Volume 234, Issue 5

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Zeitschrift für Kristallographie - New Crystal Structures

Contents

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Frontmatter

September 12, 2019

Page range: i-viii

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Open Access
Crystal structure of poly[diaqua-(μ₈-1,1′:2′,1′′-terphenyl-3,3′′,4′,5′-tetracarboxylato-κ⁸O¹:O₂:O³:O⁴:O⁵:O⁶:O⁷:O⁸)dicopper(II)], C₂₂H₁₄Cu₂O₁₀

June 14, 2019

Wenjun Li, Si Lang Jiu Mai

Page range: 849-850

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C 22 H 14 Cu 2 O 10 , orthorhombic, Pccn (no. 56), a = 8.7989(3) Å, b = 10.4284(3) Å, c = 23.6873(6) Å, V = 2173.51(11) Å 3 , Z = 8, R gt ( F ) = 0.0398, wR ref ( F 2 ) = 0.0969, T = 293(2) K.
Open Access
Crystal structure of 2-((1H-benzo[d]imidazol-2-ylimino)methyl)-4,6-di-tert-butylphenol, C₂₂H₂₇N₃O

May 27, 2019

Ai-Ping Xing, Dai Zeng, Shu-Ling Zhang, Jun-Jun Wei, Da-Feng Guo

Page range: 851-853

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C 22 H 27 N 3 O, monoclinic, P 2 1 / c (no. 14), a = 18.4984(4) Å, b = 11.4221(3) Å, c = 9.79600(19) Å, β = 90.9652(19)°, V = 2069.51(8) Å 3 , Z = 4, R gt ( F ) = 0.0605, wR ref ( F 2 ) = 0.1773, T = 293(2) K.
Open Access
Crystal structure of (4-ethoxynaphthalen-1-yl)(furan-2-yl)methanone, C₁₇H₁₄O₃

June 21, 2019

Ming-Qiang Li, Peng Wang, Kui Wang, Fei Ye, Ying Fu

Page range: 855-856

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C 17 H 14 O 3 , monoclinic, C 2/ c (no. 15), a = 17.373(4) Å, b = 7.8290(16) Å, c = 19.781(4) Å, β = 93.62(3)°, V = 2685.2(9) Å 3 , Z = 8, R gt ( F ) = 0.0447, wR ref ( F 2 ) = 0.1313, T = 293(2) K.
Open Access
Crystal structure of 1-nonylpyridazin-1-ium iodide, C₁₃H₂₃N₂I

May 17, 2019

Musa A. Said, David L. Hughes, Saud M. Almutairi, Mohamed Reda Aouad, Mouslim Messali

Page range: 857-859

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C 13 H 23 N 2 I, triclinic, P 1̄ (no. 2), a = 5.6693(3) Å, b = 8.9457(4) Å, c = 16.2919(7) Å, α = 83.341(4)°, β = 89.534(4)°, γ = 82.491(4)°, V = 813.63(7) Å 3 , Z = 2, R gt ( F ) = 0.0446, wR ref ( F 2 ) = 0.0873, T = 295(2) K.
Open Access
Crystal structure of bis[diaqua(1,10-phenanthroline-κ²N, N′)-copper(II)]diphenylphosphopentamolybdate dihydrate, C₃₆H₃₈Cu₂Mo₅N₄O₂₇P₂

June 18, 2019

Dong-Dong Li, Hui Jiang, Bing-Xin Jia, Yuan Yuan, Ye-Shun Shi, Feng-Xia Ma

Page range: 861-862

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C 36 H 38 Cu 2 Mo 5 N 4 O 27 P 2 , monoclinic, C 2/c (no. 15), a = 15.6362(11) Å, b = 13.2418(9) Å, c = 23.6641(14) Å, β = 98.858(6)°, V = 4841.2(6) Å 3 , Z = 4, R gt ( F ) = 0.0219, wR ref ( F 2 ) = 0.0522, T = 293(2) K.
Open Access
The crystal structure of tetrakis(imidazole)-copper(I) hexafluorophosphate, C₁₂H₁₆CuF₆PN₈

May 22, 2019

Wen-Wu Zhong, Qian Tang, Ying-Jie Liu, Lei Shi, Yuan-Jiao Feng, Tao Tan

Page range: 863-864

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C 12 H 16 CuF 6 PN 8 , monoclinic, C 2/ c (no. 15), a = 13.102(2) Å, b = 9.7902(18) Å, c = 14.727(3) Å, β = 102.336(6)°, V = 1845.3(6) Å 3 , Z = 4, R gt ( F ) = 0.0291, wR ref ( F 2 ) = 0.0733, T = 150(2) K.
Open Access
The crystal structure of dimethyl ((3,5-di-tert-butyl-4-hydroxyphenyl)(phenyl)methyl)phosphonate, C₂₃H₃₃O₄P

June 11, 2019

Zhang-Qin Liu, Peng-Sheng You, Min Tang, Liang-Dong Zhang, Sheng-Shu Liu

Page range: 865-867

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C 23 H 33 O 4 P, monoclinic, P 2 1 / c (no. 14), a = 10.4629(3) Å, b = 11.4909(5) Å, c = 19.3341(9) Å, β = 98.201(4)°, V = 2300.73(16) Å 3 , Z = 4, R gt ( F ) = 0.0550, wR ref ( F 2 ) = 0.1109, T = 298 K.
Open Access
Crystal structure of diaqua-bis(1,10-phenanthroline κ²N,N′)nickel(II) trifluoroacetate- trifluoroacetic acid (1/1), C₃₀H₂₁F₉N₄NiO₈

June 18, 2019

Lan Zhang, Qiang Wang, Wu-Xiu Ding, Hui-Min Hao

Page range: 869-871

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C 30 H 21 F 9 N 4 NiO 8 , monoclinic, P 2 1 / c (no. 13), a = 10.0630(11) Å, b = 9.625(1) Å, c = 18.196(2) Å, β = 116.10(3)°, V = 1582.7(5) Å 3 , Z = 2, R gt ( F ) = 0.0511, wR ref ( F 2 ) = 0.1261, T = 293(2) K.
Open Access
Crystal structure of 2-(naphthalen-2-yl)-1,8-naphthyridine, C₁₈H₁₂N₂

May 22, 2019

Guo-Kai Jia, Chen Xiu-Wen, Lv Jing-Kun, Xiao-Ming Chen

Page range: 873-874

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C 18 H 12 N 2 , monoclinic, P 2 1 / c (no. 14), a = 27.514(5) Å, b = 6.3231(11) Å, c = 7.4175(13) Å, β = 95.805(2)°, V = 1283.8(4) Å 3 , Z = 4, R gt ( F ) = 0.0439, wR ref ( F 2 ) = 0.1233, T = 296(2) K.
Open Access
Synthesis and crystal structure of a new polymorph of diisopropylammonium trichloroacetate, C₈H₁₆Cl₃NO₂

July 20, 2019

Guido J. Reiss, Michaela K. Meyer, Jürgen Graf

Page range: 875-879

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C 8 H 16 Cl 3 NO 2 , monoclinic, P 2 1 (no. 4), a = 9.1804(5), Å, b = 19.4133(10) Å, c = 13.9191(7) Å, β = 90.593(3)°, V = 2480.6(2) Å 3 , Z = 8, R gt ( F ) = 0.0605, wR ref ( F 2 ) = 0.1387, T = 296(2) K.
Open Access
Crystal structure of dimethanol-bis(1-((2-methyl-1H-benzo[d]imidazol-1-yl)methyl)-1H-benzo[d][1,2,3]triazole-κN)-bis(thiocyanato-κN)cadmium(II) C₃₄H₃₄CdN₁₂O₂S₂

May 17, 2019

Ning Ling, Xia Wang, Ya-Wen Zhang, Tian-Tian Zhao, Yuan Ruan, Jing Yang

Page range: 881-882

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C 34 H 34 CdN 12 O 2 S 2 , triclinic, P 1̄, a = 9.6872(6) Å, b = 10.4523(7) Å, c = 10.8422(9) Å, α = 113.022(7)°, β = 96.919(6)°, γ = 104.526(6)°, Z = 1, V = 948.20(13) Å 3 , R gt ( F ) = 0.0564, wR ref ( F 2 ) = 0.1511, T = 293(2) K.
Open Access
Crystal structure of ethyl 2,2-difluoro-2-(7-methoxy-2-oxo-2H-chromen-3-yl)acetate, C₁₄H₁₂F₂O₅

