Volume 233, Issue 5

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Zeitschrift für Kristallographie - New Crystal Structures

Contents

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Cover and Frontmatter

August 24, 2018

Page range: i-viii

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Open Access
Crystal structure of 2-amino-4-(2,4-dinitrophenyl)-3-cyano-7,7-dimethyl-5-oxo-4H-5,6,7,8-tetrahydrobenzo-pyran, C₁₈H₁₆N₄O₆

June 18, 2018

Li-Jing Cui, Bin Zhang, Chun-Yan Liu, Ming Bian

Page range: 753-754

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C 18 H 16 N 4 O 6 , monoclinic, C 2/ c (no. 15), a = 28.3976(19) Å, b = 10.5649(7) Å, c = 12.1155(10) Å, β = 97.662(7)°, V = 3602.4(5) Å 3 , Z = 8, R gt ( F ) = 0.0470, wR ref ( F 2 ) = 0.1247, T = 293(2) K.
Open Access
Crystal structure of catena-poly[(μ₃-5-carboxy-2-(pyridin-4-yl)benzoato-κ⁵O,O′:O′′,O′′′:O′′′)(1,10-phenanthroline-κ²N,N′)cadmium(II)], C₁₀₀H₆₀N₁₂O₁₆Cd₄

June 20, 2018

Wei Song, Xue-Li Xu, Yan-Ju Yang, Shi-Hui Li

Page range: 755-756

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C 100 H 60 N 12 O 16 Cd 4 , monoclinic, I 2/ a (no. 15), a = 21.2654(5) Å, b = 11.1493(3) Å, c = 17.3039(4) Å, β = 97.774(2)°, V = 4064.96(18) Å 3 , Z = 2, R gt ( F ) = 0.0213, wR ref ( F 2 ) = 0.0559, T = 289.23(10) K.
Open Access
Crystal structure of 2-amino-4-(3,4,5-trimethoxy-phenyl)-7-methyl-5-oxo-4H,5H-pyrano[4,3-b]pyran-3-carbonitrile, C₁₉H₁₈N₂O₆

July 13, 2018

Jing He

Page range: 757-758

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C 19 H 18 N 2 O 6 , monoclinic, P 2 1 / c (no. 14), a = 13.052(8) Å, b = 10.091(6) Å, c = 14.454(9) Å, β = 114.446(11)°, V = 1733.0(19) Å 3 , Z = 4, R gt ( F ) = 0.0490, wR ref ( F 2 ) = 0.1518, T = 296(2) K.
Open Access
Crystal structure of 1-{4-[(2-hydroxy-5-methyl benzylidene)amino]phenyl}ethanone O-ethyl-oxime, C₁₈H₂₀N₂O₂

June 13, 2018

Peng-Peng Li, Jin-Xia Ma, Qing-Lin Li, Ji-Xing Zhao, Li Zhao

Page range: 759-761

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C 18 H 20 N 2 O 2 , monoclinic, Pc (no. 7), a = 17.8843(15) Å, b = 7.1821(6) Å, c = 6.3086(6) Å, β = 98.487(3)°, Z = 2, V = 801.45(12) Å 3 , R gt ( F ) = 0.0533, wR ref ( F 2 ) = 0.1411, T = 296(2) K.
Open Access
Crystal structure of bis{4-methyl-2-((E)-((4-((E)-1-(ethoxyimino)ethyl)phenyl)imino)methyl)phenolato-κ²N,O)}copper(II), C₃₆H₃₈CuN₄O₄

June 13, 2018

Peng-Peng Li, Qing-Lin Li, Jin-Xia Ma, Ji-Xing Zhao, Li Zhao

Page range: 763-765

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C 36 H 38 CuN 4 O 4 , triclinic, P 1̄, a = 8.492(2) Å, b = 9.574(2) Å, c = 10.512(2) Å, α = 100.170(7)°, β = 103.421(7)°, γ = 95.055(8)°, Z = 1, V = 810.8(3) Å 3 , R gt ( F ) = 0.0418, wR ref ( F 2 ) = 0.1193, T = 296(2) K.
Open Access
Crystal structure of bis{5-methoxy-2-((E)-((4-((E)-1-(methoxyimino)ethyl)phenyl)imino)methyl)phenolato-κ²N,O}nickel(II), C₃₄H₃₄N₄NiO₆

June 15, 2018

Jin-Xia Ma, Qing-Lin Li, Peng-Peng Li, Ji-Xing Zhao, Li Zhao

Page range: 767-769

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C 34 H 34 N 4 NiO 6 , monoclinic, P 2 1 / c (no. 14), a = 10.5538(5) Å, b = 6.1691(2) Å, c = 24.2831(9) Å, β = 100.519(4)°, Z = 2, V = 1554.43(11) Å 3 , R gt ( F ) = 0.0402, wR ref ( F 2 ) = 0.0973, T = 294.39(10) K.
Open Access
Crystal structure of poly[μ₈-3-carboxyphthalat-κ⁸-O:O¹,O¹,O¹:O²:O³,O³:O⁴)silver(I)], C₉H₄Ag₂O₆

July 20, 2018

Xue-Guo Liu, Wei-Hong Yan, Xiao-Jing Xing, Hui-Tao Fan, Zhen-Zhen Shi

Page range: 771-772

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C 9 H 4 Ag 2 O 6 , monoclinic, P 2 1 / c (no. 14), a = 13.8224(6) Å, b = 9.5222(4) Å, c = 7.2104(3) Å, β = 101.991(4)°, V = 928.32(7) Å 3 , Z = 4, R gt ( F ) = 0.0239, wR ref ( F 2 ) = 0.0411, T = 293(2) K.
Open Access
Crystal structure of 2-((E)-((4-((E)-1-(hydroxyimino)ethyl)phenyl)iminio)methyl)-5-methoxyphenolate, C₁₆H₁₆N₂O₃

June 13, 2018

Peng-Peng Li, Jin-Xia Ma, Qing-Lin Li, Ji-Xing Zhao, Li Zhao

Page range: 773-775

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C 16 H 16 N 2 O 3 , triclinic, P 1̄ (no. 2), a = 8.7904(7) Å, b = 12.0808(11) Å, c = 14.3999(11) Å, α = 68.001(8)°, β = 81.114(6)°, γ = 83.933(7)°, Z = 4, V = 1398.9(2) Å 3 , R gt ( F ) = 0.0658, wR ref ( F 2 ) = 0.1827, T = 290.83(10) K.
Open Access
Crystal structure of (E)-1-(4-(((E)-2-hydroxy-3-methoxybenzylidene)amino)phenyl)ethan-1-one oxime, C₁₆H₁₆N₂O₃

June 15, 2018

Peng-Peng Li, Jin-Xia Ma, Qing-Lin Li, Ji-Xing Zhao, Li Zhao

Page range: 777-778

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C 16 H 16 N 2 O 3 , monoclinic, P 2 1 / c (no. 14), a = 12.929(13) Å, b = 11.966(12) Å, c = 9.742(9) Å, β = 107.449(19)°, Z = 4, V = 1438(2) Å 3 , R gt ( F ) = 0.0515, wR ref ( F 2 ) = 0.1767, T = 296(2) K.
Open Access
The crystal structure of 2-(tert-butyl)-4-chloro-6-phenyl-1,3,5-triazine, C₁₃H₁₄Cl₁N₃

