Volume 233, Issue 4

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Zeitschrift für Kristallographie - New Crystal Structures

Contents

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Cover and Frontmatter

June 30, 2018

Page range: i-viii

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Open Access
Crystal structure of (E)-1-(4-(((E)-2-hydroxy-5-methylbenzylidene)amino)phenyl)ethan-1-one O-methyl oxime, C₁₇H₁₈N₂O₂

May 22, 2018

Peng-Peng Li, Jin-Xia Ma, Qing-Lin Li, Ji-Xing Zhao, Li Zhao

Page range: 533-534

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C 17 H 18 N 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 33.536(6) Å, b = 7.0566(10) Å, c = 6.1491(10) Å, β = 91.048(5)°, Z = 4, V = 1455.0(4) Å 3 , R gt ( F ) = 0.0672, wR ref ( F 2 ) = 0.1823, T = 296(2) K.
Open Access
Crystal structure of 1,3,5,7-tetraazaadamantane-1,3-diium 2,5-dicarboxyterephthalate, C₁₆H₁₈N₄O₈

May 18, 2018

Xiao Wei, Bao Guang-Ming, Sun Ting-Ting, Hu Chun-Yan, Yuan Hou-Qun

Page range: 535-536

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C 16 H 18 N 4 O 8 , monoclinic, C 2/ m (no. 12), a = 14.517(4) Å, b = 18.006(7) Å, c = 6.916(3) Å, β = 116.97(3)°, V = 1611.2(11) Å 3 , Z = 4, R gt ( F ) = 0.0497, wR ref ( F 2 ) = 0.1387, T = 296(2) K.
Open Access
Crystal structure of guanidinium tetrabutyl-ammonium 5-hydroxyisophthalate dihydrate, C₂₅H₅₀N₄O₇

June 2, 2018

Yalin Liu, Qiufang Li

Page range: 537-538

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C 25 H 50 N 4 O 7 , monoclinic, P 2 1 / c (no. 14), a = 14.7637(11) Å, b = 12.0608(9) Å, c = 16.7391(14) Å, β = 101.086(1)°, V = 2925.0(4), Z = 4, R gt ( F ) = 0.0489, wR ref ( F 2 ) = 0.1076, T = 296(2) K.
Open Access
Crystal structure of poly[aqua-(μ₂-5-methoxyisophthalate-κ³O,O′:O′′)-(μ₂-1,4-bis((1H-1,2,4-triazol-1-yl)methyl)benzene-κ²N:N′)nickel(II), NiC₂₁H₂₀N₆O₆

May 18, 2018

Hong-Ru Fu

Page range: 539-541

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C 21 H 20 NiN 6 O 6 , triclinic, P 1̄ (no. 2), a = 10.1526(16) Å, b = 11.0670(18) Å, c = 11.1729(18) Å, α = 71.559(2)°, β = 69.827(2)°, γ = 70.439(2)°, V = 1081.3(3) Å 3 , Z = 2, R gt ( F ) = 0.0370, wR ref ( F 2 ) = 0.0911, T = 296(2) K.
Open Access
Crystal structure of aqua-bis(3,4-dimethoxybenzoato-κ¹O)-(2,2′-bipyridine-κ²N,N′)copper(II), C₂₈H₂₆CuN₂O₉

May 30, 2018

Guofang He, Junshan Sun

Page range: 543-544

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C 28 H 26 CuN 2 O 9 , monoclinic, C 2/ c , a = 12.3146(11) Å, b = 11.1769(10) Å, c = 19.3856(17) Å, β = 101.012(1), V = 2619.1(4) Å 3 , Z = 4, R gt ( F ) = 0.0350, wR ref ( F 2 ) = 0.1005, T = 296(2) K.
Open Access
Crystal structure of catena-poly[aqua-(μ₂-(3,5-di(1H-imidazol-1-yl)-pyridine-κ²N:N′)-(μ₂-2-(carboxylatomethyl)benzoato-κ²O:O′)] cadmium(II), C₂₀H₁₇CdN₅O₅

