Volume 233, Issue 3

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Zeitschrift für Kristallographie - New Crystal Structures

Contents

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Cover and Frontmatter

April 26, 2018

Page range: i-vii

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Open Access
Bis(tetraethylammonium) carbonate – boric acid – water (1/2/5), C₁₇H₅₆B₂N₂O₁₄

March 23, 2018

Peizhi Wang, Peiyu Wang, Ming Bai

Page range: 339-341

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C 17 H 56 B 2 N 2 O 14 , monoclinic, P 2 1 / c (no. 14), a = 14.3049(6) Å, b = 14.5382(7) Å, c = 15.0065(7) Å, β = 103.185(3)°, V = 3038.6(2) Å 3 , Z = 4, R gt ( F ) = 0.0556, wR ref ( F 2 ) = 0.1836, T = 296(2) K.
Open Access
Crystal structure of 4-methoxy-6-phenyl-2H-pyran-2-one, C₁₂H₁₀O₃

March 8, 2018

Grace Obi, Sizwe J. Zamisa, Fanie R. Heerden

Page range: 343-344

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C 12 H 10 O 3 , triclinic, P 1̄ (no. 2), a = 7.2709(5) Å, b = 7.3228(5) Å, c = 9.4670(7) Å, α = 82.241(4)°, β = 88.161(3)°, γ = 70.192(5)°, V = 469.84(6) Å 3 , Z = 2, R gt ( F ) = 0.0370, wR ref ( F 2 ) = 0.1082, T = 100(2) K.
Open Access
Crystal structure of tris{(3-((E)-(((E)-2-oxidobenzylidene)hydrazono)methyl)-2-oxo-2H-chromen-4-olato-κ³O,N:N′)}dicobalt(III)tris(dimethylformamide), C₆₀H₅₀Co₂N₉O₁₅

March 5, 2018

Jing Li, Zi-Heng Cheng, Hao-Ran Jia, Fu-Wen Yang, Bin Yu, Yin-Xia Sun

Page range: 345-348

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C 60 H 50 Co 2 N 9 O 15 , triclinic, P 1̅ (no. 2), a = 13.6074(19) Å, b = 13.9185(17) Å, c = 15.837(2) Å, α = 81.196(4)°, β = 86.607(4)°, γ = 81.665(4)°, Z = 2, V = 2930.7(7) Å 3 , R gt ( F ) = 0.0564, wR ref ( F 2 ) = 0.2010, T = 296(2) K.
Open Access
Crystal structure of poly[bis(1-methyl-[4,4′-bipyridin]-1-ium-κN)-tetrakis(μ₃-sulfato-κ³O:O′:O′′)trizinc(II)], C₂₂H₂₂Zn₃N₄O₁₆S₄

March 10, 2018

Hong-Ru Fu, Kai-Lu Wang, Xiao-Xiao Zhao

Page range: 349-351

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C 22 H 22 Zn 3 N 4 O 16 S 4 , monoclinic, P 2 1 / n (no. 14), a = 9.2909(2) Å, b = 16.8888(4) Å, c = 19.3547(6) Å, β = 98.924(3)°, V = 3000.22(14) Å 3 , Z = 4, R gt (F) = 0.0401, wR ref (F 2 ) = 0.0942, T = 293(2) K.
Open Access
Crystal structure of (5Z,10Z)-3,13-dichloro-17,18-dioxo-5,11-diphenyl-8,9,17,18-tetrahydro-7H-dibenzo[e,n][1,4,8,12]tetraazacyclopentadecine-16,19-diido-κ⁴N,N′,N′′,N′′′)copper(II), C₃₁H₂₂N₄O₂Cl₂Cu

March 16, 2018

Shi-Jun Chen, Shi-Hui Li, Yao Huang, Bin Liu, Ting-Song Xiong, Jun Cui, Xiao-Shuang Shen, Deng-Qian Chen

Page range: 353-354

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C 31 H 22 N 4 O 2 Cl 2 Cu, orthorhombic, C 222 1 (no. 20), a = 6.869(2) Å, b = 18.535(7) Å, c = 21.199(7) Å, V = 2698.9(16) Å 3 , Z = 4, R gt ( F ) = 0.0385, wR ref ( F 2 ) = 0.1036, T = 293 K.
Open Access
Crystal structure of bis{5-methoxy-2-(((2-oxo-2H-chromen-6-yl)imino)methyl)phenolato-κ²N,O}zinc(II), C₃₄H₂₄N₂O₈Zn

March 5, 2018

Ping Zhang, Yan-Bin Wang, Qiong Su

Page range: 355-357

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C 34 H 24 N 2 O 8 Zn, triclinic, P 1̅ (no. 2), a = 9.1202(6) Å, b = 12.2985(8) Å, c = 12.9973(9) Å, α = 83.799(2)°, β = 76.063(2)°, γ = 81.385(2)°, Z = 2, V = 1395.02(16) Å 3 , R gt ( F ) = 0.0292, wR ref ( F 2 ) = 0.0691, T = 296(2) K.
Open Access
Crystal structure of 2,2′-((((ethane-1,2-diylbis(oxy))bis(2,1-phenylene))bis(azanylylidene))bis(methanylylidene))diphenolato-κ²N;κ⁴O)nickel(II), C₂₈H₂₂N₂O₄Ni

March 5, 2018

Qiang Xu, Yan Ling Zhao, Xiao Fang Luo, Ming Wei Zhou, Guo qiang Li

Page range: 359-360

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C 28 H 22 N 2 NiO 4 , tetragonal, P 4 1 2 1 2 (no. 92), a = 10.989(4) Å, c = 18.470(2) Å, V = 2230.4(16) Å 3 , Z = 4, R gt ( F ) = 0.0571, wR ref ( F 2 ) = 0.1382, T = 293(2) K.
Open Access
Crystal structure of 1,1′-((1E,1′E)-(((ethane-1,2-diylbis(oxy))bis(2,1-phenylene))bis(azanylylidene))bis(methanylylidene))bis(naphthalen-2-olato)cobalt(II), C₃₆H₂₆N₂O₄Co

