Zeitschrift für Kristallographie - New Crystal Structures

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Volume 238, Issue 6

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Zeitschrift für Kristallographie - New Crystal Structures

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Zeitschrift für Kristallographie - New Crystal Structures

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Frontmatter

November 17, 2023

Page range: i-vii

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New Crystal Structures
Open Access
Crystal structure of bis(dimethylammonium) poly[(μ₄-1,1′-(1,4-phenylenebis(methylene))bis(1H-pyrazole-3,5-dicarboxylato))-κ⁶O¹, N²:O²:O³:O¹′,N²′]nickel (II)], C₂₂H₂₆N₆NiO₈

September 15, 2023

Fenfang Li

Page range: 1027-1029

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C 22 H 26 N 6 NiO 8 , monoclinic, P 2 1 / n (no. 14), a = 10.9372(7) Å, b = 10.4567(6) Å, c = 11.7618(7) Å, β = 116.5552(19)°, V = 1203.25(13) Å 3 , Z = 2, R gt ( F ) = 0.0406, wR ref ( F 2 ) = 0.1089, T = 297(2) K.
Open Access
Hydrothermal synthesis and crystal structure of catena-poly[diaqua-bis(μ₂-4-((pyridin-4-ylmethyl)amino)benzoato-κ²N:O)cobalt(II)] – 4,4′-bipyridine – water (1/2/2)

September 7, 2023

Guang-Zhen Liu, Xin Wang

Page range: 1031-1033

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C 23 H 23 Co 0.5 N 4 O 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 9.6428(5) Å, b = 10.3191(5) Å, c = 11.8710(6) Å, α = 86.664 ( 4 ) ∘ $86.664{(4)}^{\circ }$ , β = 69.399 ( 5 ) ∘ $69.399{(5)}^{\circ }$ , γ = 79.429 ( 4 ) ∘ $79.429{(4)}^{\circ }$ , V = 1086.90(10) Å 3 , Z = 2, R g t ${R}_{\mathit{g}\mathit{t}}$ ( F ) = 0.0432, w R r e f $w{R}_{\mathit{r}\mathit{e}\mathit{f}}$ ( F 2 ) = 0.1454, T = 293(2) K.
Open Access
Crystal structure of (2S,3S,4S,5S, Z)-2,3,5,6-tetrakis(benzyloxy)-4-hydroxyhexanal oxime, C₃₄H₃₇NO₆

September 15, 2023

Nuo Zhang, Shuo-Nan Guo, Liang-Qi Du, Xiao-Yu Ren

Page range: 1035-1037

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C 34 H 37 NO 6 , triclinic, P 1̄ (no. 2), a = 6.398(6) Å, b = 10.779(10) Å, c = 12.030(11) Å, α = 71.103(10)°, β = 89.519(11)°, γ = 74.154(11)°, V = 752.2(12) Å 3 , Z = 1, R gt (F) = 0.0599, wR ref (F 2 ) = 0.1614, T = 296 K.
Open Access
The crystal structure of hexakis(3-thiophenecarboxylato-κ²O,O″)-bis(1,10-phenanthroline-κ²N,N′) trimanganese(II), C₅₄H₃₄N₄O₁₂S₆Mn₃

November 1, 2023

Lili Zhou, Zhongyu Zhang, Xiaoxia Men, Yaxuan Zhang

Page range: 1039-1041

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C 54 H 34 N 4 O 12 S 6 Mn 3 , monoclinic, P 2 1 / c (no. 14), a = 11.0140(4) Å, b = 22.3222(9) Å, c = 11.2886(5) Å, β = 105.436(1)°, Z = 2, V = 2675.27(19) Å 3 , R gt ( F ) = 0.0361, w R ref ( F 2 ) = 0.0846, T = 273 K.
Open Access
Crystal structure of catena-poly[(μ₂-1,4-di(pyridin-4-yl)benzene-κ²N:N′)-(4-bromobenzoate-κ²O:O′)-(μ-2-bromobenzoate-κ²O,O′)nickel(II)] – water (2/1), C₃₀H₂₁Br₂N₂NiO_4.5

September 11, 2023

Xiaobo Bao, Chongchong Tian

Page range: 1043-1045

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C 30 H 21 Br 2 N 2 NiO 4.5 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.7895(17) Å, b = 13.167(3) Å, c = 14.067(3) Å, α = 109.049(3)°, β = 92.619(3)°, γ = 108.533(3)°, V = 1438.6(5) Å 3 , Z = 2, R gt ( F ) = 0.0496, wR ref ( F 2 ) = 0.1003, T = 296(2) K.
Open Access
The crystal structure of poly[(μ₃-1,3-phenylenedioxydiacetate-κ⁵O,O,O′,O″,O‴)-bis(4′-(4-(1H-imidazol-1-yl)phenyl)-4,2′:6′,4″-terpyridine-kN) cadmium(II)], C₅₈H₄₂CdN₁₀O₆

September 5, 2023

Liqiong He, Liang Xiao, Weiwei Fu

Page range: 1047-1050

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C 58 H 42 CdN 10 O 6 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 9.689(3) Å, b = 10.930(3) Å, c = 23.321(6) Å, α = 80.838(5)°, β = 84.261(5)°, γ = 79.189(5)°, V = 2388.7(12) Å 3 , Z = 2, R gt ( F ) = 0.0592, w R ref ( F 2 ) = 0.1561, T = 293 K.
Open Access
The crystal structure of 5-chloro-6′-methyl-3-(4-(methylsulfonyl)phenyl)-[2,3′-bipyridin]-1′-ium 4-methylbenzenesulfonate

September 20, 2023

Yu Fang, Cheng Zhang, Meng-Qing Yin, Xiao-Die Yang, Wen-Jing Ma

Page range: 1051-1053

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C 18 H 16 ClN 2 O 2 S·C 7 H 7 O 3 S, monoclinic, C 2/ c (no. 15), a = 36.911(9) Å, b = 9.931(2) Å, c = 14.795(3) Å, β = 112.32(3)°, V = 5017(2) Å 3 , Z = 8, R gt ( F ) = 0.0500, wR ref ( F 2 ) = 0.1447, T = 293 K.
Open Access
Crystal structure of poly[(μ-benzoato)-(μ-cis-4–hydroxy-D-proline)lithium], C₁₂H₁₄LiNO₅

