Volume 234, Issue 3

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Zeitschrift für Kristallographie - New Crystal Structures

Contents

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Cover and Frontmatter

March 22, 2019

Page range: i-vii

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Open Access
Crystal structure of poly[aqua-μ₂-4,4′-bis(pyrid-4-yl)biphenyl-κ²N:N′)-μ₄-4′-methyl-[1,1′-biphenyl]-3,5-dicarboxylato-κ⁴O:O′:O′′:O′′′)manganese(II)], C₅₂H₄₀N₂O₁₀Mn₂

January 29, 2019

Shi-Jun Chen, Shi-Hui Li, Wei-Hua Wang, Yong-Fu Long, Wen-Lai Zhang, Tao Wang, Yan-Li Xu

Page range: 373-375

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C 52 H 40 N 2 O 10 Mn 2 , monoclinic, I 2/ a (no. 15), a = 8.6162(4) Å, b = 11.0217(5) Å, c = 45.266(2) Å, β = 92.828(4)°, V = 4293.5(3) Å 3 , Z = 4, R gt ( F ) = 0.0476, wR ref ( F 2 ) = 0.0988, T = 293(2) K.
Open Access
Crystal structure of bis[2-(((3-aminopropyl)imino)methyl)-4-nitro-phenolato-κ³N,N′,O]nickel(II), C₂₀H₂₄N₆NiO₆

January 12, 2019

Li Wang, Meng Yu, Ling-Zhi Liu, Jin-Xia Ma, Wen-Kui Dong

Page range: 377-378

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C 20 H 24 N 6 NiO 6 , triclinic, P 1̄ (no. 2), a = 5.3944(6) Å, b = 10.1144(12) Å, c = 10.9297(12) Å, α = 65.236(3)°, β = 81.959(3)°, γ = 79.882(3)°, Z = 1, V = 531.61(11) Å 3 , R gt ( F ) = 0.0262, wR ref ( F 2 ) = 0.0649, T = 173(2) K.
Open Access
Synthesis and crystal structure of bis{2-((E)-((4-((E)-1-(methoxyimino)ethyl)phenyl)imino)methyl) phenolato-κ²N,O}cobalt(II) — ethanol (1/1), C₃₄H₃₆CoN₄O₅

February 4, 2019

Yu-Hua Yang, Zhi-Li Wei, Yi-Zheng Li, Ji-Xing Zhao, Wen-Kui Dong

Page range: 379-381

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C 34 H 36 CoN 4 O 5 , triclinic, P 1̅ (no. 2), a = 8.7040(5) Å, b = 12.7375(9) Å, c = 14.2626(9) Å, α = 99.054(2)°, β = 95.727(2)°, γ = 92.477(2)° V = 1550.96(17) Å 3 , Z = 2, R gt ( F ) = 0.0554, wR ref ( F 2 ) = 0.1369, T = 296(2) K.
Open Access
Crystal structure of 1-(4-{2,5-dichloro-3-hydroxy-4-[4-(1-methoxyimino-ethyl)-phenylamino]-6-methyl-phenylamino}-phenyl)-ethanone O-methyl-oxime, C₂₄H₂₂Cl₂N₄O₄

January 30, 2019

Yang Zhang, Yong-Fan Cui, Xiao-Xin An, Peng-Peng Li, Wen-Kui Dong

Page range: 383-385

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C 24 H 22 Cl 2 N 4 O 4 , triclinic, P 1̄ (no. 2), a = 9.7533(6) Å, b = 10.2969(8) Å, c = 17.9128(12) Å, α = 104.131(2)°, β = 99.242(2)°, γ = 91.106(2)°, V = 1718.7(2) Å 3 , Z = 3, R gt ( F ) = 0.0502, wR ref ( F 2 ) = 0.1256, T = 153(2) K.
Open Access
The pseudosymmetric crystal structure of 2,4,6,8,10,12-hexanitrohexaazaisowurtzitane dimethyl carbonate (2/3), C₂₁H₃₀N₂₄O₃₃

January 24, 2019

Fanfan Shen

Page range: 387-389

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C 21 H 30 N 24 O 33 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 12.6527(16) Å, b = 16.395(2) Å, c = 20.606(3) Å, V = 4274.5(9) Å 3 , Z = 4, R gt ( F ) = 0.0367, wR ref ( F 2 ) = 0.0907, T = 200(2) K.
Open Access
Crystal structure of (1,4-diazepane)₄Cu^II₂(μ-Cl)₁₀Cu^I₆, C₂₀H₄₈Cl₁₀Cu₈N₈

January 12, 2019

Zheng Xing, Heng-Bo Yin

Page range: 391-392

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C 20 H 48 Cl 10 Cu 8 N 8 , orthorhombic, Cmce (no. 64), a = 16.477(10) Å, b = 10.008(6) Å, c = 24.201(15) Å, V = 3991(4) Å 3 , Z = 4, R gt ( F ) = 0.0364, wR ref ( F 2 ) = 0.0798, T = 296(2) K.
Open Access
Crystal structure of methyl 2,7,7-trimethyl-4-(3-methylthiophen-2-yl)-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate, C₁₉H₂₃NO₃S

January 29, 2019

Xiao-Qing Lu, Huan-Hu Zhang, Rui Yang, Si-Yuan Zhu, Fu-Sheng Wang

Page range: 393-394

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C 19 H 23 NO 3 S, monoclinic, P 2 1 / n (no. 14), a = 9.0403(15) Å, b = 18.213(3) Å, c = 11.1889(19) Å, β = 107.964(2)°, V = 1752.4(5) Å 3 , Z = 4, R gt ( F ) = 0.0498, wR ref ( F 2 ) = 0.1536, T = 296(2) K.
Open Access
Crystal structure of methyl 2-(4-(pyrazolo[1,5-a]pyrimidin-6-yl)phenyl)acetate, C₁₅H₁₃N₃O₂

February 6, 2019

Bo Fang, Jiang Ping Meng, Yan Luo

Page range: 395-396

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C 15 H 13 N 3 O 2 , triclinic, P 1̄ (no. 2), a = 4.6502(18) Å, b = 11.937(3) Å, c = 13.1822(19) Å, α = 115.26(4)°, β = 94.81(5)°, γ = 96.49(5)°, V = 650.4(4) Å 3 , Z = 2, R gt ( F ) = 0.0762, wR ref ( F 2 ) = 0.1794, T = 296(2) K.
Open Access
Crystal structure of (1S,3aR,3bR,10aR,10bR,12aR)-8-amino-3a,3b,6,6,10a-pentamethyl-1-((S)-2,6,6-trimethyltetrahydro-2H-pyran-2-yl)-2,3,3a,3b,4,5,5a,6,10,10a,10b,11,12,12a-tetradecahydro-1H-cyclopenta[7,8]phenanthro[2,3-d]thiazol-12-ol – a panaxadiol dervative, C₃₁H₅₀N₂O₂S

