Zeitschrift für Kristallographie - New Crystal Structures

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Volume 232, Issue 6

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Zeitschrift für Kristallographie - New Crystal Structures

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Cover and Frontmatter

November 3, 2017

Page range: i-vi

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Open Access
Crystal structure of potassium 1-methyl-1H-1,2,3,4-tetrazole-5-thiolate, C₂H₃N₄SK

October 9, 2017

Xiuhang Wang

Page range: 845-847

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C 2 H 3 N 4 SK, orthorhombic, Pnma (no. 62), a = 13.874(2) Å, b = 6.5644(11) Å, c = 6.6911(11) Å, V = 609.39(17) Å 3 , Z = 4, R gt ( F ) = 0.02345, wR ref ( F 2 ) = 0.0594, T = 296 K.
Open Access
Crystal structure of bis(3-(3-ethylureido)-N,N-dimethylpropan-1-aminium) bis (μ₃-2-(hydroxymethyl)-2-(oxidomethyl)propane-1,3-bis(olato))-(μ₆-oxo)-hexakis(μ₂-oxo)-hexaoxo-hexavanadium(V) – dichloromethane (1/1), C₂₇H₆₀Cl₂N₆O₂₃V₆

September 16, 2017

Xiaokang Hu, Bo Huang, Zicheng Xiao, Pingfan Wu

Page range: 849-850

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C 27 H 60 Cl 2 N 6 O 23 V 6 , C 2/ c (no. 15), a = 26.1482(12) Å, b = 10.6096(4) Å, c = 17.4426(6) Å, β = 90.932(4)°, V = 4838.3(3) Å 3 , Z = 4, R gt ( F ) = 0.0565, wR ref ( F 2 ) = 0.1477, T = 106 K.
Open Access
Crystal structure of bis(μ₃-methanolato-κ³O:O:O)-bis(μ₂-methanolato-κ²O:O)-dimethanol-bis{6,6′-(1,3-dihydroxyl-2-acetylpropane-1,3-diyl)bis(2-chloro-4-bromophenolato)}tetramanganese(III) C₄₀H₄₀Br₄Cl₄Mn₄O₁₆

September 16, 2017

Ji-Xing Zhao, Li Zhao, Fei Wang, Qin-Qin An, Peng-Peng Li

Page range: 851-853

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C 40 H 40 Br 4 Cl 4 Mn 4 O 16 , triclinic, P 1̄, a = 9.3724(9) Å, b = 11.7867(16) Å, c = 12.3994(18) Å, α = 70.650(13)°, β = 75.462(10)°, γ = 81.085(10)°, V = 1247.1(3) Å 3 , Z = 1, R gt ( F ) = 0.0618, wR ref ( F 2 ) = 0.1201, T = 294 K.
Open Access
Synthesis and crystal structure of tetrakis(μ₂-methanolato)-dimethanol-bis(μ₂-2-acetyl-1,3-bis(3,5-dibromo-2-oxidophenyl)propane-1,3-bis(olato)-κ⁵O¹,O²,O³:O³,O⁴,O⁵)tetramanganese(III), C₄₀H₄₀Br₈Mn₄O₁₆

September 16, 2017

Ji-Xing Zhao, Li Zhao, Peng-Peng Li, Zhao-Bin Zhu, Qin-Qin An, Fei Wang

Page range: 855-857

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C 40 H 40 Br 8 Mn 4 O 16 , triclinic, P 1̅, a = 9.3446(11) Å, b = 11.6799(11) Å, c = 12.5833(16) Å, α = 70.937(10)°, β = 76.049(11)°, γ = 80.984(9)°, V = 1255.2(3) Å 3 , Z = 1, R gt ( F ) = 0.0641, wR ref ( F 2 ) = 0.1246, T = 293(2) K.
Open Access
Synthesis and crystal structure tetrakis(μ₂-methanolato)-dimethanol-bis(μ₂-2-acetyl-1,3-bis(3,5-dichloro-2-oxidophenyl)propane-1,3-bis(olato)-κ⁵O¹,O²,O³:O³,O⁴,O⁵), tetramanganese(III), C₄₀H₄₀Cl₈Mn₄O₁₆

September 16, 2017

Ji-Xing Zhao, Li Zhao, Peng-Peng Li, Zhao-Bin Zhu, Fei Wang, Qin-Qin An

Page range: 859-861

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C 40 H 40 Cl 8 Mn 4 O 16 , triclinic, P 1̅, a = 9.2586(5) Å, b = 11.6798(10) Å, c = 12.3267(8) Å, α = 70.237(7)°, β = 75.557(5)°, γ = 81.358(6)°, V = 1211.65(16) Å 3 , Z = 1, R gt ( F ) = 0.0333, wR ref ( F 2 ) = 0.0906, T = 294 K.
Open Access
Crystal structure of bis{5-methoxy-2-((E)-((4-((E)-1-(methoxyimino)ethyl)phenyl)imino)methyl)phenolato-κ²N,O)}copper(II), C₃₄H₃₄CuN₄O₆

September 13, 2017

Ji-Xing Zhao, Li Zhao, Peng-Peng Li, Zhao-Bin Zhu

Page range: 863-865

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C 34 H 34 CuN 4 O 6 , Monoclinic, P 2 1 / c , a = 10.4018(4) Å, b = 6.1634(2) Å, c = 24.2227(15) Å, β = 101.820(5)°, Z = 2, V = 1520.01(13) Å 3 , R gt ( F ) = 0.0565, wR ref ( F 2 ) = 0.1455, T = 292 K.
Open Access
Crystal structure of (E)-1-(2-hydroxy-3-{[2-hydroxybenzylidene]amino}phenyl)ethan-1-one, C₁₅H₁₃NO₃

October 12, 2017

Yu-Hua Yang, Sunday Folaranmi Akogun, Wen-Kui Dong

Page range: 867-868

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C 15 H 13 NO 3 , monoclinic, P 2 1 /c (no. 14) a = 7.5158(6) Å, b = 6.3940(5) Å, c = 25.881(3) Å, β = 93.243(8)°, Z = 4, V = 1241.74(19) Å 3 , R gt ( F ) = 0.0547, wR ref ( F 2 ) = 0.1582, T = 173 K.
Open Access
Crystal structure of bis(μ₂-acetato-κ²O:O′)-bis{μ₂-4-chloro-2-(8-(4-(diethylamino)-2-oxidophenyl)-3,6-dioxa-2,7-diazaocta-1,7-dien-1-yl)phenolato-κ⁶O:O,N,N′,O′′:O′′}tricobalt(II), C₄₄H₄₉Cl₂Co₃N₆O₁₂