April 18, 2018

Lu Wei-Wei, Ju Feng-Yang

Page range: 545-546

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C 20 H 17 CdN 5 O 5 , triclinic, P 1̄ (no. 2), a = 8.7620(9) Å, b = 10.7139(11) Å, c = 11.8897(12) Å, α = 63.957(2)°, β = 82.294(2)°, γ = 74.709(2)°, V = 967.10(17) Å 3 , Z = 2, R gt ( F ) = 0.0203, wR ref ( F 2 ) = 0.0489, T = 296(2) K.
Open Access
The crystal structure of catena-poly[chlorido-(μ₂-5-methyl-1,3,4-thiadiazole-2-thiolato-κ²S:N)mercury(II)], C₃H₃ClHgN₂S₂

May 30, 2018

Lian-Wei Liu, Bang-Tun Zhao

Page range: 547-548

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C 3 H 3 ClHgN 2 S 2 , orthorhombic, Pna 2 1 (no. 33), a = 18.794(8) Å, b = 4.0798(17) Å, c = 10.093(4) Å, V = 773.8(6) Å 3 , Z = 4, R gt ( F ) = 0.0437, wR ref ( F 2 ) = 0.1024, T = 291(2) K.
Open Access
Crystal structure of (E)-2,4-dichloro-6-(((4-methyl-2-nitrophenyl)imino)methyl)phenol, C₁₄H₁₀Cl₂N₂O₃

May 3, 2018

Yong Hong, Wei Liu, Jie Wu

Page range: 549-550

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C 14 H 10 Cl 2 N 2 O 3 , monoclinic, P 2 1 / c (no. 14), a = 13.3172(15) Å, b = 7.0899(7) Å, c = 14.8280(15) Å, β = 96.739(3)°, V = 1390.4(3) Å 3 , Z = 4, R gt ( F ) = 0.0423, wR ref ( F 2 ) = 0.1137, T = 150(2) K.
Open Access
Crystal structure of a new polymorph of bis[μ-1,3-bis(diphenylphosphino)propane-κ²P:P′-disilver(I)] bis(tetrafluoroborate), [Ag(dppp)]₂(BF₄)₂, C₅₄H₅₂Ag₂B₂F₈P₄

May 29, 2018

Xiao-Nan Kuang, Sen Lin, Si-Fan Li, Yue Li, Xiu-Lan Xin, Qiong-Hua Jin

Page range: 551-553

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C 54 H 52 Ag 2 B 2 F 8 P 4 , triclinic, P 1̄ a = 11.4869(4) Å, b = 12.9118(5) Å, c = 19.6858(6) Å, α = 100.8240(10)°, β = 102.185(2)°, γ = 110.470(3)°, V = 2562.31(15) Å 3 , Z = 2, R gt ( F ) = 0.0263, wR ref ( F 2 ) = 0.0666, T = 293(2) K.
Open Access
The crystal structure of 2-phenyl-4,6-bis(R-tert-butylsulfonamido)-1,3,5-triazine – ethyl acetate (2/1), C₃₈H₅₈N₁₀O₆S₄

May 18, 2018

Zhenyu Zuo, Fuhou Lei, Yang Dai, Lu Wang

Page range: 555-557

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C 38 H 58 N 10 O 6 S 4 , monoclinic, P 2 1 (no. 4), a = 11.9542(5) Å, b = 11.4057(5) Å, c = 17.2763(8) Å, β = 96.380(1)° V = 2340.97(18) Å 3 , Z = 4, R gt ( F ) = 0.0325, wR ref ( F 2 ) = 0.0836, T = 200 K.
Open Access
Crystal structure of 6-amino-8-(2-methoxy-phenyl)-2-methyl-2,3,8,8a-tetrahydro-1H-iso-quinoline-5,7,7-tricarbonitrile monohydrate, C₂₀H₂₁N₅O₂

May 16, 2018

Yan Quan

Page range: 559-560

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C 20 H 21 N 5 O 2 , monoclinic, P 2 1 / c (no. 14), a = 14.594(4) Å, b = 9.366(5) Å, c = 14.147(4) Å, β = 93.749(18)°, V = 1929.6(12) Å 3 , Z = 4, R gt ( F ) = 0.061, wR ref ( F 2 ) = 0.213, T = 296(2) K.
Open Access
Crystal structure of methyl (1-phenylethyl)carbamate, C₁₀H₁₃NO₂