May 27, 2019

Linfeng He, An-Jun Wang

Page range: 883-884

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C 14 H 12 F 2 O 5 , monoclinic, P 2 1 / n (no. 14), a = 6.8723(2) Å, b = 27.0231(7) Å, c = 7.3669(2) Å, β = 109.235(3)°, Z = 4, V = 1291.75(7) Å 3 , R gt ( F ) = 0.0484, wR ref ( F 2 ) = 0.1335, T = 100 K.
Open Access
The crystal structure of bis[μ₂-(N,N-diethylcarbamodithioato-κS:κS,κS′)] bis[1′-(diphenylphosphino-κP)-1-cyanoferrocene]disilver(I), C₅₆H₅₆Ag₂Fe₂N₄P₂S₄

June 14, 2019

Karel Škoch, Petr Štěpnička

Page range: 885-887

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C 56 H 56 Ag 2 Fe 2 N 4 P 2 S 4 , triclinic, P 1̄ (no. 2), a = 9.5058(2) Å, b = 10.8362(2) Å, c = 14.3325(3) Å, α = 72.400(1)°, β = 75.241(1)°, γ = 77.132(1)°, V = 1343.71(5) Å 3 , Z = 1, R gt ( F ) = 0.0191, wR ref ( F 2 ) = 0.0443, T = 150(2) K.
Open Access
Crystal structure of bis(di-n-butylammonium) tetrachloridodiphenylstannate(IV), C₂₈H₅₀Cl₄N₂Sn

June 6, 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 889-891

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C 28 H 50 Cl 4 N 2 Sn, monoclinic, P 2 1 / c (no. 14), a = 12.3981(2) Å, b = 13.2742(2) Å, c = 11.0847(2) Å, β = 111.657(2)°, V = 1695.49(5) Å 3 , Z = 2, R gt ( F ) = 0.0161, wR ref ( F 2 ) = 0.0431, T = 100(2) K.
Open Access
The crystal structure of poly[(μ₅-2-((5-bromo-3-formyl-2-hydroxybenzylidene)amino)benzenesulfonato-κ⁶O:O:O,O′:O′:O′′)sodium(I)], C₁₃H₉O₄NSBrNa

May 27, 2019

Xi-Shi Tai, Li-Hua Wang

Page range: 893-894

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C 13 H 9 O 4 NSBrNa, monoclinic, P 2 1 / c (no. 14), a = 26.1300(15) Å, b = 6.1547(4) Å, c = 8.3908(5) Å, β = 91.760(5)°, V = 1348.79(14) Å 3 , Z = 4, R gt ( F ) = 0.0402, wR ref ( F 2 ) = 0.0866, T = 100 K.
Open Access
Crystal structure of catena-{poly[bis(O,O′-diethyldithiophosphato-S)-(μ₂-1,2-bis(4-pyridylmethylene)hydrazine-N,N′)-zinc(II)] di-acetonitrile solvate}, {C₂₀H₃₀N₄O₄P₂S₄Zn ⋅ 2 C₂H₃N}_n

July 9, 2019

Yee Seng Tan, Edward R.T. Tiekink

Page range: 895-897

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C 24 H 36 N 6 O 4 P 2 S 4 Zn, triclinic, P 1̄ (no. 2), a = 11.2847(2) Å, b = 12.6967(3) Å, c = 13.6595(3) Å, α = 64.738(2)°, β = 72.181(2)°, γ = 76.681(2)°, V = 1673.68(7) Å 3 , Z = 2, R gt ( F ) = 0.0225, wR ref ( F 2 ) = 0.0582, T = 100(2) K.
Open Access
Halogen and hydrogen bonding in the layered crystal structure of 2-iodoanilinium triiodide, C₆H₇I₄N

May 27, 2019

Guido J. Reiss

Page range: 899-902

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C 6 H 7 I 4 N, monoclinic, P 2 1 / m (no. 11), a = 9.2818(2) Å, b = 6.55289(16) Å, c = 11.0561(3) Å, β = 114.051(3)°, V = 614.08(3) Å 3 , Z = 2, R gt ( F ) = 0.0180, wR ref ( F 2 ) = 0.0367, T = 109(2) K.
Open Access
Crystal structure of cyclohexane-1,4-diammonium 2-[(2-carboxylatophenyl)disulfanyl]benzoate — dimethylformamide — monohydrate (1/1/1), [C₆H₁₆N₂][C₁₄H₈O₄S₂] ⋅ C₃H₇NO⋅H₂O

May 22, 2019

Sang Loon Tan, Edward R.T. Tiekink

Page range: 903-905

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[C 6 H 16 N 2 ][C 14 H 8 O 4 S 2 ]⋅C 3 H 7 NO⋅H 2 O, triclinic, P 1̄ (no. 2), a = 7.86120(10) Å, b = 12.2464(2) Å, c = 14.1615(2) Å, α = 111.293(1)°, β = 105.767(2)°, γ = 93.690(1)°, V = 1202.11(3) Å 3 , Z = 2, R gt ( F ) = 0.0373, wR ref ( F 2 ) = 0.1054, T = 100(2) K.
Open Access
The synthesis and crystal structure of isobutyl 5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-((trifluoromethyl)sulfinyl)-1H-pyrazole-3-carboxylate, C₁₆H₁₃Cl₂F₆N₃O₃S

June 19, 2019

Lianqing Chen, Yanting Du

Page range: 907-909

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C 16 H 13 Cl 2 F 6 N 3 O 3 S, monoclinic, P 2 1 / n (no. 14), a = 5.8650(10) Å, b = 30.196(5) Å, c = 11.777(2) Å, β = 96.619(2)°, V = 2071.8(6) Å 3 , Z = 4, R gt ( F ) = 0.0521, wR ref ( F 2 ) = 0.1211, T = 173 K.
Open Access
Isolation and crystal structure of bufotalinin — methanol (1/1), C₂₅H₃₄O₇

May 13, 2019

Guo-Qiang Li, Yi-Ting Zhao, Qing-Peng Xu, Hai-Yan Tian, Peng-ran Guo, Fu-wang Wu

Page range: 911-913

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C 25 H 34 O 7 , monoclinic, P 2 1 (no. 4), a = 9.24730(10) Å, b = 9.9061(2) Å, c = 12.5907(2) Å, β = 101.264(2)°, V = 1131.15(3) Å 3 , Z = 2, R gt ( F ) = 0.0380, wR ref ( F 2 ) = 0.1025, T = 173 K.
Open Access
Crystal structure of benzylbis(1,3-diphenylpropane-1,3-dionato-κ²O,O′) chloridotin(IV), C₃₇H₂₉ClO₄Sn

May 27, 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 915-917

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C 37 H 29 ClO 4 Sn, monoclinic, P 2 1 / c (no. 14), a = 10.4233(3) Å, b = 19.5060(6) Å, c = 14.8084(5) Å, β = 94.148(2)°, V = 3002.91(16) Å 3 , Z = 4, R gt ( F ) = 0.0432, wR ref ( F 2 ) = 0.1036, T = 296(2) K.
Open Access
Crystal structure of Bis{1-[(benzotriazol-1-yl)methyl]-1-H-1,3-(2-methyl-imidazol)}diiodidocadmium(II), [Cd(C₁₁H₁₁N₅)₂I₂], C₂₂H₂₂N₁₀I₂Cd

May 31, 2019

Hai-Yan Yang, Fang He, Yao-Min Zhao, Hui Li, Hong-Fang Wang, Ying-Hua Li

Page range: 919-921

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C 22 H 22 N 10 I 2 Cd, triclinic, P 1̄ (no. 2), a = 10.5476(8) Å, b = 11.1759(9) Å, c = 12.7735(10) Å, α = 103.372(7)°, β = 105.811(7)°, γ = 100.270(6)°, V = 1361.85(18) Å 3 , Z = 2, R gt ( F ) = 0.0324, wR ref ( F 2 ) = 0.0661, T = 291(2) K.
Open Access
Crystal structure of 4-isobutoxybenzaldehyde oxime, C₁₁H₁₅NO₂