September 16, 2017

Yu-Hua Yang, Bao-Jun Wang, Peng-Fei Lan, Wen-Kui Dong

Page range: 869-872

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C 44 H 49 Cl 2 Co 3 N 6 O 12 , Triclinic, P 1̅, a = 9.7415(9) Å, b = 13.6440(14) Å, c = 17.5241(11) Å, α = 72.807(10)°, β = 83.019(9)°, γ = 72.246(9)°, V = 2450.6(5) Å 3 , Z = 2, R gt ( F ) = 0.0700, wR ref ( F 2 ) = 0.1505, T = 291(2) K.
Open Access
Crystal structure of bis{μ₂-2,4-dichloro-6-(8-(4-(diethylamino)-2-oxidophenyl)-3,6-dioxa-2,7-diazaocta-1,7-dien-1-yl)phenolato-κ⁵O:O,N,N′,O′}dicobalt(II) acetone solvate, C₄₃H₄₈Br₄Co₂N₆O₉

October 12, 2017

Shan-Shan Zheng, Jing Hao, Peng-Fei Lan, Xiu-Yan Dong, Wen-Kui Dong

Page range: 873-875

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C 43 H 48 Br 4 Co 2 N 6 O 9 , triclinic, P 1̅, a = 11.9298(7) Å, b = 12.8850(9) Å, c = 17.5241(11) Å, α = 84.854(6)°, β = 85.181(5)°, γ = 65.796(6)°, V = 2443.7(3) Å 3 , Z = 2, R gt ( F ) = 0.0556, wR ref ( F 2 ) = 0.1053, T = 293.51(10) K.
Open Access
Synthesis and crystal structure of bis(μ₂-acetato-κ²O:O′)-bis{μ₂-4-chloro-2-(8-(4-(diethylamino)-2-oxidophenyl)-3,6-dioxa-2,7-diazaocta-1,7-dien-1-yl)phenolato-κ⁶O:O,N,N′,O′:O′}trizinc(II), C₄₄H₄₉C_l2N₆O₁₂Zn₃

October 12, 2017

Li Li, Jing Hao, Peng-Fei Lan, Wen-Kui Dong

Page range: 877-879

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C 44 H 49 Cl 2 N 6 O 12 Zn 3 , monoclinic, P 1̅ (no. 2), a = 9.7387(8) Å, b = 13.7034(12) Å, c = 20.2498(16) Å, α = 72.539(8)°, β = 82.872(7)°, γ = 72.157(8)°, Z = 2, V = 2452.3(4) Å 3 , R gt ( F ) = 0.0604, wR ref ( F 2 ) = 0.1392, T = 293(2) K.
Open Access
Crystal structure of bis{5-(N,N′-diethylamine)-5′-methoxy -2,2′-[ethylenediyldioxybis(nitrilomethylidyne)]diphenolato}-bis(μ₂-acetato-κ²O:O′)trizinc(II), C₄₆H₅₆Zn₃N₆O₁₄

September 16, 2017

Xiu-Yan Dong, Han Zhang, Bai-Jun Wang, Peng-Fei Lan, Wen-Kui Dong

Page range: 881-883

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C 46 H 56 Zn 3 N 6 O 14 , monoclinic, C 2/ c (no. 15), a = 10.6703(7) Å, b = 27.091(4) Å, c = 17.9132(16) Å, β = 96.246(8)°, V = 5147.4(10) Å 3 , Z = 4, R gt ( F ) = 0.0647, wR ref ( F 2 ) = 0.1865, T = 291(1) K.
Open Access
Crystal structure of tris(cyano-(hydrogen tris(3,5-dimethylpyrazolyl)borate))-iron(III) 4-methoxypyridinium monohydrate, C₂₄H₃₂BN₁₀O₂Fe

September 16, 2017

Zhong-Hai Ni, Hao Sun

Page range: 885-887

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C 24 H 32 BN 10 O 2 Fe, orthorhombic, P ca2 1 (no. 29), a = 19.053(4) Å, b = 9.0666(18) Å, c = 16.439(3) Å, V = 2839.8(10) Å 3 , Z = 4, R gt ( F ) = 0.0482, wR ref ( F 2 ) = 0.1194, T = 123(2) K.
Open Access
Synthesis and crystal structure of bis{1-(((4-(1-(hydroxyimino)ethyl)phenyl)imino)methyl)naphthalen-2-olato-κ²O,N}copper(II), C₃₈H₃₀CuN₄O₄

October 16, 2017

Peng-Peng Li, Li Zhao, Ji-Xing Zhao, Zhao-Bin Zhu, Fei Wang, Qin-Qin An

Page range: 889-890

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C 38 H 30 CuN 4 O 4 , triclinic, P 1̅ (no. 2), a = 8.3882(7) Å, b = 8.5024(9) Å, c = 11.3649(15) Å, α = 89.960(10)°, β = 69.689(10)°, γ = 80.269(8)°, Z = 1, V = 747.73(15) Å 3 , R gt ( F ) = 0.0701, wR ref ( F 2 ) = 0.1308, T = 294.68(10) K.
Open Access
Crystal structure of (E)-1-(4-{[(E)-2-Hydroxy-1-naphthalenylmethylene] amino}phenyl)ethanone oxime, C₁₉H₁₆N₂O₂

October 11, 2017

Peng-Peng Li, Li Zhao, Ji-Xing Zhao, Zhao-Bin Zhu

Page range: 891-892

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C 19 H 16 N 2 O 2 , monoclinic P 2 1 /c (no. 14), a = 14.1712(6) Å, b = 7.3611(3) Å, c = 14.4212(8) Å, β = 90.665(5)°, Z = 4, V = 1504.24(12) Å 3 , R gt ( F ) = 0.0633, wR ref ( F 2 ) = 0.1648, T = 291 K.
Open Access
The pseudosymmetric crystal structure of 2-(2-naphthalenyl)-3-nitro-2H-1-benzopyran, C₃₈H₂₆N₂O₆

September 16, 2017

Zhi Hong, Yan-Li Zhan, Dang-Ran Yu, Ying Li, Wen-Jia Yuan, Hong-Yu Zhang

Page range: 893-895

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C 19 H 13 NO 3 , triclinic, P 1̅ (no. 2), a = 9.4457(6) Å, b = 11.0520(7) Å, c = 14.6746(9) Å, α = 100.779(1)°, β = 102.738(1)°, γ = 93.065(1)°, V = 1460.68(16) Å 3 , Z = 4, R gt ( F ) = 0.0410, w R ref ( F 2 ) = 0.0911, T = 291 K.
Open Access
Crystal structure of 2-benzoyl-3-(4-methoxyphenyl)cyclopropane-1,1-dicarbonitrile, C₁₉H₁₄N₂O₂