June 21, 2018

Xiao Song, Zhishu Tang, Zhenyu Zuo, Jinao Duan

Page range: 779-781

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C 13 H 14 Cl 1 N 3 , orthorhombic, Pma 2 (no. 28), a = 6.7623(2) Å, b = 21.1431(6) Å, c = 8.8708(2) Å, Z = 4, V = 1268.31(6) Å 3 , R gt ( F ) = 0.0362, wR ref ( F 2 ) = 0.0969, T = 200(2) K.
Open Access
Crystal structure of (6,6′-(((((2-aminoethyl)azanediyl)bis(ethane-2,1-diyl))bis(azanylylidene))bis(methanylylidene))bis(2,4-dichlorophenolato)-κ⁶N,N′,N′′,N′′′,O,O′)cadmium(II) – ethanol – water (1/1/1), C₂₂H₂₈CdCl₄N₄O₄

June 27, 2018

Zong-Li Ren, Ling-Zhi Liu, Yang Zhang, Wen-Kui Dong

Page range: 783-785

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C 22 H 28 CdCl 4 N 4 O 4 , monoclinic, C 2/ c (no. 15), a = 18.5053(5) Å, b = 13.0864(4) Å, c = 23.0284(9) Å, β = 102.367(3)°, V = 5447.4(3) Å 3 , Z = 8, R gt ( F ) = 0.0457, wR ref ( F 2 ) = 0.1306, T = 290.7(2) K.
Open Access
Crystal structure of 6-chloro-N-methylpyrimidin-4-amine, C₅H₆ClN₃

June 15, 2018

Dongmi Li, Tingting Wang, Lin Geng

Page range: 787-788

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C 5 H 6 ClN 3 , monoclinic, P 2 1 / c (no. 14), a = 3.8335(2) Å, b = 11.1158(7) Å, c = 15.4294(7) Å, β = 94.901(5)°, V = 655.07(6) Å 3 , Z = 4, R gt ( F ) = 0.0388, wR ref ( F 2 ) = 0.0960, T = 293 K.
Open Access
Synthesis and crystal structure of bis{((E)-((4-((E)-1-(methoxyimino)ethyl)phenyl)imino)methyl)-2-naphtholato-κ²N,O}nickel(II), C₄₀H₃₄N₄NiO₄

June 13, 2018

Jin-Xia Ma, Qing-Lin Li, Peng-Peng Li, Ji-Xing Zhao, Li Zhao

Page range: 789-791

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C 40 H 34 N 4 NiO 4 , monoclinic, P 2 1 / c (no. 14), a = 21.443(7) Å, b = 13.862(5) Å, c = 11.733(4) Å, β = 103.690(5)°, Z = 4, V = 3388(2) Å 3 , R gt ( F ) = 0.0484, wR ref ( F 2 ) = 0.1411, T = 296(2) K.
Open Access
Crystal structure of (E)-2-(4-bromophenyl)ethenesulfonyl fluoride (C₈H₆BrFO₂S)

July 13, 2018

Mzilikazi Khumalo, Marivel Samipillai, Thavendran Govender, Hendrick Gert Kruger, Tricia Naicker

Page range: 793-794

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C 8 H 6 BrFO 2 S, monoclinic, P 2 1 / m (no. 11), a = 4.7846(2) Å, b = 9.6099(4) Å, c = 10.3260(4) Å, β = 103.137(1)°, V = 462.36(3) Å 3 , Z = 2, R gt ( F ) = 0.0193, wR ref ( F 2 ) = 0.0502, T = 100(2) K.
Open Access
Synthesis and crystal structure of 2,2′-ethylenedioxybis(benzimide)-2,2′-bis[O-(1-propyloxyamide)]oxime-4,4′,6,6′-tetrachlorodiphenol, C₃₆H₃₄Cl₄N₄O₈

June 13, 2018

Zong-Li Ren, Zhi-Li Wei, Lan Wang, Jian-Chun Ma, Wen-Kui Dong

Page range: 795-797

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C 36 H 34 Cl 4 N 4 O 8 , monoclinic, C 2/ c (no. 15), a = 33.048(10) Å, b = 6.4688(7) Å, c = 24.301(7) Å, β = 133.30(5)°, Z = 4, V = 3781(3) Å 3 , R gt ( F ) = 0.0477, wR ref ( F 2 ) = 0.1016, T = 293(2) K.
Open Access
Crystal structure of bis(N-(1-(pyrazin-2-yl)ethylidene)nicotinohydrazonato-κ³N,N′,O)cadmium(II) – methanol (1/1), C₂₆H₂₈N₁₀O₄Zn

June 29, 2018

Ning Zhang, Meijie Su, Gaoyuan Xu, Huijun Li

Page range: 799-800

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C 26 H 28 N 10 O 4 Zn, monoclinic, C 2/ c (no. 15), a = 14.507(4) Å, b = 16.776(5) Å, c = 12.151(3) Å, β = 108.596(4)°, V = 2802.8(13) Å 3 , Z = 4, R gt ( F ) = 0.0258, wR ref ( F 2 ) = 0.0719, T = 293(2) K.
Open Access
Crystal structure of diaqua-(N-(1-(pyrazin-2-yl)ethylidene)nicotinohydrazonato-κ³N,N′,O)-bis(nitrato-κ²O,O′)samarium(III), C₁₂H₁₄N₇O₉Sm

July 7, 2018

Xianjie Mao, Chuntong Li, Gaoyuan Xu, Huijun Li

Page range: 801-802

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C 12 H 14 N 7 O 9 Sm, monoclinic, P 2 1 / c (no. 14), a = 16.770(3) Å, b = 7.7185(16) Å, c = 15.165(3) Å, β = 108.409(3)°, V = 1862.5(7) Å 3 , Z = 4, R gt ( F ) = 0.0262, wR ref ( F 2 ) = 0.0672, T = 296(2) K.
Open Access
Crystal structure of hexaaqua-{(E)-N′-(1-(pyrazin-2-yl)ethylidene)isonicotinohydrazide-κ³N,N′,O}praseodym(III) trichloride monohydrate, C₁₂H₂₅Cl₃N₅O₈Pr

July 7, 2018

Lingling Yan, Peng Yang, Guanghui Zhi

Page range: 803-804

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C 12 H 25 Cl 3 N 5 O 8 Pr, triclinic, P 1̄ (no. 2), a = 9.4800(10) Å, b = 9.9591(12) Å, c = 12.4897(143) Å, α = 88.855(2)°, β = 76.897(2)°, γ = 89.182(2)°, V = 1148.2(2) Å 3 , Z = 2, R gt ( F ) = 0.0372, wR ref ( F 2 ) = 0.0918, T = 296(2) K.
Open Access
Crystal structure of methyl 4-(3-cyanophenyl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydro-quinoline-3-carboxylate, C₂₁H₂₂N₂O₃

June 29, 2018

Qing-Hua Meng, Xu Long, Jing-Li Liu, Shuan Zhang, Guang-Hui Zhang

Page range: 805-806

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C 21 H 22 N 2 O 3 , orthorhombic, Pbcn (no. 60), a = 15.093(2) Å, b = 13.896(2) Å, c = 17.501(2) Å, V = 3670.5(8) Å 3 , Z = 8, R gt ( F ) = 0.0446, wR ref ( F 2 ) = 0.1208, T = 293(2) K.
Open Access
Crystal structure of ethyl 2-amino-4-(2-methoxyphenyl)-5-oxo-4H,5H-pyrano[3,2-c]chromene-3-carboxylate, C₂₂H₁₉NO₆