April 27, 2018

Amit S. Thakar, Pramod B. Pansuriya, Holger B. Friedrich, Glenn E. M. Maguire

Page range: 561-563

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C 10 H 13 NO 2 , monoclinic, P 2 1 (no. 14), a = 9.9882(7) Å, b = 8.5202(6) Å, c = 23.1403(18) Å, β = 91.010(2)°, V = 1969.0(2) Å 3 , Z = 8, R gt ( F ) = 0.0387, wR ref ( F 2 ) = 0.0919, T = 173(2)K.
Open Access
Crystal structure of dimethanol-(μ₂-squarato-κ²O:O′)-tetrakis(tri-p-tolylphosphane-κP)disilver(I) – methanol (1/2), C₉₂H₉₈Ag₂O₈P₄

April 7, 2018

Kuanguan Liu, Jing Nie

Page range: 565-567

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C 92 H 98 Ag 2 O 8 P 4 , triclinic, P 1̄ (no. 2), a = 11.179(3) Å, b = 12.623(3) Å, c = 15.656(4) Å, α = 83.607(8)°, β = 78.636(9)°, γ = 83.128(9)°, V = 2141.6(10) Å 3 , Z = 2, R gt ( F ) = 0.0398, wR ref ( F 2 ) = 0.1034, T = 294(2) K.
Open Access
Crystal structure of catena-poly[bis(μ₂-1,4-bis(triazol-1-ylmethyl)benzene-κ²N:N′)-bis(5-tert-butyl-isophthalate-κO)copper(II)]tetrahydrate, C₃₆H₄₆CuN₆O₁₂

April 12, 2018

Ying Zhao, San-Tai Wang

Page range: 569-570

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C 36 H 46 CuN 6 O 12 , triclinic, P 1̅ (no. 2), a = 8.3759(18) Å, b = 10.749(2) Å, c = 11.873(3) Å, α = 63.165(2)°, β = 82.979(2)°, γ = 80.932(2)°, V = 940.3(3) Å 3 , Z = 1, R gt ( F ) = 0.0460, wR ref ( F 2 ) = 0.1107, T = 296(2) K.
Open Access
Crystal structure of 4-aminopyridinium 4-acetyl-(pyridin-4-yl)-1H-1,2,3-triazol-5-olate monohydrate, C₁₄H₁₆N₆O₃

April 12, 2018

Jonathan Cisterna, Alejandro Cárdenas, Iván Brito

Page range: 571-573

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C 14 H 16 N 6 O 3 , triclinic, space group P 1̅ (no. 2), a = 7.7890(5) Å, b = 8.6069(6) Å, c = 12.4753(8) Å, α = 77.064(4)°, β = 72.754(3)°, γ = 67.148(3)°, V = 730.40(9) Å 3 , Z = 2, R gt ( F ) = 0.0594, w R ref ( F 2 ) = 0.1542, T = 297(2) K.
Open Access
Crystal structure of 2-(8-bromo-2-phenylimidazo[1,2-α]pyridin-3-yl)-6,7-dimethyl-3-phenylquinoxaline, C₂₉H₂₁BrN₄

April 12, 2018

Gui Ting Song, Jiang Ping Meng, Jin Zhu

Page range: 575-577

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C 29 H 21 BrN 4 , orthorhombic, Pca 2 1 (no. 29), a = 15.6577(5) Å, b = 9.6445(3) Å, c = 31.1869(10) Å, V = 4709.6(2) Å 3 , Z = 8, R gt ( F ) = 0.0435, wR ref ( F 2 ) = 0.0779, T = 293(2) K.
Open Access
Crystal structure of aqua(1-(2-pyridyl)ethanone oxime-κ²N,N′)(1-(2-pyridyl)ethanone oximato-κ²N,N′) nitrate monohydrate, C₁₄H₁₉N₅O₇Cu