February 4, 2019

Jia-Zhen Wang, Wei-Zhao Weng, Ying Ma, Xiu-Ting He, Qing-Guo Meng

Page range: 397-400

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C 31 H 50 N 2 O 2 S, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 11.9922(9) Å, b = 16.7099(8) Å, c = 29.1262(16) Å, V = 5836.6(6) Å 3 , Z = 8, R gt ( F ) = 0.0654, wR ref ( F 2 ) = 0.1230, T = 293(2) K.
Open Access
Crystal structure of bis[(((4-fluorophenyl)amino)methyl)triphenylphosphonium] tetrachloridocobaltate(II), C₅₀H₄₄Cl₄CoF₂N₂P₂

January 24, 2019

S. Kanchanadevi, Frank R. Fronczek, V. Arun, V. Mahalingam

Page range: 401-403

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C 50 H 44 Cl 4 CoF 2 N 2 P 2 , orthorhombic, Pbca (no. 61), a = 18.4662(6) Å, b = 15.2888(5) Å, c = 33.2661(10) Å, V = 9391.9(5) Å 3 , Z = 8, R gt ( F ) = 0.0403, wR ref ( F 2 ) = 0.1005, T = 180.0(5) K.
Open Access
Crystal structure of 5,4′-dihydroxy-7,3′-dimethoxyflavanone, C₁₇H₁₆O₆

January 29, 2019

Jonathan Cisterna, Jorge Bórquez, Rubén Muñoz, Mario Simirgiotis, Alejandro Cárdenas, Iván Brito

Page range: 405-407

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C 17 H 16 O 6 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 5.2601(3) Å, b = 12.7161(6) Å, c = 22.0116(11) Å, V = 1472.31(13) Å 3 , Z = 4, R gt ( F ) = 0.0430, wR ref ( F 2 ) = 0.1089, T = 296(2) K.
Open Access
Crystal structure of 3-methyl-cyclobis(1-(1,1′-ferrocenylmethyl)-4-butyl-1H-1,2,3-triazole) tetrafluoroborate, C₂₁H₂₅FeN₆⋅BF₄

February 19, 2019

Jianghua Xu, Jian Li, Yun Ling, Bo Xu

Page range: 409-410

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C 21 H 25 FeN 6 ⋅BF 4 , monoclinic, Pn (no. 7), a = 9.6166(5) Å, b = 10.8331(6) Å, c = 11.0982(6) Å, β = 105.997(2)°, V = 1111.41(10) Å 3 , Z = 2, R gt ( F ) = 0.0388, wR ref ( F 2 ) = 0.0831, T = 180(2) K.
Open Access
Crystal structure of 3-(2-diethylaminoethyl)-2,3-dihydro-2-thioxoquinazolin-4(1H)-one, C₁₄H₁₉N₃OS

January 12, 2019

Xiao-Xing Liu, Hong-Xin Cai

Page range: 411-412

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C 14 H 19 N 3 OS, monoclinic, P 2 1 / c (no. 14), a = 7.641(3) Å, b = 24.184(8) Å, c = 7.947(3) Å, β = 111.196(5)°, V = 1369.2(8) Å 3 , Z = 4, R gt ( F ) = 0.0322, wR ref ( F 2 ) = 0.0968, T = 296(2) K.
Open Access
Crystal structure of 2-(bis(3,5-dimethylphenyl) ((methyldiphenylsilyl)oxy)methyl) pyrrolidine, C₃₄H₃₉NOSi

January 12, 2019

Kimberleigh B. Govender, Marivel Samipillai, Thavendran Govender, Hendrik G. Kruger, Tricia Naicker

Page range: 413-415

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C 34 H 39 NOSi, triclinic, P 1̅ (no. 2), a = 10.0901(2) Å, b = 11.5016(2) Å, c = 14.4098(3) Å, α = 69.207(1)°, β = 86.555(2)°, γ = 65.579(3)°, V = 1416.10(6) Å 3 , Z = 2, R gt ( F ) = 0.0463, wR ref ( F 2 ) = 0.1200, T = 100(2) K.
Open Access
The crystal structure of 1,4-dinitro-2,3,5,6-tetraacetoxy-piperazine, C₁₂H₁₆N₄O₁₂

January 15, 2019

Li Yunlu, Xue Mei, Wang Jianlong, Zhang Luyao, Ning Jie

Page range: 417-418

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C 12 H 16 N 4 O 12 , orthorhombic, Pbam (no. 55), a = 16.0836(17) Å, b = 8.0165(7) Å, c = 14.7754(15) Å, V = 1905.1(3) Å 3 , Z = 4, R gt ( F ) = 0.0499, wR ref ( F 2 ) = 0.1606, T = 173 K.
Open Access
Crystal structure of rac-3,6-dimethyl-5-(prop-1-en-2-yl)-6-vinyl-1,4,5,6-tetrahydro-2H-indol-2-one, C₁₅H₁₉NO

December 22, 2018

Yunli Bai, Yanhong Wang, Xingyi Li, Miao-Miao Xun, Changchun Yuan

Page range: 419-420

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C 15 H 19 NO, M = 229.32, triclinic, P 1̄ (no. 2), a = 6.9535(5) Å, b = 7.4037(6) Å, c = 14.5179(9) Å, α = 97.879(4), β = 93.543(5), γ = 116.785(5), V = 654.43(9) Å 3 , Z = 2, R gt ( F ) = 0.0520, wR ref ( F 2 ) = 0.1518, T = 173 K.
Open Access
Crystal structure of (Cu_0.51In_0.49)_tet[Cr_1.74In_0.26]_octSe₄ selenospinel, Cu_0.51In_0.75Cr_1.74Se₄

January 24, 2019

Silvana Moris, Patricia Barahona, Antonio Galdámez

Page range: 421-422

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Cu 0.51 In 0.75 Cr 1.74 Se 4 , cubic, Fd 3̄ m (no. 227), a = 10.6506(13) Å, V = 1208.2 Å 3 , Z = 8, R gt ( F ) = 0.0371, wR ref ( F 2 ) = 0.0912, T = 293(2) K.
Open Access
Crystal structure of 7-hydroxy-5-methoxy-4,6-dimethylisobenzofuran-1(3H)-one, C₁₁H₁₂O₄

December 22, 2018

Pei-Wen Chen, Yi-Wen Tao

Page range: 423-424

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C 11 H 12 O 4 , monoclinic, P 2 1 / c (no. 14), a = 7.1609(3) Å, b = 4.6329(2) Å, c = 30.0028(14) Å, β = 96.635(4)°, V = 988.70(8) Å 3 , Z = 4, R gt ( F ) = 0.0708, wR ref ( F 2 ) = 0.1761, T = 100.01(10) K.
Open Access
Crystal structure of trans-tetrakis(acetonitrile-κN)bis(triphenylphosphine-κP)ruthenium(II) dihexafluorophosphate - dichloroform (1/2), C₄₆H₄₄Cl₆F₁₂N₄P₄Ru