June 29, 2018

Ning Wang, Yu-Hang Liu, Ming-Lei Gao, Ye Zhao, Ping Wen

Page range: 807-808

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C 22 H 19 NO 6 , monoclinic, P 2 1 / n (no. 14), a = 9.055(3) Å, b = 17.601(6) Å, c = 11.817(4) Å, β = 91.361(5)°, V = 1882.8(11) Å 3 , Z = 4, R gt ( F ) = 0.0368, wR ref ( F 2 ) = 0.1038, T = 296(2) K.
Open Access
Crystal structure of 2,12-dibromo-5,15-dihexyl-5,15-dihydrobenzo [1,2-b:5,6-c′]dicarbazole, C₃₈H₃₈Br₂N₂

June 30, 2018

Ying Feng, Wei Guo, Zhi Liu, Xinyu Luo, Dingchao Zhang, Li Li, Zhenhao Hu

Page range: 809-811

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C 38 H 38 Br 2 N 2 , triclinic, P 1̄, a = 8.2069(11) Å, b = 11.9435(15) Å, c = 16.817(2) Å, α = 90.119(1)°, β = 97.992(1)°, γ = 106.995(1)°, V = 1559.5(4) Å 3 , Z = 2, R gt ( F ) = 0.0300, wR ref ( F 2 ) = 0.1025, T = 130(2) K.
Open Access
Crystal structure of ethyl 2-amino-4-(3-hydroxy-4-methoxyphenyl)-5-oxo-4H,5H-pyrano[3,2-c]chromene-3-carboxylate, C₂₂H₁₉NO₇

June 27, 2018

Ning Wang, Yu-Hang Liu, Da-Wei Liu, Ye Zhao, Ping Wen

Page range: 813-814

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C 22 H 19 NO 7 , monoclinic, P 2 1 / c (no. 14), a = 9.292(5) Å, b = 13.230(3) Å, c = 17.115(4) Å, β = 106.04(5)°, V = 2022.1(14) Å 3 , Z = 4, R gt ( F ) = 0.0441, wR ref ( F 2 ) = 0.1156, T = 293(2) K.
Open Access
Crystal structure of ethyl 2-amino-4-(3,4-dimethylphenyl)-5-oxo-4H,5H-pyrano[3,2-c] chromene-3-carboxylate, C₂₃H₂₁NO₅

June 27, 2018

Xue-Kun Liu, Xiao-Yu Geng, Meng Zhang, Bai-Jun Ye, Zhan Shi, Yan-Qiu Wang

Page range: 815-816

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C 23 H 21 NO 5 , monoclinic, P 2 1 / c (no. 14), a = 15.829(11) Å, b = 8.294(6) Å, c = 14.718(10) Å, β = 93.339(12)°, V = 1929(2) Å 3 , Z = 4, R gt ( F ) = 0.073, wR ref ( F 2 ) = 0.206, T = 296(2) K.
Open Access
Crystal structure of 2-hydroxy-N′-(pyrimidin-2-yl)benzohydrazide, C₁₁H₁₀N₄O₂

June 27, 2018

Juan Yuan, Ai-Ping Xing, Di Cheng

Page range: 817-818

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C 11 H 10 N 4 O 2 , monoclinic P 2 1 / c (no. 14), a = 6.6161(7) Å, b = 24.064(2) Å, c = 7.1768(9) Å, β = 115.463(15)°, Z = 4, V = 1031.6(2) Å 3 , R gt ( F ) = 0.0412, wR ref ( F 2 ) = 0.0953, T = 173(2) K.
Open Access
Crystal structure of 2-(3,4-dimethylphenyl)-1,8-naphthyridine, C₁₆H₁₄N₂

June 20, 2018

Guo-Kai Jia, Xiao-Ming Chen, Fu-Lin He, Xiu-Wen Chen, Zong-Cheng Wang

Page range: 819-820

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C 16 H 14 N 2 , orthorhombic, P 2 1 2 1 2 1 , a = 6.449(8) Å, b = 10.548(14) Å, c = 17.84(2) Å, V = 1213(3) Å 3 , Z = 4, R gt ( F ) = 0.0406, wR ref ( F 2 ) = 0.0933, T = 296(2) K.
Open Access
Crystal structure of ethyl 4-(3,4-dimethylphenyl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate, C₂₃H₂₉NO₃

June 29, 2018

Xuanhuang Chen, Feng Wu, Manwei Huang, Jinqing Zheng, Zhengxi Yu, Jinhui Chen

Page range: 821-822

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C 23 H 29 NO 3 , orthorhombic, Pbcn (no. 60), a = 18.781(7) Å, b = 15.749(6) Å, c = 14.081(5) Å, V = 4165(3) Å 3 , Z = 8, R gt ( F ) = 0.0614, wR ref ( F 2 ) = 0.1874, T = 296(2) K.
Open Access
Crystal structure of ethyl 4-(3-cyanophenyl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate, C₂₂H₂₄N₂O₃

June 27, 2018

Ji-Dong Song, Li-Li Wang

Page range: 823-824

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C 22 H 24 N 2 O 3 , orthorhombic, Pbca (no. 61), a = 15.333(11) Å, b = 14.146(11) Å, c = 17.640(13) Å, V = 3826(5) Å 3 , Z = 8, R gt ( F ) = 0.0533, wR ref ( F 2 ) = 0.1431, T = 296 K.
Open Access
Crystal structure of 7β,9β-dihydroxy-15-oxo-ent-kauran-16-en-19,6β-olide, C₂₀H₂₆O₅

June 21, 2018

Juan Zou, Chen-Liang Zhao, Jiang-Hai Ye, Kang He, Ren-Tao Tang, Lu-Tai Pan

Page range: 825-826

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C 20 H 26 O 5 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 7.302(4) Å, b = 11.307(5) Å, c = 20.414(10) Å, V = 1685.5(14) Å 3 , Z = 4, R gt ( F ) = 0.0670, wR ref ( F 2 ) = 0.1748, T = 296(2) K.
Open Access
Crystal structure of Ent-7β,20-epoxy-kaur-16-en-1β,6α,7α,14α,15α-pentaol-20-one, C₂₀H₃₀O₈

June 29, 2018

Jiang-Hai Ye, Chen-Liang Zhao, Juan Zou, Kang He, Chao-Jie Teng, Lu-Tai Pan

Page range: 827-828

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C 20 H 30 O 8 , monoclinic, C 2 (no. 5), a = 21.684(13) Å, b = 7.275(4) Å, c = 14.320(9) Å, β = 118.975(11), V = 1976(2) Å 3 , Z = 4, R gt ( F ) = 0.0362, wR ref ( F 2 ) = 0.0920, T = 298 K.
Open Access
Crystal structure of 1,4-bis(benzo[d][1,3]dioxol-5-ylmethyl)dihydro-1H,3H-furo[3,4-c]furan-3a(4H)-yl acetate, C₂₂H₂₀O₈