April 7, 2018

Jian Zuo

Page range: 579-581

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C 14 H 19 N 5 O 7 Cu, triclinic, P 1̅ (no. 2), a = 10.8164(15) Å, b = 11.4831(17) Å, c = 15.423(2) Å, α = 101.035(3)°, β = 100.538(2)°, γ = 101.708(2)°, V = 1791.5(4) Å 3 , Z = 4, R gt ( F ) = 0.0416, wR ref ( F 2 ) = 0.1131, T = 298(2) K.
Open Access
Crystal structure of poly[tetraaqua-(μ₄-oxalato-κ⁴O,O′:O′′,O′′′)-(μ₈-benzene-1,2,4,5-tetracarboxylato-κ⁸O¹:O²:O³:O⁴:O⁵:O⁶:O⁷:O⁸)yttrium(III)], C₆H₅O₈Y

May 22, 2018

Zhi-Hui Wen, Xiao-Xi Zhao, Dan Zhao

Page range: 583-584

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C 6 H 5 O 8 Y, triclinic, P 1̄ (no. 2), a = 6.2090(17) Å, b = 8.573(4) Å, c = 8.863(2) Å, α = 111.018(6)°, β = 109.850(4)°, γ = 91.866(6)°, V = 407.8(2) Å 3 , Z = 2, R gt (F) = 0.0435, wR ref ( F 2 ) = 0.1332, T = 296(2) K.
Open Access
Crystal structure of bis{catena-poly[(μ₂-1,2-bis(4-pyridyl)ethane-κ²N:N′)silver(I)]} diaqua-bis(5-(4-carboxyphenyl)pyridine-2-carboxylato-κ²N,O)-(μ₂-1,2-bis(4-pyridyl)ethane-κ²N:N′)disilver(I) octahydrate, C₃₁H₃₅Ag₂N₄O₉

April 30, 2018

Hui-Tao Fan, Jie Ding, Jing-Peng Xie, Kun Wang

Page range: 585-587

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C 31 H 35 Ag 2 N 4 O 9 , triclinic, P 1̄ (No. 2), a = 8.8351(5) Å, b = 13.1492(6) Å, c = 14.7094(8) Å, V = 1618.76(15) Å 3 , α = 85.491(4) Å, β = 84.285(5) Å, γ = 72.413(4) Å, Z = 2, R gt ( F ) = 0.0382, wR ref ( F 2 ) = 0.0796, T = 293(2) K.
Open Access
Crystal structure of (E)-N-(2-(benzylamino)-2-oxo-1-(4-oxo-4H-chromen-3-yl)ethyl)-N-(4-bromophenyl)-3-chloroacrylamide hydrate, C₂₇H₂₂BrClN₂O₅

May 29, 2018

Jiang Ping Meng, Jie Lei

Page range: 589-590

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C 27 H 22 BrClN 2 O 5 , triclinic, P 1̄, a = 6.8549(4) Å, b = 13.2863(12) Å, c = 14.3690(13) Å, α = 85.944(7)°, β = 84.882(6)°, γ = 89.932(6)°, V = 1300.18(18) Å 3 , Z = 2, R gt ( F ) = 0.0655, wR ref ( F 2 ) = 0.1841, T = 293(2) K.
Open Access
Crystal structure of catena-poly[octaaqua-bis(μ₂-4,6-dicarboxyisophthalate-κ²O:O′)cadmium(II)disodium(I)] dihydrate, C₂₀H₂₈CdNa₂O₂₆

May 30, 2018

Ya-Li Xue, Ai-Yun Zhang, Dan Zhao

Page range: 591-592

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C 20 H 28 CdNa 2 O 26 , monoclinic, C 2/ m (no. 12), a = 7.4169(8) Å, b = 20.183(2) Å, c = 10.5403(11) Å, β = 103.5520(10)°, V = 1533.9(3) Å 3 , Z = 2, R gt ( F ) = 0.0434, wR ref ( F 2 ) = 0.1271, T = 296(2) K.
Open Access
Crystal structure of acetonitrile{bis(2-benzimidazolylmethyl)amine-κ³N,N′,N′′}-{maleato-κO}zinc(II) perchlorate - acetonitrile (1/1), C₂₄H₂₄ClN₇O₈Zn