May 14, 2019

Xian Tang, De-Cai Wang

Page range: 923-924

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C 11 H 15 O 2 N, monoclinic, P 2 1 / n (no. 14), a = 13.5152(2) Å, b = 6.19120(10) Å, c = 14.3917(2) Å, β = 115.467(2)°, V = 1087.22(3) Å 3 , Z = 4, R gt ( F ) = 0.0384, wR ref ( F 2 ) = 0.1104 T = 170(2) K.
Open Access
The crystal structure of bis(acetato-κ¹O)-bis(N′-hydroxypyrimidine-2-carboximidamide-κ²N,N′)manganese(II) — methanol (1/2), C₁₄H₁₈MnN₈O₆, 2(CH₃OH)′

May 27, 2019

Xiu-Ju Yin, Long-Guan Zhu

Page range: 925-926

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C 16 H 26 MnN 8 O 8 , monoclinic, C 2/ c (no. 15), a = 15.3188(9) Å, b = 10.9014(7) Å, c = 14.3601(9) Å, β = 90.516(5)°, Z = 4, V = 2398.0(3) Å 3 , R gt ( F ) = 0.0377, wR ref ( F 2 ) = 0.0942, T = 293(2) K.
Open Access
Crystal structure of poly[bis(μ₂-bis(4-(1H-imidazol-1-yl)phenyl)amine-κ²N:N′)-bis(nitrato-κO)cadmium(II)], C₃₆H₃₀CdN₁₂O₆

May 31, 2019

Boyang Wang, Jian Wang

Page range: 927-928

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C 36 H 30 CdN 12 O 6 , monoclinic, P 2 1 / c (no. 14), a = 9.9673(10) Å, b = 8.6759(9) Å, c = 20.756(2) Å, β = 98.926(7)°, V = 1773.1(3) Å 3 , Z = 2, R gt ( F ) = 0.0554, wR ref ( F 2 ) = 0.1561, T = 2932 K.
Open Access
Crystal structure and optical properties of 1,6-bis(methylthio)pyrene, C₁₈H₁₄S₂

May 27, 2019

Guang-Qing Wang, Hong-Bo Fang, Li-Hua Xu, Zhong-Hai Ni

Page range: 929-931

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C 18 H 14 S 2 , monoclinic, P 2 1 / c (no. 14), a = 10.196(3) Å, b = 14.756(4) Å, c = 9.508(3) Å, β = 103.965(14)°, V = 1388.3(7) Å 3 , Z = 4, R gt ( F ) = 0.0480, wR ref ( F 2 ) = 0.1207, T = 200(2) K.
Open Access
The crystal structure of hexaquamagnesium(II) bis(3,4-dinitropyrazol-1-ide), C₆H₁₄MgN₈O₁₄

May 17, 2019

Liu TianLi, Wang Jianlong, Chen Lizhen, Cao DuanLin, Lu ZhiYan, Wu NaNa

Page range: 933-934

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C 6 H 14 MgN 8 O 14 , monoclinic, P 1̄ (no. 2), a = 6.1154(3) Å, b = 7.9529(4) Å, c = 9.0459(5) Å, α = 77.744(2)° β = 82.589(2)°, γ = 81.134(3)°, V = 422.67(4) Å 3 , Z = 1, R gt ( F ) = 0.0454, wR ref ( F 2 ) = 0.1112, T = 150 K.
Open Access
Halogen bonds in the crystal structure of 4,3:5,4-terpyridine – 1,4-diiodotetrafluorobenzene (1/1), C₂₁H₁₁F₄I₂N₃

June 19, 2019

Weizhou Wang

Page range: 935-937

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C 21 H 11 F 4 I 2 N 3 , monoclinic, C 2/ c (no. 15), a = 17.9705(8) Å, b = 6.5423(3) Å, c = 17.8916(8) Å, β = 98.634(4)°, Z = 4, V = 2079.65(16) Å 3 , R gt ( F ) = 0.0313, wR ref ( F 2 ) = 0.0784, T = 290 K.
Open Access
Crystal structure and photochromic properties of a novel photochromic perfluordiarylethene containing a triazole bridged pyridine group moiety, C₂₄H₁₈F₆N₄S₂

June 21, 2019

Yongjie Li, Chunhong Zheng, Shouzhi Pu

Page range: 939-941

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C 24 H 18 F 6 N 4 S 2 , monclinic, P 2 1 / c (no. 14), a = 19.0525(18) Å, b = 8.5569(9) Å, c = 15.3792(15) Å, β = 97.241(2)°, V = 2487.3(4) Å 3 , Z = 4, R gt ( F ) = 0.0513, wR ref ( F 2 ) = 0.1425, T = 296(2) K.
Open Access
Crystal structure of bis[(μ₃-oxido)-(μ₂-(N,N-diisopropylthiocarbamoylthio) acetato-κ²O,O′)-((N,N-diisopropylthiocarbamoylthio)acetato-κO)-bis(di-4-methylbenzyl-tin(IV))], C₁₀₀H₁₃₆N₄O₁₀S₈Sn₄

June 19, 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 943-946

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C 100 H 136 N 4 O 10 S 8 Sn 4 , triclinic, P 1̄ (no. 2), a = 13.7756(4) Å, b = 13.9663(5) Å, c = 16.6392(5) Å, α = 71.501(2)°, β = 73.952(2)°, γ = 63.180(2)°, V = 2675.49(16) Å 3 , Z = 1, R gt ( F ) = 0.0383, wR ref ( F 2 ) = 0.1209, T = 296(2) K.
Open Access
Crystal structure of dibromidobis(4-bromobenzyl)tin(IV), C₁₄H₁₂Br₄Sn

June 19, 2019

See Mun Lee, Kong Mun Lo, Edward R.T. Tiekink

Page range: 947-948

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C 14 H 12 Br 4 Sn, monoclinic, I 2/ a (no. 15), a = 12.6379(2) Å, b = 4.9674(1) Å, c = 26.1845(4) Å, β = 94.507(1)°, V = 1638.71(5) Å 3 , Z = 4, R gt ( F ) = 0.0142, wR ref ( F 2 ) = 0.0358, T = 100 K.
Open Access
The crystal structure of (4Z)-2-[(E)-(1-ethyl-3,3-dimethyl-1,3-dihydro-2H-indol-2-ylidene)methyl]-4-[(1-ethyl-3,3-dimethyl-3H-indolium-2-yl)methylidene]-3-oxocyclobut-1-en-1-olate, C₃₀H₃₂N₂O₂

July 19, 2019

Abdullah M. Asiri, Muhammad Nadeem Arshad, Soha M. Albukhari, Amerah M. Al-Soliemy

Page range: 949-951

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C 30 H 32 N 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 9.8611(2) Å, b = 15.8027(3) Å, c = 16.2473(3) Å, β = 100.150(2)°, V = 2492.23(8) Å 3 , Z = 4, R gt ( F ) = 0.0542, wR ref ( F 2 ) = 0.1677, T = 296(3) K.
Open Access
The crystal structure of (E)-3-(4-(dimethylamino)styryl)-5,5-dimethylcyclohex-2-en-1-one, C₁₈H₂₃NO

May 27, 2019

Abdullah M. Asiri, Muhammad Nadeem Arshad, Soha M. Albukhari, Amerah M. Al-Soliemy, Salman A. Khan

Page range: 953-955

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C 18 H 23 NO, triclinic, P 1̄ (no. 2), a = 6.0033(3) Å, b = 11.5667(7) Å, c = 23.5556(12) Å, α = 77.121(5)°, β = 89.635(4)°, γ = 78.852(5)°, V = 1563.27(15) Å 3 , Z = 4, R gt ( F ) = 0.0630, wR ref ( F 2 ) = 0.1733, T = 296(2) K.
Open Access
Crystal structure of dihydrazinium 1H-pyrazole-3,5-dicarboxylate, C₅H₁₂N₆O₄

June 22, 2019

Nedeljko Latinović, Sladjana B. Novaković, Goran A. Bogdanović, Vlatko Kastratović, Gerald Giester, Željko K. Jaćimović