June 27, 2018

Rui Deng, Chen-Liang Zhao, Jiang-Hai Ye, Ya-Hua Liu, Juan Zou, Lu-Tai Pan

Page range: 829-830

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C 22 H 20 O 8 , monoclinic, P 2 1 (no. 4), a = 7.5482(10) Å, b = 7.0055(9) Å, c = 18.245(3) Å, β = 101.709(4)°, V = 944.7(2) Å 3 , Z = 2, R gt ( F ) = 0.0444, wR ref ( F 2 ) = 0.1199, T = 293(2) K.
Open Access
Crystal structure of methyl 2-((4-((2-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl) benzoate, C₁₈H₁₆N₄O₅

July 31, 2018

Zhe Wang, Wei Hong, Hao Wang

Page range: 831-832

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C 18 H 16 N 4 O 5 , triclinic, P 1̄ (no. 2), a = 8.4076(6) Å, b = 8.6630(5) Å, c = 12.0763(8) Å, α = 102.046(3)°, β = 97.453(3)°, γ = 99.280(3)°, V = 836.70(9) Å 3 , Z = 2, R gt ( F ) = 0.0396, wR ref ( F 2 ) = 0.0972, T = 150(2) K.
Open Access
Crystal structure of diaqua-bis(5-carboxy-1-methyl-1H-imidazole-4-carboxylato-κ²N,O)zinc(II), C₁₂H₁₄N₄O₁₀Zn

July 20, 2018

Li Xiao-Ling, Zhang Ru-Meng, Liu Li

Page range: 833-834

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C 6 H 7 N 2 O 5 Zn 0.5 , monoclinic, C 2/ c (no. 15), a = 9.0277(4) Å, b = 12.0102(5) Å, c = 15.3939(5) Å, β = 95.040(3)°, V = 1662.62(11) Å 3 , Z = 8, R gt ( F ) = 0.0242, wR ref ( F 2 ) = 0.0637, T = 292(1) K.
Open Access
Hydrothemal synthesis and crystal structure of triaqua-bis(5-carboxy-1-methyl-1H-imidazole-4-carboxylato-κ²N,O;κ¹O)manganese(II), C₁₂H₁₆N₄O₁₁Mn

June 29, 2018

Liu Guang-Zhen, Yan Meng-Zhen

Page range: 835-836

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C 12 H 16 N 4 O 11 Mn, triclinic, P 1̄ (no. 2), a = 7.7186(3) Å, b = 9.8439(3) Å, c = 11.6084(3) Å, α = 104.288(3)°, β = 94.024(3)°, γ = 97.365(3)°, V = 842.93(5) Å 3 , Z = 2, R gt (F) = 0.0322, T = 291 K.
Open Access
Redetermination of methyl 4-(4-chlorophenyl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydro-quinoline-3-carboxylate, C₂₀H₂₂ClNO₃

July 7, 2018

Qian-Qian Wang, Da-Xiang Wang, Qian-Qian Liu

Page range: 837-838

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C 20 H 22 ClNO 3 , monoclinic, P 2 1 / n (no. 14), a = 9.275(5) Å, b = 18.213(9) Å, c = 11.403(6) Å, β = 109.718(9)°, V = 1813.4(16) Å 3 , Z = 4, R gt ( F ) = 0.0483, wR ref ( F 2 ) = 0.1346, T = 296(2) K.
Open Access
Crystal structure of bis{1-[(benzotriazol-1-yl)methyl]-1-H-1,3-(2-methyl-imdazol)-κN}-dithiocyano-κN-zinc(II) C₂₄H₂₂N₁₂S₂Zn

June 30, 2018

Hai-Yan Yang, Yao-Min Zhao, Fang He, Hui Li, Hong-Fang Wang, Ying-Hua Li

Page range: 839-841

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C 24 H 22 N 12 S 2 Zn, monoclinic, C 2/ c (no. 15), a = 27.6123(9) Å, b = 9.6238(4) Å, c = 21.1748(8) Å, β = 101.088(4)°, Z = 8, V = 5521.8(4) Å 3 , R gt ( F ) = 0.0481, wR ref ( F 2 ) = 0.1047, T = 291(2) K.
Open Access
Crystal structure of (5-fluoro-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)methyl furan-2-carboxylate, C₁₀H₇FN₂O₅

June 18, 2018

Xiaowei Yan, Dongjian Zhu, Xing Zhong, Sujuan Wang

Page range: 843-844

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C 10 H 7 FN 2 O 5 , monoclinic, P 2 1 / n (no. 14), a = 8.5781(17) Å, b = 5.3121(11) Å, c = 23.578(5) Å, β = 96.68(3)°, V = 1067.1(4) Å 3 , Z = 4, R gt ( F ) = 0.0375, wR ref ( F 2 ) = 0.1138, T = 293(2) K.
Open Access
Crystal structure of bis(η⁶-cymene)-tri-μ₂-chlorido-ruthenium(II) tetrafluoroborate, C₂₀H₂₈BCl₃F₄Ru₂

June 20, 2018

Xiaowei Yan, Dongjian Zhu, Xing Zhong, Sujuan Wang

Page range: 845-847

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C 20 H 28 BCl 3 F 4 Ru 2 , triclinic, P 1̄ (no. 2), a = 7.7061(15) Å, b = 12.654(3) Å, c = 13.993(3) Å, α = 68.25(3)°, β = 78.71(3)°, γ = 88.89(3)°, V = 1240.8(5) Å 3 , Z = 2, R gt ( F ) = 0.0686, wR ref ( F 2 ) = 0.2017, T = 293(2) K.
Open Access
Crystal structure of 3,6-diphenyl-7H-[1,2,4]-triazolo[3,4-b][1,3,4]thiadiazine, C₁₆H₁₂N₄S

June 27, 2018

Qichun Ding, Shudong Dai, Li-Xue Zhang

Page range: 849-851

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C 16 H 12 N 4 S, monoclinic, P 2 1 / c (no. 14), a = 22.151(4) Å, b = 12.484(2) Å, c = 10.2018(19) Å, β = 101.073(6)°, Z = 8, V = 2768.7(8) Å 3 , R gt ( F ) = 0.0522, wR ref ( F 2 ) = 0.1428, T = 296(2) K.
Open Access
Synthesis and crystal structure of 1,3-bis[(3,4-dicyano)phenoxy]-4,6-dinitro-benzene, C₂₂H₈N₆O₆

June 13, 2018

Ateyatallah Aljuhani, Musa A. Said, David L. Hughes, Andrew N. Cammidge

Page range: 853-855

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C 22 H 8 N 6 O 6 , monoclinic, P 2 1 / n (no. 14), a = 15.3939(6) Å, b = 7.3053(3) Å, c = 16.8282(6) Å, β = 91.567(3)°, V = 1891.74(13) Å 3 , Z = 4, R gt ( F ) = 0.0510, wR ref ( F 2 ) = 0.0867, T = 140(2) K.
Open Access
Crystal structure of ethyl 2-amino-4-(2,6-dichlorophenyl)-7-methyl-5-oxo-4H,5H-pyrano [4,3-b]pyran-3-carboxylate, C₁₈H₁₅Cl₂NO₅