April 13, 2018

Jiang-Li Chen, Chen Wang, Guo-Hua Su, Feng-Mei Nie

Page range: 593-595

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C 24 H 24 ClN 7 O 8 Zn, triclinic, P 1̅ (no. 2), a = 10.0834(7) Å, b = 10.8269(7) Å, c = 13.1958(8) Å, α = 77.658(5)°, β = 77.135(5)°, γ = 87.797(5)°, V = 1371.93(15) Å 3 , Z = 2, R gt ( F ) = 0.0410, wR ref ( F 2 ) = 0.1015, T = 105.6 K.
Open Access
Crystal structure of 2-amino-4-(3,5-dibromo-4-hydroxyphenyl)-7-methyl-5-oxo-2H,5H-pyrano[4,3-b]pyran-3-carbonitrile, C₁₆H₁₀Br₂N₂O₄

May 22, 2018

Jing Li, Wei Gou

Page range: 597-598

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C 16 H 10 Br 2 N 2 O 4 , monoclinic, P 2 1 / n (no. 14), a = 12.885(9) Å, b = 8.781(6) Å, c = 15.692(11) Å, β = 112.258(13)°, V = 1643.2(19) Å 3 , Z = 4, R gt ( F ) = 0.0526, wR ref ( F 2 ) = 0.1284, T = 296(2) K.
Open Access
Crystal structure of catena-poly[diaqua-(μ₂-3,5-bis(pyridin-4-ylmethoxy)benzoate-κ²N:O) manganese(II)] tetrahydrate [(3,5-bis-(pyridin-4-ylmethoxy)-benzoic-κ¹Oκ¹N) manganese(II)] trihydrate, C₃₈H₄₂MnN₄O₁₄

April 18, 2018

Gui-Hua Zou, Yu-Long Zou, Guang-Zhi Shen

Page range: 599-600

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C 38 H 42 MnN 4 O 14 , monoclinic, C 2/ c (no. 15), a = 19.165(12) Å, b = 10.116(6) Å, c = 20.734(13) Å, β = 99.021(11)°, V = 3970(4) Å 3 , Z = 4, R gt ( F ) = 0.0486, wR ref ( F 2 ) = 0.1442, T = 293(2) K.
Open Access
The crystal structure of 2-carboxybenzaldehyde-2-phenylacetohydrazone, C₁₆H₁₄N₂O₃

April 13, 2018

Li Peng-Fei, Cao Chang-Qing, Tai Xi-Shi

Page range: 601-602

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C 16 H 14 N 2 O 3 , triclinic, P 1̄ (no. 2), a = 7.7698(16) Å, b = 8.3020(17) Å, c = 12.197(2) Å, α = 92.94(3)°, β = 107.03(3)°, γ = 110.41(3)°, V = 694.6(3) Å 3 , Z = 2, R gt ( F ) = 0.0582, wR ref ( F 2 ) = 0.1683, T = 293(2) K.
Open Access
The crystal structure of poly[μ₂-aqua-(μ₂-2-naphthylamine-1-sulfonato-κ³O,O′:O′′)sodium(I)], C₁₀H₁₀N₁O₄S₁Na

May 18, 2018

Feng Yi-Min, Guo Hong-Mei, Liu Qing-Yun, Tai Xi-Shi

Page range: 603-604

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C 10 H 10 N 1 O 4 S 1 Na, monoclinic, P 2 1 / c , a = 16.737(3) Å, b = 6.6610(13) Å, c = 10.427(2) Å, β = 97.69(3)°, V = 1152.0(4) Å 3 , Z = 4, R gt ( F ) = 0.0419, wR ref ( F 2 ) = 0.1104, T = 293(2) K.
Open Access
The crystal structure of phthalazin-1(2H)-one, C₈H₆N₂O₁

April 18, 2018

Zhang Yun-Chen, Guo Hong-Mei, Li Peng-Fei, Liu Qing-Yun, Tai Xi-Shi

Page range: 605-606

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C 8 H 6 N 2 O 1 , monoclinic, P 2 1 / c (no. 14), a = 8.6277(17) Å, b = 13.134(3) Å, c = 13.062(5) Å, β = 110.54(3)°, V = 1386.0(7) Å 3 , Z = 8, R gt ( F ) = 0.0512, wR ref ( F 2 ) = 0.1581, T = 293(2) K.
Open Access
Crystal structure of 3,5-bis(trifluoromethyl)benzyl(Z)-N-(adamantan-1-yl)morpholine-4-carbothioimidate, C₂₄H₂₈F₆N₂OS