December 15, 2018

Zheng Junwei, Xiu Lian Lu

Page range: 425-427

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C 46 H 44 Cl 6 F 12 N 4 P 4 Ru, orthorhombic, Pbca (no. 61), a = 14.319(2) Å, b = 16.7358(5) Å, c = 22.6972(16) Å, Z = 4, V = 5439.1(9) Å 3 , R gt ( F ) = 0.0727, wR ref ( F 2 ) = 0.1673, T = 235.38 K.
Open Access
Crystal structure of 2-((4-nitrophenyl)thio)ethan-1-ol, C₈H₉NO₃S

December 19, 2018

Mu-Xuan Lv, Lin-Yan Bian

Page range: 429-430

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C 8 H 9 NO 3 S, triclinic, P 1̅ (no. 2), a = 6.984(4) Å, b = 7.494(4) Å, c = 9.174(5) Å, α = 97.249(9)°, β = 95.155(8)°, γ = 108.515(8)°, V = 447.4(4) Å 3 , Z = 2, R gt ( F ) = 0.0538, wR ref ( F 2 ) = 0.1617, T = 296(2) K.
Open Access
Crystal structure of diaqua-dichlorido-bis(μ₃-6,6′-(hydrazine-1,2-diylidenebis(methanylylidene))bis(2-methoxyphenolato)κ⁶O,N:N′,O′,O′:O′′)trizinc(II) - ethanol (1/2), C₃₆H₄₄Cl₂N₄O₁₂Zn₃

January 24, 2019

Yuye Tan, Junjie Huang, Hui Lu, Jianhua Sun

Page range: 431-432

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C 36 H 44 Cl 2 N 4 O 12 Zn 3 , orthorhombic, Pbca (no. 61), a = 8.3378(8) Å, b = 21.188(2) Å, c = 22.802(2) Å, Z = 4, V = 4028.3(7) Å 3 , R gt (F) = 0.0513, wR ref ( F 2 ) = 0.1193, T = 296(2) K.
Open Access
Crystal structure of the co-crystal 2-[(2-carboxyphenyl)disulfanyl]benzoic acid – 3-chlorobenzoic acid (2/1), C₃₅H₂₅ClO₁₀S₄

February 28, 2019

Sang Loon Tan, Edward R.T. Tiekink

Page range: 433-436

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C 35 H 25 ClO 10 S 4 , triclinic, P 1̄ (no. 2), a = 7.9798(2) Å, b = 10.2392(3) Å, c = 20.6956(4) Å, α = 103.632(2)°, β = 96.082(2)°, γ = 96.053(2)°, V = 1619.13(7) Å 3 , Z = 2, R gt ( F ) = 0.0493, wR ref ( F 2 ) = 0.1413, T = 100(2) K.
Open Access
The crystal structure of 4-(3-chloro-4-fluorophenylamino)-7-methoxyquinazolin-6-ol, C₁₅H₁₁ClFN₃O₂

January 24, 2019

Yong Li, Yun-Deng Wu, Jingjing Wang

Page range: 437-438

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C 15 H 11 ClFN 3 O 2 , monoclinic, P 2 1 / c (no. 14), a = 12.9430(8) Å, b = 9.3196(5) Å, c = 12.5959(8) Å, β = 115.861(8)° V = 1367.21(16) Å 3 , Z = 4, R gt ( F ) = 0.0512, wR ref ( F 2 ) = 0.1359, T = 296(2) K.
Open Access
Crystal structure of ethyl (E)-1-(3-ethoxy-3-oxoprop-1-en-1-yl)-2-(4-nitrophenyl)-2,5-dihydro-1H-benzo[b][1,4]diazepine-3-carboxylate, C₂₃H₂₃N₃O₆

January 12, 2019

Hong-bo Tan, Chun-sheng Hu

Page range: 439-440

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C 23 H 23 N 3 O 6 , monoclinic, P 2 1 / c (no. 14), a = 11.235(6) Å, b = 11.251(7) Å, c = 17.814(10) Å, β = 98.872(12)°, V = 2225(2) Å 3 , Z = 4, R gt ( F ) = 0.0581, wR ref ( F 2 ) = 0.1590, T = 296(2) K.
Open Access
Crystal structure of (E)-2-(4-cyanophenyl)ethenesulfonyl fluoride, C₉H₆FNO₂S

February 1, 2019

Edikarlos Brasil, Marivel Samipillai, Thavendran Govender, Hendrik G. Kruger, Tricia Naicker

Page range: 441-442

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C 9 H 6 FNO 2 S, triclinic, P 1̄ (no. 2), a = 7.2786(2) Å, b = 8.1014(3) Å, c = 16.1084(5) Å, α = 76.320(1)°, β = 87.918(1)°, γ = 80.784(1)°, V = 911.00(5) Å 3 , Z = 4, R gt ( F ) = 0.0298, wR ref ( F 2 ) = 0.0857, T = 100(2) K.
Open Access
Crystal structure of bis(4-bromo-2-(((3-chloropropyl)imino)methyl)phenolato-κ²N,O)-oxidovanadium(IV), C₂₀H₂₀Br₂Cl₂N₂O₃V

February 4, 2019

Wei Wei, Qiong Wu, Heng-Qiang Zhang, Rui Liu, Hong-Li Chen

Page range: 443-444

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C 20 H 20 Br 2 Cl 2 N 2 O 3 V, monoclinic, P 2 1 / c (no. 14), a = 11.9615(8) Å, b = 16.5865(7) Å, c = 12.9110(10) Å, β = 115.879(9)°, V = 2304.7(3) Å 3 , Z = 4, R gt ( F ) = 0.0459, wR ref ( F 2 ) = 0.1132, T = 153(2) K.
Open Access
The crystal structure of 1,1,1,3,3,3-hexaphenyldistannoxane – 2,2′-bipyridine (1/1), C₄₆H₃₈N₂OSn₂

February 4, 2019

Junshan Sun, Yan Kong

Page range: 445-447

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C 46 H 38 N 2 OSn 2 , triclinic, P 1̄ (no. 2), a = 9.657(4) Å, b = 9.679(4) Å, c = 24.324(9) Å, α = 95.397(5)°, β = 90.138(5)°, γ = 119.283(5)°, V = 1971.2(12) Å 3 , Z = 2, R gt ( F ) = 0.0369, wR ref ( F 2 ) = 0.0873, T = 298(2) K.
Open Access
Crystal structure of coordination polymer catena-poly[diaqua-(2,6-dichloropyridine-4-carboxyliato-κ²O,O′)-bis(μ₂-2,6-dichloropyridine-4-carboxyliato-κ²O:O′)terbium(III), C₁₈H₁₀Cl₆N₃O₈Tb

January 24, 2019

Guang-Zhen Liu, Ling-Yun Xin, Xiao-Ling Li

Page range: 449-450

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C 18 H 10 Cl 6 N 3 O 8 Tb, monoclinic, I 2/ a (no. 15), a = 9.8281(2) Å, b = 11.8792(2) Å, c = 21.1568(4) Å, β = 91.1599(19)°, V = 2469.54(9) Å 3 , Z = 8, R gt ( F ) = 0.0196, wR ref ( F 2 ) = 0.0473, T = 293(2) K.
Open Access
The crystal structure of 4-((2-(4,5-dihydro-1,5-diphenyl-1H-pyrazol-3-yl)anthracen-10-yl) methyl)morpholine, C₃₄H₃₁N₃O