September 6, 2023

Dejing Yin, Lingling Wang, Zhenbo Yuan

Page range: 1055-1056

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(C 12 H 14 LiNO 5 ) n , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 5.1481(4) Å, b = 8.9342(7) Å, c = 25.733(2) Å, Z = 4, V = 1183.57(16) Å 3 , R gt ( F ) = 0.0539, wR ref ( F 2 ) = 0.1478, T = 100 K.
Open Access
The crystal structure of catena-poly[aqua-(4-iodopyridine-2,6-dicarboxylato-κ³N,O,O^′)-copper(II)] monohydrate, C₇H₆NO₆ICu

September 5, 2023

Yang Kong, ChenFei Lu, Chang-Zhao Wang, Bin Tian, YiXuan Dang, ZiHao Han

Page range: 1057-1059

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C 7 H 6 NO 6 ICu, monoclinic, P 2 1 / n (no. 14), a = 9.7229(4) Å, b = 5.1728(2) Å, c = 20.8336(8) Å, β = 97.636(4) ∘ , V = 1038.52(7) Å 3 , Z = 4, R gt ( F ) = 0.0287, wR ref ( F 2 ) = 0.0687, T = 293 K.
Open Access
The crystal structure of catena-[diaqua-(4-acetylphenoxyacetato-κ²O,O)-bis(4-acetylphenoxyacetato-κ³O,O:O)-dihydrate-lanthanum(III)]–4,4′-bipyridine (2/1), C₃₅H₃₅NO₁₄La

September 12, 2023

Liu Ying, Yan Xi-Hai, Wang Yuan-Fang, Tai Xi-Shi

Page range: 1061-1063

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C 35 H 35 NO 14 La, triclinic, P ‾ $\overline{P}$ 1 (no. 2), a = 9.06760(10) Å, b = 13.6139(2) Å, c = 15.5964(2) Å, α = 115.2310(10) ∘ , ß = 97.4010(10) ∘ , γ = 95.4830(10) ∘ , V = 1702.65(4) Å 3 , Z = 2, R gt ( F ) = 0.0431, wR ref ( F 2 ) = 0.1059, T = 296.13(10) K.
Open Access
The crystal structure of catena-poly[(4-iodopyridine-2,6-dicarboxylato-κ⁴ O,N,O′,O′′)(4-imidazol-1-yl-pyridine-κN)copper(II)], C₁₅H₉N₄O₄ICu

September 5, 2023

Yang Kong, YiXuan Dang, Bin Tian, Chang-Zhao Wang, ZiHao Han, ChenFei Lu

Page range: 1065-1067

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C 15 H 9 N 4 O 4 ICu, monoclinic, P 2 1 / c (no. 14), a = 13.6216(4) Å, b = 13.4754(4) Å, c = 8.5023(3) Å, β = 102.610(3)°, V = 1522.99(9) Å 3 , Z = 4, R gt ( F ) = 0.0297, w R ref ( F 2 ) = 0.0781, T = 293 K.
Open Access
Crystal structure of polybis(μ ₄-3,5-dicarboxylatopyrazol-1-yl)-bis(N,N-dimethylformamide)tri-copper(II)–acetonitrile (1/2), C₂₀H₂₂Cu₃N₈O₁₀

September 5, 2023

Yan-Qing Wang, Wen-Qing Yan, Li-Xue Nie, Ping-Ping Luan, Chao-Qun Li

Page range: 1069-1070

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C 20 H 22 Cu 3 N 8 O 10 , monoclinic, C 2/ c (no. 15), a = 12.0766(11) Å, b = 16.2778(14) Å, c = 14.7605(13) Å, β = 97.8580(10) ∘ , V = 2874.4(4) Å 3 , Z = 4, R gt ( F ) = 0.0420, wR ref ( F 2 ) = 0.0988, T = 298.15 K.
Open Access
Crystal structure of poly[(μ₂-5-hydroxy-isophthalato-κ⁴O,O′:O″,O‴)-(μ₂-1,5-bis(imidazol-2-methyl)pentane-κ²N:N′)cadmium(II)], C₂₁H₂₄CdN₄O₅

September 5, 2023

Jin Cai, Xin-Tong Yao, Man-Sheng Chen

Page range: 1071-1073

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C 21 H 24 CdN 4 O 5 , monoclinic, P 2 1 / n (no. 14), a = 9.5381(7) Å, b = 20.9393(14) Å, c = 11.4813(8) Å, β = 104.3660(10)°, V = 2221.4(3) Å 3 , Z = 4, R gt ( F ) = 0.0319, wR ref ( F 2 ) = 0.0873, T = 296(2) K.
Open Access
The crystal structure of poly[bis(μ₂-1,4-bi(1-imidazolyl)benzene-κ²N:N′)bis(μ₂-4,4′-methylenebis(3-hydroxy-2-naphthoate)-κ²O:O′)cobalt(II)], C₃₅H₂₄CoN₄O₆

September 4, 2023

Ji Qi, Shu-Ying Wang, Jin-Feng Chu

Page range: 1075-1077

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C 35 H 24 CoN 4 O 6 , monoclinic, P 2 1 / n (no. 14), a = 11.444(2) Å, b = 11.648(2) Å, c = 21.478(4) Å, β = 97.05(3)°, V = 2841.5(10) Å 3 , Z = 4, R gt ( F ) = 0.0849, wR ref ( F 2 ) = 0.1393, T = 153(2) K.
Open Access
The crystal structure of a cobalt-vanadium-oxido hydrate