June 29, 2018

Jing-Yao Li

Page range: 857-858

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C 18 H 15 Cl 2 NO 5 , monoclinic, P 2 1 / c (no. 14), a = 7.423(5) Å, b = 27.798(3) Å, c = 9.550(2) Å, β = 117.62(4)°, V = 1746.0(14) Å 3 , Z = 4, R gt ( F ) = 0.0395, wR ref ( F 2 ) = 0.1030, T = 293(2) K.
Open Access
Crystal structure of poly[μ₃-hydroxy-(μ₅-(5-(2-carboxylatophenoxy)isophthalato-κ⁶O¹:O²:O³:O⁴:O⁵,O⁶)-(μ₂-1,4-di(1H-imidazol-1-yl)butane-κ²N:N′)dicobalt(II)] hemihydrate, C₂₅H₂₂Co₂N₄O_8.5

June 30, 2018

Ganlin Zhao

Page range: 859-861

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C 25 H 22 Co 2 N 4 O 8.5 , orthorhombic, Fdd 2 (no. 43), a = 19.046(3) Å, b = 45.458(6) Å, c = 11.4233(16) Å, V = 9890(2) Å 3 , Z = 16, R gt ( F ) = 0.0339, wR ref ( F 2 ) = 0.0618, T = 296(2) K.
Open Access
Crystal structure of methyl 4-(4-bromophenyl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate, C₂₀H₂₂BrNO₃

July 12, 2018

Tao-Wen Ren, Xing-Peng Xiao, Bai-Yu Li, Yu-Mei Zhao, Shao-Peng Peng

Page range: 863-864

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C 20 H 22 BrNO 3 , monoclinic, P 2 1 / n (no. 14), a = 9.597(2) Å, b = 18.236(5) Å, c = 11.640(3) Å, β = 111.355(5)°, V = 1897.3(8) Å 3 , Z = 4, R gt ( F ) = 0.0497, wR ref ( F 2 ) = 0.1240, T = 296(2) K.
Open Access
Crystal structure of 9,10-dimethoxy-5,6-dihydro-[1,3]dioxolo[4,5-g]isoquinolino[3,2-a]isoquinolin-7-ium 5-hydroxy-2-(4-hydroxyphenyl)-4-oxo-4H-chromen-7-olate trihydrate, C₃₅H₃₃NO₁₂

July 20, 2018

Zhang Yanjie, Lou Benyong, Huang Yali, Huang Xiaodong, Wu Huazhong

Page range: 865-867

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C 35 H 33 NO 12 , monoclinic, P 2 1 / c (no. 14), a = 7.595(4) Å, b = 19.478(9) Å, c = 20.910(11) Å, β = 99.124(10)°, V = 3054(3) Å 3 , Z = 4, R gt ( F ) = 0.0689, wR ref ( F 2 ) = 0.1793, T = 100(2) K.
Open Access
Crystal structure of 2,5-bis(4-(10H-phenothiazin-10-yl)phenyl)-1,3,4-oxadiazole, C₃₈H₂₄N₄OS₂

July 7, 2018

Qiong Wu, Heng-Qiang Zhang, Braveenth Ramanaskanda, Kyu-Yun Chai

Page range: 869-871

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C 38 H 24 N 4 OS 2 , monoclinic, P 2 1 / c (no. 14), a = 10.9621(6) Å, b = 19.7851(11) Å, c = 14.1928(9) Å, β = 100.957(6)°, V = 3022.1(3) Å 3 , Z = 4, R gt ( F ) = 0.0528, wR ref ( F 2 ) = 0.1294, T = 172.99(10) K.
Open Access
The crystal structure of (E)-2-(4-hydroxyphenyl)-5-(prop-1-en-1-yl)benzofuran-3-carbaldehyde, C₁₈H₁₄O₃

July 13, 2018

Guoyong Luo, Wude Yang, Tianqiong Lang, Chenliang Zhao, Jingjie Zhang

Page range: 873-874

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C 18 H 14 O 3 , monoclinic, P 2 1 / n (no. 14), a = 11.115(4) Å, b = 6.878(3) Å, c = 18.024(7) Å, β = 99.964(8)°, V = 1357.1(9) Å 3 , Z = 4, R gt ( F ) = 0.0601, wR ref ( F 2 ) = 0.1892, T = 173 K.
Open Access
Crystal structure of bis{5H-dibenzo[c,f][1,5]oxabismocin-12(7H)-yl} carbonate, C₂₉H₂₄O₅Bi₂

July 20, 2018

Nianyuan Tan, Limin Dang, Donghui Lan, Shuisheng Wu, Chak-Tong Au, Bing Yi

Page range: 875-877

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C 29 H 24 O 5 Bi 2 , orthorhombic, Pbca (no. 61), a = 14.8835(6) Å, b = 14.5551(6) Å, c = 23.6000(9) Å, V = 5112.5(4) Å 3 , Z = 8, R gt ( F ) = 0.0293, wR ( F 2 ) = 0.0579, T = 296(2) K.
Open Access
Crystal structure of ethyl-5-formyl-3,4-dimethylpyrrole-2-carboxylate — N-(5-ethoxycarbonyl-3,4-dimethylpyrrole)-2-methylene-5-nitrobenzene-1,2-diamine (1:1), C₂₆H₃₁N₅O₇

July 13, 2018

Zhongliang Lu, Zhen Wei, Wei-Na Wu

Page range: 879-880

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C 26 H 31 N 5 O 7 , monoclinic, P 2 1 / n (no. 14), a = 7.0353(5) Å, b = 15.1943(8) Å, c = 24.8536(13) Å, β = 92.314(4)°, V = 2654.6(3) Å 3 , Z = 4, R gt ( F ) = 0.0535, wR ref ( F 2 ) = 0.1615, T = 296(2) K.
Open Access
Crystal structure of (E)-2-(1-((2-aminophenyl)imino)ethyl)-6-bromo-4-chlorophenol, C₁₄H₁₂BrClN₂O

June 29, 2018

Yong Hong, Wei Liu

Page range: 881-882

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C 14 H 12 BrClN 2 O, monoclinic, P 2 1 / c (no. 14), a = 3.9454(10) Å, b = 24.189(6) Å, c = 13.728(3) Å, β = 90.07°, V = 643.99(7) Å 3 , Z = 4, R gt ( F ) = 0.0589, wR ref ( F 2 ) = 0.1584, T = 293(2) K.
Open Access
Crystal structure of (Z)-2-(4-chlorophenyl)-4-(furan-2-yl(phenylamino)methylene)-5-methyl-2,4-dihydro-3H-pyrazol-3-one, C₂₁H₁₆ClN₃O₂

June 30, 2018

Heng-Qiang Zhang, Qiong Wu, Tong-Yin Jin, Ying-Ying Li, Hong-Li Chen

Page range: 883-884

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C 21 H 16 ClN 3 O 2 , monoclinic, C 2/ c (no. 15), a = 19.0523(19) Å, b = 9.3818(8) Å, c = 21.0602(17) Å, β = 107.303(10)°, V = 3594.0(6) Å 3 , Z = 8, R gt ( F ) = 0.0644, wR ref ( F 2 ) = 0.1655, T = 173(1) K.
Open Access
Crystal structure of N²,N⁴-dibutyl-6-chloro-N²,N⁴-bis(1,2,2,6,6-pentamethylpiperidin-4-yl)-1,3,5-triazine-2,4-diamine, C₃₁H₅₈ClN₇ – Important intermediate of Chimassorb 119 synthesis