April 7, 2018

Guo Qiang Li, Yan Ling Zhao, Yong Sen Jiang, Yun Chun Yu, Jun Ran Fang, Qiang Xu

Page range: 361-363

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C 36 H 26 N 2 O 4 Co, monolinic, C 2/ c (no. 15), a = 43.230(14) Å, b = 17.100(6) Å, c = 11.275(4) Å, β = 103.112(4)°, V = 8118(5) Å 3 , Z = 12, R gt ( F ) = 0.0370, wR ref ( F 2 ) = 0.0931, T = 100(2) K.
Open Access
Crystal structure of camptothecin, C₂₀H₁₆N₂O₄

February 16, 2018

Zhuo-Jie Tan, Yun-Bo Wang, Quan-Nu Yang, Yao-Lan Li, Guo-Cai Wang, Yong-Zhong Ouyang, Guo-Qiang Li

Page range: 365-367

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C 20 H 16 N 2 O 4 , monoclinic, P 2 1 (no. 4), a = 8.0094(5) Å, b = 6.7689(3) Å, c = 29.577(2) Å, β = 95.809(6)°, V =1595.27(16) Å 3 , Z = 4, R gt ( F ) = 0.0457, wR ref ( F 2 ) = 0.1209, T = 293 K.
Open Access
Crystal structure of (2-(chlorophenyl)-5-methyl-1,3-dioxane-5-carboxylato–κ²O,O′)(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ⁴N,N′,N′′,N′′′)nickel(II) perchlorate monohydrate, Ni(C₁₆H₃₆N₄)(C₁₂H₁₂O₄Cl)ClO₄⋅H₂O

February 16, 2018

Guang-Chuan Ou, Guo-Kai Jia, Fei Zeng, Ying-zhi Tan, Qiong Wang

Page range: 369-370

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C 28 H 50 Cl 2 N 4 NiO 9 , monoclinic, P 2 1 / n , a = 10.333(4) Å, b = 26.305(9) Å, c = 12.640(5) Å, β = 102.421(4)°, V = 3355(2) Å 3 , Z = 4, R gt ( F ) = 0.0391, wR ref ( F 2 ) = 0.1090, T = 296(2) K.
Open Access
Crystal structure of 3-(2-chloro-6-methoxyquinolin-3-yl)-5-phenylisoxazole (C₁₉H₁₃ClN₂O₂)

March 5, 2018

Carlos Fernández-Galleguillos, Jorge Bórquez, Alejandro Cárdenas, Iván Brito

Page range: 371-372

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C 19 H 13 ClN 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 11.2461(18) Å, b = 15.967(2) Å, c = 9.2864(13) Å, β = 106.770(9)°, V = 1596.6(4) Å 3 , Z = 4, R gt = 0.0670, wR ref ( F 2 ) = 0.1606, T = 296(2) K.
Open Access
Crystal structure of tetrakis(μ₂-acetato-κ²O:O′)-bis{[(E)-2,6-diisopropyl-N-(pyridin-3-ylmethylene)aniline]copper (II)}, C₄₄H₅₆Cu₂N₄O₈

February 27, 2018

Eric M. Njogu, Bernard Omondi, Vincent O. Nyamori

Page range: 373-375

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C 44 H 56 Cu 2 N 4 O 8 , monoclinic, P 2 1 / c (no. 14), a = 11.1061(10) Å, b = 20.5117(17) Å, c = 9.8185(9) Å, β = 101.302(2)°, V = 2193.27(15) Å 3 , Z = 2, R gt ( F ) = 0.0283, wR ref ( F 2 ) = 0.0753, T = 100 K.
Open Access
Crystal structure of diethyl 2-(2-chlorophenyl)-1,3-dioxane-5,5-dicarboxylate, C₁₆H₁₉Cl₁O₆

March 16, 2018

Lin Yuan, Min Zhang, Xian-You Yuan, Fang Liu

Page range: 377-378

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C 16 H 19 Cl 1 O 6 , triclinic, P 1̅ (no. 2), a = 7.827(8) Å, b = 9.253(9) Å, c = 12.978(13) Å, α = 101.910(11)°, β = 100.040(11)°, γ = 110.345(10)°, V = 830.7(14) Å 3 , Z = 2, R gt ( F ) = 0.0873, wR ref ( F 2 ) = 0.0909, T = 296(2) K.
Open Access
Crystal structure of (μ₂-2,2′-bipyridine-3,3′-dicarboxylato)-bis(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane)-di-nickel(II) perchlorate N,N′-dimethylformamide solvate, C₅₀H₉₂Cl₂N₁₂Ni₂O₁₄

February 16, 2018

Huan-Yong Li, Wang Lin, Feng-Xian Han, Guang-Chuan Ou

Page range: 379-381

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C 50 H 92 Cl 2 N 12 Ni 2 O 14 , monoclinic, C 2/ c (no. 15), a = 25.731(5) Å, b = 9.940(2) Å, c = 26.574(5) Å, β = 114.825(4)°, V = 6169(2) Å 3 , Z = 4, R gt ( F ) = 0.0675, w R ref ( F 2 ) = 0.2209, T = 173(2) K.
Open Access
Crystal structure of catena-poly[triaqua(μ₂-1,2-bis(4-pyridyl)ethane-κ²N:N′)-(1,2-bis(4-pyridyl)ethane-κN)nickel(II)] 2-aminonicotinate nitrate – 1,2-bis(4-pyridyl)ethane – water (2/1/8), C₃₆H₄₄N₈NiO₁₂