Page range: 957-958

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C 5 H 12 N 6 O 4 , monoclinic, P 2 1 / n (no. 14), a = 4.3368(6) Å, b = 15.483(2) Å, c = 13.8852(19) Å, β = 97.714(3)°, V = 923.9(2) Å 3 , Z = 4, R gt ( F ) = 0.0411, wR ref ( F 2 ) = 0.1109, T = 200(2) K.
Open Access
Crystal structure of poly[μ₂-1,4-bis((1H-imidazol-1-yl)methyl)benzene-κ²N:N′)-(μ₂-4-sulfidobenzoate-κ²O:S)cobalt(II)] dihydrate, C₄₂H₄₄Co₂N₈O₇S₂

June 19, 2019

Chonglan Yin, Wei Jiang, Jihong Dai

Page range: 959-960

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C 42 H 44 Co 2 N 8 O 7 S 2 , monoclinic, P 2 1 (no. 4), a = 7.3941(6) Å, b = 15.3043(14) Å, c = 9.7831(7) Å, β = 101.315(7)°, V = 1085.56(15) Å 3 , Z = 1, R gt ( F ) = 0.0392, wR ref ( F 2 ) = 0.0749, T = 293(2) K.
Open Access
Crystal structure of 8-(3,4-dimethylbenzylidene)-6,10-dioxaspiro[4.5]decane-7,9-dione, C₁₇H₁₈O₄

May 17, 2019

Xia Wang, Wu-Lan Zeng

Page range: 961-963

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C 17 H 18 O 4 , monoclinic, P 2 1 / c (no. 14), a = 8.6020(17) Å, b = 14.835(3) Å, c = 11.624(2) Å, β = 90.07(3), V = 1483.3(5) Å 3 , Z = 4, R gt ( F ) = 0.0474, wR ref ( F 2 ) = 0.1439, T = 293(2) K.
Open Access
Crystal structure of 4-(2-bromo-4-(6-morpholino-3-phenyl-3H-benzo[f]chromen-3-yl) cyclohexa-2,5-dien-1-yl)morpholine, C₃₃H₃₁BrN₂O

May 13, 2019

Fu-Jie Liu, Guo-Xi Wang

Page range: 965-967

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C 31 H 31 BrN 2 O 3 , monoclinic, P 2 1 / c (no. 14), a = 10.2014(15) Å, b = 21.499(3) Å, c = 12.1885(18) Å, β = 95.175(2)°, V = 2662.3(7) Å 3 , Z = 4, R gt ( F ) = 0.0521, wR ref ( F 2 ) = 0.1993, T = 296(2) K.
Open Access
Synthesis and crystal structure of 2-((1-phenyl-3-(thiophen-2-yl)-1H-pyrazol-4-yl)methylene)-2,3-dihydro-1H-inden-1-one, C₂₃H₁₆N₂OS

May 17, 2019

Alaa Alqahtani, Bakr F. Abdel-Wahab, Amany S. Hegazy, Benson M. Kariuki, Gamal A. El-Hiti

Page range: 969-971

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C 23 H 16 N 2 OS, orthorhombic, Pna 2 1 (no. 33), a = 19.4988(9) Å, b = 19.5060(9) Å, c = 9.2893(4) Å, V = 3533.1(3) Å 3 , Z = 8, R gt ( F ) = 0.0501, wR ref ( F 2 ) = 0.1269, T = 296(2) K.
Open Access
Crystal structure of poly[(μ₂-1,1′-(oxybis(4,1-phenylene)bis(1H-imidazole)-κ²N,N′)(μ₂-1,3-benzenecarboxylato-κ³O,O′:O′′)zinc(II)] dihydrate, C₂₆H₂₂N₄O₇Zn

May 22, 2019

Bo-Tao Xu, Ze-Jun Mao, Li-Xiang He, Sheng-Cong Guo, Guo-Dong Zhang

Page range: 973-974

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C 26 H 22 N 4 O 7 Zn, monoclinic, P 2 1 / c (no. 14), a = 9.1134(4) Å, b = 16.0238(7) Å, c = 17.8763(7) Å, β = 103.376(7)°, V = 2539.7(2) Å 3 , Z = 4, R gt ( F ) = 0.0465, wR ref ( F 2 ) = 0.0990, T = 293 K.
Open Access
Crystal structure of diaqua-bis(cinnamato-κ²O,O′)zinc(II), C₁₈H₁₈ZnO₆

May 13, 2019

Jaeun Kang, Kang Min Ok, Junghwan Do

Page range: 975-976

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C 18 H 18 ZnO 6 , monoclinic, C 2 (no. 5), a = 11.7049(4) Å, b = 5.09430(10) Å, c = 14.3230(4) Å, β = 100.370(2)°, V = 840.11(4) Å 3 , Z = 2, R gt ( F ) = 0.0309, wR ref ( F 2 ) = 0.0583, T = 293(2) K.
Open Access
Crystal structure of 2-(prop-2-yn-1-yloxy)-1-naphthaldehyde, C₁₄H₁₀O₂

May 27, 2019

Ghadah Aljohani, Dieter Lentz, Musa A. Said, Shaya Y. Alraqa, Adeeb A. Ali, Norazah Basar

Page range: 977-978

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C 14 H 10 O 2 , triclinic, P 1̄ (no. 2), a = 7.498(3) Å, b = 7.973(3) Å, c = 9.660(4) Å, α = 67.211(13)°, β = 84.489(14)°, γ = 72.224(14)°, V = 506.8(4) Å 3 , Z = 2, R gt (F ) = 0.0394, wR ref ( F 2 ) = 0.1135, T = 100(2) K.
Open Access
Crystal structure and photochromic properties of 1-(2-methyl-5-phenyl-3-thienyl)-2-{2-methyl-5-[4-(9-fluorenone hydrazone)-phenyl]-3-thienyl}perfluorocyclopentene, C₄₁H₂₆F₆N₂S₂

May 27, 2019

Dongming Xu, Chunhong Zheng, Shouzhi Pu

Page range: 979-981

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C 41 H 26 F 6 N 2 S 2 , triclinic, P 1̄ (no. 2), a = 11.7525(12) Å, b = 12.2430(12) Å, c = 13.4210(13) Å, α = 84.914(1)°, β = 66.860(1)°, γ = 82.543(1)°, V = 1759.2(3) Å 3 , Z = 2, R gt ( F ) = 0.0459, wR ref ( F 2 ) = 0.1268, T = 296(2) K.
Open Access
Hydrothermal synthesis and crystal structure of cylo[tetraaqua-bis(μ₂-1,4-bis(1H-benzo[d]imidazol-1-yl)but-2-ene-κ²N:N′)-bis(μ₂-4-nitro-phthalate-κ²O,O′)dinickel(II)], C₂₆H₂₃N₅O₈Ni

May 17, 2019

Yin Wei-Dong, Li Gui-Lian, Liu Qian-Long

Page range: 983-986

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C 26 H 23 N 5 O 8 Ni, monoclinic, P 2 1 / c (no. 14), a = 15.4152(5) Å, b = 10.8836(3) Å, c = 16.1172(5) Å, β = 112.097(4)°, V = 2505.42(14) Å 3 , Z = 4, R gt ( F ) = 0.0361, wR ref ( F 2 ) = 0.0876, T = 293(2) K.
Open Access
Crystal structure of 3-[methyl(phenyl)amino]-1-phenylthiourea, C₁₄H₁₅N₃S

July 9, 2019

Chien Ing Yeo, Edward R.T. Tiekink

Page range: 987-988

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C 14 H 15 N 3 S, monoclinic, P 2 1 / c (no. 14), a = 10.4801(1) Å, b = 10.8132(1) Å, c = 12.1341(1) Å, β = 107.823(1)°, V = 1309.08(2) Å 3 , Z = 4, R gt ( F ) = 0.0266, wR ref ( F 2 ) = 0.0728, T = 100(2) K.
Open Access
Crystal structure of 1-(4-chlorophenyl)-3-[methyl(phenyl)amino]thiourea, C₁₄H₁₄ClN₃S