July 12, 2018

Jian Xiao, Kai Wang, Qiang Chen, Xiu-Qin Zhang, Guo-Yuan Lu

Page range: 885-888

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C 31 H 58 ClN 7 , monoclinic, P 2 1 /c (no. 14), a = 29.9370(18) Å, b = 15.6432(8) Å, c = 14.2792(8) Å, β = 90.819(2)°, V = 6686.4(6) Å 3 , Z = 8, R gt ( F ) = 0.0671, wR ref ( F 2 ) = 0.1925, T = 173(2) K.
Open Access
Crystal structure of 1-(5-bromo-2-(4-methoxyphenyl)-1H-indol-7-yl)ethanone oxime, C₁₇H₁₅BrN₂O₂

July 17, 2018

Malose J. Mphahlele

Page range: 889-891

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C 17 H 15 BrN 2 O 2 , monoclinic, P 2 1 / c , a = 14.4197(9) Å, b = 7.5423(5) Å, c = 14.9602(9) Å, β = 114.665(2)°, V = 1478.59(16) Å 3 , Z = 4, R gt ( F ) = 0.0196, wR ref ( F 2 ) = 0.0526, T = 173(2) K.
Open Access
Crystal structure of poly-{diaqua-bis[(μ₂-3-nitrobenzenesulfonylglycine-κ³N:O:O′)(4,4′-bipyridine)manganese(II)]}-dimethylformamide (1/1), C₃₉H₃₅Mn₂N₉O₁₅S₂

June 29, 2018

Xiao-Miao Chen, Zheng-Jun Liu, Tao-Li Deng

Page range: 893-895

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C 39 H 35 Mn 2 N 9 O 15 S 2 , orthorhombic, Pna 2 1 (no. 33), a = 17.2427(6) Å, b = 11.7453(3) Å, c = 21.1828(7) Å, V = 4290.0(2) Å 3 , Z = 4, R gt ( F ) = 0.0366, wR ref ( F 2 ) = 0.0960, T = 293(2) K.
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Crystal structure of 4-(dimethylamino)-1-(prop-2-yn-1-yl)pyridin-1-ium perchlorate, C₁₀H₁₃ClN₂O₄

July 7, 2018

Mouslim Messali, Mohamed Reda Aouad, Nadjet Rezki, M. Saud Almutairi, Ismail Warad

Page range: 897-898

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C 10 H 13 ClN 2 O 4 , orthorhombic, Pnma , a = 14.903(2) Å, b = 9.1004(15) Å, c = 8.7560(14) Å, V = 1187.5(3) Å 3 , Z = 4, R int = 0.036, R gt ( F ) = 0.0284, wR ref ( F 2 ) = 0.0795, T = 296 K.
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Crystal structure of 2-amino-5-oxo-4-(4-chloro-phenyl)-4,5,6,7-tetrahydro-cyclopenta[b]pyran-3-carbonitrile, C₁₅H₁₁ClN₂O₂

July 7, 2018

Da Li, Yan Zhou, Wei Zhong, Ling Peng

Page range: 899-900

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C 15 H 11 ClN 2 O 2 , monoclinic, C 2/ c (no. 15), a = 12.955(7) Å, b = 10.425(7) Å, c = 20.149(13) Å, β = 102.415(14)°, V = 2658(3) Å 3 , Z = 8, R gt ( F ) = 0.0361, wR ref ( F 2 ) = 0.0917, T = 296(2) K.
Open Access
Crystal structure of triaqua-(pyridine-2,6-dicarboxylato-κ³O,N,O′)cobalt(II) – 6-phenyl-1,3,5-triazine-2,4-diamine (1/1), C₁₆H₁₈CoN₆O₇

July 7, 2018

Wang Ren-Shu, Feng Jing

Page range: 901-902

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C 16 H 18 CoN 6 O 7 , monoclinic, P 2 1 / c (no. 14), a = 12.6820(11) Å, b = 7.9486(6) Å, c = 19.6429(15) Å, V = 1928.9(3) Å 3 , Z = 4, R gt ( F ) = 0.0429, wR ref ( F 2 ) = 0.1077, T = 296(2) K.
Open Access
Crystal structure of ethyl 2-amino-4-(3-cyanophenyl)-7,7-dimethyl-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carboxylate, C₂₁H₂₂N₂O₄

July 13, 2018

Dao-Qiu Yang, Zhen-Ming Li

Page range: 903-904

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C 21 H 22 N 2 O 4 , monoclinic, P 2 1 / n (no. 14), a = 8.1261(14) Å, b = 11.829(2) Å, c = 20.123(4) Å, β = 98.002(3)°, V = 1915.4(6) Å 3 , Z = 4, R gt ( F ) = 0.0394, wR ref ( F 2 ) = 0.1043, T = 296(2) K.
Open Access
Crystal structure of 2-(4-chloro-2,6-dinitrophenyl)-1-(4-chloro-3-nitrophenyl)diazene 1-oxide, C₁₂H₅Cl₂N₅O₇

July 7, 2018

Cao Junyan, Wang Jianlong, Chen Lizhen, Zhang Luyao

Page range: 905-906

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C 12 H 5 Cl 2 N 5 O 7 , triclinic, P 1̄ (no. 2), a = 8.2425(8) Å, b = 8.2814(7) Å, c = 12.4713(12) Å, α = 93.370(4)°, β = 101.590(4)°, γ = 118.222(3)°, V = 723.03(12) Å 3 , Z = 2, R gt ( F ) = 0.0516, wR ref ( F 2 ) = 0.0858, T = 173(2) K.
Open Access
Crystal structure of 3,4-dimethyl-2,6-dinitrophenol, C₈H₈N₂O₅

June 30, 2018

Xue Shaomin, Wang Jianlong, Shen Fanfan, Liu Chuangang

Page range: 907-908

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C 8 H 8 N 2 O 5 , monoclinic, P 2 1 / n (no. 14), a = 10.7951(12) Å, b = 8.1053(9) Å, c = 10.8626(9) Å, β = 100.371(4)°, V = 934.92(17) Å 3 , Z = 4, R gt ( F ) = 0.0686, wR ref ( F 2 ) = 0.1382, T = 293(2) K.
Open Access
Crystal structure of 1,2-dimethyl-3,5-dinitrobenzene, C₈H₈N₂O₄

June 30, 2018

Wang Jianlong, Xue Shaomin, Shen Fanfan, Xu Zishuai

Page range: 909-910

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C 8 H 8 N 2 O 4 , monoclinic, P 2 1 / n (no. 14), a = 14.6418(13) Å, b = 3.8852(4) Å, c = 15.7884(15) Å, β = 108.417(3)°, V = 852.14(14) Å 3 , Z = 4, R gt ( F ) = 0.0505, wR ref ( F 2 ) = 0.1159, T = 173(2) K.
Open Access
Crystal structure of ethyl 4-(3-chlorophenyl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate, C₂₁H₂₄ClNO₃