March 5, 2018

Yu-Fang Wang, Jing-Jing Wei, Xiao-Hui Zhai

Page range: 383-385

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C 36 H 44 N 8 NiO 12 , triclinic, P 1̅ (no. 2), a = 10.6451(5) Å, b = 12.1086(6) Å, c = 17.2600(7) Å, α = 76.624(4)°, β = 72.200(4)°, γ = 70.802(5)°, V = 1979.18(18) Å 3 , Z = 2, R gt ( F ) = 0.0414, wR ref ( F 2 ) = 0.1058, T = 293(2) K.
Open Access
Hydrothermal synthesis and crystal structure of poly[bis(μ₂-3-(3,5-dicarboxyphenoxy)phthalato-κ³O,O′:O′′)-(μ₂-1,2-di(pyridin-4-yl)ethane-κ²N:N′)copper(II)], C₂₂H₁₄CuNO₉

March 3, 2018

Li Yun-Ping, Ju Feng-Yang

Page range: 387-389

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C 22 H 14 CuNO 9 , triclinic, P 1̅ (no. 2), a = 7.9208(4) Å, b = 10.2954(4) Å, c = 13.1361(7) Å, α = 72.719(4)°, β = 79.598(5)°, γ = 85.190(4)°, V = 1005.53(9) Å 3 , Z = 2, R gt ( F ) = 0.0423, wR ref ( F 2 ) = 0.1051, T = 264(1) K.
Open Access
Crystal structure of catena-poly[aqua-(methanol-κO)-bis(μ₂-4-(pyridin-4-yl)benzoato-κ²N:O)-bis(triphenylphospine-κP)disilver(I)], C₆₁H₅₂Ag₂N₂O₆P₂

April 5, 2018

Ning Zhu, Yan Ma, Jian-Ming Liu, Yue-Xue Li, Min Liu, Xiu-Lan Xin, Qiong-Hua Jin

Page range: 391-393

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C 61 H 52 Ag 2 N 2 O 6 P 2 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 14.4634(11) Å, b = 17.7866(18) Å, c = 20.5509(19) Å, V = 5286.8(8) Å 3 , Z = 4, R gt ( F ) = 0.0424, wR ref ( F 2 ) = 0.0997, T = 298(2) K.
Open Access
The crystal structure of 6-(4-bromobenzyl)-1,3,5-trimethyl-7-phenyl-1,5-dihydro-2H-pyrrolo[3,2-d]pyrimidine-2,4(3H)-dione, C₂₂H₂₀BrN₃O₂

March 9, 2018

Orbett T. Alexander, Rajasekhar Donka, Johannes H. van Tonder, Barend C.B. Bezuidenhoudt, Hendrik G. Visser

Page range: 395-397

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C 22 H 20 BrN 3 O 2 , monoclinic, P 2 1 /c (no. 14), a = 15.889(12) Å, b = 16.332(13) Å, c = 7.324(5) Å, β = 94.985(5), V = 1893(2) Å 3 , Z = 4, R gt (F) = 0.0295, wR ref (F 2 ) = 0.0790, T = 100(2) K.
Open Access
Synthesis and crystal structure of catena-poly[bis(2-(2-((2,6-dichlorophenyl)amino)phenyl)acetato-κO;κ²O′,O′′)-(μ₂-1,4-di(pyridin-4-yl)benzene-κ²N:N′)zinc(II)], C₄₄H₃₂N₄ZnCl₄O₄

March 8, 2018

Wei Song, Xue-Li Xu, Yan-Ju Yang, Shi-Hui Li

Page range: 399-401

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C 44 H 32 N 4 O 4 Cl 4 Zn, triclinic, P 1̅ (no. 2), a = 7.3158(2) Å, b = 13.6944(5) Å, c = 20.4081(6) Å, α = 82.930(3)°, β = 89.667(2)°, γ = 88.034(3)°, V = 2027.85(11) Å 3 , Z = 2, R gt ( F ) = 0.0430, wR ref ( F 2 ) = 0.1141, T = 293(2) K.
Open Access
Crystal structure of diaqua-bis[N-phenyl-2-(quinolin-8-yloxy)acetamide-κ³-N,O,O′]-nitrato(κ²O,O′)-cerium(III) dinitrate - acetone (1/2), C₄₀H₄₄N₇O₁₇Ce

February 28, 2018

Hao Wu, Hai-Yan Li, Wei-Na Wu

Page range: 403-404

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C 40 H 44 N 7 O 17 Ce, monoclinic, C 2/ c (no. 15), a = 28.5754(11) Å, b = 9.2819(3) Å, c = 20.2035(8) Å, β = 123.576(2)°, V = 4464.6(3) Å 3 , Z = 4, R gt ( F ) = 0.0321, wR ref ( F 2 ) = 0.0844, T = 296(2) K.
Open Access
Crystal structure of the 2D coordination polymer poly[aqua(μ₂-2,2′-(1,2-phenylene)diacetato-κ³O,O′:O′)-(μ₂-4,4′-bis((1H-1,2,4-triazol-1-yl)methyl)-1,1′-biphenyl-κ²N:N′)cobalt(II)], C₂₈H₂₆CoN₆O₅

March 8, 2018

Xin Ling-Yun, Li Yun-Ping, Liu Guang-Zhen

Page range: 405-407

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C 28 H 26 CoN 6 O 5 , monoclinic, P 2 1 / c (no. 14), a = 13.2393(8) Å, b = 8.6608(5) Å, c = 22.4553(12) Å, β = 91.073(2)°, V = 2574.3(3) Å 3 , Z = 4, R gt ( F ) = 0.0327, wR ref ( F 2 ) = 0.0804, T = 293(2) K.
Open Access
Crystal structure of (dimethylformamide-κO)(perchlorato-κ²O,O′){μ₂-6,6′-((1,2-phenylenebis(azanylylidene))bis(methanylylidene))bis(4-bromo-2-methoxyphenolate)-κ⁸N,N′,O:O,O′:O′,O′′,O′′′}sodium(I)nickel(II), C₂₅H₂₃Br₂ClN₃NaNiO₉