February 4, 2019

Zhao Bo, Cai Lin, Luo Jiewei

Page range: 451-452

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C 34 H 31 N 3 O, monoclinic, P 2 1 / c (no. 14), a = 26.803(5) Å, b = 5.8243(12) Å, c = 16.893(3) Å, β = 98.53(3)°, V = 2608.1(9) Å 3 , Z = 4, R gt ( F ) = 0.0759, wR ref ( F 2 ) = 0.2028, T = 113(2) K.
Open Access
The crystal structure of bis(N,N-dimethylformamide-κO)-tetrakis(9H-xanthene-9-carboxylic-carboxylate-κ²O:O′)dicopper(II) - acetonitrile (1/2), C₆₆H₅₆Cu₂N₄O₁₄

February 1, 2019

Wang Ren-Shu, Feng Jing

Page range: 453-454

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C 66 H 56 Cu 2 N 4 O 14 , triclinic, P 1̄ (no. 2), a = 11.0791(5) Å, b = 11.5747(5) Å, c = 12.4037(6) Å, α = 77.782(4)°, β = 86.304(4)°, γ = 69.491(4)°, V = 1455.97(12) Å 3 , Z = 2, R gt ( F ) = 0.0361, wR ref ( F 2 ) = 0.0830, T = 293(2) K.
Open Access
Crystal structure of trans-dichlorido-(1,3-dimesityl-1H-imidazol-2(3H)-ylidene)-(5-methyl-3,4-dihydro-2H-pyrrole-κN)palladium(II), C₂₅H₃₁Cl₂N₃OPd

February 1, 2019

Kai-Xin Sun, Xiang-Ting Wu, Guo-Xing Li

Page range: 455-456

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C 25 H 31 Cl 2 N 3 OPd, orthorhombic, Pbca (no. 61), a = 9.4083(4) Å, b = 17.1334(8) Å, c = 31.9251(14) Å, V = 5146.2(4) Å 3 , Z = 8, R gt ( F ) = 0.0600, wR ref ( F 2 ) = 0.1232, T = 293(2) K.
Open Access
Crystal structure of 8,8′-di-p-tolyl-8′H-7,8′-biacenaphtho[1,2-d]imidazole, C₄₀H₂₆N₄

February 11, 2019

Al-Anood M. Al-Dies, Abdullah M. Asiri, Salman A. Khan, Edward R.T. Tiekink

Page range: 457-459

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C 40 H 26 N 4 , triclinic, P 1̄ (no. 2), a = 9.5201(6) Å, b = 12.1701(8) Å, c = 12.8721(7) Å, α = 79.949(5)°, β = 88.350(5)°, γ = 75.893(6)°, V = 1424.05(16) Å 3 , Z = 2, R gt ( F ) = 0.0519, wR ref ( F 2 ) = 0.1403, T = 293 K.
Open Access
The crystal structure of 3-amino-(2,4-dioxopent-3-yl)-4,5-dihydro-1,2,4-triazinium nitrate, C₈H₁₃N₅O₅

January 31, 2019

Matouš Kloda, Irena Matulková, Ivana Císařová, Ivan Němec

Page range: 461-463

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C 8 H 13 N 5 O 5 , triclinic, P 1̄ (no. 2), a = 9.1462(4) Å, b = 9.9732(5) Å, c = 13.5252(6) Å, α = 90.098(2)°, β = 91.031(2)°, γ = 109.874(2)°, V = 1160.02(9) Å 3 , Z = 4, R gt ( F ) = 0.0392, wR ref ( F 2 ) = 0.1015, T = 150(2) K.
Open Access
Crystal structure of 4,4′,5,5′-tetraphenyl-2,2′-di-p-tolyl-2′H-1,2′-biimidazole, C₄₄H₃₄N₄

February 4, 2019

Al-Anood M. Al-Dies, Abdullah M. Asiri, Salman A. Khan, Edward R.T. Tiekink

Page range: 465-467

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C 44 H 34 N 4 , monoclinic, P 2 1 (no. 4), a = 10.1233(5) Å, b = 12.1414(7) Å, c = 13.7420(7) Å, β = 98.389(5)°, V = 1670.97(15) Å 3 , Z = 2, R gt ( F ) = 0.0452, wR ref ( F 2 ) = 0.1136, T = 293(2) K.
Open Access
Halogen bonds in the crystal structure of 2-bromo-1,10-phenanthroline – 1,4-diiodotetrafluorobenzene (2/1), C₃₀H₁₄Br₂F₄I₂N₄

January 29, 2019

Limin Dang, Saijin Huang, Aiwu Yin

Page range: 469-471

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C 30 H 14 Br 2 F 4 I 2 N 4 , monoclinic, P 2 1 / c (no. 14), a = 9.4531(3) Å, b = 40.9487(15) Å, c = 7.5118(3) Å, β = 95.110(3)°, V = 2896.20(18) Å 3 , Z = 4, R gt ( F ) = 0.0410, wR ref ( F 2 ) = 0.0828, T = 287.15(10) K.
Open Access
Crystal structure of tris(1-phenyl-1,2-propanedione-2-oximato-κ²N,O)cobalt(III), C₂₇H₂₄N₃O₆Co

January 30, 2019

Zhang Cuihong, Ge Yuan, Huo Xiaoping, Yang Liguo, Li Xin, Miao Zongcheng

Page range: 473-474

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C 27 H 24 N 3 O 6 Co, monoclinic, P 2 1 / c (no. 14), a = 11.309(3) Å, b = 19.477(5) Å, c = 11.615(3) Å, β = 109.071(9)°, V = 2418.0(11) Å 3 , Z = 4, R gt ( F ) = 0.0296, wR ref ( F 2 ) = 0.0845, T = 293(2) K [1–3].
Open Access
Crystal structure of chlorido-(6,6′-((1,2-phenylenebis(azanylylidene))bis(methanylylidene))bis(3-methoxyphenolato)-κ⁴O,N,N′,O′)iron(III), C₂₂H₁₈ClN₂FeO₄

January 31, 2019

Zhang Cuihong, Ge Yuan, Huo Xiaoping, Yang Liguo, Li Xin, Miao Zongcheng

Page range: 475-476

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C 22 H 18 ClN 2 FeO 4 , monoclinic, P 2 1 /n (no. 14), a = 7.0779(6) Å, b = 19.0203(16) Å, c = 14.7233(12) Å, β = 103.1570(10)°, V = 1930.1(3) Å 3 , Z = 4, R gt ( F ) = 0.0278, wR ref ( F 2 ) = 0.1037, T = 296(2) K.
Open Access
Crystal structure of bis(μ₂-1-(4-chlorophenyl)-3-phenyl-4-thenoyl-1H-pyrazol-5-olato-κ³O,O′:O′)-bis-(1-(4-chlorophenyl)-3-phenyl-4-thenoyl-1H-pyrazol-5-olato-κ²O,O)-bis(ethyl acetate-κO)dicadmium(II), C₈₈H₆₄Cl₄N₈O₁₂S₄Cd₂

