yloxy)-6-phenyl-1,3,5-triazine, C₁₂H₈ClN₃O

March 26, 2019

Zhenyu Zuo, Xiaomei Song, Rui Liu, Lei Xue, Xiaojuan Han

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C 12 H 8 ClN 3 O, monoclinic, C 2/ c (no. 15), a = 19.2743(18) Å, b = 7.3515(7) Å, c = 17.8170(16) Å, β = 112.593(2)°, V = 2330.8(4) Å 3 , Z = 8, R gt ( F ) = 0.0333, wR ref ( F 2 ) = 0.0906, T = 153(2) K.
Open Access
The crystal structure of 2,6-di-tert-butyl-4-(phenyl(phenylsulfonyl)methyl)phenol, C₂₇H₃₂O₃S

April 27, 2019

Zhang-Qin Liu, Min Tang, Liang-Dong Zhang, Peng-Sheng You, Sheng-Shu Liu

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C 27 H 32 O 3 S, triclinic, P 1̄, a = 12.2441(2) Å, b = 14.9350(2) Å, c = 15.2081(3) Å, α = 73.6710(16)°, β = 70.1267(17)°, γ = 70.7828(15)°, V = 2424.41(8) Å 3 , Z = 4, R gt ( F ) = 0.0442, wR ref ( F 2 ) = 0.1319, T = 297.1(2) K.
Open Access
Crystal structure of bis{μ₂-bis{(((((1-methoxyimino)ethyl)phenyl)imino)methyl)-2-phenolato-κ³N,O:O}copper(II)}, C₆₈H₆₈Cu₂N₈O₈

May 8, 2019

Jing Huang, Jin-Xia Ma, Ping Wei, Ji-Xing Zhao

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C 68 H 68 Cu 2 N 8 O 8 , monoclinic, P 2 1 / c , a = 16.241(3) Å, b = 12.1604(19) Å, c = 15.531(3) Å, β = 96.364(3)°, Z = 2, V = 3048.3(9) Å 3 , R gt ( F ) = 0.0497, wR ref ( F 2 ) = 0.1263, T = 296(2)K.
Open Access
Crystal structure of catena-poly[tetraaqua-bis(μ₂-2-(4-carboxylatophenoxy)benzoato-κ²O:O′)-pentakis(pyridine-κ¹N)dinickel(II)], C₅₃H₄₇N₅Ni₂O₁₃

April 8, 2019

Hao Wu, Li Zhang, Yun Ma, Weichao Du

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C 53 H 47 N 5 O 13 Ni 2 , monoclinic, C 2/ c (no. 15), a = 24.0549(15) Å, b = 14.5539(4) Å, c = 18.8986(11) Å, β = 130.953(10)°, V = 4996.9(7) Å 3 , Z = 4, R gt ( F ) = 0.0435, wR ref ( F 2 ) = 0.1158, T = 293(2) K.
Open Access
Synthesis and crystal structure of 1-(2,6-dichloro-4-trifluoromethyl-phenyl)-5-(3-methoxy-benzylamino)-4-trifluoromethanesulfinyl-1H-pyrazole-3-carbonitrile, C₂₀H₁₂N₄Cl₂F₆O₂S

March 11, 2019

Lianqing Chen, Zhongda Wu

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C 20 H 12 N 4 Cl 2 F 6 O 2 S, triclinic, P 1̄ (no. 2), a = 8.581(3) Å, b = 10.967(4) Å, c = 13.802(5) Å, α = 106.287(4)°, β = 105.505(4)°, γ = 101.592(4)°, V = 1146.7(7) Å 3 , Z = 2, R gt ( F ) = 0.0500, wR ref ( F 2 ) = 0.1426, T = 173 K.
Open Access
Redetermination of the crystal structure of bis(μ₂-di-ethyldithiocarbamato-κ³S,S′:S;κ³S:S: S′)-hexacarbonyl-di-rhenium(I), C₁₆H₂₀N₂O₆Re₂S₄