September 18, 2023

Chen Wu-Hua, Chen Ran, Mi Jin-Xiao, Wang Hua-Feng, Song Jia-Yu

Page range: 1079-1080

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H 4 O 14 CoV 4.4 , monolinic, P 2/ m (no. 10), a = 8.1091(8) Å, b = 3.5128(2) Å, c = 9.7590(9) Å, β = 111.553(11)°, V = 258.55(4) Å 3 , Z = 1, R gt ( F ) = 0.0401, wR ref ( F 2 ) = 0.0922, T = 293(2) K.
Open Access
The crystal structure of catena-poly[(μ ₂-2H-1,2,3-triazole-4,5-dicarboxylato-κ ² O, O′)-(μ ₂-1,3-bis((1H-imidazol-1-yl)methyl)benzene-κ ² N,N′) zinc(II)], C₁₈H₁₅N₇O₄Zn

September 5, 2023

Qian Mao, Yanfei Wang, Zhonghua Zhang, Jinlan Ji

Page range: 1081-1083

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C 18 H 15 N 7 O 4 Zn, triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 9.1100(8) Å, b = 10.6451(7) Å, c = 12.0479(8) Å, α = 95.238(5) ∘ , β = 112.154(7) ∘ , γ = 112.971(7) ∘ , V = 956.56(13) Å 3 , Z = 2, R gt ( F ) = 0.0264, wR ref ( F 2 ) = 0.0731, T = 298 K.
Open Access
Crystal structure of poly[diaqua-(bis(m₂-1,4-bis(imidazol-1-ylmethyl)benzene)-κ²N,N′-manganese] dichloride, C₂₈H₃₂MnN₈O₂Cl₂

September 5, 2023

Si-Na Gu, Zhi-Ying Ou, Ting-Ting Wu, Ting-Yu Nie, Yang Liu

Page range: 1085-1087

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C 28 H 32 MnN 8 O 2 Cl 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.987(4) Å, b = 9.061(3) Å, c = 10.706(2) Å, α = 88.65(2)°, β = 66.12(2)°, γ = 89.89(2)°, V = 796.9(5) Å 3 , Z = 1, R gt ( F ) = 0.1033, w R ref ( F 2 ) = 0.2218, T = 293(2) K.
Open Access
The crystal structure of 9,10-dimethoxy-5,6-dihydro-[1,3]dioxolo[4,5-g]isoquinolino [3,2-a]isoquinolin-7-ium (E)-3-(4-nitrophenyl)acrylate pentahydrate, C₂₉H₃₄N₂O₁₃

September 6, 2023

Shi-Yun Chen, Wei Wang, Yong He, Deng-ke Yin

Page range: 1089-1091

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C 29 H 34 N 2 O 13 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 8.1996(2) Å, b = 13.1993(3) Å, c = 13.5119(3) Å, α = 94.208(1) ∘ , β = 99.787(1) ∘ , γ = 90.247(1) ∘ , V = 1437.00(6) Å 3 , Z = 2, R gt ( F ) = 0.0457, wR ref ( F 2 ) = 0.1218, T = 193 K.
Open Access
Crystal structure of poly[(μ₆-ammoniotris(methylene))tris(hydrogen phosphonato)cadmium(II)], C₃H₁₀CdNO₉P₃

September 26, 2023

Si N. Gu, Zhi Y. Ou, Ting T. Wu, Ting Y. Nie, Yang Liu

Page range: 1093-1095

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C 3 H 10 CdNO 9 P 3 , monoclinic, P 2 1 / c (no. 14), a = 9.1770(5) Å, b = 8.3742(4) Å, c = 15.4660(6) Å, β = 119.657(2)°, V = 1032.86(9) Å 3 , Z = 4, R gt ( F ) = 0.0202, w R ref ( F 2 ) = 0.0515, T = 296 K.
Open Access
Crystal structure of Zn₂[(1,1′-(hexane-1,6-diyl)bis(3-(pyridin-3-yl)urea))·(H₂O)₂·(DMF)₂·(SO₄)₂], C₂₄H₅₀N₈O₁₈S₂Zn₂

November 2, 2023

Wen-Ze Zhao, Hua Tian

Page range: 1097-1099

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C 24 H 50 N 8 O 18 S 2 Zn 2 , triclinic, P 1̄ (no. 2), a = 7.9797(5) Å, b = 10.4923(6) Å, c = 11.4835(7) Å, α = 97.512(2)°, β = 100.089(2)°, γ = 94.156(2)°, V = 933.98(10) Å 3 , Z = 1, R gt ( F ) = 0.0382, wR ref ( F 2 ) = 0.1202, T = 293(2) K.
Open Access
The crystal structure of 2-anilino-1,4-naphthoquinone, C₁₀H₁₁NO₂

September 4, 2023

Mohammed A. Elmakki, Thato N. Taoana, Frederick J. F. Jacobs, Johan A. Venter

Page range: 1101-1102

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C 10 H 11 NO 2 , monoclinic, P 2 1 / n (no. 14), a = 3.7617(3) Å, b = 12.9267(10) Å, c = 23.4609(17) Å, β = 92.337(3)°, V = 1139.87(15) Å 3 , Z = 4, R gt ( F ) = 0.0413, wR ref ( F 2 ) = 0.1071, T = 100 K.
Open Access
Crystal structure of (E)-2-(2-(4-(diethylamino)styryl)-1-ethyl-1,4-dihydroquinolin-4-yl) malononitrile, C₂₆H₂₆N₄

September 5, 2023

Cheng-Tao Sun, Qin Li

Page range: 1103-1104

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C 26 H 26 N 4 , monoclinic, P 2 1 / c (no. 14), a = 16.565(2) Å, b = 17.468(2) Å, c = 7.5778(10) Å, β = 94.551(4)°, V = 2185.8(5) Å 3 , Z = 4, R gt ( F ) = 0.0591, wR ref ( F 2 ) = 0.1830, T = 300(2) K.
Open Access
Crystal structure of ethyl 2-((2,6-dichloro-4-(cyanomethyl)phenyl) amino)benzoate, C₁₇H₁₄Cl₂N₂O₂