June 21, 2018

Wei Gou, Yan Zhou, Wei Zhong, Yang Wang, Bai-Yuan Yang, An-Rong Zhao

Page range: 911-912

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C 21 H 24 ClNO 3 , orthorhombic, Pbcn (no. 60), a = 17.215(11) Å, b = 15.749(11) Å, c = 14.136(9) Å, V = 3832(4) Å 3 , Z = 8, R gt ( F ) = 0.058, wR ref ( F 2 ) = 0.177, T = 296(2) K.
Open Access
Crystal structure of N-(4-chlorophenyl)-2-(2,6-dichlorophenyl)acetamide, C₁₄H₁₀Cl₃NO

June 27, 2018

Wei Sun, Li-Min Zuo, Ting Zhao, Zhi-Ling Zhu, Yong-Hua Liu, Guang-Zhi Shan

Page range: 913-914

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C 14 H 10 Cl 3 NO, monoclinic, P 2 1 / n (no. 14), a = 13.7865(2) Å, b = 13.0725(2) Å, c = 15.9606(2) Å, β = 100.7371(14)°, V = 2826.11(7) Å 3 , Z = 8, R gt ( F ) = 0.0662, wR ref ( F 2 ) = 0.1980, T = 293(2) K.
Open Access
Crystal structure of 2-amino-4-(4-fluorophenyl)-3-cyano-5-oxo-4H,5H-pyrano[3,2c] chromene, C₁₉H₁₁FN₂O₃

July 7, 2018

Lian-Man He, Chuan-Yu Gao

Page range: 915-916

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C 19 H 11 FN 2 O 3 , monoclinic, P 2 1 / c (no. 14), a = 8.8312(5) Å, b = 12.9378(9) Å, c = 13.1531(8) Å, β = 93.022(5)°, V = 1500.73(16) Å 3 , Z = 4, R gt ( F ) = 0.0411, wR ref ( F 2 ) = 0.1059, T = 293(2) K.
Open Access
The crystal structure of (4-nitrophenyl) (5-ferrocenyl-3-(trifluoromethyl)-1H-pyrazol-1-yl) methanone, C₂₁H₁₂F₃FeN₃O₃

July 31, 2018

Ying Guo, Ban-Feng Ruan

Page range: 917-918

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C 21 H 14 F 3 FeN 3 O 3 , triclinic, P 1̄ (no. 2), a = 7.961(3) Å, b = 11.136(4) Å, c = 11.588(4) Å, α = 76.357(10)°, β = 84.998(10)°, γ = 76.989(10)° V = 972.1(6) Å 3 , Z = 2, R gt ( F ) = 0.0509, wR ref ( F 2 ) = 0.1304, T = 273(2) K.
Open Access
Crystal structure of 5,5′-((3-hydroxy-4-methoxyphenyl)methylene)bis(1,3-diethyl-6-hydroxy-2-thioxo-2,3-dihydropyrimidin-4(1H)-one), C₂₄H₃₀N₄O₆S₂

June 13, 2018

Mezna saleh Altowyan, M. Ali, Obaid S. AlRuqi, Abdullah Mohammed Al-Majid, Assem Barakat

Page range: 919-921

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C 24 H 30 N 4 O 6 S 2 , triclinic, P 1̄ with a = 9.2557(4) Å, b = 10.2606(5) Å, c = 14.0972(7) Å, α = 71.949(2)°, β = 89.305(2)°, γ = 86.061(2)° V = 1269.84(10) Å 3 , Z = 2, R gt ( F ) = 0.058, wR ref ( F 2 ) = 0.142, T = 293(2) K.
Open Access
Crystal structure of (3aR,4R,5R,7R,8S,9R,9aS,12R)-7-ethyl-5-(1-hydroxy-2-((R)-3-hydroxypyrrolidin-1-yl)ethoxy)-4,7,9,12-tetramethyldecahydro-4,9a-propanocyclopenta[8]annulene-3,8-diol – a pleuromutilin derivative, C₂₆H₄₁NO₅

July 20, 2018

Yan Liang, Yun-Xing Fu, Jian-Ping Liang

Page range: 923-925

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C 26 H 41 NO 5 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 9.6178(8) Å, b = 13.3335(11) Å, c = 19.0758(16) Å, V = 2446.3(4) Å 3 , Z = 4, R gt ( F ) = 0.0389, wR ref ( F 2 ) = 0.0888, T = 296(2) K.
Open Access
Crystal structure of bis(μ₂-3-formyl-5-methoxy-2-oxidobenzoato-κ³O,O′:O′)-hexapyridine-dicadmium(II) – pyridine (1/1), C₅₃H₄₇Cd₂N₇O₁₀

July 13, 2018

Xue L. Niu, Hua Yang

Page range: 927-929

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C 53 H 47 Cd 2 N 7 O 10 , triclinic, P 1̄, a = 9.6670(9) Å, b = 10.5089(11) Å, c = 13.2081(12) Å, α = 109.879(2)°, β = 97.894(1)°, γ = 92.201(1)°, V = 1244.7(2) Å 3 , Z = 1, R gt ( F ) = 0.0388, wR ref ( F 2 ) = 0.0926, T = 298(2) K.
Open Access
Crystal structure of ethyl 2-amino-4-(3-methoxyphenyl)-5-oxo-4H,5H-pyrano[3,2-c]chromene-3-carboxylate, C₂₂H₁₉NO₆

July 13, 2018

Lei Shi, Dehui Zhang, Liangyu Zhang

Page range: 931-932

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C 22 H 19 NO 6 , monoclinic, P 2 1 / n (no. 14), a = 9.195(4) Å, b = 17.253(5) Å, c = 12.127(5) Å, β = 95.100(16)°, V = 1916.4(12) Å 3 , Z = 4, R gt ( F ) = 0.0405, wR ref ( F 2 ) = 0.1084, T = 296(2) K.
Open Access
Crystal structure of methyl 4-(3,5-ditrifluoromethylphenyl)-2,7,7-trimethyl-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate — water (2/1), C₂₂H₂₁F₆NO₃

July 18, 2018

Liyan Chen

Page range: 933-934

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C 22 H 21 F 6 NO 3 , monoclinic, C 2/ c (no. 15), a = 14.849(4) Å, b = 10.497(3) Å, c = 28.694(7) Å, β = 97.682(5)°, V = 4432(2) Å 3 , Z = 4, R gt ( F ) = 0.0736, wR ref ( F 2 ) = 0.2405, T = 293(2) K.
Open Access
Crystal structure of 2-(4-bromophenyl)-2,3-dihydro-1H-perimidine, C₁₇H₁₃BrN₂

July 23, 2018

Min Zhang, Zhong-Yan Li, Xian-You Yuan, Lin Yuan

Page range: 935-936

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C 17 H 13 BrN 2 , orthorhombic, Pbca (no. 61), a = 9.995(4) Å, b = 13.845(5) Å, c = 20.213(7) Å, V = 2797.2(18) Å 3 , Z = 8, R gt ( F ) = 0.0304, wR ref ( F 2 ) = 0.0784, T = 296(2) K.
Open Access
Crystal structure of (5-ethyl-2-(4-methoxyphenyl)-1,3-dioxan-5-yl)methanol, C₁₄H₂₀O₄