June 18, 2019

Chien Ing Yeo, Edward R.T. Tiekink

Page range: 989-990

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C 14 H 14 ClN 3 S, orthorhombic, Pbca (no. 61), a = 10.4000(2) Å, b = 11.5622(2) Å, c = 23.4776(4) Å, V = 2823.11(9) Å 3 , Z = 8, R gt ( F ) = 0.0284, wR ref ( F 2 ) = 0.0774, T = 100(2) K.
Open Access
Crystal structure of 2-tert-butyl-1H-imidazo[4,5-b]pyridine, C₁₀H₁₃N₃

June 18, 2019

Guo-Ling Huang, Xiu-Wen Chen, Lu Chen, Yi-Biao Li

Page range: 991-992

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C 10 H 13 N 3 , orthorhombic, Pbca (no. 14), a = 9.4795(7) Å, b = 10.7585(10) Å, c = 18.8783(13) Å, V = 1925.3(3) Å 3 , Z = 8, R gt ( F ) = 0.0702, wR ref ( F 2 ) = 0.1959, T = 296(2) K.
Open Access
Crystal structure of 5-carboxy-2-(2-carboxyphenyl)-1H-imidazol-3-ium-4-carboxylate dihydrate, C₁₂H₈N₂O₆⋅2(H₂O)

July 2, 2019

Xiao-Fei Li, Ke Wang, Wei Zhang, Zi-Ying Fu

Page range: 993-995

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C 12 H 12 N 2 O 8 , monoclinic, P 2 1 / n (no. 14), a = 5.1122(5) Å, b = 15.0150(13) Å, c = 17.3561(15) Å, β = 95.152(4)°, V = 1326.9(2) Å 3 , Z = 4, R gt ( F ) = 0.0711, wR ref ( F 2 ) = 0.1509, T = 293(2) K.
Open Access
The crystal structure of dichlorido-μ₂-dichlorido-(η²-1,4-bis(4-vinylbenzyl)-1,4-diazabicyclo[2.2.2]octane-1,4-diium)dicopper(I), C₂₄H₃₀N₂Cu₂Cl₄

May 17, 2019

Guo-Xi Wang, Zheng Xing

Page range: 997-999

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C 24 H 30 N 2 Cu 2 Cl 4 , triclinic, P 1̄ (no. 2), a = 7.204(4) Å, b = 8.593(5) Å, c = 21.112(12) Å, α = 89.153(7)°, β = 85.294(7)°, γ = 84.604(6)°, V = 1296.7(12) Å 3 , Z = 2, R gt ( F ) = 0.0535, wR ref ( F 2 ) = 0.1471, T = 296(2) K.
Open Access
Crystal structure of 4-bromobenzyl (Z)-N-(adamantan-1-yl)morpholine-4-carbothioimidate, C₂₂H₂₉BrN₂OS

May 13, 2019

Hanan A. Al-Ghulikah, Hazem A. Ghabbour, Edward R.T. Tiekink, Ali A. El-Emam

Page range: 1001-1003

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C 22 H 29 BrN 2 OS, triclinic, P 1̄ (no. 2), a = 7.1722(3) Å, b = 10.2350(4) Å, c = 14.8756(6) Å, α = 73.607(2)°, β = 84.7020(10)°, γ = 88.7210(10)°, V = 1043.11(7) Å 3 , Z = 2, R gt ( F ) = 0.0467, wR ref ( F 2 ) = 0.0870, T = 296(2) K.
Open Access
Crystal structure of (4S,4aS,6aR,6bR,12aS,12bR,14aS,14bR)-3,3,6a,6b,9,9,12a-heptamethyloctadecahydro-1H,3H-4,14b-ethanophenanthro[1,2-h]isochromene-1(6bH)-one, C₃₀H₄₈O₂

May 24, 2019

Kang He, Lin-Lin Fan, Tian-Tai Wu, Qi-Long Zhang, Juan Zou

Page range: 1005-1007

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C 30 H 48 O 2 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 10.8192(12) Å, b = 16.4915(17) Å, c = 28.832(3) Å, V = 5144.4(10) Å 3 , Z = 4, R gt ( F ) = 0.0582, wR ref ( F 2 ) = 0.1169, T = 293(2) K.
Open Access
Crystal structure of 3,5-bis(trifluoromethyl)benzyl (Z)-N′-(adamantan-1-yl)-4-phenylpiperazine-1-carbothioimidate, C₃₀H₃₃F₆N₃S

May 27, 2019

Lamya H. Al-Wahaibi, Nora H. Al-Shaalan, Hazem A. Ghabbour, Edward R.T. Tiekink, Ali A. El-Emam

Page range: 1009-1012

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C 30 H 33 F 6 N 3 S, triclinic, P 1̄ (no. 2), a = 9.3012(5) Å, b = 10.2734(5) Å, c = 15.1850(8) Å, α = 81.982(2)°, β = 78.696(2)°, γ = 83.882(2)°, V = 1404.25(13) Å 3 , Z = 2, R gt ( F ) = 0.0779, wR ref ( F 2 ) = 0.2499, T = 293(2) K.
Open Access
The crystal structure of 3-methoxyphenanthridin-6(5H)-one, C₁₄H₁₁NO₂

May 13, 2019

Deng-Ze Wu

Page range: 1013-1014

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C 14 H 11 NO 2 , monoclinic, P 2 1 / c (no. 14), a = 12.7731(19) Å, b = 5.4767(9) Å, c = 17.3616(18) Å, β = 119.747(7)°, V = 1054.5(3) Å 3 , Z = 4, R gt ( F ) = 0.0562, wR ref ( F 2 ) = 0.1907, T = 298(2) K.
Open Access
Crystal structure of 4-(5,5-difluoro-1,3,7,9-tetramethyl-3H,5H-5λ⁴-dipyrrolo[1,2-c:2′,1′-f][1,3,2]diazaborinin-10-yl)pyridin-1-ium tetraiodidoferrate(III), C₁₈H₁₉BF₂FeI₄N₃

May 22, 2019

Yan Gao, Zhiyin Xiao, Peipei Zhang, Yali Xiang, Wei Wang, Haimeng Hu

Page range: 1015-1016

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C 18 H 19 BF 2 FeI 4 N 3 , triclinic, P 1̄ (no. 2), a = 8.2997(3) Å, b = 11.8180(9) Å, c = 14.0849(7) Å, α = 106.388(5)°, β = 101.841(4)°, γ = 95.200(4)°, V = 1280.88(13) Å 3 , Z = 2, R gt ( F ) = 0.0393, wR ref ( F 2 ) = 0.1045, T = 293(2) K.
Open Access
Crystal structure of 2-(3-methoxyphenyl)-3-((phenylsulfonyl)methyl)imidazo[1,2-a]pyridine, C₂₁H₁₈N₂O₃S

May 24, 2019

Xia Mi, Zheng Zhong, Jing Yang, Jingyu Zhang

Page range: 1017-1018

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C 21 H 18 N 2 O 3 S, monoclinic, P 2 1 / n (no. 14), a = 12.1263(2) Å, b = 11.6913(3) Å, c = 12.7643(3) Å, β = 92.340(2)°, V = 1808.11(7) Å 3 , Z = 4, R gt ( F ) = 0.0433, wR ref ( F 2 ) = 0.1310, T = 293(2) K.
Open Access
Crystal structure of [(2-(2-chlorophenyl)-5-ethyl-1,3-dioxane-5-carboxylato-κ²O,O′) (5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ⁴N,N′,N′′,N′′′)]nickel(II) perchlorate, C₂₉H₅₀Cl₂N₄NiO₈

June 19, 2019

Ou Guang-Chuan, Guo-Kai Jia, Ying-Zhi Tan

Page range: 1019-1021

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C 29 H 50 Cl 2 N 4 NiO 8 , orthorhombic, Pbca (no. 61), a = 20.601(3) Å, b = 13.5059(16) Å, c = 25.015(3) Å, Z = 8, V = 6960.3(15) Å 3 , R gt ( F ) = 0.0495, wR ref ( F 2 ) = 0.1652, T = 296(2) K.
Open Access
Crystal structure of (Z)-6-(dimethylamino)-3,3-bis(4-(dimethylamino)phenyl)-2-(2-(quinoxalin-2-ylmethylene)hydrazinyl)-2,3-dihydroinden-1-one, C₃₅H₃₅N₇O