September 16, 2017

Changming You, Changqing Wang

Page range: 897-898

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C 19 H 14 N 2 O 2 , monoclinic C 2/ c (no. 15), a = 19.8907(8) Å, b = 12.0860(5) Å, c = 15.5260(7) Å, β = 120.588(1)°, V = 3213.06(20) Å 3 , Z = 8, R gt ( F ) = 0.0504, wR ref ( F 2 ) = 0.1426, T = 296 K.
Open Access
N′-(5-ethoxycarbonyl-3,4-dimethyl-pyrrol-2-yl-methylidene)-4-hydroxybenzohydrazide monohydrate, C₁₇H₂₁N₃O₅

September 13, 2017

Pan-Dong Mao, Ling-Ling Yan, Wei-Na Wu, Hong-Xin Cai

Page range: 899-900

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C 17 H 21 N 3 O 5 , monoclinic, P 2 1 / n (no. 14), a = 9.2278(16) Å, b = 15.093(3) Å, c = 12.698(2) Å, β = 105.195(12)°, V = 1706.7(5) Å 3 , Z = 4, R gt ( F ) = 0.0553, wR ref ( F 2 ) = 0.1662, T = 296 K.
Open Access
The crystal structure of carbonyl-[4-(2,4-dichlorophenylamino)pent-3-en-2-onato-κ²N,O]-(triphenylphosphine-κP)rhodium(I), RhC₃₀H₂₅Cl₂NO₂P

October 6, 2017

Gertruida J.S. Venter

Page range: 901-903

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RhC 30 H 25 Cl 2 NO 2 P, orthorhombic P 2 1 2 1 2 1 (no. 19), a = 7.6656(5) Å, b = 16.6097(11) Å, c = 20.9423(14) Å, V = 2666.4(3) Å 3 , Z = 4, R gt ( F ) = 0.0649, wR ref ( F 2 ) = 0.1632, T = 100 K.
Open Access
Crystal structure of (E)-5-(diethylamino)-2-(((1,1,2-trihydroxyethyl)iminio)methyl)phenolate, C₁₅H₂₄N₂O₄

September 16, 2017

Lin Yuan, Zhong-Yan Li, Xian-You Yuan, Min Zhang

Page range: 905-907

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C 15 H 24 N 2 O 4 , orthorhombic, Pca 2 1 , a = 18.528(6) Å, b = 8.123(2) Å, c = 20.797(6) Å, V = 3129.9(16) Å 3 , Z = 8, R gt ( F ) = 0.0396, wR ref ( F 2 ) = 0.1082, T = 296(2) K.
Open Access
Crystal structure of poly[(μ₂-1,4-bis((2-ethyl-1H-benzo[d]imidazol-1-yl)methyl)benzene-κ²N:N′)(μ₂-isophthalato-κ⁴O,O′:O′′,O′′′)cadmium(II)], C₃₄H₃₀N₄O₄Cd

September 13, 2017

Chunying Xu, Wenjuan Chu, Lu Cui, Minghui Li

Page range: 909-911

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C 34 H 30 N 4 O 4 Cd, monoclinic, P 2 1 /c (no. 14), a = 10.382(2) Å, b = 18.102(4) Å, c = 18.449(5) Å, β = 123.32(2)°, V = 2897.3(12) Å 3 , Z = 4, R gt ( F ) = 0.0540, ω R ref ( F 2 ) = 0.1069, T = 293(2) K.
Open Access
Crystal structure of 5,6-Dihydro-9,10-dimethoxybenzo[g]-1,3-benzodioxolo[5,6-a]chinolizinium 3-(4-hydroxyphenyl)-4-oxo-4H-chromen-7-olate - methanol - water (1/1/1), C₃₆H₃₃NO₁₀

September 13, 2017

Benyong Lou, Yali Huang, Guocai Zheng, Qi Lin

Page range: 913-915

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C 36 H 33 NO 10 , monoclinic, P 2 1 / c (no. 14), a = 14.113(7) Å, b = 17.883(9) Å, c = 12.724(7) Å, β = 108.218(9)°, V = 3050(3) Å 3 , Z = 4, R gt ( F ) = 0.0788, wR ref ( F 2 ) = 0.1967, T = 293 K.
Open Access
A single crystal study on 2-(methylcarbamoyl)benzoic acid, C₉H₉NO₃

September 16, 2017

Pengfei Wei, Xiao-Li Yang, Kun-Yan Wang

Page range: 917-918

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C 9 H 9 NO 3 , monoclinic, P 2 1 / c (no. 14), a = 8.7201(8) Å, b = 8.6453(9) Å, c = 11.8083(9) Å, β = 100.830(3)°, V = 874.35(14) Å 3 , Z = 4, R gt ( F ) = 0.0489, wR ref ( F 2 ) = 0.1142, T = 296(2) K.
Open Access
Crystal structure of the salt 1,1′-(ethane-1,2-diyl)bis(1,4-diazabicyclo[2.2.2]octan-1-ium) diperchlorate, C₁₄H₂₈N₄(ClO₄)₂

October 9, 2017

Gao-Ju Wen, Lian-Shuai Gu

Page range: 919-920

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C 14 H 28 N 4 O 8 Cl 2 , monoclinic, P 2 1 / n a = 8.7538(18) Å, b = 11.393(2) Å, c = 9.942(4) Å, β = 97.50(3)°, V = 983.1(5) Å 3 , Z = 2, R gt ( F ) = 0.0706, wR ref ( F 2 ) = 0.2036, T = 293(2) K.
Open Access
Crystal structure of 2,5-bis((E)-2-(trifluoromethyl)benzylidene)cyclopentan-1-one, C₂₁H₁₄F₆O

September 23, 2017

Wenxin Zhang, Chenyu Qiu, Shanshan Li, Lina Zhou, Mengwei Hu, Xiaojing Chen, Bin Yu, Yan Hong, Zhiguo Liu, Qinqin Xia

Page range: 921-922

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C 21 H 14 F 6 O, triclinic, P 1̅ (no. 2), a = 7.8470(16) Å, b = 7.9390(16) Å, c = 14.993(3) Å, α = 83.25(3)°, β = 89.18(3)°, γ = 73.79(3)°, V = 890.5(3) Å, Z = 2, R gt ( F ) = 0.0658, wR ref ( F 2 ) = 0.1261, T = 293 K.
Open Access
Crystal structure of catena-poly[(μ₂-benzene-1,4-dicarboxylato-κ²O:O′)-(1-ethyl-6-fluoro-7-(4-methylpiperazin-1-ium-1-yl)-4-oxo-1,4-dihydroquinoline-3-carboxylato-κ²O,O′)zinc(II)] 1.25 hydrate, C₂₅H_26.5N₃O_8.25FZn