March 10, 2018

Qingguo Meng, Chen Yue, Jiangkun Yu, Qingyun Liu, Jitao Lu

Page range: 409-411

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C 25 H 23 Br 2 ClN 3 NaNiO 9 , monoclinic, P 2 1 / n (no. 14), a = 15.595(4) Å, b = 10.993(3) Å, c = 18.660(5) Å, β = 114.536(4), V = 2910.2(14) Å 3 , Z = 4, R gt ( F ) = 0.0390, wR ref ( F 2 ) = 0.0998, T = 293 K.
Open Access
The crystal structure of catena-poly[bis((4-aminophenyl)sulfonyl)(pyrimidin-2-yl)amido-κ²N,N′)-bis(μ₂-4,4′-bipyridine-N,N′-κ²N:N′)zinc(II) – methanol (1/2), C₃₂H₃₄N₁₀O₆S₂Zn

February 15, 2018

Xiaofeng Zhang, Yi Cao, Yanwei Wang, Shimin Wang, Zhizhong Xu

Page range: 413-415

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C 32 H 34 N 10 O 6 S 2 Zn, monoclinic, C 2/ c (no. 15), a = 24.243(4) Å, b = 11.2766(17) Å, c = 15.799(5) Å, β = 127.986(2)°, V = 3404.0(13) Å 3 , Z = 4, R gt ( F ) = 0.0432, wR ref ( F 2 ) = 0.1146, T = 100(2) K.
Open Access
Synthesis and crystal structure poly[aqua(μ₃-2-(((7-hydroxy-3-(4-hydroxy-3-sulfonatophenyl)-4-oxo-4H-chromen-8-yl)methyl)ammonio)acetate-κ⁴O,O′:O′′:O′′′) sodium] monohydrate, C₁₈H₁₈NNaO₁₁S

February 16, 2018

Hai-Lin Chen, Hong-Fang Lai, Yong-Ling Qin, Yue-Ning Guo, Ting Chen, Xiao-Yuan Huang

Page range: 417-419

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C 18 H 18 NN a O 11 S, triclinic, P 1̅ (no. 2), a = 8.2627(12) Å, b = 8.6490(11) Å, c = 14.1791(17) Å, α = 82.883(10)°, β = 76.954(12)°, γ = 69.729(12)°, V = 924.8(2) Å 3 , Z = 2, R gt ( F ) = 0.0574, wR ref ( F 2 ) = 0.1609, T = 293(2) K.
Open Access
Crystal structure of methyl 4′-amino-3′,5′-diisopropyl-[1,1′-biphenyl]-4-carboxylate, C₂₀H₂₅NO₂

March 3, 2018

Mao-Yuan Zhang, Da-Bin Shi

Page range: 421-422

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C 20 H 25 NO 2 , monoclinic, P 2 1 / n (no. 14), a = 16.873(4) Å, b = 6.2095(16) Å, c = 16.992(4) Å, β = 100.775(4)°, V = 1748.9(8) Å 3 , Z = 4, R gt ( F ) = 0.0473, wR ref ( F 2 ) = 0.1417, T = 296(2) K.
Open Access
Crystal structure of (η⁶-1-isopropyl-4-methyl benzene)-(N-(2,5-dichlorophenyl)-1-(pyridin-2-yl)methanimine-κ²N,N′)ruthenium(II) perchlorate, C₂₂H₂₂Cl₄N₂O₄Ru

March 30, 2018

Joel M. Gichumbi, Bernard Omondi, Holger B. Friedrich

Page range: 423-425

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C 22 H 22 Cl 4 N 2 O 4 Ru, monoclinic, P 2 1 / c (no. 14), a = 15.0181(3) Å, b = 10.3983(2) Å, c = 16.6496(3) Å, β = 112.459(1)°, V = 2402.84(8) Å 3 , Z = 4, R gt ( F ) = 0.0180, wR ref ( F 2 ) = 0.0474, T = 173(2) K.
Open Access
Crystal structure of 2-(2-(1-Chlorocyclopropyl)-3-(2-chlorophenyl)-2-hydroxypropyl)-1H-1,2,4-triazole-3(2H)-thione, C₁₄H₁₅Cl₂N₃OS

March 10, 2018

Lu Tao, Nie Xu-Liang, Li Zhong-Chao, Lin Ping, Shang-guan Xin-Chen, Yin Zhong-Ping, Peng Da-Yong

Page range: 427-429

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C 14 H 14 Cl 2 N 3 OS, monoclinic, P 2 1 / n (no. 14), a = 9.9215(8) Å, b = 9.5992(7) Å, c = 16.5801(13) Å, β = 92.702(1)°, V = 1577.3(2) Å 3 , Z = 4, R gt ( F ) = 0.0323, wR ref ( F 2 ) = 0.0918, T = 296 K.
Open Access
Crystal structure of methyl 4′-amino-3′,5′-dimethyl-[1,1′-biphenyl]-4-carboxylate, C₁₆H₁₇NO₂

March 8, 2018

Mao-Yuan Zhang, Da-Bin Shi

Page range: 431-433

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C 16 H 17 NO 2 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 6.3761(2) Å, b = 12.0521(4) Å, c = 17.3288(5) Å, V = 1331.64(7) Å 3 , Z = 4, R gt ( F ) = 0.0462, wR ref ( F 2 ) = 0.1243, T = 153(2) K.
Open Access
The crystal structure of 1-(5-ferrocenyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)pentan-1-on, C₁₉H₁₉F₃FeN₂O