March 11, 2019

See Mun Lee, Kong Mun Lo, Peter J. Heard, Edward R.T. Tiekink

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C 16 H 20 N 2 O 6 Re 2 S 4 , monoclinic, C 2/ c (no. 15), a = 15.3490(2) Å, b = 11.79920(10) Å, c = 13.33770(10) Å, β = 103.9980(10)°, V = 2343.80(4) Å 3 , Z = 4, R gt ( F ) = 0.0166, wR ref ( F 2 ) = 0.0445, T = 100(2) K.
Open Access
The crystal structure of (E)-N′-((2-hydroxynaphthalen-1-yl)methylene)-2-phenylacetohydrazide, C₁₉H₁₆O₂N₂

April 1, 2019

Tai Xi-Shi, Wang Li-Hua, Liu Li-Li, Zhou Xiao-Jing

Page range: 723-724

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C 19 H 16 O 2 N 2 , orthorhombic, Pbca (no. 61), a = 12.200(2) Å, b = 9.5800(19) Å, c = 25.060(5) Å, V = 2928.9(10) Å 3 , Z = 8, R gt ( F ) = 0.0818, wR ref ( F 2 ) = 0.2438, T = 293(2) K.
Open Access
Crystal structure of 6-hydroxy-4,8,11b-trimethyltetradecayhdro-8,11-epoxy-6a,9-methanocyclohepta[a]naphthalene-4-carboxylic acid – methanol (1/1), C₂₀H₃₀O₄

April 22, 2019

Juan Zou, Tian-Tian Tang, Jiang-Hai Ye, Chen-Liang Zhao, Kang He, Lu-Tai Pan

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C 20 H 30 O 4 , orthorhombic, P 2 1 2 1 2 (no. 18), a = 12.6727(4) Å, b = 19.8422(7) Å, c = 7.5471(3) Å, V = 1897.75(12) Å 3 , Z = 2, R gt ( F ) = 0.0448, wR ref ( F 2 ) = 0.1311, T = 243(2) K.
Open Access
The crystal structure of aqua-bis(3-acetyl-2-oxo-2H-chromen-4-olato-κ²O,O′)zinc(II) monohydrate, C₂₂H₁₈O₁₀Zn

May 8, 2019

Milenko N. Ristić, Marko V. Rodić, Niko S. Radulović, Biljana R. Dekić, Vidoslav S. Dekić, Novica R. Ristić, Dejan M. Gurešić

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C 22 H 18 O 10 Zn, triclinic, P 1̄ (no. 2), a = 7.9616(3) Å, b = 9.5386(3) Å, c = 14.2569(4) Å, α = 81.713(3)°, β = 82.724(3)°, γ = 73.103(3)°, V = 1021.03(6) Å 3 , Z = 2, R gt ( F ) = 0.0223, wR ref ( F 2 ) = 0.0603, T = 295(2) K.
Open Access
Crystal structure of poly[bis(μ₂-4-bromoisophthalate-κ²O:O′)-tris(μ₂-1-(3-((1H-1,2,4-triazol-1-yl)methyl)benzyl)-1H-1,2,4-triazole-κ²N:N′)dicobalt(II)] monohydrate, C₂₆H₂₃CoN₉O₅Br

March 30, 2019

Tao Sun

Page range: 733-735

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C 26 H 23 CoN 9 O 5 Br, triclinic, P 1̄ (no. 2), a = 8.3522(10) Å, b = 13.6076(16) Å, c = 14.1028(17) Å, α = 64.664(1)°, β = 76.130(1)°, γ = 79.045(1)°, V = 1405.4(3) Å 3 , Z = 2, R gt ( F ) = 0.0445, wR ref ( F 2 ) = 0.1156, T = 296(2) K.
Open Access
A cyclic I₁₀²⁻ anion in the layered crystal structure of theophyllinium pentaiodide, C₇H₉I₅N₄O₂