September 13, 2017

Yong-Jun Hu, Lie Jin, Ling Zhu, Tian Zhou

Page range: 923-925

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C 25 H 26.5 N 3 O 8.25 FZn, Triclinic, P 1̅ (no. 2) a = 10.2889(6) Å, b = 10.6034(5) Å, c = 12.9576(8) Å, α = 105.984(5)°, β = 109.785(6)°, γ = 93.257(4)°, V = 1261.05(12) Å 3 , Z = 2, R gt ( F ) = 0.0344, wR ref ( F 2 ) = 0.0783, T = 293 K.
Open Access
Crystal structure of 1-methyl-1,4-diazabicyclo[2.2.2]octan-1-ium poly[aqua-bis(μ₂-perchlorato-κ³O,O′:O′′)sodium], C₇H₁₇Cl₂N₂NaO₉

September 16, 2017

Mei-Ying Liu

Page range: 927-928

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C 7 H 17 Cl 2 N 2 NaO 9 , orthorhombic, Pbca (no. 61), a = 13.907(3) Å, b = 10.927(2) Å, c = 19.194(4) Å, V = 2916.8(10) Å 3 , Z = 8, R gt ( F ) = 0.0472, wR ref ( F 2 ) = 0.1129, T = 298 K.
Open Access
Crystal structure of trimethyammonium 2,6-dicarboxyisonicotinate monohydrate, C₁₁H₁₆N₂O₇

October 20, 2017

Huahui Zeng, Qianjin Shen

Page range: 929-930

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C 11 H 16 N 2 O 7 , orthorhombic, Pnma (no. 62), a = 13.753(3) Å, b = 6.9471(15) Å, c = 13.797(3) Å, V = 1318.2(5) Å 3 , Z = 4, R gt ( F ) = 0.0386, wR ref ( F 2 ) = 0.1650, T = 296 K.
Open Access
Crystal structure of dodecaguanidinium bis(tetrapropylammonium) heptacarbonate, C₄₃H₁₂₈N₃₈O₂₁

September 13, 2017

Xin Zhu, Xianghua Liu

Page range: 931-933

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C 43 H 128 N 38 O 21 , orthorhombic, Pbca (no. 61), a = 19.556(4) Å, b = 20.105(4) Å, c = 20.573(4) Å, V = 8089(3) Å 3 , Z = 4, R gt ( F ) = 0.0592, wR ref ( F 2 ) = 0.1028, T = 296 K.
Open Access
Crystal structure of poly[tetraaqua-bis(μ₆-benzene-1,2,4,5-tetracarboxylato)nickel(II)diyttrium(III)]dihydrate, C₂₀H₁₆NiO₂₂Y₂

September 29, 2017

Chong-Yang Zhao, Dan Zhao, Cong-Kui Nie

Page range: 935-936

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C 20 H 16 NiO 22 Y 2 , monoclinic C 2/ c (no. 15), a = 17.8995(9) Å, b = 7.5278(4) Å, c = 19.9682(10) Å, β = 109.592(1)°, V = 2534.8(2) Å 3 , Z = 4, R gt ( F ) = 0.0298, wR ref ( F 2 ) = 0.0744, T = 296(2) K.
Open Access
Halogen bonds and π–π interactions in the crystal structure of 1,3,5-trifluoro-2,4,6-triiodobenzene–N,N-dimethylformamide (1/1), C₉H₇F₃I₃NO

September 29, 2017

Limin Dang, Jiangnan Yang, Hui Liu, Weizhou Wang

Page range: 937-938

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C 9 H 7 F 3 I 3 NO, monoclinic, P 2 1 / n (no. 14), a = 7.5581(4) Å, b = 20.9303(11) Å, c = 9.3548(5) Å, β = 92.208(5)°, V = 1478.78(13) Å 3 , Z = 4, R gt (F) = 0.0336, w R ref (F 2 ) = 0.0610, T = 290 K.
Open Access
Crystal structure of guanidinium tetraethylammonium carbonate dihydrate, C₁₀H₃₀N₄O₅

October 9, 2017

Xiaokun Li, Linlin Zhu

Page range: 939-940

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C 10 H 30 N 4 O 5 , orthorhombic, Pna 2 1 , a = 18.1934(5) Å, b = 7.25480(10) Å, c = 11.8168(2) Å, V = 1559.69(5) Å 3 , Z = 4, R gt ( F ) = 0.0358, wR ref ( F 2 ) = 0.0978, T = 296 K.
Open Access
The crystal structure of oxonium chlorido-ethylenediaminetetraactetotin(IV) hydrate, C₁₀H₁₇ClN₂O₁₀Sn

October 16, 2017

Zhihai Fu, Bo Chen, Aidang He, Xia Lv, Xin Wei, Xiaojie Feng, Chao Huang, ChuanQin Xia, Yongdong Jin

Page range: 941-942

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C 10 H 17 ClN 2 O 10 Sn, triclinic, P 1 (no. 1), a = 6.6666(3) Å, b = 6.6892(4) Å, c = 8.8779(6) Å, α = 101.340(5)°, β = 99.624(5)°, γ = 91.279(4)°, V = 382.08(4) Å 3 , Z = 1, R gt ( F ) = 0.0318, wR ref ( F 2 ) = 0.0726, T = 294 K.
Open Access
Crystal structure of 8-((E)-((4-((E)-1-((benzyloxy)imino)ethyl)phenyl)imino)methyl)-7-hydroxy-4-methyl-2H-chromen-2-one, C₂₆H₂₂N₂O₄

September 29, 2017

Jing Li, Hao-Ran Jia, Yin-Xia Sun

Page range: 943-945

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C 26 H 22 N 2 O 4 , triclinic P 1̅, a = 8.035(3) Å, b = 10.387(4) Å, c = 13.126(5) Å, α = 83.831(10)°, β = 78.214(10)°, γ = 81.470(10)°, Z = 2, V = 1101.78(19) Å 3 , R gt ( F ) = 0.0663, wR ref ( F 2 ) = 0.1830, T = 296(2) K.
Open Access
Crystal structure of bis{5-(diethylamino)-2-(((2-oxo-2H-chromen-6-yl)imino)methyl)phenolato-κ²O,N}copper(II), C₄₀H₃₈CuN₄O₆