October 10, 2023

Meimei Zhao, Mo Du, Bin Liu

Page range: 1105-1106

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C 17 H 14 Cl 2 N 2 O 2 , monoclinic, P 2 1 / n (no. 14), a = 8.4863(17) Å, b = 12.654(2) Å, c = 15.088(3) Å, β = 103.612(5)°, V = 1574.8(5) Å 3 , Z = 4, R gt ( F ) = 0.0423, wR ref ( F 2 ) = 0.1472, T = 205 K.
Open Access
Synthesis and crystal structure of 2-(3-oxo-3-phenylpropyl)isoindoline-1,3-dione, C₁₇H₁₃NO₃

September 5, 2023

Ju-Mei Shi, Yong-Jia Hao, Lian-Hua Xu, Ying Zhou, Hua-Bin Wang

Page range: 1107-1108

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C 17 H 13 NO 3 , monoclinic, P 2 1 / c (no. 14), a = 9.5306(2) Å, b = 6.1971(2) Å, c = 23.3849(7) Å, β = 101.445(3)°, V = 1353.70(7) Å 3 , Z = 4, R gt ( F ) = 0.0644, wR ref ( F 2 ) = 0.1909, T = 120 K.
Open Access
The crystal structure of bis(acetonitrile-κ¹N)tetrakis(μ₂-2,6-difluorobenzoato-κ²O:O′)rhodium(II) (Rh–Rh), C₃₂H₁₈F₈O₈N₂Rh₂

September 15, 2023

Zihao Zhong, Miao Meng

Page range: 1109-1111

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C 32 H 18 F 8 O 8 N 2 Rh 2 , monoclinic, P 2 1 / n (no. 11), a = 9.28200(12) Å, b = 11.33638(13) Å, c = 16.0352(2) Å, β = 105.9326(14)° V = 1622.47 Å 3 , Z = 4, R gt ( F ) = 0.0297, wR ref ( F 2 ) = 0.0763, T = 150 K.
Open Access
The crystal structure of a new polymorph of 6-hydroxy-2-naphthoic acid, C₁₁H₈O₃

September 5, 2023

Mark G. Smith

Page range: 1113-1114

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C 11 H 8 O 3 , monoclinic, P 2 1 / c (no. 14), a = 8.6478(8) Å, b = 5.2261(5) Å, c = 18.7921(18) Å, β = 94.518(3) ∘ , V = 846.66(14) Å 3 , Z = 4, R gt ( F ) = 0.0419, wR ref ( F 2 ) = 0.1181, T = 173 K.
Open Access
The crystal structure of [(8-carboxymethoxy-quinoline-2-carboxylate-κ⁴N,O,O,O)-2,2′-bipyridine-κ²N-copper(II)] tetrahydrate, C₂₂H₂₃N₃O₉Cu

November 1, 2023

Zhao Zeng-Bing, Yang Shu-Cheng, Yang Bing-Qi, Cheng Lan-Xing, Tai Xi-Shi

Page range: 1115-1117

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C 22 H 23 N 3 O 9 Cu, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 9.0356(2) Å, b = 9.6247(3) Å, c = 14.2969(3) Å, α = 86.989(2)°, β = 86.414(2)°, γ = 66.913(2)°, V = 1140.98(5) Å 3 , Z = 2, R gt ( F ) = 0.0405, wR ref ( F 2 ) = 0.1172, T = 297.88(10) K.
Open Access
The crystal structure of ethyl 4-hydroxy-2-(4-methoxyphenyl)-5-oxo-1-(2-oxo-2H-chromen-6-yl)-2,5-dihydro-1H-pyrrole-3-carboxylate, C₂₃H₁₉NO₇

September 22, 2023

Bimal Bhushan Chakraborty, Saurav Paul, Siddique Anwar, Sudip Choudhury

Page range: 1119-1121

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C 23 H 19 NO 7 , monoclinic, P 2 1 / n (no. 14), a = 17.9964(9) Å, b = 5.9211 Å, c = 18.8608(10) Å, β = 98.201(3)°, V = 1989.23(18) Å 3 , Z = 4, R gt ( F ) = 0.0496, wR ref ( F 2 ) = 0.1561, T = 296 K.
Open Access
Crystal structure of 7-hydroxy-3,4-dihydronaphthalen-1(2H)-one, C₁₀H₁₀O₂

September 5, 2023

Boye Jiang, Yun Hou, Feng-Lan Zhao, Qing-Guo Meng

Page range: 1123-1125

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C 10 H 10 O 2 , monoclinic, C 2/ c (no. 15), a = 16.6341(14) Å, b = 7.4319(4) Å, c = 14.8943(10) Å, β = 123.243(8)°, V = 1540.0(2) Å 3 , Z = 8, R gt ( F ) = 0.0371, wR ref ( F 2 ) = 0.0997, T = 293 K.
Open Access
Crystal structure of bis(tetrapropylammonium) dodecacarbonyltetratelluridotetraferrate(2-), (Pr₄N)₂[Fe₄Te₄(CO)₁₂]

September 5, 2023

Kang-Woo Kim, Hyoyi Yang

Page range: 1127-1129

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C 36 H 56 O 12 N 2 Fe 4 Te 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 11.3615(9) Å, b = 11.8540(9) Å, c = 12.1267(9) Å, α = 61.419(2)°, β = 64.289(3)°, γ = 71.088(3)°, V = 1278.10(17) Å 3 , Z = 1, R gt ( F ) = 0.0213, wR ref ( F 2 ) = 0.0638, T = 223(2) K.
Open Access
The crystal structure of poly[bis(μ₂−3−aminopyridine−4−carboxylato−κ²N:O)Zinc(II)], [Zn(C₆H₅N₂O₂)₂]_n