March 6, 2018

Ben-Guo Zhou, Li-Na Zhang

Page range: 435-436

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C 19 H 19 F 3 FeN 2 O, monoclinic, P 2 1 /c (no. 14), a = 10.9948(6) Å, b = 21.9829(10) Å, c = 7.8962(4) Å, β = 108.643(2)° V = 1808.35(16) Å 3 , Z = 4, R gt ( F ) = 0.0380, wR ref ( F 2 ) = 0.0934, T = 273(2) K.
Open Access
The crystal structure of (3S,12R,20R,24S)-3,12-diacetyl-20,24-epoxy-dammarane-3,12,25-triol acetone solvate, C₃₄H₅₆O₆

February 20, 2018

Liu Hongzhang, Wang Yingting

Page range: 437-439

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C 34 H 56 O 6 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 8.0343(8) Å, b = 17.7992(16) Å, c = 24.153(3) Å, V = 3453.9(6) Å 3 , Z = 4, R gt ( F ) = 0.0642, wR ref ( F 2 ) = 0.1573, T = 293(2) K.
Open Access
Crystal structure of methyl 10-(pyridin-4-yl)-anthracene-9-carboxylate, C₂₁H₁₅NO₂

March 6, 2018

Xiang Huang, Da-Bin Shi

Page range: 441-443

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C 21 H 15 NO 2 , orthorhombic, Aba 2 (no. 41), a = 22.149(2) Å, b = 13.2899(12) Å, c = 10.6679(10) Å, V = 3140.2(5) Å 3 , Z = 8, R gt ( F ) = 0.0418, wR ref ( F 2 ) = 0.0953, T = 296(2) K.
Open Access
Crystal structure of catena-poly[diaqua-bis(di(N²,N⁶-dihydroxypyridine-2,6-dicarboxamide))potassium(I)]tetrahydrate, C₁₄H₂₅N₆O₁₄K

April 5, 2018

Jian Zuo

Page range: 445-446

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C 14 H 25 N 6 O 14 K, triclinic, P 1̅ (no. 2), a = 6.9630(15) Å, b = 9.2770(17) Å, c = 9.6100(18) Å, α = 69.822(2)°, β = 87.225(2)°, γ = 85.559(2)°, V = 580.8(2) Å 3 , Z = 1, R gt ( F ) = 0.0366, wR ref ( F 2 ) = 0.1052, T = 293(2) K.
Open Access
Crystal structure of poly{[μ₂-(E)-1,4-bis(1H-benzo[d]imidazol-1-yl)but-2-ene-κ²N:N′][μ₃–cyclohexane-1,4-dicarboxylato-κ⁴O,O′:O′′:O′′′]cadmium(II)}, C₂₆H₂₆CdN₄O₄

March 27, 2018

Wen-bo Huang, Yan Yang, Jian Suo

Page range: 447-448

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C 26 H 26 CdN 4 O 4 , monoclinic, P 2 1 / c (no. 14), a = 12.1676(8) Å, b = 13.4592(9) Å, c = 15.5782(10) Å, β = 112.1310(10) Å, V = 2363.2(3) Å 3 , Z = 4, R gt ( F ) = 0.0244, wR ref ( F 2 ) = 0.0584, T = 293(2) K.
Open Access
Crystal structure of poly[aqua(μ₃-[2,2′-bipyridine]-3,3′-dicarboxylato-κ⁴N,N′:O:O′)zinc(II)] – dimethylformamide (1/1), C₁₅H₁₅N₃O₆Zn

March 9, 2018

Yingying Kou, Xianghao Ren, Junzhi Zhang

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C 15 H 15 N 3 O 6 Zn, monoclinic, P 2 1 / n (no. 14), a = 9.607(6) Å, b = 13.747(8) Å, c = 12.754(8) Å, β = 105.368(7)°, V = 1624.2(18) Å, Z = 4, R gt (F) = 0.0416, wR ref (F 2 ) = 0.1001, T = 113(2) K.
Open Access
The crystal structure of poly[tetraaqua-tris(μ₂-2,6-di(1H-imidazol-1-yl)naphthalene-κ²N:N′)-bis(thiophene-2,5-dicarboxylato-κ¹O)]dicobalt(II), C₃₀H₂₄CoN₆O₆S

April 5, 2018

Di Wang

Page range: 451-453

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C 30 H 24 CoN 6 O 6 S, monoclinic, P 2 1 / c (no. 14), a = 11.892(6) Å, b = 11.206(6) Å, c = 20.694(11) Å, β = 93.558(13)°, V = 2752(3) Å 3 , Z = 4, R gt ( F ) = 0.0413, wR ref ( F 2 ) = 0.1030, T = 293(2) K.
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Crystal structure of (S)-1-(5-(anthracen-9-yl)-3-phenyl-4,5-dihydro-1H-pyrazol-1-yl)propan-1-one, C₂₆H₂₂N₂O

March 10, 2018

Pingting Zhu, Jiaojiao Zhou

Page range: 455-456

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C 26 H 22 N 2 O, orthorhombic, Pca 2 1 (no. 29), a = 22.8108(10) Å, b = 9.8328(5) Å, c = 8.7361(3) Å, V = 1959.45(15) Å 3 , Z = 4, R gt ( F ) = 0.0380, wR ref ( F 2 ) = 0.0853, T = 296(2) K.
Open Access
Crystal structure of 5-methyl-3,3-diphenyl-1-tosyl-1,2,3,4-tetrahydropyridine, C₂₅H₂₅NO₂S

March 16, 2018

Xie Huang, Ping-an Wang, Wei He, Xiaoxia Ye

Page range: 457-458

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C 25 H 25 NO 2 S, monoclinic, P 2 1 (no. 4), a = 9.371(4) Å, b = 11.397(4) Å, c = 9.777(4) Å, β = 95.117(6)°, V = 1040.0(7) Å 3 , Z = 2, R gt ( F ) = 0.0423, wR ref ( F 2 ) = 0.0921, T = 296(2) K.
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Synthesis and crystal structure of μ-[1,1′-di(mesitylphosphanido)ferrocene]bis[η⁵-cyclopentadienylnickel(II)] tetrahydrofurane solvate, C₄₂H₄₈FeNi₂OP₂