September 20, 2017

Jing Li, Hao-Ran Jia, Yin-Xia Sun

Page range: 947-949

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C 40 H 38 CuN 4 O 6 , monoclinic, P 2 1 / c (no. 14), a = 10.590(4) Å, b = 7.273(3) Å, c = 23.345(9) Å, β = 102.347(7)°, Z = 2, V = 1756.5(12) Å 3 , R gt ( F ) = 0.0682, wR ref ( F 2 ) = 0.2373, T = 296 K.
Open Access
Crystal structure of fac-(acetylacetonato-κ²O,O′)tricarbonyl(tri(p-tolyl)phosphine-κP)rhenium(I), C₂₉H₂₈O₅PRe

September 13, 2017

Amanda-Lee Manicum, Marietjie Schutte-Smith, Hendrik G. Visser

Page range: 951-955

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C 29 H 28 O 5 PRe, triclinic, P 1̄ (no. 2), a = 12.733(7) Å, b = 18.668(11) Å, c = 24.779(15) Å, α = 101.442(20)°, β = 100.844(18)°, γ = 104.240(19)°, V = 5419(9) Å 3 , Z = 8, R gt ( F ) = 0.0307, wR ref ( F 2 ) = 0.0772, T = 100 K.
Open Access
Crystal structure of fac-(acetylacetonato-κ²O,O′)tricarbonyl(benzyldiphenylphosphine-κP)rhenium(I), C₂₇H₂₄O₅PRe

September 16, 2017

Amanda-Lee Manicum, Orbett Alexander, Marietjie Schutte-Smith, Hendrik G. Visser, Andreas Roodt

Page range: 957-959

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C 27 H 24 O 5 PRe, triclinic, P 1̄ (no. 2), a = 9.0305(17) Å, b = 12.084(2) Å, c = 12.403(2) Å, α = 89.688(6)°, β = 70.083(6)°, γ = 76.315(6)°, V = 1232.2(4) Å 3 , Z = 2, R gt ( F ) = 0.0180, wR ref ( F 2 ) = 0.0432, T = 100(2) K.
Open Access
Crystal structure of triethylammonium bis{3-(((3-oxidonaphthalen-1-yl)methylene)amino)-2-oxo-2H-chromen-4-olato-κ³O,N,O′}manganese(III), C₄₆H₃₈MnN₃O₈

October 16, 2017

Jing Li, Hao-Ran Jia, Yin-Xia Sun

Page range: 961-963

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C 46 H 38 MnN 3 O 8 , triclinic P 1̅ (no. 2), a = 8.9705(6) Å, b = 12.0309(8) Å, c = 18.4209(13) Å, α = 96.303(2)°, β = 103.884(2)°, γ = 101.636(2)°, Z = 2, V = 1864.0(2) Å 3 , R gt ( F ) = 0.0496, wR ref ( F 2 ) = 0.1274, T = 296 K.
Open Access
Crystal structure of bis(N,N,N-ethyldimethylethanaminium) bis(heptaselenido-κ²Se¹,Se⁷)palladate(II), C₁₂H₃₂N₂PdSe₁₄

September 16, 2017

Kang-Woo Kim, Di Wang

Page range: 965-967

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C 12 H 32 N 2 PdSe 14 , monoclinic, P 2 1 / n (no. 14), a = 9.2236(9) Å, b = 15.1503(14) Å, c = 12.2198(12) Å, β = 109.683(2)°, V = 1607.8(3) Å 3 , Z = 2, R gt ( F ) = 0.0397, wR ref ( F 2 ) = 0.0958, T = 173 K.
Open Access
Crystal structure of bis(4-(1H-pyrazol-5-yl)pyridine-κ²N:N′)-bis(2-(2-((2,6-difluorophenyl)amino)phenyl)acetate-κO)cadmium(II), C₄₄H₃₄N₈CdCl₄O₄

October 20, 2017

Jin-Bo Guo, Shi-Hui Li

Page range: 969-970

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C 44 H 34 N 8 CdCl 4 O 4 , monoclinic, P 2 1 / c (no. 14), a = 9.7056(2) Å, b = 14.3244(3) Å, c = 15.3626(3) Å, β = 99.7540(10)°, V = 2104.94(7) Å 3 , Z = 2, R gt ( F ) = 0.0271, wR ref ( F 2 ) = 0.0717, T = 296(2) K.
Open Access
Crystal structure of 4,4′-(1,4-phenylene)bis(pyridin-1-ium) catena-poly[diaqua-bis(μ₂-3′,5′-dicarboxy-[1,1′-biphenyl]-2,5-dicarboxylato-κ²O:O′] dihydrate, C₄₈H₄₂O₂₂N₂Ca

October 20, 2017

Dong-Mi Li, Shi-Hui Li

Page range: 971-973

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C 48 H 42 O 22 N 2 Ca, triclinic, P 1̅ (no. 2), a = 7.2548(2) Å, b = 11.7056(4) Å, c = 14.6024(4) Å, α = 72.687(3)°, β = 82.667(2)°, γ = 73.303(3)°, V = 1132.76(6) Å 3 , Z = 1, R gt ( F ) = 0.0403, wR ref ( F 2 ) = 0.0993, T = 293(2) K.
Open Access
The crystal structure of (S)-2-benzylsuccinic acid, C₁₁H₁₂O₄

September 13, 2017

Yun-Peng Zhang, Bing Li

Page range: 975-976

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C 11 H 12 O 4 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 9.960(2) Å, b = 9.960(2) Å, c = 10.967(2) Å, V = 1083.9(4) Å 3 , Z = 4, R gt ( F ) = 0.0505, wR ref ( F 2 ) = 0.1861, T = 293(2) K.
Open Access
Crystal structure of poly[aqua-(μ₃-4-(pyridin-4-yl)isophthalato-κ⁴O,O′:O′′:O′′′)-(μ₂-5-carboxy-2-(pyridin-4-yl)benzoato-κ²O:O′)yttrium(III)], C₂₆H₁₇N₂O₉Y

September 16, 2017

Ying Duan, Jia Zang

Page range: 977-978

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C 26 H 17 N 2 O 9 Y, monoclinic, P 2 1 / n (no. 14), a = 8.9349(7) Å, b = 9.3488(12) Å, c = 28.1854(18) Å, β = 95.061(7)°, V = 2345.2(4) Å 3 , Z = 4, R gt ( F ) = 0.0496, wR ref ( F 2 ) = 0.1248, T = 293(2) K.
Open Access
Crystal structure of ethyl 1-(3,4-dimethylphenyl)-5-methyl-1H-1,2,3-triazole-4-carboxylate, C₁₄H₁₇N₃O₂

October 7, 2017

Iván Brito, Victor Kesternich, Marcia Pérez-Ferhmann, Pilar Narea, Alejandro Cárdenas