February 5, 2019

Yong-Jie Ding, Chun-Xiang Zhao, Si-Shi Hu, Peng-Hui Wang, Chen-Cheng Ye, Hua-Li Jia, Guang-Ying Chen

Page range: 477-479

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C 88 H 64 Cl 4 N 8 O 12 S 4 Cd 2 , monoclinic, P 2 1 / c (no. 14), a = 13.5247(6) Å, b = 15.3257(7) Å, c = 20.6985(8) Å, β = 101.8630(10)°, V = 4198.7(3) Å 3 , Z = 2, R gt ( F ) = 0.0484, wR ref ( F 2 ) = 0.0967, T = 173(2) K.
Open Access
Crystal structure of catena-poly[dichlorido-(μ₂-3-(2-pyridyl)-4-(4-pyridyl)-5-(3-pyridyl)-1,2,4-triazole-κ²N:N′)] copper(II), C₁₇H₁₂N₆Cl₂Cu

February 14, 2019

Lili Zhang, Xuefan Gu, Ming Xue, Chengtun Qu, Yun Ma, Gang Chen

Page range: 481-482

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C 17 H 12 Cl 2 CuN 6 , monoclinic, P 2 1 / c (no. 14), a = 13.113(3) Å, b = 7.1325(4) Å, c = 19.527(3) Å, β = 103.628(2)°, V = 1774.8(5) Å 3 , Z = 4, R gt ( F ) = 0.0310, wR ref ( F 2 ) = 0.0682, T = 296(2) K.
Open Access
Crystal structure of dichlorido-([2,2′:6′,2′′-terpyridine]-4′-carboxylic acid-κ³N,N′,N′′)copper(II) monohydrate, C₁₆H₁₃Cl₂CuN₃O₃

January 31, 2019

Xuan Feng, Zhannan Yang, Xin-Hua Li

Page range: 483-484

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C 16 H 13 Cl 2 CuN 3 O 3 , monoclinic, P 2 1 / c (no. 14), a = 11.2656(9) Å, b = 17.1737(14) Å, c = 8.7774(7) Å, β = 98.1940(10)°, V = 1680.8(2) Å 3 , Z = 4, R gt ( F ) = 0.0270, wR ref ( F 2 ) = 0.0852, T = 298(2) K.
Open Access
Crystal structure of triethylammonium(5-carboxypyridine-2-thiolato-κ²N,S)-bis(dimethylsulfoxide-κ¹S)-(6-sulfidonicotinato-κ²N,S)ruthenium(II) trihydrate, C₂₂H₄₁N₃O₉RuS₄

February 4, 2019

Zheng Junwei, Wang Fuqiang, Gu Jiacheng, Xiu Lian Lu

Page range: 485-487

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C 22 H 41 N 3 O 9 RuS 4 , monoclinic, P 2 1 / n (no. 14), a = 8.6882(1) Å, b = 25.5660(1) Å, c = 14.1187(1) Å, β = 90.393(1)°, V = 3136.01(4) Å 3 , Z = 4, R gt ( F ) = 0.0220, wR ref ( F 2 ) = 0.0561, T = 120(1) K.
Open Access
The crystal structure of poly[(μ₅-2,5-dicarboxy-benzoato-κ⁴O:O:O′:O′′,O′′′)silver(I)], C₉H₅AgO₆

February 28, 2019

Ling Tong, Dong Tian

Page range: 489-491

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C 9 H 5 AgO 6 , triclinic, P 1̄ (no. 2), a = 3.7933(5) Å, b = 7.6762(11) Å, c = 15.534(2) Å, α = 79.109(2)°, β = 89.864(2)°, γ = 78.122(2)°, V = 434.35(10) Å 3 , Z = 2, R gt ( F ) = 0.0302, wR ref ( F 2 ) = 0.0650, T = 296(2) K.
Open Access
Crystal structure of (E)-1-(thiophen-2-yl)-N-(5-((triphenylstannyl)thio)-1,3,4-thiadiazol-2-yl)methanimine, C₂₅H₁₉N₃S₃Sn

February 14, 2019

Junshan Sun

Page range: 493-494

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C 25 H 19 N 3 S 3 Sn, monoclinic, P 2 1 / n (no. 14), a = 14.347(4) Å, b = 9.908(3) Å, c = 17.834(5) Å, V = 2405.6(11) Å 3 , Z = 4, R gt ( F ) = 0.0287, wR ref ( F 2 ) = 0.0777, T = 298(2) K.
Open Access
Crystal structure of diaqua-bis(3,5-dichloroisonicotinato-κ¹O)-bis(1,3-di(pyridin-4-yl)propane-κ¹N)cobalt(II), C₃₈H₃₆Cl₄N₆O₆Co

February 4, 2019

Xin Ling-Yun, Ji Zhou-Ru, Guo Rong-Rong

Page range: 495-497

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C 38 H 36 Cl 4 N 6 O 6 Co, triclinic, P 1̄ (no. 2), a = 9.2687(4) Å, b = 9.7747(6) Å, c = 12.0131(6) Å, α = 87.947(4)°, β = 82.062(4)°, γ = 67.258(5)°, V = 993.96(10) Å 3 , Z = 1, R gt ( F ) = 0.0397, wR ref ( F 2 ) = 0.0881, T = 292.6(3) K.
Open Access
Crystal structure of dodecaaqua-bis(μ₂-4,4′-bipyridine-κ²N:N′)-bis(4,4′-((5-carboxylato-1,3-phenylene)bis(oxy))dibenzoato-κ¹O)tricopper(II) - water (1/4), C₆₂H₇₀Cu₃N₄O₃₂

February 4, 2019

Peng Deng, Da Li, Yan Zhou, Zhi-Hong Ling, Yue-Ming Li

Page range: 499-501

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C 62 H 70 Cu 3 N 4 O 32 , monoclinic, C 2/ c (no. 15), a = 44.710(7) Å, b = 12.8847(17) Å, c = 11.9901(18) Å, β = 102.286(13)°, V = 6749.0(17) Å 3 , Z = 4, R gt ( F ) = 0.0618, wR ref ( F 2 ) = 0.1978, T = 293(2) K.
Open Access
Crystal structure of bis(5-methoxy-2-(((2-oxidoethyl)imino)methyl)phenolate-κ³O,N,O′)manganes(IV), C₂₀H₂₂N₂O₆Mn

February 5, 2019

Zhang Cuihong, Wei Xiaohu, Yang Liguo, He Zhenzhen, Li Xin, Miao Zongcheng

Page range: 503-504

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C 20 H 22 N 2 O 6 Mn, orthorhombic, Pccn (no. 56), a = 14.1678(16) Å, b = 14.3469(18) Å, c = 19.335(2) Å, V = 3930.1(8) Å 3 , Z = 8, R gt ( F ) = 0.0504, wR ref ( F 2 ) = 0.1441, T = 293(2) K.
Open Access
Crystal structure of tetramethylammonium (2-(3-ethoxy-2-oxidobenzylidene)-1-(2-hydroxybenzoyl)hydrazin-1-ido-κ³N,N′,O)cobalt(III), C₃₆H₄₀N₅O₈Co