May 3, 2019

Guido J. Reiss

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C 7 H 9 I 5 N 4 O 2 , monoclinic, P 2 1 / c (no. 14), a = 9.46793(10) Å, b = 11.58276(12) Å, c = 16.41497(18) Å, β = 100.844(1)°, Z = 4, V = 1768.00(3) Å 3 , R gt ( F ) = 0.0306, wR ref ( F 2 ) = 0.0728, T = 130(2) K.
Open Access
Crystal structure of catena-poly[diaqua-bis(μ₂-4-((4-(pyridin-2-ylmethoxy)phenyl)diazenyl)benzoato-κ³O,O′:N)cadmium(III)], Cd(C₁₉H₁₄O₃N₃)₂(H₂O)

April 2, 2019

Ying Zhao

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C 38 H 30 N 6 O 7 Cd, monoclinic, C 2/ c (no. 15), a = 16.937(3) Å, b = 6.1323(12) Å, c = 33.322(7) Å, β = 99.31(3)°, V = 3415.4(12) Å 3 , Z = 4, R gt ( F ) = 0.0314, wR ref ( F 2 ) = 0.0668, T = 296(2) K.
Open Access
Crystal structure of catena-poly[(μ₂-4,4′-bipyridyl-κN,N′)-bis(O,O′-dimethyldithiophosphato-κS)-zinc(II)], {C₁₄H₂₀N₂O₄P₂S₄Zn}_n

March 26, 2019

Yee Seng Tan, Edward R.T. Tiekink

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C 14 H 20 N 2 O 4 P 2 S 4 Zn, triclinic, P 1̄ (no. 2), a = 8.0014(2) Å, b = 10.3376(2) Å, c = 14.2488(3) Å, α = 84.676(2)°, β = 76.042(2)°, γ = 79.752(2)°, V = 1124.01(4) Å 3 , Z = 2, R gt ( F ) = 0.0265, wR ref ( F 2 ) = 0.0655, T = 100(2) K.
Open Access
Crystal structure of 3-amino-2-hydroxy-6-methoxybenzamide hydrate, C₁₆H₂₂N₄O₇

March 14, 2019

Lin Ling Gan, Bo Wang

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C 16 H 22 N 4 O 7 , orthorhombic, Fdd 2 (no.43), a = 26.279(15) Å, b = 30.020(17) Å, c = 4.404(2) Å, V = 3474(3) Å 3 , Z = 8, R gt ( F ) = 0.0332, wR ref ( F 2 ) = 0.0899, T = 296(2) K.
Open Access
Crystal structure of hemikis(cyclohexane-1,4-diammonium) (pyridine-2-carboxylate), [C₆H₁₆N₂]_0.5[C₆H₄NO₂]

April 22, 2019

Sang Loon Tan, Edward R.T. Tiekink

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[C 6 H 16 N 2 ] 0.5 [C 6 H 4 NO 2 ], triclinic, P 1̄ (no. 2), a = 6.7956(2) Å, b = 7.2840(3) Å, c = 10.2615(4) Å, α = 70.483(3)°, β = 80.902(3)°, γ = 66.404(3)°, V = 438.55(3) Å 3 , Z = 2, R gt ( F ) = 0.0359, wR ref ( F 2 ) = 0.0988, T = 100(2) K.
Open Access
Crystal structure of 2-chloro-4-(prop-2-yn-1-yloxy)-6-(thiophen-2-yl)-1,3,5-triazine, C₁₀H₆ClN₃OS

March 14, 2019

Zhenyu Zuo, Tianyu Guo, Xiaomei Song, Dongyan Guo, Xiao Song

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C 10 H 6 ClN 3 OS, monoclinic, C 2/ c (no. 15), a = 18.3141(4) Å, b = 7.31845(15) Å, c = 17.7885(4) Å, β = 110.495(3)°, V = 2233.30(9) Å 3 , Z = 8, T = 150(2), R gt ( F ) = 0.0331, wR ref ( F 2) = 0.0904.
Open Access
The crystal structure of 3-butyl-1-methyl-1H-imidazol-3-ium catena-poly[tris(μ₂-bromido-κ²Br:Br)lead(II)], C₈H₁₅Br₃N₂Pb