Page range: 979-980

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C 14 H 17 N 3 O 2 , monoclinic, P 2 1 / c (no. 14), a = 14.9289(7) Å, b = 7.8070(4) Å, c = 12.4664(7) Å, β = 106.821(4)°, V = 1390.79(13) Å 3 , Z = 4, R gt ( F ) = 0.0646, wR ref ( F 2 ) = 0.1682, T = 293(2) K.
Open Access
Crystal structure of tetrakis(methanol-κO)-bis{μ₂-3-((4-methoxy-2-oxidobenzylidene)amino)-2-oxo-2H-chromen-4-olate-κ⁴O,N;O′:O′}dizinc(II), C₃₈H₃₈Zn₂N₂O₁₄

September 29, 2017

Jing Li, Hao-Ran Jia, Yin-Xia Sun

Page range: 981-983

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C 38 H 38 Zn 2 N 2 O 14 , monoclinic, P 2 1 / n (no. 14), a = 9.6906(6) Å, b = 7.9055(5) Å, c = 24.0501(18) Å, β = 99.878(7)°, Z = 2, V = 1815.1(2) Å 3 , R gt ( F ) = 0.0474, wR ref ( F 2 ) = 0.1143, T = 293 K.
Open Access
Crystal structure of bromido(4,4′-dimethoxy-2,2′-bipyridine-κ²N,N′)(isopropyl(diphenyl)phosphane-κP)copper(I), C₂₇H₂₉BrCuN₂O₂P

September 29, 2017

Mohammed Fettouhi

Page range: 985-986

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C 27 H 29 BrCuN 2 O 2 P, monoclinic, Cc (no. 9), a = 15.5806(10) Å, b = 10.5071(10) Å, c = 16.9748(15) Å, β = 110.729(2)°, V = 2599.0(4) Å 3 , Z = 4, R gt ( F ) = 0.0186 , wR ref ( F 2 ) = 0.0445, T = 120 K.
Open Access
Crystal structure of bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)-9,9-dioctylfluorene, C₄₁H₆₄B₂O₄

October 16, 2017

Yingfan Liu, Kaiming Mao, Xiaochuan Li, Young-A Son

Page range: 987-989

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C 41 H 64 B 2 O 4 , triclinic P 1̅ (no. 2), a = 12.8189(8) Å, b = 13.4808(9) Å, c = 14.1592(12) Å, α = 110.394(3)°, β = 90.170(1)°; γ = 115.623(3)°; V = 2033.5(3) Å 3 , Z = 2, R gt ( F ) = 0.0562, wR ref ( F 2 ) = 0.1629 , T = 296 K.
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Crystal structure of 11-oxo-2,3,6,7-tetrahydro-1H,5H,11H-pyrano[2,3-f]pyrido[3,2,1-ij]quinoline-10-carbaldehyde - a julolidine derivative, C₁₆H₁₅NO₃

September 25, 2017

Yingfan Liu, Kaiming Mao, Xiaochuan Li, Young-A Son

Page range: 991-992

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C 16 H 15 NO 3 , monoclinic, P 2 1 /c (no. 14), a = 9.802(1) Å, b = 14.492(1) Å, c = 9.667(1) Å, β = 112.027(1)°, V = 1272.9 Å 3 , Z = 4, R gt ( F ) = 0.0422, wR ref ( F 2 ) = 0.1249, T = 296 K.
Open Access
Crystal structure of 1,3-dimethyl-5,5-dibenzylbarbituric acid, C₂₀H₂₀N₂O₃

September 29, 2017

Ya-Nan Wei, Chuan-Bi Li, Xue Li, Han-Yang Sun

Page range: 993-994

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C 20 H 20 N 2 O 3 , orthorhombic, Pbca (no. 61), a = 9.1300(18) Å, b = 16.170(3) Å, c = 24.000(5) Å, V = 3543.2(12) Å 3 , Z = 8, R gt ( F ) = 0.1274, wR ref ( F 2 ) = 0.1434, T = 293 K.
Open Access
Crystal structure of bis(N,N,N-trimethylethanaminium) poly[bis(μ₂-heptaselenido-κ²Se¹,Se⁷)palladate(II)], C₁₀H₂₈N₂PdSe₁₄

September 29, 2017

Di Wang, Hoseop Yun, Kang-Woo Kim

Page range: 995-997

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C 10 H 28 N 2 PdSe 14 , monoclinic, P 2 1 /c (no. 14), a = 9.4146(7) Å, b = 14.3446(11) Å, c = 12.4731(9) Å, β = 113.403(2)°, V = 1545.9(2) Å 3 , Z = 2, R gt ( F ) = 0.0510, wR ref ( F 2 ) = 0.1446, T = 293 K.
Open Access
Crystal structure of 1-{4-[(5-Chloro-2-hydroxy-benzylidene)amino]phenyl} ethanone O-ethyl-oxime, C₁₇H₁₇ClN₂O₂

October 16, 2017

Ji-Xing Zhao, Li Zhao, Guo-Hua Liu, Peng-Peng Li, Zhao-Bin Zhu

Page range: 999-1001

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C 17 H 17 ClN 2 O 2 , monoclinic, Pc (no. 7), a = 17.789(2) Å, b = 7.1127(7) Å, c = 6.2885(6) Å, β = 97.513(10)°, Z = 2, V = 788.83(15) Å 3 , R gt ( F ) = 0.0600, wR ref ( F 2 ) = 0.1651, T = 290.83(10) K.
Open Access
The crystal structure of methyl N-(4-bromophenyl)carbamate, C₈H₈BrNO₂

September 16, 2017

Zbigniew Karczmarzyk, Monika Pitucha, Waldemar Wysocki, Maja Morawiak, Karolina Sobótka-Polska, Zofia Urbańczyk-Lipkowska

Page range: 1003-1004

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C 8 H 8 BrNO 2 , orthorhombic, Pbca (no. 61), a = 10.1313(3) Å, b = 8.5416(4) Å, c = 20.4597(7) Å, V = 1770.53(12) Å 3 , Z = 8, R gt ( F ) = 0.0394, wR ref ( F 2 ) = 0.1214, T = 296 K.
Open Access
Synthesis and crystal structure of 1-{4-[(2-hydroxy-benzylidene)amino]phenyl}ethanone oxime, C₁₅H₁₄N₂O₂

October 16, 2017

Peng-Peng Li, Li Zhao, Guo-Hua Liu, Ji-Xing Zhao, Zhao-Bin Zhu

Page range: 1005-1006

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C 15 H 14 N 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 13.5809(12) Å, b = 9.7794(14) Å, c = 9.8883(9) Å, β = 97.972(9)°, Z = 4, V = 1300.6(3) Å 3 , R gt ( F ) = 0.0635, wR ref ( F 2 ) = 0.1758, T = 291(2) K.
Open Access
Crystal structure of 1,1′-butanebis(3-methyl-1H-imidazol-3-ium)bis(hexafluorophosphate), C₁₂H₂₀F₁₂N₄P₂