March 8, 2018

Christina Langen, Clemens Bruhn, Ulrich Siemeling

Page range: 459-461

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C 42 H 48 FeNi 2 OP 2 , orthorhombic, Pbca (no. 61), a = 9.4551(4) Å, b = 19.7133(9) Å, c = 39.693(2) Å, V = 7398.4(6) Å 3 , Z = 8, R gt ( F ) = 0.0598, wR ref ( F 2 ) = 0.1481, T = 100(2) K.
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Synthesis and crystal structure of (E)-1-(4-(((E)-5-chloro-2-hydroxybenzylidene)amino)phenyl)ethan-1-one O-methyl oxime, C₁₆H₁₅ClN₂O₂

March 16, 2018

Jin-Xia Ma, Qing-Lin Li, Peng-Peng Li, Ji-Xing Zhao, Li Zhao

Page range: 463-464

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C 16 H 15 ClN 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 33.491(11) Å, b = 7.124(2) Å, c = 6.1977(19) Å, β = 92.212(6)°, V = 1477.6(8) Å 3 , Z = 4, R gt ( F ) = 0.0418, wR ref ( F 2 ) = 0.1193, T = 296(2) K.
Open Access
Crystal structure of bis(1-(phenylsulfonyl)-2-(1-(pyrazin-2-yl)ethylidene)hydrazin-1-ido-κ³N,N′,O)nickel(II), C₂₄H₂₂N₈O₄S₂Ni

March 27, 2018

Hao Wu, Wei-Na Wu

Page range: 465-466

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C 24 H 22 N 8 O 4 S 2 Ni, orthorhombic, Aba 2 (no. 41), a = 11.845(6) Å, b = 21.937(11) Å, c = 9.907(5) Å, V = 2574(2) Å 3 , Z = 4, R gt ( F ) = 0.0285, wR ref ( F 2 ) = 0.0657, T = 296(2) K.
Open Access
Crystal Structure of bis(1-(phenylsulfonyl)-2-(1-(pyrazin-2-yl)ethylidene)hydrazin-1-ido-κ³N,N′,O)copper(II), C₂₄H₂₂N₈O₄S₂Cu

April 5, 2018

Wan-Wan Wang, Wei-Na Wu, Yuan Wang

Page range: 467-468

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C 24 H 22 N 8 O 4 S 2 Cu, orthorhombic, Aba 2 (no. 41), a = 11.9395(18) Å, b = 21.813(3) Å, c = 10.1184(15) Å, V = 2635.2(7) Å 3 , Z = 4, R gt ( F ) = 0.0395, wR ref ( F 2 ) = 0.0912, T = 296(2) K.
Open Access
Synthesis and crystal structure of poly[aqua{μ₃-(1S,2S)-1-((7-hydroxy-3-(4-hydroxy-3-sulfonatophenyl)-4-oxo-4H-chromen-8-yl)methyl)pyrrolidin-1-ium-2-carboxylato-κ⁴O,O′:O′′:O′′′}sodium(I)] monohydrate, C₂₁H₂₂NNaO₁₁S

March 10, 2018

Hai-Lin Chen, Li-Wei Pan, Hui-Ying Zhang, Xiu-Ju Yin

Page range: 469-471

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C 21 H 22 NN a O 11 S, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 8.0489(4) Å, b = 10.6418(5) Å, c = 24.4850(10) Å, V = 2097.26(17) Å 3 , Z = 4, R gt (F) = 0.0513, wR ref (F 2 ) = 0.1350, T = 150(2) K.
Open Access
Halogen bonds in the crystal structure of 1,4-diiodotetrafluorobenzene–1,2-bis(4-pyridyl)propane (1/1), C₁₉H₁₄F₄I₂N₂

March 8, 2018

Limin Dang, Saijin Huang, Aiwu Yin

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C 19 H 14 F 4 I 2 N 2 , monoclinic, I 2/ a (no. 15), a = 20.997(2) Å, b = 4.4785(3) Å, c = 23.242(3) Å, β = 113.532(14)°, V = 2003.8(4) Å 3 , Z = 8, R gt (F) = 0.0684, w R ref (F 2 ) = 0.0706, T = 287 K.
Open Access
Crystal structure of bis(μ-N-i-propyl-N-n-propyldithiocarbamato-κ²S:S′) bis(N-i-propyl-N-n-propyldithiocarbamato-κ²S,S′)dizinc(II), C₂₈H₅₆N₄S₈Zn₂

March 16, 2018

Yee Seng Tan, Edward R.T. Tiekink

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C 28 H 56 N 4 S 8 Zn 2 , monoclinic, P 2 1 / n (no. 14), a = 9.4123(2) Å, b = 19.2708(4) Å, c = 11.5228(3) Å, β = 107.202(2)°, V = 1996.54(8) Å 3 , Z = 2, R gt ( F ) = 0.0254, wR ref ( F 2 ) = 0.0572, T = 100(2) K.
Open Access
Crystal structure of bis(μ-N-i-propyl-N-n-propyldithiocarbamato-κ³S,S′:S)bis(N-i-propyl-N-n-propyldithiocarbamato-κ²S,S′)dicadmium(II), C₂₈H₅₆Cd₂N₄S₈

March 30, 2018

Yee Seng Tan, Edward R.T. Tiekink

Page range: 481-483

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C 28 H 56 Cd 2 N 4 S 8 , monoclinic, P 2 1 / n (no. 14), a = 9.9003(3) Å, b = 11.7373(3) Å, c = 17.4539(5) Å, β = 102.999(3)°, V = 1976.22(10) Å 3 , Z = 2, R gt ( F ) = 0.0243, wR ref ( F 2 ) = 0.0582, T = 100 K.
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Crystal structure of bis(μ₂-di-n-butyldithiocarbamato-κ³S,S′:S;κ³S:S:S′)-hexacarbonyl-di-rhenium(I), C₂₄H₃₆N₂O₆Re₂