June 14, 2019

Dai Zeng, Ai-Ping Xing

Page range: 1023-1025

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C 35 H 35 N 7 O, triclinic, P 1̄ (no. 2), a = 10.2870(3) Å, b = 11.9918(4) Å, c = 13.8995(5) Å, α = 109.210(3)°, β = 96.833(3)°, γ = 107.594(3)°, Z = 2, V = 1497.32(9) Å 3 , R gt ( F ) = 0.0401, wR ref ( F 2 ) = 0.1091, T = 110(1) K.
Open Access
5-Methyl-N′-[5-methyl-1-(4-methylphenyl)-1H-1,2,3-triazole-4-carbonyl]-1-(4-methylphenyl)-1H-1,2,3-triazole-4-carbohydrazide, C₂₂H₂₂N₈O₂

May 24, 2019

Obaid Fahad Aldosari, Bakr F. Abdel-Wahab, Mohammad Hayal Alotaibi, Amany S. Hegazy, Benson M. Kariuki, Gamal A. El-Hiti

Page range: 1027-1029

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C 22 H 22 N 8 O 2 , monoclinic, P 2 1 / c (no. 14), a = 15.5175(5) Å, b = 7.9715(3) Å, c = 17.3941(5) Å, β = 90.005(3)°, V = 2151.61(12) Å 3 , Z = 4, R gt ( F ) = 0.0592, wR ref ( F 2 ) = 0.1780, T = 293(2) K.
Open Access
Crystal structure of 2,3-dichloro-6-methoxyquinoxaline, C₉H₆Cl₂N₂O

June 19, 2019

Zhi-Hai Yang, Zi-Yin Guo, Jia-Xin Shao, Shi-Yong Peng, Zhong-Zhi Zhu, Xiu-Wen Chen

Page range: 1031-1032

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C 9 H 6 Cl 2 N 2 O, monoclinic, P 2 1 / n (no. 14), a = 15.597(6) Å, b = 3.9346(16) Å, c = 15.614(6) Å, β = 101.834(4)°, V = 937.8(6) Å 3 , Z = 4, R gt ( F ) = 0.0360, wR ref ( F 2 ) = 0.1019, T = 296(2) K.
Open Access
Synthesis and crystal structure of 7-chloro-2-(ethylsulfinyl)-6-fluoro-3-(1H-pyrazole-1-yl)-4H-thiochromen-4-one, C₁₃H₁₀FN₃OS₂

July 18, 2019

Yuming Zhang, Tao Xiao, Xuan Guo, Chaolong Dou, Wenyuan Wu

Page range: 1033-1034

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C 14 H 10 ClFN 2 O 2 S 2 , monoclinic, P 2 1 / n (no. 14), a = 15.070(3) Å, b = 4.9050(10) Å, c = 21.018(4) Å, β = 105.59(3)°, V = 1496.5(5) Å 3 , Z = 4, R gt ( F ) = 0.0667, wR ref ( F 2 ) = 0.1363, T = 293(2) K.
Open Access
Crystal structure of 4-ethylpiperazine-1-carbothioic dithioperoxyanhydride, C₁₄H₂₆N₄S₄

July 24, 2019

Gwaza E. Ayom, Malik D. Khan, Sizwe J. Zamisa, Neerish Revaprasadu

Page range: 1035-1036

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C 14 H 26 N 4 S 4 , monoclinic, C 2/ c (no. 15), a = 16.9951(10) Å, b = 11.4397(7) Å, c = 9.7678(6) Å, β = 103.913(1)°, V = 1843.33(19) Å 3 , Z = 4, R gt ( F ) = 0.0200, wR ref ( F 2 ) = 0.0553, T = 100(2) K.
Open Access
Crystal structure of 2-(2-(6-methylpyridin-2-yl)naphthalen-1-yl)pyrimidine, C₂₀H₁₅N₃

August 2, 2019

Xin-Hua Lou

Page range: 1037-1038

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C 20 H 15 N 3 , orthorhombic, Pbca (no. 61), a = 11.0487(4) Å, b = 13.5000(6) Å, c = 21.1032(10) Å, V = 3147.7(2) Å 3 , Z = 8, R gt ( F ) = 0.0448, wR ref ( F 2 ) = 0.1136, T = 293(2) K.
Open Access
The crystal structure of N′-((1E,2E)-4-(7-methoxy-2-oxo-2H-chromen-8-yl)-2-methylbut-2-en-1-ylidene)-3-methylbenzohydrazide, C₂₃H₂₂N₂O₄

June 22, 2019

Xiang Yu, You-Fang Zhao, Yan Qin, Jing Yan, Ya-Fang Chen

Page range: 1039-1041

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C 23 H 22 N 2 O 4 , monoclinic, P 2 1 / c (no. 14), a = 17.7478(4) Å, b = 10.0041(2) Å, c = 24.4749(6) Å, β = 111.111(2)°, V = 4053.88(17) Å 3 , Z = 8, R gt ( F ) = 0.0614, wR ref ( F 2 ) = 0.1749, T = 290 K.
Open Access
Crystal structure of catena-poly[(μ₂-isophthalato-κ²O:O′)-(2,5-di(pyrazin-2-yl)-4,4′-bipyridine-κ³N,N′,N′′)zinc(II)] — water (2/5), C₂₆H₂₁N₆O_6.5Zn

July 19, 2019

Yu-Fang Wang, Yong-Hua Zhang

Page range: 1043-1045

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C 26 H 21 N 6 O 6.5 Zn, monoclinic, C 2/ c (no. 15), a = 18.3123(3) Å, b = 8.97463(15) Å, c = 30.1437(5) Å, β = 99.5396(16)°, V = 4885.51(14) Å 3 , Z = 4, R gt ( F ) = 0.0352, wR ref ( F 2 ) = 0.0746, T = 293(2) K.
Open Access
Crystal structure of (3E,5E)-3,5-bis(3-nitrobenzylidene)-1-((4-(trifluoromethyl)phenyl)sulfonyl)piperidin-4-one — dichloromethane (2/1), C₅₃H₃₈Cl₂F₆N₆O₁₄S₂

June 18, 2019

Yue Sun, Shu-Xia Wang, Gui-Ge Hou

Page range: 1047-1049

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C 53 H 38 Cl 2 F 6 N 6 O 14 S 2 , triclinic, P 1̄ (no. 2), a = 12.1975(6) Å, b = 13.9973(7) Å, c = 16.3818(10) Å, α = 69.365(5)°, β = 76.620(5)°, γ = 77.292(4)°, V = 2516.8(3) Å 3 , Z = 2, R gt ( F ) = 0.0540, wR ref ( F 2 ) = 0.1413, T = 100.02(10) K.
Open Access
Crystal structure of (μ₂-oxido)-bis(N,N′-o-phenylenebis(salicylideneiminato))diiron(III) — N,N′-dimethylformamide, C₄₇H₄₃Fe₂N₄O₉

July 9, 2019

Li Ya, Fang Xiangqing, Liu Junyi, Dong Chi, Yang Liguo

Page range: 1051-1053

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C 47 H 43 Fe 2 N 4 O 9 , orthorhombic, Pbca (no. 61), a = 24.6961(8) Å, b = 14.0952(5) Å, c = 24.696(3) Å, V = 8596.6(4) Å 3 , Z = 8, R gt ( F ) = 0.0374, wR ref ( F 2 ) = 0.1209, T = 296(2) K [1–3].
Open Access
Crystal structure of N¹,N³-bis(2-hydroxyethyl)-N¹, N¹,N³,N³-tetramethylpropane-1,3-diaminium dibromide, C₁₁H₂₈Br₂N₂O₂

June 19, 2019

Chang-Ming Su, Chun-Hua Wang, Gui-Ge Hou

Page range: 1055-1057

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C 11 H 28 Br 2 N 2 O 2 , triclinic, P 1̄ (no. 2), a = 12.0519(11) Å, b = 12.6670(12) Å, c = 12.9161(12) Å, α = 117.088(3)°, β = 92.459(1)°, γ = 108.199(2))°, V = 1627.2(3) Å 3 , Z = 4, R gt ( F ) = 0.0645, wR ref ( F 2 ) = 0.1632, T = 298(2) K.
Open Access
Crystal structure of (E)-N-(4-chlorophenyl)-1-(pyridin-2-yl)methanimine, C₁₂H₉ClN₂