September 29, 2017

Xiong Wan-Ming, Chen Jing, Peng Da-Yong, Nie Xu-Liang, Chang-gan Huang

Page range: 1007-1008

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C 12 H 20 F 12 N 4 P 2 , triclinic, P 1̅ (no. 2), a = 7.388(4) Å, b = 8.499(4) Å, c = 9.347(4) Å, α = 90.198(5)°, β = 106.496(5)°, γ = 113.042(5)°, V = 513.4(4) Å 3 , Z = 1, R gt ( F ) = 0.0652, wR ref ( F 2 ) = 0.2037, T = 296(2) K.
Open Access
(E)-N-benzylidene-3-(benzylthio)-5-p-tolyl-4H-1,2,4-triazol-4-amine, C₂₃H₂₀N₄S

September 16, 2017

Qichun Ding, Shudong Dai, Hongxu Guo, Li-Xue Zhang

Page range: 1009-1010

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C 23 H 20 N 4 S, Monoclinic, P 2 1 / n (no. 14), a = 11.439(3) Å, b = 8.868(2) Å, c = 20.557(5) Å, β = 104.542(4)°, V = 2018.7(8) Å 3 , Z = 4, R gt ( F ) = 0.0449, wR ref ( F 2 ) = 0.1266, T = 298(2) K.
Open Access
Crystal structure of ethyl 5-methyl-1-(pyridin-3-yl)-1H-1,2,3-triazole-4-carboxylate, C₁₁H₁₂N₄O₂

October 6, 2017

Iván Brito, Victor Kesternich, Marcia Pérez-Fehrmann, Catherine Araneda, Alejandro Cárdenas

Page range: 1011-1012

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C 11 H 12 N 4 O 2 , monoclinic, P 2 1 / c (no. 14), a = 12.0258(15) Å, b = 8.0563(10) Å, c = 12.4478(13) Å, β = 104.157(4)°, V = 1169.4(2) Å 3 , Z = 4, R gt ( F ) = 0.0619, wR ref ( F 2 ) = 0.1616, T = 293(2) K.
Open Access
Crystal structure of 5,5-difluoro-10-(4-fluorophenyl)-1,3,7,9-tetramethyl-5H-4l4,5l4-dipyrrolo[1,2-c:2′,1′-f][1,3,2]diazaborinine - a Z′ = 3 structure, C₁₉H₁₈B₂F₃N₂

October 16, 2017

Yingfan Liu, Ming Yan, Xiaochuan Li, Yajuan Li, Young-A Son

Page range: 1013-1015

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C 19 H 18 B 2 F 3 N 2 , triclinic, P 1̅ (no. 2), a = 10.8885(6) Å, b = 13.9767(8) Å, c = 18.1330(10) Å, α = 79.3484(19)°, β = 86.2213(9)°; γ = 73.461(2)°; V = 2599.6(3) Å 3 , Z = 6, R gt ( F ) = 0.0450, wR ref ( F 2 ) = 0.1105, T = 296 K.
Open Access
The crystal structure of the Matrine derivative: 12-(1H-indol-1-yl)dodecahydro-1H,5H,10H-dipyrido[2,1-f:3′,2′,1′-ij][1,6]naphthyridin-10-one hydrate, C₂₃H₂₉N₃O

October 9, 2017

Cheng Xing-An, Liu Zhan-Mei, Liang Wei-Xin, Wu Bo, Jiang Xu-Hong

Page range: 1017-1019

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C 23 H 29 N 3 O, orthorhombic P 2 1 2 1 2 1 (no. 19), a = 8.62130(10) Å, b = 18.25770(10) Å, c = 25.6873(2) Å, V = 4043.31(6) Å 3 , Z = 8, R gt ( F ) = 0.0305, wR ref ( F 2 ) = 0.0807, T = 293(2) K.
Open Access
The crystal structure of tris(μ₂-1,3-bis(4,4,4-trifluoro-3-oxido-1-(oxo)but-2-en-1-yl)phenyl-κ⁴O,O′:O′′,O′′′)-bis(1,2-dimethoxyethane-κ²O,O′)dilutetium(III), C₅₀H₃₈F₁₈Lu₂O₁₆

October 16, 2017

WeiCan Zhao, Jing Shi, YanJun Hou

Page range: 1021-1022

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C 50 H 38 F 18 Lu 2 O 16 , monoclinic, C 2/ c (no. 15), a = 15.7024(12) Å, b = 12.6169(10) Å, c = 29.715(2) Å, β = 91.919(10)°, V = 5883.7(8) Å 3 , Z = 4, R gt ( F ) = 0.0273, wR ref ( F 2 ) = 0.066, T = 273 K.
Open Access
The crystal structure of (Z)-2-(3-(2-(4-chlorobenzoyl)hydrazono)-2-oxoindolin-1-yl) acetic acid, C₁₇H₁₂ClN₃O₄

September 29, 2017

Su Wang, Han-Yu Liu, Juan Sun

Page range: 1023-1024

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C 17 H 12 ClN 3 O 4 , monoclinic, P 2 1 /c (no. 14), a = 6.8425(7) Å, b = 14.1931(16) Å, c = 17.0132(17) Å, β = 101.044(3)°, V = 1621.1(3) Å 3 , Z = 4, R gt ( F ) = 0.0522, wR ref ( F 2 ) = 0.1171, T = 296 K.
Open Access
Synthesis and crystal structure of trans-tetraqua-bis(2-(((7-hydroxy-3-(4-hydroxy-3-sulfonatophenyl)-4-oxo-4H-chromen-8-yl)methyl)ammonio)acetato-κO)cobalt(II) hexahydrate, C₃₆H₄₈CoN₂O₂₈S₂

October 16, 2017

Hai-Lin Chen, Hong-Fang Lai, Lian-Qiang Wei, Li-Rong Jiang, Yan-Xiang Su

Page range: 1025-1027

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C 36 H 48 CoN 2 O 28 S 2 , monoclinic, P 2 1 / c (no. 14), a = 18.2239(13) Å, b = 7.1282(6) Å, c = 17.8550(13) Å, β = 97.883(2)°, V = 2297.5(3) Å 3 , Z = 2, R gt ( F ) = 0.0906, wR ref ( F 2 ) = 0.1998, T = 293(2) K.
Open Access
The crystal structure of N,N-dimethyl-2,6-di-p-tolylpyrimidin-4-amine, C₂₀H₂₁N₃