July 23, 2018

Xian-You Yuan, Lin Yuan, Min Zhang, Zhong-Yan Li

Page range: 937-938

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C 14 H 20 O 4 , triclinic, P 1̄, a = 6.1028(13) Å, b = 10.885(2) Å, c = 20.737(4) Å, α = 100.673(2)°, β = 92.465(2)°, γ = 98.973(2)°, V = 1333.5(5) Å 3 , Z = 4, R gt ( F ) = 0.0431, wR ref ( F 2 ) = 0.1225, T = 296(2) K.
Open Access
Crystal structure of (E)-N-(4-bromo-2-(1-(hydroxyimino)ethyl)phenyl)benzamide, C₁₅H₁₃BrN₂O₂

July 17, 2018

Malose J. Mphahlele

Page range: 939-940

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C 15 H 13 BrN 2 O 2 , monoclinic, P 2 1 / c , a = 7.4754(3) Å, b = 17.6666(7) Å, c = 10.9145(4) Å, β = 103.520(1)°, V = 1401.48(9) Å 3 , Z = 4, R gt ( F ) = 0.0290, wR ref ( F 2 ) = 0.0713, T = 173(2) K.
Open Access
Crystal structure of caffeinium triiodide – caffeine (1/1), C₁₆H₂₁I₃N₈O₄

May 18, 2018

Johannes Merkelbach, Martha A. Majewski, Guido J. Reiss

Page range: 941-944

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C 16 H 21 I 3 N 8 O 4 , monoclinic, P 2 1 / n (no. 14), a = 14.7257(7) Å, b = 10.5712(5) Å, c = 16.7501(8) Å, β = 114.408(2)°, V = 2374.4(2) Å 3 , Z = 4, R gt ( F ) = 0.0254, wR ref ( F 2 ) = 0.0760, T = 290(2) K.
Open Access
Crystal structure of methyl 2-methyl-4-(3-methoxyphenyl)-5-oxo-1,4,5,6,7,8-hexahydroquinoline-3-carboxylate, C₁₉H₂₁NO₄

July 31, 2018

Jun Ma, Weiwei Dai, Weiwei Feng, Tingting Lin, Lijing Zhou, Wei Qin, Xuyang Wang

Page range: 945-946

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C 19 H 21 NO 4 , monoclinic, C 2/ c (no. 15), a = 17.349(5) Å, b = 7.354(2) Å, c = 25.757(7) Å, β = 97.637(5)°, V = 3257.1(16) Å 3 , Z = 8, R gt ( F ) = 0.0444, wR ref ( F 2 ) = 0.1141, T = 296(2) K.
Open Access
Crystal structure of (E)-3-(3,5-di-tert-butyl-4-hydroxyphenyl)-1-phenylprop-2-en-1-one, C₂₃H₂₈O₂

June 29, 2018

Ali N. Khalilov, Ayten R. Asgarova, Atash V. Gurbanov, Farid N. Nagiyev, Iván Brito

Page range: 947-948

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C 23 H 28 O 2 , monoclinic, P 2 1 / n (no. 14), a = 8.9114(3) Å, b = 17.7151(6) Å, c = 12.6087(5) Å, β = 100.0520(10), V = 1959.93(12) Å 3 , Z = 4, R gt ( F ) = 0.061, wR ref ( F 2 ) = 0.171, T = 296(2) K.
Open Access
Crystal structure of 1,4-bis(2-azidoethyl)piperazine-1,4-diium dichloride, C₈H₁₈N₈Cl₂

June 18, 2018

Fu Lei Gao, Ying Lei Wang, Bing Chen, Wei Xiao Liu, Ya Jing Liu

Page range: 949-950

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C 8 H 18 N 8 Cl 2 , monoclinic, P 2 1 / n (no. 14), a = 6.5246(3) Å, b = 7.7090(4) Å, c = 13.9243(6) Å, β = 101.240(3)°, V = 686.93(6) Å 3 , Z = 2, R gt ( F ) = 0.0320, wR ref ( F 2 ) = 0.0878, T = 302(2) K.
Open Access
The crystal structure of dichlorido-(1,3-bis(2,6-dimethylphenyl)-1H-imidazol-2(3H)-ylidene)-(morpholine-κ¹N)palladium(II), C₂₃H₂₉Cl₂N₃OPd(II)

July 13, 2018

Li Guo-Xing

Page range: 951-952

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C 23 H 29 Cl 2 N 3 OPd, monoclinic, P 2 1 / c (no. 14), a = 9.6053(2) Å, b = 17.4544(4) Å, c = 14.5156(3) Å, β = 104.6440(10)°, V = 2354.55(9) Å 3 , Z = 4, R gt ( F ) = 0.0184, wR ref ( F 2 ) = 0.0455, T = 173(2) K.
Open Access
The crystal structure of 1-((5-chloro-3-methyl-1-phenyl-1H-pyrazole-4-yl)methyl)-1,3-diphenylurea, C₂₄H₂₁Cl_N4O

July 23, 2018

Xing-Tao Zhang, Hai-Chao Wang, Teng Wang, Chao Liu

Page range: 953-954

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C 24 H 21 Cl N4 O, monoclinic, P 2 1 /n (no. 14), a = 10.2630(11) Å, b = 17.8954(16) Å, c = 12.3517(14) Å, β = 102.510(11)°, V = 2214.7(4) Å 3 , Z = 4, R gt ( F ) = 0.0569, wR ref ( F 2 ) = 0.1617, T = 293(2) K.
Open Access
Crystal structure of 6-(2-bromoacetamido)tetrahydro-2H-pyran-2,3,4,5-Tetrayl tetraacetate, C₁₆H₂₂BrNO₁₀

June 9, 2018

Ping Lin, Xu-Liang Nie, Zhong-Ping Yin, Zhong-Chao Li, Jia Liu, Xin-Chen Shang-Guan, Da-Yong Peng

Page range: 955-957

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[C 16 H 22 BrNO 10 ], orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 9.7453(13) Å, b = 9.9023(13) Å, c = 21.885(3) Å, V = 2111.9(5) Å 3 , Z = 4, R gt ( F ) = 0.0357, wR ref ( F 2 ) = 0.0981, T = 296(2) K.
Open Access
Crystal structure of 5-methylpyrazine-2-carbohydrazide, C₆H₈N₄O

July 20, 2018

Liang-Liang Gao, Xiao-Lei Zhao, Wei-Na Wu

Page range: 959-960

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C 6 H 8 N 4 O, monoclinic, P 2 1 / c (no. 14), a = 8.019(5) Å, b = 9.990(6) Å, c = 9.050(6) Å, β = 98.474(10)°, V = 717.1(7) Å 3 , Z = 4, R gt ( F ) = 0.0405, wR ref ( F 2 ) = 0.1205, T = 296(2) K.
Open Access
Crystal structure of catena-poly[(μ₂-5-(tert-butyl)isophthalato-κ⁴O,O′:O′′,O′′′)(-4′-(pyridin-4-yl)-2,2′:6′,2′′-terpyridine-κ³N,N′,N′′)manganese(II)], C₃₂H₂₈N₄O₅Mn

July 23, 2018

Yu-Fang Wang, Jing-Jing Wei, Xiao-Hui Zhai

Page range: 961-963

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C 32 H 28 N 4 O 5 Mn, monoclinic, P 2 1 / c (no. 14), a = 8.777(3) Å, b = 30.975(11) Å, c = 10.229(4) Å, β = 105.412(7)°, V = 2680.9(16) Å 3 , Z = 4, R gt ( F ) = 0.0448, wR ref ( F 2 ) = 0.1136, T = 296(2) K.

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