September 19, 2023

Fang-Fang Liu, Zhao-Yan Ping, Wei-Wei Zhou, Wang Zhao

Page range: 1131-1132

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[Zn ( C 6 H 5 N 2 O 2 ) 2 ${({\mathrm{C}}_{6}{\mathrm{H}}_{5}{\mathrm{N}}_{2}{\mathrm{O}}_{2})}_{2}$ ] n , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 7.6139(7) Å, b = 12.4890(13) Å, c = 13.9382(13) Å, V = 1325.4(2) Å 3 , Z = 4, R gt ( F ) = 0.0391, wR ref ( F 2 ) = 0.0710, T = 296 K.
Open Access
The crystal structure of methyl 5-nitro-2-(tosyloxy)benzoate, C₁₅H₁₃NO₇S

September 14, 2023

Shao-Wen Deng, Lin Yuan, Zhong-Yan Li

Page range: 1133-1134

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C 15 H 13 NO 7 S, triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 6.5990(11) Å, b = 7.7259(13) Å, c = 16.428(3) Å, α = 79.1416(18)°, β = 79.4782(16)°, γ = 81.1835(18)°, V = 802.6(2) Å 3 , Z = 2, R gt ( F ) = 0.0340, wR ref ( F 2 ) = 0.0960, T = 296(2) K.
Open Access
The crystal structure of 18-crown-6 ― tetraaqua-dichlorido-di-μ₂-chloridodicopper(II) (2/1), C₁₂H₃₂O₁₀Cu₂Cl₄

September 22, 2023

Zhaolong Liu, Shifeng Jin

Page range: 1135-1136

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C 12 H 32 O 10 Cu 2 Cl 4 , monoclinic, P 2 1 / n (no. 14), a = 9.0202(4) Å, b = 9.5791(4) Å, c = 13.6994(6) Å, β = 92.555(1) ° , V = 1182.53(9) Å 3 , Z = 2, R gt ( F ) = 0.0308, wR ref ( F 2 ) = 0.0800, T = 293(2) K.
Open Access
Crystal structure of 6,6a,7,8,9,10-hexahydro-5H-pyrazino [2,3-e]pyrido[1,2-a]pyrazine, C₁₀H₁₄N₄

September 5, 2023

Zhu Dali, Yu Yu

Page range: 1137-1139

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C 10 H 14 N 4 , orthorhombic, Pbca (no. 61), a = 15.5356(2) Å, b = 9.8551(2) Å, c = 25.5551(4) Å, V = 3912.61(11) Å 3 , Z = 16, R gt ( F ) = 0.0873, wR ref ( F 2 ) = 0.2481, T = 150 K.
Open Access
Crystal structure of catena-poly-{diaqua-bis[μ-(((4-chlorophenyl)sulfonyl)glycinato-κO)](μ₂-4, 4′-bipyridine-κ²N:N′)cobalt(II)} dihydrate, C₂₆H₃₀Cl₂CoN₄O₁₂S₂

September 8, 2023

Xiao-Miao Chen, Zheng-Jun Liu, Qing Liu, Yu-Tao Zhang, Xue He, Yun Deng

Page range: 1141-1143

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C 26 H 30 Cl 2 CoN 4 O 12 S 2 , monoclinic, P 2 1 / c (no. 14), a = 11.4094(5) Å, b = 14.2343(6) Å, c = 11.6775(4) Å, β = 114.3130(10) ∘ , V = 1728.28(12) Å 3 , Z = 2, R gt ( F ) = 0.0393, wR ref ( F 2 ) = 0.1046, T = 293(2) K.
Open Access
Crystal structure of bis{N′-[1,3-diphenylprop-2-en-1-ylidene]-N-phenylcarbamohydrazonothioato}zinc(II), C₄₄H₃₆N₆S₂Zn

October 10, 2023

Ming Yueh Tan, Karen A. Crouse, Sang Loon Tan, Edward R. T. Tiekink

Page range: 1145-1148

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C 44 H 36 N 6 S 2 Zn, monoclinic, P 2 1 / c (no. 14), a = 14.5676(4) Å, b = 26.1767(8) Å, c = 10.0963(3) Å, β = 99.140(3)°, V = 3801.2(2) Å 3 , Z = 4, R gt ( F ) = 0.0397, wR ref ( F 2 ) = 0.1000, T = 100 K.
Open Access
Crystal structure of tetraaqua-bis(((4-chlorophenyl)sulfonyl)glycinato-κO)cobalt(II) dihydrate, C₁₆H₂₆Cl₂CoN₂O₁₄S₂

September 8, 2023

Zheng-Jun Liu, Xiao-Miao Chen, Qiang Wu, Yu-Tao Zhang, Wu-Chao Zhou, Li Wei, Ying-Xian Zhao

Page range: 1149-1151

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C 16 H 26 Cl 2 CoN 2 O 14 S 2 , monoclinic, P 2 1 / n (no. 14), a = 5.3261(4) Å, b = 39.755(2) Å, c = 6.2518(4) Å, β = 96.880(6) ∘ , V = 1314.21(15) Å 3 , Z = 2, R gt ( F ) = 0.0487, wR ref ( F 2 ) = 0.1040, T = 153(2) K.
Open Access
Crystal structure of 2-(5-phenyl-1-(quinolin-2-yl)-4,5-dihydro-1H-pyrazol-3-yl)phenol, C₂₄H₁₉N₃O

September 15, 2023

Dai Zeng, Kai Tan, Ziyan Fang, Aiping Xing

Page range: 1153-1155

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C 24 H 19 N 3 O, monoclinic, P 2 1 / c (no. 14), a = 10.4783(5) Å, b = 11.7171(5) Å, c = 14.9194(6) Å, β = 93.991(2)°, Z = 4, V = 1827.29(14) Å 3 , R gt ( F ) = 0.0521, wR ref ( F 2 ) = 0.1508, T = 150(2) K.
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Crystal structure of 2-((2-fluoro-4-(trifluoromethyl)phenyl)(hydroxy)methyl)-7-methoxy-3,4-dihydronaphthalen-1((2H))-one, C₁₉H₁₆F₄O₃