August 2, 2019

Nyameka Diko, Sizwe J. Zamisa, Holger B. Friedrich, Mzamo L. Shozi

Page range: 1059-1061

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C 12 H 9 ClN 2 , monoclinic, P 2 1 / c (no. 14), a = 19.0184(3) Å, b = 4.81220(10) Å, c = 11.3896(2) Å, β = 107.388(1)°, Z = 4, V = 994.75(3) Å 3 , R gt ( F ) = 0.0284, wR ref ( F 2 ) = 0.0800, T = 100(2) K.
Open Access
Crystal structure of 8-bromo-6-oxo-2-phenyl-6H-pyrrolo[3,2,1-ij]quinoline-5-carbaldehyde, C₁₈H₁₁BrNO₂

June 14, 2019

Marole M. Maluleka, Malose J. Mphahlele, Eugene E. Onwu

Page range: 1063-1065

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C 18 H 11 BrNO 2 , orthorhombic, Pbcn (no. 60), a = 20.745(2) Å, b = 6.7956(8) Å, c = 20.470(3) Å, V = 2885.8(6) Å 3 , Z = 8, R gt ( F ) = 0.034, wR ref ( F 2 ) = 0.0846, T = 173(2) K.
Open Access
Crystal structure of 1,4-bis(2-azidoethyl)piperazine-1,4-diium dichloride trihydrate, C₈H₁₈N₈C_l2 ⋅ 3 H₂O

June 22, 2019

Zhi Jian Hao

Page range: 1067-1068

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C 8 H 24 N 8 O 3 , monoclinic, C 2/ c (no. 15), a = 17.3812(11) Å, b = 7.3688(5) Å, c = 14.0744(9) Å, β = 107.915°, V = 1715.2(2) Å 3 , Z = 4, R gt ( F ) = 0.0365, wR ref ( F 2 ) = 0.1012, T = 296(2) K.
Open Access
Crystal structure of (E)-4-bromo-N-(pyridin-2-ylmethylene)aniline, C₁₂H₉BrN₂

July 27, 2019

Nyameka Diko, Sizwe J. Zamisa, Holger B. Friedrich, Mzamo L. Shozi

Page range: 1069-1070

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C 12 H 9 BrN 2 , monoclinic, P 2 1 / c (no. 14), a = 19.2197(12) Å, b = 4.8579(3) Å, c = 11.4679(9) Å, β = 106.880(4)°, V = 1024.60(12) Å 3 , Z = 4, R gt ( F ) = 0.0449, wR ref ( F 2 ) = 0.1257, T = 100(2) K.
Open Access
Crystal structure of bis[(2-(3-bromophenyl)-5-methyl-1,3-dioxane-5-carboxylato-κ-O)-(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ⁴N,N′,N′′,N′′′)]nickel(II), C₄₀H₆₀Br₂N₄NiO₈

June 14, 2019

Ying-Zhi Tan, Guo-Kai Jia, Xiao-Wen Liu

Page range: 1071-1072

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C 40 H 60 Br 2 N 4 NiO 8 , triclinic, P 1̄ (no. 2), a = 8.546(7) Å, b = 10.162(7) Å, c = 13.831(13) Å, α = 92.943(9)°, β = 101.096(8)°, γ = 111.710(5)°, V = 1085.1(15) Å 3 , Z = 1, R gt ( F ) = 0.0317, wR ref ( F 2 ) = 0.0905, T = 296(2) K.
Open Access
The crystal structure of (1E,2E)-2-methyl-4-((7-oxo-7H-furo[3,2-g]chromen-9-yl)oxy)but-2-enal O-isonicotinoyl oxime–trichloromethane (3/1), C₆₇H₄₉Cl₃N₆O₁₈

June 22, 2019

Xiang Yu, Xu-Li Yang, You-Fang Zhao, Yan Qin, Jing Yan, Ya-Fang Chen

Page range: 1073-1075

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C 67 H 49 Cl 3 N 6 O 18 , triclinic, P 1̄ (no. 2), a = 12.3281(4) Å, b = 15.8887(5) Å, c = 16.9037(6) Å, α = 89.015(2)°, β = 77.885(3)°, γ = 72.021(3)°, V = 3075.20(19) Å 3 , Z = 2, R gt ( F ) = 0.0658, wR ref ( F 2 ) = 0.1558, T = 291.2(3) K.
Open Access
Crystal structure of 3-(2-ethoxy-2-oxoethyl)-1-methyl-1H-imidazol-3-ium hexafluoridophosphate(V), C₈H₁₃F₆N₂O₂P

July 25, 2019

Ting Huang, Xu-Liang Nie, Jing Chen, Wen Zhao, Wan-Ming Xiong

Page range: 1077-1079

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C 8 H 13 F 6 N 2 O 2 P, monoclinic, P 2 1 / c (no. 14), a = 9.0228(12) Å, b = 13.6501(18) Å, c = 11.2771(15) Å, β = 112.904(1)°, V = 1279.4(3) Å 3 , Z = 4, R gt ( F ) = 0.0773, wR ref ( F 2 ) = 0.2385, T = 296(2) K.
Open Access
Crystal structure of bis[(2-(2-bromophenyl)-5-ethyl-1,3-dioxane-5-carboxylato-κO)-(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ⁴N,N′,N′′,N′′′)]nickel(II) hemihydrate C₄₂H₆₅Br₂N₄NiO_8.5

June 21, 2019

Wang Qiong, Guo-Kai Jia, Xiao-Wen Liu

Page range: 1081-1082

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C 42 H 65 Br 2 N 4 NiO 8.5 , monoclinic, P 2 1 / c (no. 14), a = 14.852(2) Å, b = 12.1965(18) Å, c = 14.166(2) Å, β = 117.755(1)°, V = 2270.8(6) Å 3 , Z = 2, R gt ( F ) = 0.0449, wR ref ( F 2 ) = 0.1276, T = 296(2) K.
Open Access
The crystal structure of N-(7-(4-fluorobenzylidene)-3-(4-fluorophenyl)-3,3a,4,5,6,7-hexahydro-2H-indazole-2-carbonothioyl)benzamide, C₂₈H₂₃F₂N₃OS

July 19, 2019

Mohammad Hayal Alotaibi, Bakr F. Abdel-Wahab, Obaid Fahad Aldosari, Amany S. Hegazy, Benson M. Kariuki, Gamal A. El-Hiti

Page range: 1083-1085

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C 28 H 23 F 2 N 3 OS, monoclinic, I 2 /a (no. 15), a = 20.3481(8) Å, b = 10.2647(4) Å, c = 23.6975(11) Å, β = 105.317(5)°, V = 4773.8(4) Å 3 , Z = 8, R gt ( F ) = 0.0489, wR ref ( F 2 ) = 0.1543, T = 296(2) K.
Open Access
The crystal structure of N¹,N⁴-bis(pyridin-3-yl)cyclohexane-1,4-dicarboxamide, C₁₈H₂₀N₄O₂

June 25, 2019

Xiao-Li Luo, Tao Yang

Page range: 1087-1089

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C 18 H 20 N 4 O 2 , monoclinic, P 2 1 / n (no. 14), a = 7.8951(5) Å, b = 9.9303(7) Å, c = 10.5446(7) Å, β = 105.508(7)°, V = 796.61(10) Å 3 , Z = 2, R gt ( F ) = 0.0357, wR ref ( F 2 ) = 0.0923, T = 298(2) K.
Open Access
Crystal structure of (E)-2-(3,6-bis(ethylamino)-2,7-dimethyl-9H-xanthen-9-yl)-N′-((6-methylpyridin-2-yl)methylene)benzohydrazide – methanol (1/1), C₃₄H₃₇N₅O₃