September 16, 2017

Zhi-Mao Zhang, Lian-Hui Chen

Page range: 1029-1030

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C 20 H 21 N 3 , Orthorhombic, Pbca , a = 12.2422(16) Å, b = 7.1996(10) Å, c = 39.037(5) Å, V = 3440.6(8) Å 3 , Z = 8, R gt ( F ) = 0.0686, wR ref ( F 2 ) = 0.1723, T = 293(2) K.
Open Access
The crystal structure (E)-4-methyl-N′-(2-nitrobenzylidene)benzenesulfonohydrazide, C₁₄H₁₃N₃O₄S

October 12, 2017

Tai Xi-Shi, Li Peng-Fei

Page range: 1031-1032

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C 14 H 13 N 3 O 4 S, triclinic, P 1̅ (no. 2), a = 5.6735(11) Å, b = 10.509(2) Å, c = 12.180(2) Å, α = 93.76(3)°, β = 95.11(3)°, γ = 98.13(3)°, V = 713.8(2) Å 3 , Z = 2, R gt ( F ) = 0.0446, wR ref ( F 2 ) = 0.1179, T = 293(2) K.
Open Access
Crystal structure of catena-poly[(μ₂-1,3-bis(benzimidazol-1-yl)propane κ²N:N′)-(μ₂-5-methoxyisophthalato-κ²O:O′)zinc(II)] hydrate, C₂₆H₂₄ZnN₄O₆

October 20, 2017

Zhan Zhou, Zhe Zhou, Peng-Jing Jing

Page range: 1033-1035

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C 26 H 24 ZnN 4 O 6 , triclinic, P 1̅ (no. 2), a = 9.724(3) Å, b = 10.173(3) Å, c = 14.642(4) Å, α = 70.380(3)°, β = 85.642(4)°, γ = 63.925(3)°, V = 1221.2(6) Å 3 , Z = 2, R gt ( F ) = 0.0411, wR ref ( F 2 ) = 0.0981, T = 296 K.
Open Access
The crystal structure of (E)-N′-(quinolin-2-ylmethylene)furan-2-carbohydrazide monohydrate, C₁₅H₁₃N₃O₃

October 20, 2017

Wang Li-Hua, Tai Xi-Shi

Page range: 1037-1038

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C 15 H 13 N 3 O 3 , triclinic, P 1̅, a = 6.4662(13) Å, b = 7.1213(14) Å, c = 15.373(3) Å, α = 80.09(3)°, β = 88.40(3)°, γ = 74.81(3)°, V = 672.9(3) Å 3 , Z = 2, R gt ( F ) = 0.0503, wR ref ( F 2 ) = 0.1572, T = 293(2) K.
Open Access
Crystal structure of 2,8-diphenyl-3,7,9-trioxa-1-azaspiro[4.5]dec-1-ene, C₁₈H₁₇N₁O₃

October 16, 2017

Min Zhang, Zhong-Yan Li, Xian-You Yuan, Lin Yuan

Page range: 1039-1040

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C 18 H 17 N 1 O 3 , monoclinic, P 2 1 / c (no. 14), a = 14.9752(8) Å, b = 9.0793(5) Å, c = 11.1030(6) Å, β = 106.431(1)°, V = 1447.96(14) Å 3 , Z = 4, R gt ( F ) = 0.0342, wR ref ( F 2 ) = 0.0903, T = 296(2) K.
Open Access
Crystal structure of diethyl 2-(4-chlorophenyl)-1,3-dioxane-5,5-dicarboxylate, C₁₆H₁₉ClO₆

October 20, 2017

Xian-You Yuan, Min Zhang, Lin Yuan, Zhong-Yan Li

Page range: 1041-1042

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C 16 H 19 ClO 6 , triclinic, P 1̅ (no. 2), a = 7.905(3) Å, b = 9.194(4) Å, c = 13.094(5) Å, α = 99.928(4)°, β = 105.341(4)°, γ = 109.283(4)°, V = 830.2(6) Å 3 , Z = 2, R gt ( F ) = 0.0343, wR ref ( F 2 ) = 0.0898, T = 296(2)K.
Open Access
Crystal structure of 1-(carboxymethyl)-1H-benzo[d][1,2,3]triazole 3-oxide, C₈H₇N₃O₃

October 12, 2017

Minxia Yu

Page range: 1043-1044

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C 8 H 7 N 3 O 3 , monoclinic, P 2 1 / c (no. 14), a = 7.2526(12) Å, b = 10.0770(18) Å, c = 11.906(2) Å, β = 104.393(3)°, V = 842.8(2) Å 3 , Z = 4, R gt ( F ) = 0.0375, wR ref ( F 2 ) = 0.0766, T = 293 K.
Open Access
Crystal structure of (acetylacetonato-κ²O,O′)-(2-amino-6-chlorobenzoato-κO)-oxido(1,10-phenanthroline-κ²N,N′)vanadium(IV) – trichloromethane (1/1)

October 12, 2017

Ning Yin, Qiong Wu, Heng-Qiang Zhang, Qi-Ying Zhang

Page range: 1045-1047

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C 25 H 21 Cl 4 N 3 O 5 V, triclinic, P 1̅ (no. 2), a = 10.8055(5) Å, b = 11.5657(6) Å, c = 12.0494(6) Å, α = 78.058(1)°, β = 80.405(2)°, γ = 69.388(1)°, V = 1371.69(12) Å 3 , Z = 2, R gt ( F ) = 0.0549, wR ref ( F 2 ) = 0.1673, T = 295(2) K.
Open Access
Crystal structure of (1E,4E)-1,5-bis(4-chlorophenyl)penta-1,4-dien-3-one, C₁₇H₁₂Cl₂O

October 12, 2017

Marole M. Maluleka, Malose J. Mphahlele

Page range: 1049-1050

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C 17 H 12 Cl 2 O, monoclinic, P 2 1 / c , a = 17.2845(14) Å, b = 14.2007(11) Å, c = 5.8795(5) Å, β = 99.088(3)°, V = 1425.0(2) Å 3 , Z = 4, R gt ( F ) = 0.0567, wR ref ( F 2 ) = 0.1395, T = 263 K.
Open Access
The crystal structure of trans-dibromido-bis(pyridine-κN)platinum(II), C₁₀H₁₀Br₂N₂Pt

October 16, 2017

Kwang Ha

Page range: 1051-1052

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C 10 H 10 Br 2 N 2 Pt, triclinic, P 1̄ (no. 2), a = 5.6590(9) Å, b = 7.0204(12) Å, c = 7.7623(11) Å, α = 79.262(5)°, β = 84.603(4)°, γ = 88.928(5)°, V = 301.64(8) Å 3 , Z = 1, R gt ( F ) = 0.0440, wR ref ( F 2 ) = 0.0946, T = 223 K.

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