May 14, 2019

Hui Zhang, Shan Shan Yu

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C 8 H 15 Br 3 N 2 Pb, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 7.7781(9) Å, b = 9.7129(15) Å, c = 19.158(2) Å, V = 1447.3(3) Å 3 , Z = 4, R gt ( F ) = 0.0376, wR ref ( F 2 ) = 0.0780, T = 100 K.
Open Access
Crystal structure of 3-(5-amino-1H-1,2,4-triazol-3-yl)-1-(piperidin-1-yl)propan-1-one, C₁₀H₁₇N₅O

March 15, 2019

Lin Yuing Tan, Felicia Phei Lin Lim, Anton V. Dolzhenko, Edward R.T. Tiekink

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[C 10 H 17 N 5 O], monoclinic, P 2 1 / c (no. 14), a = 8.12150(10) Å, b = 13.2833(2) Å, c = 11.0258(2) Å, β = 110.083(2)°, V = 1117.14(3) Å 3 , Z = 4, R gt ( F ) = 0.0311, wR ref ( F 2 ) = 0.0790, T = 100(2) K.
Open Access
Crystal structure of aqua-2,2′,2′′-(((nitrilo-κN-tris(ethane-2,1-diyl))tris(azanylylidene-κ³N′,N′′,N′′′))tris(methanylylidene))tris(4-chlorophenolato-κ³O,O′,O′′)neodymium(III), C₂₇H₂₆Cl₃N₄NdO₄

March 30, 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

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C 27 H 26 Cl 3 N 4 NdO 4 , monoclinic, P 2 1 / c (no. 14), a = 13.6408(1) Å, b = 20.3377(2) Å, c = 10.7272(1) Å, β = 109.896(1)°, V = 2798.34(5) Å 3 , Z = 4, R gt ( F ) = 0.0258, wR ref ( F 2 ) = 0.0590, T = 100(2) K.
Open Access
Crystal structure of dichlorido-(μ₂-2,2′-(diazene-1,2-diyl)bis(benzen-1-ido)-κ²C:C′)dimercury(II), C₁₂H₈Cl₂Hg₂N₂

May 14, 2019

Ying Zhao

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C 12 H 8 Cl 2 Hg 2 N 2 , triclinic, P 1̄ (no. 2), a = 3.9815(8) Å, b = 8.9837(18) Å, c = 9.755(2) Å, α = 102.10(3)°, β = 99.54(3)°, γ = 98.82(3)°, V = 329.98(12) Å 3 , Z = 1, R gt ( F ) = 0.0368, wR ref ( F 2 ) = 0.1061, T = 296(2) K.
Open Access
Crystal structure of (3E,5E)-3,5-bis(4-cyanobenzylidene)-1-((4-fluorophenyl)sulfonyl)piperidin-4-one, C₂₇H₁₈FN₃O₃S

March 19, 2019

Xiao-Yan Li, Qing-Guo Meng, Gui-Ge Hou

Page range: 771-773

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C 27 H 18 FN 3 O 3 S, monoclinic, P 2 1 / c (no. 14), a = 8.091(6) Å, b = 42.84(3) Å, c = 7.096(6) Å, β = 107.806(10)°, V = 2342(3) Å 3 , Z = 4, R gt ( F ) = 0.0616, wR ref ( F 2 ) = 0.1321, T = 173(2) K.
Open Access
Crystal structure of dichlorido(pyridine-κN)(2,4,6-tri-2-pyridyl-1,3,5-triazine-κ³N²,N¹,N⁶)nickel(II), C₂₃H₁₇Cl₂N₇Ni

March 14, 2019

Kwang Ha

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C 23 H 17 Cl 2 N 7 Ni, monoclinic, P 2 1 / c (no. 14), a = 12.5392(5) Å, b = 11.5655(6) Å, c = 15.5085(8) Å, β = 102.4634(17)°, V = 2196.07(18) Å 3 , Z = 4, R gt ( F ) = 0.0348, wR ref ( F 2 ) = 0.0792, T = 223(2) K.
Open Access
Redetermination of the crystal structure of tetrakis(4-chlorobenzyl)tin(IV), C₂₈H₂₄Cl₄Sn