February 14, 2019

Zhang Cuihong, Ge Yuan, Huo Xiaoping, Yang Liguo, Li Xin, Miao Zongcheng

Page range: 505-507

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C 36 H 40 N 5 O 8 Co, monoclinic, P 2 1 / c (no. 14), a = 17.353(4) Å, b = 11.474(2) Å, c = 18.074(4) Å, β = 101.056(2)°, V = 3532.0(13) Å 3 , Z = 4, R gt ( F ) = 0.0464, wR ref ( F 2 ) = 0.1323, T = 296(2) K 1–3.
Open Access
Crystal structure of 6-cyclohexyl-6,7-dihydrodibenzo[c,f][1,5]azabismocin-12(5H)-yl nitrate, C₂₀H₂₃O₃N₂Bi

February 1, 2019

Nianyuan Tan, Shuisheng Wu, Yang Huiqiong, Donghui Lan, Chak-Tong Au, Bing Yi

Page range: 509-511

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C 20 H 23 O 3 N 2 Bi, monoclinic, P 2 1 / n (no. 14), a = 10.6897(5) Å, b = 10.5590(5) Å, c = 17.4099(9) Å, β = 105.491(2)°, V = 1893.71(16) Å 3 , Z = 4, R gt ( F ) = 0.0253, wR ( F 2 ) = 0.0576, T = 296(2) K.
Open Access
Crystal structure of (E)-N-((2S,3S,4R,10R,13S, 17S)-17-(1-(dimethylamino) ethyl)-2,4-dihydroxy-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-3-yl)-2-methylbut-2-enamide, C₂₄H₄₈N₂O₃

February 1, 2019

Qi-Yun Wu, Ji-Chun Wu, Shao-Jie Huo, Xi-Chen He, Jiang Du

Page range: 513-516

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C 24 H 48 N 2 O 3 , monoclinic, P 2 1 (no. 4), a = 14.805(3) Å, b = 10.0557(18) Å, c = 18.061(3) Å, β = 98.935(5)°, V = 2656.3(8) Å 3 , Z = 4, R gt ( F ) = 0.0674, wR ref ( F 2 ) = 0.1955, T = 173 K.
Open Access
Crystal structure of (E)-2-((4-chlorophenyl)(phenyl)methylene)hydrazine-1-carbothioamide, C₁₄H₁₂ClN₃S

February 1, 2019

Chao Liu

Page range: 517-518

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C 14 H 12 ClN 3 S, monoclinic, C 2/ c (no. 15), a = 27.967(7) Å, b = 5.9290(13) Å, c = 19.698(5) Å, β = 118.122(3)°, V = 2880.6(11) Å 3 , Z = 8, R gt ( F ) = 0.0369, wR ref ( F 2 ) = 0.1082, T = 293(2) K.
Open Access
Crystal structure of 1-benzyl-3-cyano-6-phenyl-1,2-dihydropyridine, C₁₉H₁₆N₂

February 1, 2019

Shi-Jun Chen, Hao Zhu, Meng-Meng Zhang, Wen-Wu Xu, Yu-Cai Wang, Zhi-Fei Zhang

Page range: 519-520

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C 19 H 16 N 2 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 7.5177(10) Å, b = 12.4761(16) Å, c = 16.118(2) Å, V = 1511.7(3) Å 3 , Z = 4, R gt ( F ) = 0.0424, wR ref ( F 2 ) = 0.0967, T = 293(2) K.
Open Access
Isolation and crystal structure of 4-((2-(methoxycarbonyl)phenyl)amino)-2-methyl-4-oxobutanoic acid from Delphinium Grandiflorum, C₁₃H₁₅N₁O₅

February 21, 2019

Guo-Qiang Li, Yun-Yi Li, Yi-Ting Zhao, Qing-Peng Xu, Yao-Lan Li, Guo-Cai Wang

Page range: 521-522

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C 13 H 15 N 1 O 5 , triclinic, P 1̄ (no. 2), a = 7.9457(7) Å, b = 8.7190(9) Å, c = 9.9964(10) Å, α = 100.254(8)°, β = 100.036(8)°, γ = 94.760(8)°, V = 666.38(11) Å 3 , Z = 2, R gt ( F ) = 0.0453, wR ref ( F 2 ) = 0.1243, T = 298 K.
Open Access
Crystal structure of tetraqua-bis(4-(hydroxymethyl)benzoato-κO)nickel(II), C₁₆H₂₂O₁₀Ni

February 1, 2019

Lanlan Jin, Defu Tao, Rongyue Hu, Haixia Pang

Page range: 523-525

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C 16 H 22 O 10 Ni, monoclinic, P 2 1 / c (no. 14), a = 9.7643(12) Å, b = 15.440(2) Å, c = 13.6274(13) Å, β = 122.235(6)°, V = 1737.5(4) Å 3 , Z = 4, R gt ( F ) = 0.0382, wR ref ( F 2 ) = 0.1282, T = 297(2) K.
Open Access
Crystal structure of ajacisine D monohydrate, C₃₀H₄₄N₂O₉

February 1, 2019

Guo-Qiang Li, Qing-Peng Xu, Yi-Ting Zhao, Yun-Yi Li, Yao-Lan Li, Guo-Cai Wang

Page range: 527-529

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C 30 H 44 N 2 O 9 , monoclinic, P 2 1 (no. 4), a = 7.9827(3) Å, b = 12.6787(6) Å, c = 14.0183(9) Å, β = 90.903(5)°, V = 1418.62(13) Å 3 , Z = 2, R gt ( F ) = 0.0607, wR ref ( F 2 ) = 0.1298, T = 298(2) K.
Open Access
The crystal structure of (E)-4-(1-(2-aminophenylimino)ethyl)benzene-1,3-diol, C₁₄H₁₄N₂O₂

February 14, 2019

Xiao-Ming Shi, Shu-Jing Li, Li-Na Xiao, Bin Cai, Peng Peng

Page range: 531-532

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C 14 H 14 N 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 8.5030(9) Å, b = 7.6199(8) Å, c = 18.738(2) Å, β = 92.852(2)°, V = 1212.6(2) Å 3 , Z = 4, R gt ( F ) = 0.0413, wR ref ( F 2 ) = 0.1247, T = 296.15 K.
Open Access
Crystal structure of poly[(μ₄-(4H-1,2,4-triazol-4-yl)phenyl)acetato-κ⁴N,N′,O,O′)(formiato-κ¹O)cobalt(II)], C₁₁H₉CoN₃O₄