October 10, 2023

Yu-Lun Li, Qing-Guo Meng, Gui-Ge Hou, Zi-Kai Geng

Page range: 1157-1159

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C 19 H 16 F 4 O 3 , monoclinic, P 2 1 / n (no. 14), a = 9.5792(5) Å, b = 9.5542(4) Å, c = 17.6986(9) Å, β = 99.508(5) ∘ , V = 1597.55(14) Å 3 , Z = 4, R gt ( F ) = 0.0481, wR ref ( F 2 ) = 0.1153, T = 293 K.
Open Access
Crystal structure of 2-amino-4-(2-fluoro-3-(trifluoromethyl)phenyl)-9-methoxy-1,4,5,6-tetrahydrobenzo[h]quinazolin-3-ium chloride, C₂₀H₁₈ClF₄N₃O

October 11, 2023

Lu Yu, Qing-Guo Meng, Gui-Ge Hou, Yong-Jun Liu, Zi-Kai Geng

Page range: 1161-1163

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C 20 H 18 ClF 4 N 3 O, orthorhombic, Pbca (no. 61), a = 12.5254(4) Å, b = 12.6845(5) Å, c = 24.1490(11) Å, V = 3836.8(3) Å 3 , Z = 8, R gt ( F ) = 0.0485, wR ref ( F 2 ) = 0.1343, T = 293 K.
Open Access
Crystal structure of (2-phenylimino methylquinoline-κ ² N,N′)-bis(1–phenylpyrazole-κ ² C,N)-iridium(III) hexafluorophosphate, C₃₄H₂₆F₆IrN₆P

September 18, 2023

Jun Qian, Chunjie Chen, Liang Ma, Yida Wang

Page range: 1165-1167

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C 34 H 26 F 6 IrN 6 P, monoclinic, P 2 1 / c (no. 4), a = 11.929(2) Å, b = 12.653(3) Å, c = 21.707(4) Å, β = 105.48(3) ∘ , V = 3157.5(12) Å 3 , Z = 4, R gt ( F ) = 0.0241, w R ref ( F 2 ) = 0.0461, T = 293 K.
Open Access
Crystal structure of (3-hydroxy-4-methoxyphenyl)(pyrrolidin-1-yl)methanone, C₁₂H₁₅NO₃

October 10, 2023

Xiaona Xu, Hongjuan Tong, Zhoujing Zhu, Bin Liu

Page range: 1169-1170

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C 12 H 15 NO 3 , monoclinic, P 2 1 / c (no. 14), a = 6.7230(2) Å, b = 11.1182(3) Å, c = 14.4996(5) Å, β = 94.8870 ( 10 ) ° $94.8870(10){}^{\circ}$ , V = 1079.87(6) Å 3 , Z = 4, R gt ( F ) = 0.0511, wR ref ( F 2 ${F}^{2}$ ) = 0.1525, T = 170 K.
Open Access
The crystal structure of bis(trimethylsulfoxonium) catena-poly[µ₂-hexabromido-indium(III)sodium(I)] C₆H₁₈O₂S₂NaInBr₆

October 10, 2023

Shifeng Jin, Jiali Lu

Page range: 1171-1173

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C 6 H 18 O 2 S 2 NaInBr 6 , orthorhombic, Pmn 2 1 (no. 31), a = 10.5451(3) Å, b = 7.1169(2) Å, c = 13.7034(4) Å, V = 1028.42(5) Å 3 , Z = 2, R gt ( F ) = 0.0354, wR ref ( F 2 ) = 0.0923, T = 293 K.
Open Access
Crystal structure of N-cyclopropyl-3-hydroxy-4-methoxybenzamide, C₁₁H₁₃NO₃

September 21, 2023

Hongjuan Tong, Xiaona Xu, Zhoujing Zhu, Bin Liu

Page range: 1175-1176

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C 11 H 13 NO 3 , monoclinic, P 2 1 / n (no. 14), a = 8.0478(3) Å, b = 9.8093(4) Å, c = 13.1602(5) Å, β = 104.712(2)°, V = 1004.85(7) Å 3 , Z = 1, R gt ( F ) = 0.0395, wR ref ( F 2 ) = 0.1010, T = 170 K.
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The crystal structure of (bis(benzimidazol-2-yl-methyl)amine-κ³N,N^′,N^″ )-(dihydrogen L-malate-κ²O,O ^′)copper(II) perchlorate dihydrate, CuC₂₀H₂₄ClN₅O₁₂

October 10, 2023

Yu Yang, Huanru Liu, Yuhang Wang, Xianggao Meng

Page range: 1177-1179

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CuC 20 H 24 ClN 5 O 12 , monoclinic, P 1 ‾ $\overline{1}$ (no. 4), a = 7.4467(4) Å, b = 17.3823(9) Å, c = 9.6974(5) Å, α = 90°, β = 103.373(2)°, γ = 90°, V = 1221.20(11) Å 3 , Z = 2, R gt ( F ) = 0.0642, wR ref ( F 2 ) = 0.1757, T = 100(2) K.
Open Access
Crystal structure of (1E,1′E)-4,4′-(9,9-diethyl-9H-fluorene-2,7-diyl)dibenzaldehyde dioxime, C₃₁H₂₈N₂O₂

October 10, 2023

Ying-Hong Ma, Hong-Yan Zhao, Yu Tian, Yi Wu, Lei Wang

Page range: 1181-1183

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C 31 H 28 N 2 O 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 9.0809(9) Å, b = 9.2626(9) Å, c = 14.8540(15) Å, α = 93.574(8)°, β = 98.554(8)°, γ = 99.558(8)°, V = 99.558(8) Å 3 , Z = 2, R gt ( F ) = 0.0541, wR ref ( F 2 ) = 0.1424, T = 293(2) K.
Open Access
Crystal structure of diethyl 1,9-bis(4-fluorophenyl)-4,6-diphenylhexahydro-3H-2,7,3,5-(epimethanetriyliminomethanetriyl)cyclopenta [b]pyridine-3,7(2H)-dicarboxylate, C₄₀H₃₆F₂N₂O₄