April 4, 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

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[C 28 H 24 Cl 4 Sn], orthorhombic, Fdd 2 (no. 43), a = 22.01600(10) Å, b = 20.79690(10) Å, c = 11.15230(10) Å, V = 5106.24(6) Å 3 , Z = 8, R gt ( F ) = 0.0134, wR ref ( F 2 ) = 0.0370, T = 100(2) K.
Open Access
The crystal structure of 2,6-bis(pyridin-1-ium-3-ylmethyl)hexahydro-4,8-ethenopyrrolo-[3,4-f] isoindole-1,3,5,7-tetrone tetrachloridocuprate(II) monohydrate, C₂₄H₂₄Cl₄CuN₄O₅

April 8, 2019

Zhi-Min Liu

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C 24 H 24 Cl 4 CuN 4 O 5 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 11.8748(12) Å, b = 13.3493(13) Å, c = 16.4721(17) Å, V = 2611.2(5) Å 3 , Z = 4, R gt ( F ) = 0.0351, wR ref ( F 2 ) = 0.0873, T = 173(2) K.
Open Access
Crystal structure of cyclo-[octaaqua-tetrakis(μ₂-5,5′-(1H-imidazole-4,5-diyl)bis(tetrazol-2-ido)-κ⁴N,N′,N′′,N′′′)tetramagnesium(II)], C₂₀H₂₄N₄₀O₈Mg₄

March 26, 2019

Nan Zhang, Shao Gang Hou

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C 10 H 12 N 20 O 4 Mg 2 , monoclinic, P 2 1 / n (no. 14), a = 7.4934(3) Å, b = 16.1409(5) Å, c = 16.1522(5) Å, β = 101.827(3)°, Z = 2, V = 1912.14(12) Å 3 , R gt ( F ) = 0.0577, wR ref ( F 2 ) = 0.1726, T = 293(2) K.
Open Access
The crystal structure of a matrine derivative, 13-(4-Cl-pyrrole)-matrine, C₁₈H₂₆ClN₄O

May 14, 2019

Ye Jing-Min, He Hui-Qing, Jiang Xu-Hong, Liu Zhan-Mei, Cheng Xing-An, He Zhao-Chang

Page range: 785-786

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C 18 H 26 ClN 4 O, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 5.3476(1) Å, b = 14.4068(2) Å, c = 22.3285(4) Å, V = 1720.23(5) Å 3 , Z = 4, R gt ( F ) = 0.0328, wR ref ( F 2 ) = 0.0774, T = 100 K.
Open Access
Crystal structure of (dibenzyl sulphoxide-κO)bis(2-chlorobenzyl-κC¹)dichloridotin(IV), C₂₈H₂₆Cl₄OSSn

March 14, 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

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C 28 H 26 Cl 4 OSSn, monoclinic, P 2 1 / c (no. 14), a = 10.6342(2) Å, b = 12.9298(3) Å, c = 20.3576(4) Å, β = 101.820(1)°, V = 2739.78(10) Å 3 , Z = 4, R gt ( F ) = 0.0197, wR ref ( F 2 ) = 0.0520, T = 100(2) K.
Open Access
Crystal structure of catena-poly[(μ₂-azido-κ²N:N)(μ₂-4-cyanobenzoato-κ²O:O′)-(μ₂-methanol-κ²O:O)copper(II)], C₉H₈CuN₄O₃

April 22, 2019

Dong Li, Ping-Ping Deng, Li Wu

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C 9 H 8 CuN 4 O 3 , triclinic, P 1̄ (no. 2), a = 6.3568(4) Å, b = 8.8323(6) Å, c = 10.8584(7) Å, α = 103.891(1)°, β = 94.868(1)°, γ = 105.453(1)°, V = 563.16(6) Å 3 , Z = 2, R gt ( F ) = 0.0245, wR ref ( F 2 ) = 0.0701, T = 296(2) K.
Open Access
Crystal structure of 1,1′-dibenzyl-3,3′-dicyano-1,1′,4,4′-tetrahydro-4,4′-bipyridine, C₂₆H₂₂N₄