February 4, 2019

Xiao-Jun Li, Xu-Li Zeng, Li-Rui Che, Zhen Xu

Page range: 533-534

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C 11 H 9 CoN 3 O 4 , monoclinic, C 2/ c (no. 15), a = 12.6503(9) Å, b = 8.0959(6) Å, c = 22.9723(14) Å, β = 99.424(6)°, V = 2321.0(3) Å 3 , Z = 8, R gt ( F ) = 0.0370, wR ref ( F 2 ) = 0.1101, T = 293(2) K.
Open Access
The crystal structure of bis tetrabutylammonium bis(μ₃-2,2,2-tri(hydroxymethyl)ethyl-4-((3-methoxy-3-oxopropyl)amino)-4-oxobutanoato)-(μ₆-oxido)-hexakis(μ₂-oxido)-hexaoxido-hexavanadium(V), C₅₈H₁₁₂N₄O₂₉V₆

February 4, 2019

Zicheng Xiao, Bo Huang, Xiaokang Hu, Pingfan Wu

Page range: 535-537

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C 58 H 112 N 4 O 29 V 6 , P 2 1 / n (no. 14), a = 15.3310(5) Å, b = 15.6093(4) Å, c = 15.9394(5) Å, β = 109.132(4)°, V = 3603.7(2) Å 3 , Z = 2, R gt ( F ) = 0.0579, wR ref ( F 2 ) = 0.1450, T = 104.0 K.
Open Access
Crystal structure of (N-benzylpropane-1,3-diamine-κ²N, N′)(2,2′-bipyridine-κ²N,N′)platinum(II) chloride, C₂₀H₂₄Cl₂N₄Pt

February 6, 2019

Tatsuto Kiwada, Hiromu Katakasu, Akira Odani

Page range: 539-541

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C 20 H 24 Cl 2 N 4 Pt, monoclinic, P 2 1 / c (no. 14), a = 13.1119(7) Å, b = 13.5673(8) Å, c = 11.7167(5) Å, β = 99.714(7)°, V = 2054.43(19) Å 3 , Z = 4, R gt ( F ) = 0.0233, wR ref ( F 2 ) = 0.0516, T = 103 K.
Open Access
Crystal structure of 5-(5-(4-chlorophenyl)-1-phenyl-1H-pyrazol-3-yl)-N-phenyl-2-amine, C₂₃H₁₆ClN₅O

March 4, 2019

Mohammad Hayal Alotaibi, Hanan A. Mohamed, Bakr F. Abdel-Wahab, Amany S. Hegazy, Benson M. Kariuki, Gamal A. El-Hiti

Page range: 543-545

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C 23 H 16 ClN 5 O, monoclinic, P 2 1 / c (no. 14), a = 10.0503(6) Å, b = 17.5265(9) Å, c = 22.8763(16) Å, β = 91.554(6)°, V = 4028.1(4) Å 3 , Z = 8, R gt ( F ) = 0.0748, wR ref ( F 2 ) = 0.2274, T = 296(2) K.
Open Access
Crystal structure of poly-[(μ₂(carboxylatomethyl)((3-nitrophenyl)sulfonyl)amido-κ³N: O:O′)(μ₂-4,4′-bipyridine-κ²N:N′)copper(II)], C₁₈H₁₄CuN₄O₆S

February 21, 2019

Zheng-Jun Liu, Xiao-Miao Chen, Jing-Song Cheng, Tao-Li Deng, Lan Qin

Page range: 547-548

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C 18 H 14 CuN 4 O 6 S, trigonal, R 3̄ (no. 148), a = 31.125(7) Å, b = 31.125(3) Å, c = 10.133(2) Å, V = 8501(3) Å 3 , Z = 18, R gt ( F ) = 0.0346, wR ref ( F 2 ) = 0.0900, T = 296(2) K.
Open Access
Crystal structure of poly-[(μ₂-(carboxylatomethyl)((3-nitrophenyl)sulfonyl)amido-κ³N:O:O′)(μ₂-4,4′-bipyridine-κ²N:N′) nickel(II)], C₁₈H₁₄NiN₄O₆S

February 21, 2019

Zheng-Jun Liu, Xiao-Miao Chen, Jing-Song Cheng, Tao-Li Deng, Lan Qin

Page range: 549-550

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C 18 H 14 NiN 4 O 6 S, trigonal, R 3̄ (no. 148), a = 31.014(11) Å, b = 31.014(11) Å, c = 10.125(7) Å, V = 8434(8) Å 3 , Z = 18, R gt ( F ) = 0.0380, wR ref ( F 2 ) = 0.0941, T = 296(2) K.
Open Access
Crystal structure of N-((3R,10S,13S,17S)-17-((S)-1-(dimethylamino)ethyl)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-3-yl)-N-methylbenzamide, C₃₁H₄₈N₂O

February 21, 2019

Bo Tan, Qi-Yun Wu, Ji-Chun Wu, Shao-Jie Huo, Xi-Cheng He, Jiang Du

Page range: 551-553

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C 31 H 48 N 2 O, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 6.530(2) Å, b = 11.728(4) Å, c = 35.236(12) Å, V = 2698.6(15) Å 3 , Z = 4, R gt ( F ) = 0.0492, wR ref ( F 2 ) = 0.1034, T = 173 K.
Open Access
The crystal structure of dichloroido(1,3-bis(2,6-dimethyl-phenyl)-1H-3l⁴-imidazol-2-yl)(2-methyl-4,5-dihydrooxazol-κN)palladium(IV)-water (1/1), C₂₃H₂₉Cl₂N₃O₂Pd

February 19, 2019

Kai-Xin Sun, Xiang-Ting Wu, Guo-Xing Li

Page range: 555-557

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C 23 H 29 Cl 2 N 3 O 2 Pd, monoclinic, P 2 1 / c (no. 14), a = 8.7287(6) Å, b = 31.5431(18) Å, c = 9.5605(6) Å, β = 108.893(2)°, V = 2490.5(3) Å 3 , Z = 4, R gt ( F ) = 0.0438, wR ref ( F 2 ) = 0.1033, T = 293(2) K.
Open Access
Crystal structure of catena-poly[dibromido-{μ₂-1,5-dimethyl-2-phenyl-4-((pyridin-4-ylmethylene)amino)-1,2-dihydro-3H-pyrazol-3-one-κ²N:O}zinc(II)], C₃₄H₃₂Br₄N₈O₂Zn₂

February 21, 2019

Haixia Pang

Page range: 559-561

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C 34 H 32 Br 4 N 8 O 2 Zn 2 , triclinic, P 1̄ (no. 2), a = 11.441(2) Å, b = 13.422(2) Å, c = 14.370(3) Å, α = 101.129(3)°, β = 99.587(2)°, γ = 114.972(3)°, V = 1885.0(6) Å 3 , Z = 2, R gt ( F ) = 0.0510, wR ref ( F 2 ) = 0.1775, T = 298(2) K.
Open Access
Crystal structure of diaqua-dichlorido-bis(μ₂-2-(((1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)imino)methyl)phenolato-κ⁴O:O,N,O′)dicobalt(II), C₃₆H₃₆Cl₂N₆O₆Co₂