March 16, 2018

Peter J. Heard, Nathan R. Halcovitch, Lee See Mun, Edward R.T. Tiekink

Page range: 485-487

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C 24 H 36 N 2 O 6 Re 2 , triclinic, P 1̅ (no. 2), a = 10.3013(2) Å, b = 11.3471(2) Å, c = 14.5967(3) Å, α = 72.540(2)°, β = 73.074(2)°, γ = 85.369(2)°, V = 1557.05(6) Å 3 , Z = 2, R gt ( F ) = 0.0214, wR ref ( F 2 ) = 0.0466, T = 100(2) K.
Open Access
Crystal structure of 7-(4-methylphenyl)imidazo[1,2-a][1,3,5]triazin-4-amine, C₁₂H₁₁N₅

March 15, 2018

Felicia Phei Lin Lim, Anton V. Dolzhenko, Nathan R. Halcovitch, Edward R.T. Tiekink

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C 12 H 11 N 5 , monoclinic, P 2 1 / n (no. 14), a = 7.3455(1) Å, b = 12.2470(1) Å, c = 12.1689(1) Å, β = 103.505(1)°, V = 1064.45(2) Å 3 , Z = 4, R gt ( F ) = 0.0365, wR ref ( F 2 ) = 0.0987, T = 100 K.
Open Access
Crystal structure of the co-crystal O-isopropyl phenylcarbamothioate – 4,4′-bipyridine (2/1), C₁₅H₁₇N₂OS

April 5, 2018

Chien Ing Yeo, Edward R.T. Tiekink

Page range: 491-492

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C 15 H 17 N 2 OS, triclinic, P 1̄ (no. 2), a = 5.8595(3) Å, b = 9.2967(4) Å, c = 14.0545(8) Å, α = 83.320(4), β = 89.240(4), γ = 74.524(4), V = 732.71(7) Å 3 , Z = 2, R gt ( F ) = 0.0458, wR ref ( F 2 ) = 0.1231, T = 100 K.
Open Access
Crystal structure of the coordination polymer catena-poly[chlorido-{μ₂-2-(((3,5-dimethyl-1H-pyrazol-1-yl)methyl)amino)-3-hydroxybutanoato-κ⁴N,N,O:O′}copper(II)], C₁₁H₁₆ClCuN₂O₃

March 10, 2018

Mouslim Messali, Rafika El Ati, Rachid Touzani, Mohamed Reda Aouad, Ismail Warad

Page range: 493-494

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C 11 H 16 ClCuN 2 O 3 , monoclinic, P 2 1 / n (no. 14), a = 5.6017(4) Å, b = 10.7601(8) Å, c = 10.4036(8) Å, β = 95.697(2)°, V = 623.98(8) Å 3 , Z = 2, R gt ( F ) = 0.0321, wR ref ( F 2 ) = 0.0833, T = 100(1) K.
Open Access
Synthesis and crystal structure of bis(μ₂-acetato-κ²O:O′)-di(ethanol)-bis{μ₂-5-(N,N′-diethylamine)-5′-methoxyl-2,2′-[ethylenediyldioxybis(nitrilomethylidyne)]diphenolato-κ⁶O:O,N,N,O′:O′}trinickel(II) – ethanol – acetonitrile (1/2/2), C₅₈H₈₆Ni₃N₈O₁₈

March 30, 2018

Ren Zong-Li, An Xiao-Xin, Liu Ling-Zhi, Lan Peng-Fei, Dong Wen-Kui

Page range: 495-497

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C 58 H 86 Ni 3 N 8 O 18 , triclinic, P 1̅ (no. 2), a = 11.4561(8) Å, b = 13.1859(8) Å, c = 13.5063(11) Å, α = 109.620(7)°, β = 101.234(7)°, γ = 114.469(6)°, V = 1611.1(2) Å 3 , Z = 1, R gt ( F ) = 0.0518, wR ref ( F 2 ) = 0.1315, T = 173.69(10) K.
Open Access
Crystal structure of the bis((E)-O-ethyl-N-phenylthiocarbamate) – 4,4′-bipyridine co-crystal (2/1), C₂₈H₃₀N₄O₂S₂

March 15, 2018

Chien Ing Yeo, Edward R.T. Tiekink

Page range: 499-501

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C 28 H 30 N 4 O 2 S 2 , triclinic, P 1̄ (no. 2), a = 10.1450(6) Å, b = 11.6401(11) Å, c = 11.8506(10) Å, α = 102.850(8)°, β = 105.028(6)°, γ = 94.135(6)°, V = 1305.14(19) Å 3 , Z = 2, R gt ( F ) = 0.047, wR ref ( F 2 ) = 0.139, T = 100(2) K.
Open Access
Crystal structure of the (E)-O-methyl-N-phenyl-thiocarbamate – 4,4′-bipyridine (1/1), C₁₈H₁₇N₃OS

March 16, 2018

Chien Ing Yeo, Edward R.T. Tiekink

Page range: 503-505

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C 18 H 17 N 3 OS, monoclinic, C 2/ c (no. 15), a = 13.4754(3) Å, b = 13.8997(3) Å, c = 18.0300(4) Å, β = 107.202(3)°, V = 3226.03(13) Å 3 , Z = 8, R gt ( F ) = 0.0341, wR ref ( F 2 ) = 0.0878, T = 100(2) K.
Open Access
Crystal structure of bis(μ₂-diethyldithiocarbamato-κ³S,S′:S′)-bis(tricyclohexylphosphane-κP)dicopper(I), C₄₆H₈₆Cu₂N₂P₂S₄