March 20, 2019

Hao Zhu, Shi-Jun Chen, Yu-Xuann Lin, Qi-Di Zhong, Wu-Ji Sun, Xiu-Jun Zhang

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C 26 H 22 N 4 , monoclinic, P 2 1 / c (no. 14), a = 11.472(2) Å, b = 6.0805(12) Å, c = 29.787(6) Å, β = 92.448(3)°, V = 2075.9(7) Å 3 , Z = 4, R gt ( F ) = 0.0427, wR ref ( F 2 ) = 0.0882, T = 296(2) K.
Open Access
Crystal structure of (2-bromobenzyl)((1-bromonaphthalen-2-yl)methyl)sulfane, C₁₈H₁₄Br₂S

April 27, 2019

Nianyuan Tan, Shuisheng Wu, Yang Huiqiong, Donghui Lan, Chak-Tong Au, Bing Yi

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C 18 H 14 Br 2 S, triclinic, P 1̄ (no. 2), a = 7.1658(10) Å, b = 7.6868(11) Å, c = 14.971(2) Å, α = 76.328(3)°, β = 84.313(3)°, γ = 81.952(3)°, V = 791.51(19) Å 3 , Z = 2, R gt ( F ) = 0.0436, wR ref ( F 2 ) = 0.1237, T = 296(2) K.
Open Access
Crystal structure of 2-(4-ammoniocyclohexyl)-3-(pyridin-2-yl)imidazo[1,5-a]pyridin-2-ium 2-[(2-carboxylatophenyl)disulfanyl]benzoate dihydrate, [C₁₈H₂₂N₄][C₁₄H₈O₄S₂] ⋅ 2H₂O

May 8, 2019

Sang Loon Tan, Edward R.T. Tiekink

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[C 18 H 22 N 4 ][C 14 H 8 O 4 S 2 ]⋅2H 2 O, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 9.7616(1) Å, b = 16.7411(2) Å, c = 18.6843(2) Å, V = 3053.39(6) Å 3 , Z = 4, R gt ( F ) = 0.0265, wR ref ( F 2 ) = 0.0679, T = 100(2) K.
Open Access
Crystal structure of (E)-N-((3R,5S,10S, 13S,14S,17S)-17-((S)-1-(dimethylamino)ethyl)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-3-yl)-2-methylbut-2-enamide – water – methanol (1/1/1), C₂₉H₅₄N₂O₃

April 27, 2019

Bo Tan, Qi-Yun Wu, Ji-Chun Wu, Shao-Jie Huo, Xi-Cheng He, Jiang Du

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C 29 H 54 N 2 O 3 , monoclinic, P 2 1 (no. 4), a = 9.8091(11) Å, b = 7.6661(8) Å, c = 19.095(2) Å, β = 93.171(4)°, V = 1433.7(3) Å 3 , Z = 2, R gt ( F ) = 0.0657, wR ref ( F 2 ) = 0.1362, T = 250 K.
Open Access
Crystal structure of methyl 2-(4-(3-(2,4-difluorophenyl)pyrazolo[1,5-a]pyrimidin-6-yl)phenyl)acetate, C₂₁H₁₅F₂N₃O₂

May 3, 2019

Jiang Ping Meng, Bo Fang, Hong Bo Tan

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C 21 H 15 F 2 N 3 O 2 , triclinic, P 1̄ (no. 2), a = 7.389(5) Å, b = 14.011(9) Å, c = 16.733(11) Å, α = 96.568(13)°, β = 100.432(13)°, γ = 94.589(13)°, V = 1683.6(19) Å 3 , Z = 4, R gt ( F ) = 0.0589, wR ref ( F 2 ) = 0.1621, T = 296 K.
Open Access
Crystal structure of poly[triaqua-(μ₄-benzene-1,3,5-tricarboxylato-κ⁵O¹,O²:O³:O⁴:O⁵)-(μ₂-5-(3-pyridyl)tetrazolato-κ²N¹:N³)dizinc(II)], C₁₅H₁₃N₅O₉Zn₂