February 21, 2019

Haixia Pang, Xiong He, Xiang Feng, Ximing Yuan

Page range: 563-565

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C 36 H 36 Cl 2 N 6 O 6 Co 2 , triclinic, P 1̄ (no. 2), a = 7.4399(9) Å, b = 9.5362(11) Å, c = 13.1754(15) Å, α = 73.589(2)°, β = 84.396(2)°, γ = 74.709(2)°, V = 864.68(17) Å 3 , Z = 1, R gt ( F ) = 0.0306, wR ref ( F 2 ) = 0.1068, T = 298(2) K.
Open Access
Crystal structure of catena-poly[diaqua-(μ₂-1,2-bis(4-pyridinyl)ethyane-κ²N:N′)-(μ₂–pyridazine-4,5-dicarboxylato-κ²O:O′)]dizinc(II) dihydrate, C₁₂H₁₂ZnN₃O₆

February 21, 2019

Ju Feng-Yang, Ding Ke-Xin, Liu Fang

Page range: 567-569

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C 12 H 12 ZnN 3 O 6 , monoclinic, I 2/ a (no. 15), a = 17.6153(6) Å, b = 6.6922(2) Å, c = 24.1330(9) Å, β = 107.899(4)°, V = 2707.22(17) Å 3 , Z = 8, R gt ( F ) = 0.0262, wR ref ( F 2 ) = 0.0691, T = 293(2) K.
Open Access
The crystal structure of 2-(4-chloro-2,6-dinitrophenyl)-1-(4-chloro)diazene oxide, C₁₂H₆Cl₂N₄O₅

March 4, 2019

Junyan Cao, Jianlong Wang, Jun Chen, Xiyu Zhang, Zhiang Qin

Page range: 571-572

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C 12 H 6 Cl 2 N 4 O 5 , triclinic, P 1̄ (no. 2), a = 8.1022(14) Å, b = 9.6916(17) Å, c = 10.2476(17) Å, α = 78.346(4)°, β = 68.657(4)°, γ = 71.167(4)°, V = 706.1(2) Å 3 , Z = 2, R gt ( F ) = 0.0356, wR ref ( F 2 ) = 0.1109, T = 120 K.
Open Access
Crystal structure of 2-isopropylthioxanthone, C₁₆H₁₄OS

January 31, 2019

Jin-Qiang Liu, Li Ji, Weizhou Wang

Page range: 573-574

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C 16 H 14 OS, monoclinic, P 2 1 (no. 4), a = 8.1588(5) Å, b = 7.8670(4) Å, c = 10.2161(5) Å, V = 655.70(6) Å 3 , Z = 2, R gt ( F ) = 0.0539, wR ref ( F 2 ) = 0.1312, T = 290 K.
Open Access
Crystal structure of methyl 2-(4-(3-(1-methyl-1H-pyrazol-4-yl)pyrazolo[1,5-a]pyrimidin-6-yl)phenyl)acetate, C₁₉H₁₇N₅O₂

February 21, 2019

Bo Fang, Jiang Ping Meng, Lin Ling Gan

Page range: 575-577

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C 19 H 17 N 5 O 2 , monoclinic, C 2/ c (no. 15), a = 14.734(6) Å, b = 13.565(5) Å, c = 33.385(12) Å, β = 91.311(9)°, V = 6671(4) Å 3 , Z = 16, R gt ( F ) = 0.0638, wR ref ( F 2 ) = 0.1783, T = 293(2) K.
Open Access
Crystal structure of 4,4-dimethyl-2-(trifluoromethyl)-4,5-dihydro-1H-imidazole, C₆H₉F₃N₂

February 4, 2019

A. Musa Said, Ismail Warad, O. Seraj Alzahrani, Abdelkader Zarrouk, Dieter Lentz

Page range: 579-580

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C 6 H 9 F 3 N 2 , monoclinic, P 2 1 / n (no. 14), a = 10.6224(9) Å, b = 11.8639(9) Å, c = 13.3139(11) Å, β = 105.903(3)°, V = 1613.6(2) Å 3 , Z = 8, R gt ( F ) = 0.0618, wR ref ( F 2 ) = 0.1629, T = 102(2) K [1–3].
Open Access
Crystal structure of N-methylanilinium 5,7-dihydroxy-4-oxo-2-phenyl-4H-chromene-8-sulfonate monohydrate, C₂₂H₂₁NO₈S

February 5, 2019

Wu-Wu Li, Min-Yan Zheng, Guo Ying, Yan-Ping Jiang, Qiao Wang, Mei Wang, Min-Xiang Ji, Yu-Tao Zhang, Zun-Ting Zhang

Page range: 581-583

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C 22 H 21 NO 8 S, triclinic, P 1̄ (no. 2), a = 7.095(4) Å, b = 11.882(7) Å, c = 13.661(8) Å, α = 95.004(9)°, β = 104.918(9)°, γ = 107.323(9)°, V = 1045.4(11) Å 3 , Z = 2, R gt ( F ) = 0.0627, wR ref ( F 2 ) = 0.1745, T = 296(2) K.
Open Access
Crystal structure of methyl 4-acetoxybenzoate, C₁₀H₁₀O₄

March 4, 2019

Fang Li-Min, Huang Jian-Ping, Dai Jian-Cheng, Nie Xu-Liang, Liu Chang-Xiang, Kang Nian-Qian, Huang Lin

Page range: 585-586

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C 10 H 10 O 4 , monoclinic, C 2/ c (no. 15), a = 25.400(4) Å, b = 5.9738(10) Å, c = 12.746(2) Å, β = 94.318(2)°, V = 1928.5(6) Å 3 , Z = 8, R gt ( F ) = 0.0434, wR ref ( F 2 ) = 0.1276, T = 296(2) K.
Open Access
Crystal structure of catena-poly[(bis(μ-1,1′-[(5-methoxy-2,4,6-trimethyl-1,3-phenylene)bis(methylene)]bis(1H-1,2,4-triazole)-κ²N:N′)-bis(isothiocyanato-κN)manganese(II)], C₃₄H₄₀MnN₁₄O₂S₂

February 21, 2019

Mengyang Wang, Kaiqiang Yang, Yujiu Wang, Ying Ying

Page range: 587-588

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C 34 H 40 MnN 14 O 2 S 2 , triclinic, P 1̄ (no. 2), a = 9.1383(4) Å, b = 9.5039(6) Å, c = 10.5526(6) Å, α = 91.564(4)°, β = 94.624(5)°, γ = 91.737(4)°, V = 912.68(9) Å 3 , Z = 1, R gt ( F ) = 0.0374, wR ref ( F 2 ) = 0.0910, T = 125 K.
Open Access
Crystal structure of N-(2-methylphenyl)(propan-2-yloxy)carbothioamide, C₁₁H₁₅NOS

February 22, 2019

Chien Ing Yeo, Edward R.T. Tiekink

Page range: 589-591

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C 11 H 15 NOS, monoclinic, P 2 1 / n (no. 14), a = 7.3979(4) Å, b = 8.5384(4) Å, c = 18.2771(10) Å, β = 90.999(3)°, V = 1154.32(10) Å 3 , Z = 4, R gt ( F ) = 0.0409, wR ref ( F 2 ) = 0.1093, T = 100(2) K.

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