October 11, 2023

Zi-Ang Zhang, Jun-Xiang Li, Sen-Bao Lu, Peng Li

Page range: 1185-1187

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C 40 H 36 F 2 N 2 O 4 , monoclinic, P 2 1 / c (no. 14), a = 9.8180(16) Å, b = 19.355(3) Å, c = 17.930(3) Å, β = 102.353(3)°, V = 3328.3(9) Å 3 , Z = 4, R gt ( F ) = 0.0564, wR ref ( F 2 ) = 0.1866, T = 296(2) K.
Open Access
Crystal structure of bis(benzene-1 carboxylato-O 3,5-carboxyl-κ¹O)-[(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ⁴N,N′,N′′,N′′′)nickel(II) ─ benzene-1,3,5-tricarboxylic acid ─ water (1/2/4), C₅₂H₆₆N₄NiO₂₈

November 1, 2023

Xiao-Ming Chen, Guang-Chuan Ou

Page range: 1189-1191

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C 52 H 66 N 4 NiO 28 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 11.292(6) Å, b = 11.670(6) Å, c = 12.165(6) Å, α = 81.872(6)°, β = 67.036(5)°, γ = 75.624(6)°, V = 1428.1(12) Å 3 , Z = 1, R gt ( F ) = 0.0439, wR ref ( F 2 ) = 0.1216, T = 296(2) K.
Open Access
Crystal structure of 1,4-dibromo-2,5-bis(2-methoxyethoxy)benzene-1,4-diol, C₁₂H₁₆Br₂O₄

October 10, 2023

Zhi-Yong Wang, Wan-Li Lu, Xu Zhou, Xian-Jiong Yang, Qi-Long Zhang, Hong Xu

Page range: 1193-1194

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C 12 H 16 Br 2 O 4 , monoclinic, P 2 1 / n (no. 14), a = 12.594(5) Å, b = 4.4613(16) Å, c = 12.878(4) Å, β = 91.209(12) ∘ , V = 723.4(4) Å 3 , Z = 2, R gt ( F ) = 0.0450, wR ref ( F 2 ) = 0.1103, T = 293 (2) K.
Open Access
Crystal structure of dicarbonyl[N,N′-(1,2-dimethyl-1,2-ethanediylidene)bis[2,6-bis(1-methylethyl)benzenamine]-N,N′]nickel(0), C₃₀H₄₀N₂NiO₂

November 3, 2023

Lingyi Shen, Na Xu, Mengna Jiang, Jiang Zhao, Xiaoling Xu, Xian-Jiong Yang, Qi-Long Zhang

Page range: 1195-1197

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C 30 H 40 N 2 NiO 2 , orthorhombic, Pnma (no. 62), a = 12.8114(19) Å, b = 21.301(3) Å, c = 10.6536(16) Å, V = 2907.3(8) Å 3 , Z = 4, R gt ( F ) = 0.0290, wR ref ( F 2 ) = 0.0808, T = 273(2) K.
Open Access
Crystal structure of 1,4-dibromo-2,5-bis(prop-2-yn-1-yloxy)benzene, C₁₂H₈Br₂O₂

October 23, 2023

Zhi-Yong Wang, Qi-Long Zhang, Xiu-Ming Zhang, Xu Zhou, Xian-Jiong Yang, Hong Xu

Page range: 1199-1200

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C 12 H 8 Br 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 4.1957(13) Å, b = 13.402(4) Å, c = 11.160(3) Å, β = 99.645(10)°, V = 618.7(3) Å 3 , Z = 2, R gt ( F ) = 0.0287, wR ref ( F 2 ) = 0.0701, T = 273(2) K.
Open Access
Crystal structure of O-(3-(benzo[d]thiazol-2-yl)naphthalen-2-yl) O-phenyl carbonothioate, C₂₄H₁₅NO₂S₂

October 31, 2023

Qian Wang, Yong-Lang Liu, Jiang-Hai Ye, Juan Zou, Chong Wu, Wu-De Yang

Page range: 1201-1203

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C 24 H 15 NO 2 S 2 , monoclinic, P 2 1 / c (no. 14), a = 20.8250(11) Å, b = 5.3649(3) Å, c = 18.8787(11) Å, β = 106.278(2)°, V = 2024.7(2) Å 3 , Z = 4, R gt ( F ) = 0.0439, wR ref ( F 2 ) = 0.1015, T = 273 K.
Open Access
The crystal structure of (E)-4-fluoro-N′-(1-(4-hydroxyphenyl)propylidene)benzohydrazide, C₁₆H₁₅FN₂O₂

October 23, 2023

Juanjuan Wen, Langlang Liu, Wenqiang Tang, Bin Liu

Page range: 1205-1207

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C 16 H 15 FN 2 O 2 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 7.2516(6) Å, b = 11.3780(9) Å, c = 17.1177(13) Å, V = 1412.36(19) Å 3 , Z = 4, R gt (F) = 0.0498, wR ref ( F 2 ) = 0.1201, T = 293 K.
Open Access
Crystal structure of (E)-1-(benzo[d]thiazol-2-yl)-N-(4,5-dihydropyren-2-yl)methanimine, C₂₄H₁₆N₂S

October 31, 2023

Lingyi Shen, Qianjin Gong, Na Xu, Xiaoling Xu, Mengna Jiang, Jiang Zhao, Ya-Li Huang, Zhi-Yong Wang, Qi-Long Zhang

Page range: 1209-1210

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C 24 H 16 N 2 S, monoclinic, P 2 1 /n (no. 14), a = 18.443(2) Å, b = 4.0161(6) Å, c = 23.396(4) Å, β = 99.246(6)°, V = 1710.4(4) Å 3 , Z = 4, R gt ( F ) = 0.0589, wR ref ( F 2 ) = 0.1173, T = 273.15 K.
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Crystal structure of 3-((4-bromophenyl)thio)-1H-indole, C₁₄H₁₀BrNS