May 8, 2019

Gaoxiang Meng, Qiang Li, Yongming Yang

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C 15 H 13 N 5 O 9 Zn 2 , monoclinic, P 2 1 / n (no. 14), a = 6.7739(13) Å, b = 14.160(3) Å, c = 18.506(4) Å, β = 97.908(4)°, V = 1758.1(6) Å 3 , Z = 4, R gt ( F ) = 0.0597, wR ref ( F 2 ) = 0.1125, T = 298(2) K.
Open Access
Crystal structure of N-(3-methylphenyl)(propan-2-yloxy)carbothioamide, C₁₁H₁₅NOS

April 4, 2019

Chien Ing Yeo, Edward R. T. Tiekink

Page range: 813-815

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C 11 H 15 NOS, monoclinic, C 2/ c (no. 15), a = 21.0452(12) Å, b = 6.1447(4) Å, c = 17.1892(10) Å, β = 93.3520(10)°, V = 2219.0(2) Å 3 , Z = 8, R gt ( F ) = 0.0291, wR ref ( F 2 ) = 0.0854, T = 100(2) K.
Open Access
Crystal structure of poly[(μ₂-1,3-bis(imidazol-1-ylmethyl)benzene-κ²N:N′)(nitrato-κ¹O)cadmium(II)] — water (2/1), C₂₈H₃₂CdN₁₀O₇

April 27, 2019

Bo Wang, Yu Zhou, Yu Wang, Gao-Hui Chen, Qi-Xin Lian, Hai-Dong Wang

Page range: 817-818

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C 28 H 32 CdN 10 O 7 , triclinic, P 1̄ (no. 2), a = 8.2649(5) Å, b = 9.7841(6) Å, c = 10.0808(6) Å, α = 94.069(7)°, β = 104.912(7)°, γ = 97.695(7)°, V = 775.89(9) Å 3 , Z = 1, R gt ( F ) = 0.0432, wR ref ( F 2 ) = 0.1140, T = 293(2) K.
Open Access
Crystal structure of 4-phenyl-2,4-dihydro-3H-1,2,4-triazole-3-thione, C₈H₇N₃S

May 8, 2019

Chien Ing Yeo, Edward R.T. Tiekink

Page range: 819-820

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C 8 H 7 N 3 S, monoclinic, P 2 1 / c (no. 14), a = 6.0155(1) Å, b = 14.1062(1) Å, c = 10.1990(1) Å, β = 98.871(1)°, V = 855.092(18) Å 3 , Z = 4, R gt ( F ) = 0.0241, wR ref ( F 2 ) = 0.0609, T = 100(2) K.
Open Access
Crystal structure of benzyltrichloridobis(1H-pyrazole-κ²N)tin(IV), C₁₃H₁₅Cl₃N₄Sn

March 28, 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 821-822

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C 13 H 15 Cl 3 N 4 Sn, monoclinic, C 2/ c (no. 15), a = 32.4593(4) Å, b = 7.43400(10) Å, c = 14.7108(2) Å, β = 106.084(1)°, V = 3410.80(8) Å 3 , Z = 8, R gt ( F ) = 0.0151, wR ref ( F 2 ) = 0.0410, T = 293(2) K.
Open Access
Crystal structure of chlorido-4-fluorobenzyl-bis(2-methylquinolin-8-olato-κ²N,O)tin(IV), C₂₇H₂₂ClFN₂O₂Sn

April 22, 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 823-825

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C 27 H 22 ClFN 2 O 2 Sn, tetragonal, P 4 1 (no. 76), a = 9.38970(10) Å, c = 26.2753(4) Å, V = 2316.60(6) Å 3 , Z = 4, R gt ( F ) = 0.0141, wR ref ( F 2 ) = 0.0381, T = 293(2) K.
Open Access
Crystal structure of tetrakis(O,O′-diisopropyldithiophosphato-κ²S,S′)-(μ₂-1,2-bis(4-pyridylmethylene)hydrazine-κ²N:N′)zinc(II), C₃₆H₆₆N₄O₈P₄S₈Zn₂