March 10, 2018

Yi Jiun Tan, Chien Ing Yeo, Nathan R. Halcovitch, Edward R.T. Tiekink

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C 46 H 86 Cu 2 N 2 P 2 S 4 , triclinic, P 1̄ (no. 2), a = 9.9626(3) Å, b = 11.0489(3) Å, c = 12.3604(3) Å, α = 106.205(3)°, β = 99.165(2)°, γ = 100.306(3)°, V = 1253.53(6) Å 3 , Z = 1, R gt ( F ) = 0.0232, wR ref ( F 2 ) = 0.0555, T = 100(2) K.
Open Access
Crystal structure of N-(3-chlorophenyl)ethoxycarbothioamide, C₉H₁₀ClNOS

March 30, 2018

Yee Seng Tan, Chien Ing Yeo, Edward R.T. Tiekink

Page range: 511-512

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C 9 H 10 ClNOS, monoclinic, C 2/ c (no. 15), a = 18.8783(6) Å, b = 4.5518(2) Å, c = 23.6739(8) Å, β = 91.501(4)°, V = 2033.61(13) Å 3 , Z = 8, R gt ( F ) = 0.033, wR ref ( F 2 ) = 0.082, T = 100(2) K.
Open Access
Crystal structure of bis(μ₂-pyrrolidine-1-carbodithioato-κ³S,S′:S;κ³S:S:S′)-bis(tricyclohexylphosphane-P)-di-copper(I), C₄₆H₈₂Cu₂N₂P₂S₄

March 30, 2018

Yi Jiun Tan, Chien Ing Yeo, Nathan R. Halcovitch, Edward R.T. Tiekink

Page range: 513-515

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C 46 H 82 Cu 2 N 2 P 2 S 4 , triclinic, P 1̄ (no. 2), a = 11.6189(2) Å, b = 12.2846(2) Å, c = 18.1744(2) Å, α = 97.3210(10)°, β = 106.3080(10)°, γ = 99.312(2)°, V = 2415.65(7) Å 3 , Z = 2, R gt ( F ) = 0.025, wR ref ( F 2 ) = 0.066, T = 100(2) K.
Open Access
Crystal structure of N-(2-chlorophenyl)methoxycarbothioamide, C₈H₈ClNOS

March 27, 2018

Chien Ing Yeo, Edward R.T. Tiekink

Page range: 517-518

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C 8 H 8 ClNOS, triclinic, P 1̅ (no. 2), a = 6.7658(5) Å, b = 8.0344(10) Å, c = 9.6285(12) Å, α = 66.279(12)°, β = 72.245(9)°, γ = 87.699(8)°, V = 454.31(10) Å 3 , Z = 2, R gt ( F ) = 0.056, wR ref ( F 2 ) = 0.158, T = 100 K.
Open Access
Crystal structure of chlorido-methanol-(N-(2-(oxy)-3-methoxybenzylidene)pyridine-4-carbohydrazonato-κ³O,N,O′)-(4-methylphenyl)methyl-tin(IV), C₂₃H₂₄ClN₃O₄Sn

April 5, 2018

Lee See Mun, Nathan R. Halcovitch, Edward R.T. Tiekink

Page range: 519-521

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C 23 H 24 ClN 3 O 4 Sn, triclinic, P 1̄ (no. 2), a = 9.7536(2) Å, b = 10.0755(2) Å, c = 12.4215(3) Å, α = 84.928(2)°, β = 72.544(2)°, γ = 74.382(2)°, V = 1121.44(4) Å 3 , Z = 2, R gt ( F ) = 0.021, wR ref ( F 2 ) = 0.054, T = 100(2) K.
Open Access
Crystal structure of N-(3-chlorophenyl)(propan-2-yloxy)carbothioamide, C₁₀H₁₂ClNOS

April 6, 2018

Chien Ing Yeo, Edward R.T. Tiekink

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C 10 H 12 ClNOS, monoclinic, P 2 1 / n (no. 14), a = 13.2003(12) Å, b = 6.0448(6) Å, c = 13.9403(13) Å, β = 101.9180(10)°, V = 1088.36(18) Å 3 , Z = 4, R gt ( F ) = 0.0291, wR ref ( F 2 ) = 0.0807, T = 100(2) K.
Open Access
Crystal structure of 1-[(Z)-[4-(4-methoxyphenyl)butan-2-ylidene]amino]-3-phenylurea, C₁₈H₂₁N₃O₂

March 27, 2018

Ming Yueh Tan, Karen A. Crouse, Thahira B.S.A. Ravoof, Edward R.T. Tiekink

Page range: 525-527

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C 18 H 21 N 3 O 2 , triclinic, P 1̅ (no. 2), a = 8.5155(4) Å, b = 10.6415(4) Å, c = 19.0732(10) Å, α = 80.918(4)°, β = 89.689(4)°, γ = 80.666(4)°, V = 1683.74(14) Å 3 , Z = 4, R gt ( F ) = 0.055, wR ref ( F 2 ) = 0.133, T = 100 K.
Open Access
A triclinic polymorph of bis(μ-N,N-bis(2-hydroxyethyl)dithiocarbamato-κ³S,S′:S′) bis(N,N-bis(2-hydroxyethyl)dithiocarbamato-κ²S:S′)zinc(II), C₂₀H₄₀N₄O₈S₈Zn₂

February 20, 2018

Pavel Poplaukhin, Edward R.T. Tiekink

Page range: 529-531

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C 20 H 40 N 4 O 8 S 8 Zn 2 , triclinic, P 1̄ (no. 2), a = 7.0675(10) Å, b = 9.9000(10) Å, c = 12.9252(17) Å, α = 106.813(10)°, β = 93.741(9)°, γ = 109.863(8)°, V = 800.65(18) Å 3 , Z = 2, R gt ( F ) = 0.069, wR ref ( F 2 ) = 0.176, T = 98(2) K.

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