November 2, 2023

Ning Wang, Ya-Fei Guo, Jun-Ying Ma, Ming-Ming Liu, Yu-Long Qu

Page range: 1211-1213

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C 14 H 10 BrNS, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 5.6392(2) Å, b = 7.7930(3) Å, c = 28.2476(8) Å, V = 1241.37(8) Å 3 , Z = 4, R gt ( F ) = 0.0414, wR ref ( F 2 ) = 0.1079, T = 293 K.
Open Access
Synthesis and crystal structure of 1-((7-hydroxy-3-(4-hydroxy-3-nitrophenyl)-4-oxo-4H-chromen-8-yl)methyl)piperidin-1-ium-4-carboxylate monohydrate, C₂₂H₂₂N₂O₉

November 1, 2023

Hai-Lin Chen, Xian Li, Dong-Mei Yao, Ze-Ping Luo, Yan-Ping Wang, Jian-Jing Lan

Page range: 1215-1217

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C 22 H 22 N 2 O 9 , monoclinic, P 2 1 / c (no. 14), a = 7.7374(3) Å, b = 29.1082(11) Å, c = 8.7595(3) Å, β = 96.853 ( 3 ) ∘ $96.853{(3)}^{\circ }$ , V = 1958.74(13) Å 3 , Z = 4, R gt ( F ) = 0.0520, wR ref ( F 2 ) = 0.1501, T = 100 K.
Open Access
Synthesis and crystal structure of (3E,5S,10S,13S,14S,17Z)-17-ethylidene-10,13-dimethylhexadecahydro-3H-cyclopenta[α]phenanthren-3-one O-(methacryloyl) oxime, C₅₀H₇₄N₂O₄

October 23, 2023

Peng Wei, Jin-Feng Zhao, Juan Zou, Jiang-Hai Ye, Kang He, Hong Xu

Page range: 1219-1222

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C 50 H 74 N 2 O 4 , orthorhombic, P 1 (no. 1), a = 7.3320(3) Å, b = 11.8132(4) Å, c = 13.1604(5) Å, α = 99.1910(10)°, β = 95.039(1)°, γ = 95.8560(10)°, V = 1113.06(7) Å 3 , Z = 1, R gt ( F ) = 0.0662, wR ref ( F 2 ) = 0.1655, T = 273(2) K.
Open Access
Crystal structure of the hydrogen storage active phase La₁₂Mg₄₆LiMn

November 1, 2023

Nazar Pavlyuk, Vitalii Nytka, Vasyl Kordan, Volodymyr Pavlyuk

Page range: 1223-1225

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La 12 Mg 46 LiMn, cubic, F m 3 ‾ m $Fm\overline{3}m$ (no 225), a = 14.7119(3) Å, V = 3184.24(19) Å 3 , Z = 2, R gt ( F ) = 0.0330, wR ref ( F 2 ) = 0.0601, T = 293(2) K.
Open Access
The crystal structure of the salt: 4-((1,3-dioxoisoindolin-2-yl)carbamoyl)pyridine-1-ium 2-carboxybenzoate, C₁₄H₁₀N₃O₃·C₈H₅O₄

November 1, 2023

Mark G. Smith

Page range: 1227-1228

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C 14 H 10 N 3 O 3 ·C 8 H 5 O 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.1312(3) Å, b = 10.5732(4) Å, c = 12.0961(4) Å, α = 110.933 ( 2 ) ∘ $110.933{(2)}^{\circ }$ , β = 101.603 ( 2 ) ∘ $101.603{(2)}^{\circ }$ , γ = 91.295 ( 2 ) ∘ $91.295{(2)}^{\circ }$ , V = 946.37(6) Å 3 , Z = 2, R g t ${R}_{gt}$ ( F ) = 0.0493, w R r e f $w{R}_{ref}$ ( F 2 ) = 0.1369, T = 173 K.
Open Access
Crystal structure of (2-(2-pyridine)-benzimidazole-κ² N,N′)-bis(1-phenylpyrazole-κ² C,N)iridium(III) hexafluorophosphate, C₃₀H₂₂F₆IrN₇P

November 1, 2023

Jun Qian, Chunjie Chen, Liang Ma, Yida Wang

Page range: 1229-1231

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C 30 H 22 F 6 IrN 7 P, monoclinic, P 2 1 / c (no. 4), a = 8.8876(3) Å, b = 32.8428(9) Å, c = 10.5010(3) Å, β = 106.623(2) ∘ , V = 2937.07(16) Å 3 , Z = 4, R gt ( F ) = 0.0572, wR ref ( F 2 ) = 0.1171, T = 293 K.
Open Access
Crystal structure of dichlorido-bis[2-(2,4-difluorophenyl)pyridine-κ¹N]platinum(II), C₂₂H₁₄Cl₂F₄N₂Pt

November 1, 2023

Chen-En-Ze Cheng, Jian-Guo Zhang, Wei Tan, Hao Zou

Page range: 1233-1235

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C 22 H 14 Cl 2 F 4 N 2 Pt, monoclinic, P 2 1 / n (no. 14), a = 16.858(9) Å, b = 14.876(8) Å, c = 17.125(9) Å, β = 98.552(6)°, V = 4247(4) Å 3 , Z = 8, R gt ( F ) = 0.0337, wR ref ( F 2 ) = 0.0778, T = 296 K.
Open Access
Crystal structure of (5R,8R,9R,10R,12R,13R,14R, 17S,17Z)-2-((3-fluoropyridin-4-yl)methylene)-12-hydroxy-4,4,8,10,14-pentamethyl-17-((R)-2,6,6-trimethyltetrahydro-2H-pyran-2-yl)hexadecahydro-3H-cyclopenta[a]phenanthren-3-one, C₃₆H₅₂FNO₃

November 2, 2023

Zi-Yu Liu, Wen-Shui Wang, Sheng Jiang, Feng-Lan Zhao, Qing-Guo Meng

Page range: 1237-1239

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C 36 H 52 FNO 3 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 7.8101(5) Å, b = 13.1592(7) Å, c = 30.5721(15) Å, V = 3142.0(3) Å 3 , Z = 4, R gt ( F ) = 0.0488, w R ref ( F 2 ) = 0.1048, T = 293 K.

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