May 8, 2019

Yee Seng Tan, Edward R.T. Tiekink

Page range: 827-829

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C 36 H 66 N 4 O 8 P 4 S 8 Zn 2 , triclinic, P 1̄ (no. 2), a = 7.94960(10) Å, b = 11.5638(2) Å, c = 16.5616(2) Å, α = 75.604(1)°, β = 86.321(1)°, γ = 83.103(2)°, V = 1463.06(4) Å 3 , Z = 1, R gt ( F ) = 0.0424, wR ref ( F 2 ) = 0.1072, T = 100(2) K.
Open Access
Crystal structure of tetrabutylammonium 4,4-oxydibenzoate – boric acid – water (1/2/6) C₄₆H₉₈B₂N₂O₁₇

May 14, 2019

Yongxia Cui, Xiaohui Chen, Tingting Zhang

Page range: 831-834

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C 46 H 98 B 2 N 2 O 17 , orthorhombic, Pbca (no. 61), a = 16.485(3) Å, b = 17.441(3) Å, c = 41.100(7) Å, V = 11817(3) Å 3 , Z = 8, R gt ( F ) = 0.0516, wR ref ( F 2 ) = 0.1557, T = 296(2) K.
Open Access
Redetermination of the crystal structure of catena-poly[[tribenzyltin(IV)]-(μ₂-pyridine-4-carboxylato-κ²N:O)], C₂₇H₂₅NO₂Sn

April 4, 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 835-837

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C 27 H 25 NO 2 Sn, monoclinic, P 2 1 / c (no. 14), a = 9.61670(10) Å, b = 16.3285(2) Å, c = 14.5921(2) Å, β = 97.6430(10)°, V = 2270.99(5) Å 3 , Z = 4, R gt ( F ) = 0.0221, wR ref ( F 2 ) = 0.0566, T = 296(2) K.
Open Access
The synthysis and crystal structure of cyclohexyl 5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-((trifluoromethyl)sulfinyl)-1H-pyrazole-3-carboxylate, C₁₈H₁₅N₃Cl₂F₆O₃S

May 8, 2019

Lianqing Chen, Xiaoshan Wei

Page range: 839-841

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C 18 H 15 N 3 Cl 2 F 6 O 3 S, monoclinic, P 2 1 / n (no. 14), a = 5.6682(7) Å, b = 31.130(4) Å, c = 12.2829(16) Å, β = 98.328(2)°, V = 2144.5(5) Å 3 , Z = 4, R gt ( F ) = 0.0535, wR ref ( F 2 ) = 0.1133, T = 173 K.
Open Access
The crystal structure of 5,7-bis(2-hydroxyethoxy)-2-phenyl-4H-chromen-4-one, C₁₉H₁₈O₆

May 8, 2019

Ying Yang, Jin Shao, Tong Zhao, Hui-Ping Ma, Dong-Mei Zhang, Lin-Lin Jing

Page range: 843-844

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C 19 H 18 O 6 , monoclinic, P 2 1 / n (no. 14), a = 9.94437(14) Å, b = 8.33132(15) Å, c = 22.5305(4) Å, β = 92.5633(14)°, V = 1864.78(5) Å 3 , Z = 4, R gt ( F ) = 0.0507, wR ref ( F 2 ) = 0.1564, T = 295.22(10) K.
Open Access
Synthesis and crystal structure of (±)-Ethyl 5′-(difluoromethyl)-2-oxo-4′,5′-dihydrospiro[indoline-3,3′-pyrazole]-4′-carboxylate, C₁₄H₁₃F₂N₃O₃

May 14, 2019

Wu-Wu Li, Min-Yan Zheng, Ying Guo, Yan-Ping Jiang, Qiao Wang, Mei Wang, Min-Xiang Ji, Yu-Tao Zhang, Zun-Ting Zhang

Page range: 845-847

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C 14 H 13 F 2 N 3 O 3 , triclinic, P 1̄ (no. 2), a = 9.4486(7) Å, b = 12.4694(8) Å, c = 13.8690(8) Å, α = 65.734(6)°, β = 74.523(5)°, γ = 83.726(6)°, V = 1435.63(18) Å 3 , Z = 4, R gt ( F ) = 0.0495, wR ref ( F 2 ) = 0.1249, T = 293(2) K.

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