July 20, 2019

Juan Yuan

Page range: 1091-1093

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C 34 H 37 N 5 O 3 , triclinic, P 1̄ (no. 2), a = 8.9446(3) Å, b = 13.4223(4) Å, c = 13.4559(4) Å, α = 83.371(3)°, β = 71.724(3)°, γ = 75.383(3)°, Z = 2, V = 1483.18(9) Å 3 , R gt ( F ) = 0.0383, wR ref ( F 2 ) = 0.0981, T = 105.6(5) K.
Open Access
Crystal structure of 2-oxo-1-(pyrimidin-5-ylmethyl)-3-(3-(trifluoromethyl)phenyl)-1,2-dihydro-5l4-pyrido[1,2-a]pyrimidin-4-olate, C₂₀H₁₃F₃N₄O₂

June 19, 2019

Shi Yun-lian, Huang Tao, Nie Xu-Liang, Zhang Feng-Rong, Peng Da-Yong, Shi Xu-Gen, Li Bao-Tong

Page range: 1095-1097

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C 20 H 13 F 3 N 4 O 2 , triclinic, P 1̄ (no. 2), a = 11.3525(10) Å, b = 12.7530(11) Å, c = 13.1926(12) Å, α = 83.894(1)°, β = 69.314(1)°, γ = 84.720(1)°, V = 1773.7(3) Å 3 , Z = 4, R gt ( F ) = 0.0477, wR ref ( F 2 ) = 0.1433, T = 296(2) K.
Open Access
Crystal structure of poly[(μ₃-9H-carbazole-3,6-dicarboxylato-κ³O¹: O²: O³)(μ₂-4-(pyridin-4-yl)pyridine-κ²N¹:N¹′)zinc(II)], C₁₉H₁₁N₂O₄Zn

July 20, 2019

Daguang Wang, Wei Li, Yabin Sun

Page range: 1099-1101

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C 19 H 11 N 2 O 4 Zn, monoclinic, C 2/ c (no. 15), a = 21.645(3) Å, b = 11.4467(18) Å, c = 12.985(2) Å, β = 103.156(3)°, Z = 8, V = 3132.8(8) Å 3 , R gt ( F ) = 0.0436, wR ref ( F 2 ) = 0.1193, T = 172(2) K.
Open Access
Crystal structure of (E)-N′-((1,8-dihydropyren-1-yl)-methylene)picolinohydrazide, C₂₃H₁₅N₃O

July 18, 2019

Yang Huanhuan, Xu Qingqing, Feng Haodong, Juan Yuan

Page range: 1103-1104

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C 23 H 15 N 3 O, monoclinic, P 2 1 / c (no. 14), a = 14.4372(3) Å, b = 11.9366(2) Å, c = 10.23409(19) Å, β = 106.963(2)°, V = 1686.92(6) Å 3 , Z = 4, R gt ( F ) = 0.0380, wR ref ( F 2 ) = 0.1055, T = 115.2(3) K.
Open Access
Crystal structure of catena-poly{[μ₂-1,2-bis(diphenylphosphino)ethane]dichloridocadmium(II)}, C₂₆H₂₄CdCl₂P₂

August 17, 2019

Yee Seng Tan, Edward R.T. Tiekink

Page range: 1105-1107

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C 26 H 24 CdCl 2 P 2 , monoclinic, P 2 1 / n (no. 14), a = 13.2003(1) Å, b = 11.4655(1) Å, c = 16.7390(1) Å, β = 100.955(1)°, V = 2487.25(3) Å 3 , Z = 4, R gt ( F ) = 0.0173, wR ref ( F 2 ) = 0.0451, T = 100(2) K.
Open Access
Crystal structure of the 1:2 co-crystal between N,N′-bis(4-pyridylmethyl)oxalamide and acetic acid as a dihydrate, C₁₄H₁₄N₄O₂⋅2 C₂H₄O₂⋅2 H₂O

August 17, 2019

Sang Loon Tan, Edward R.T. Tiekink

Page range: 1109-1111

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C 18 H 26 N 4 O 8 , triclinic, P 1̄ (no. 2), a = 4.7975(2) Å, b = 9.8725(3) Å, c = 11.0244(3) Å, α = 85.312(3)°, β = 79.872(3)°, γ = 87.600(3)°, V = 512.09(3) Å 3 , Z = 1, R gt ( F ) = 0.0381, wR ref ( F 2 ) = 0.1064, T = 100(2) K.
Open Access
Crystal structure of the co-crystal N,N′-bis(3-pyridylmethyl)oxalamide acetic acid (1/2), C₁₄H₁₄N₄O₂⋅2C₂H₄O₂

August 23, 2019

Sang Loon Tan, Edward R.T. Tiekink

Page range: 1113-1116

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C 18 H 22 N 4 O 6 , triclinic, P 1̄ (no. 2), a = 5.03050(10) Å, b = 12.4151(4) Å, c = 15.5353(5) Å, α = 96.186(3)°, β = 98.961(2)°, γ = 96.669(2)°, V = 944.05(5) Å 3 , Z = 2, R gt ( F ) = 0.0421, wR ref ( F 2 ) = 0.1213, T = 100 K.
Open Access
Crystal structure of the co-crystal N,N′-bis(4-pyridylmethyl)oxalamide and 2,3,5,6-tetrafluoro-1,4-di-iodobenzene (1/1), C₁₄H₁₄N₄O₂⋅C₆F₄I₂

August 29, 2019

Sang Loon Tan, Edward R.T. Tiekink

Page range: 1117-1119

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C 20 H 14 F 4 I 2 N 4 O 2 , triclinic, P 1̄ (no. 2), a = 5.0726(1) Å, b = 10.9432(2) Å, c = 19.8090(3) Å, α = 104.475(2)°, β = 90.427(2)°, γ = 92.908(2)°, V = 1063.10(3) Å 3 , Z = 2, R gt ( F ) = 0.0329, wR ref ( F 2 ) = 0.0907, T = 100 K.
Open Access
Crystal structure of the co-crystal 4-[(4-carboxyphenyl)disulfanyl]benzoic acid–(1E,4E)-1-N,4-N-bis(pyridin-4-ylmethylidene)cyclohexane-1,4-diamine (1/1), C₁₄H₁₀O₄S₂⋅C₁₈H₂₀N₄

August 17, 2019

Sang Loon Tan, Edward R.T. Tiekink

Page range: 1121-1123

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C 32 H 30 N 4 O 4 S 2 , monoclinic, I 2/ a (no. 15), a = 21.2034(7) Å, b = 5.0614(2) Å, c = 27.5987(12) Å, β = 105.991(4)°, V = 2847.3(2) Å 3 , Z = 4, R gt ( F ) = 0.0431, wR ref ( F 2 ) = 0.1246, T = 100(2) K.
Open Access
Crystal structure of hexacarbonyl-bis(μ₂-di-n-propyldithiocarbamato-κ³S,S′:S;κ³S:S:S′)-di-rhenium(I), C₂₀H₂₈N₂O₆Re₂S₄

August 23, 2019

Kong Mun Lo, See Mun Lee, Peter J. Heard, Edward R.T. Tiekink

Page range: 1125-1127

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C 20 H 28 N 2 O 6 Re 2 S 4 , monoclinic, C 2/ c (no. 15), a = 17.9296(4) Å, b = 9.60120(10) Å, c = 16.1859(3) Å, β = 103.934(2)°, V = 2704.34(9) Å 3 , Z = 4, R gt ( F ) = 0.0336, wR ref ( F 2 ) = 0.0902, T = 100 K.
Open Access
Crystal structure of fac-tricarbonyl-morpholine-κN-(morpholinocarbamodithioato-κ²S,S′)rhenium(I), C₁₂H₁₇N₂O₅ReS₂

August 17, 2019

See Mun Lee, Kong Mun Lo, Peter J. Heard, Edward R.T. Tiekink

Page range: 1129-1132

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C 12 H 17 N 2 O 5 ReS 2 , monoclinic, P 2 1 / c (no. 14), a = 11.99393(5) Å, b = 20.48791(11) Å, c = 13.67105(6) Å, β = 103.3351(5)°, V = 3268.82(3) Å 3 , Z = 8, R gt ( F ) = 0.0238, wR ref ( F 2 ) = 0.0629, T = 100(2) K.

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