April 7, 2018

Lamya H. Al-Wahaibi, Hanan M. Hassan, Hazem A. Ghabbour, Ali A. El-Emam

Page range: 607-609

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C 24 H 28 F 6 N 2 OS, monoclinic, P 2 1 / n (no. 14), a = 17.4112(7) Å, b = 8.3694(3) Å, c = 17.6728(7) Å, β = 104.612(2)°, V = 2492.01(17) Å 3 , Z = 4, R gt ( F ) = 0.0603, wR ( F 2 ) = 0.1704, T = 293(2) K.
Open Access
Crystal structure of diazido-bis(μ₂-pyridin-2-ylmethanolato-κ²N:O)-bis(pyridin-2-ylmethanolato-κ²N,O)dicobalt(III) – methanol (1/3), C₂₇H₃₅Co₂N₁₀O₇

April 20, 2018

Yu Youzhu, Shen Yanhong, Niu Yongsheng, Zheng Xiaoming, Han Xi, Chang Songyang

Page range: 611-613

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C 27 H 35 Co 2 N 10 O 7 , orthorhombic, Pna 2 1 (no. 33), a = 29.6280(13) Å, b = 7.5784(3) Å, c = 14.3600(7) Å, V = 3224.3(2) Å 3 , Z = 4, R gt ( F ) = 0.0409, wR ref ( F 2 ) = 0.1133, T = 296(2) K.
Open Access
Crystal structure of N-[[(4,6-dimethoxy-2-pyrimidinyl)amino]carbonyl]-3-(2,2,2-trifluoroethoxy)-2-pyridinesulfonamide, C₁₄H₁₄F₃N₅O₆S

April 20, 2018

Song Xiu-Ying, Fu Ling, Xiong Wan-Ming, Kang Nian-Qian, Nie Xu-Liang

Page range: 615-616

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[C 14 H 14 F 3 N 5 O 6 S], monoclinic, P 2 1 / c (No. 14), a = 12.512(4) Å, b = 12.572(4) Å, c = 12.511(4) Å, β = 114.39(1)°, V = 1792.5(11) Å 3 , Z = 4, R gt ( F ) = 0.0366, wR ref ( F 2 ) = 0.0849, T = 296(2) K.
Open Access
Crystal structure of 1-phenyl-N′-(1-phenyl-5-(thiophen-2-yl)-1H-pyrazole-3-carbonyl)-5-(thiophen-2-yl)-1H-pyrazole-3-carbohydrazide, C₂₈H₂₀N₆O₂S₂

May 30, 2018

Mohammed Baashen, Bakr F. Abdel-Wahab, Amany S. Hegazy, Benson M. Kariuki, Gamal A. El-Hiti

Page range: 617-619

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C 28 H 20 N 6 O 2 S 2 , triclinic, P 1̅ (no. 2), a = 10.6738(6) Å, b = 11.7869(7) Å, c = 12.5381(7) Å, α = 112.842(6)°, β = 91.963(4)°, γ = 116.129(6)°, V = 1264.38(15) Å 3 , Z = 2, R gt ( F ) = 0.0523, wR ref ( F 2 ) = 0.1390, T = 296(2) K.
Open Access
The crystal structure of poly[bis(4-hydroxybenzoato-κO)-(μ₂-4,4′-bipyridine-κ²N:N′)copper(II)] hydrate, C₂₄H₂₀N₂O₇Cu

May 22, 2018

Haiyan He, Yuyang Li, Qiucheng Yang, Lei Li

Page range: 621-623

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C 24 H 20 N 2 O 7 Cu, monoclinic, C 2/ c , a = 19.6241(4) Å, b = 10.4639(2) Å, c = 10.7024(2) Å, β = 96.163(2)° V = 2184.99(8) Å 3 , Z = 4, R gt ( F ) = 0.0312, wR ref ( F 2 ) = 0.0863, T = 293 K.
Open Access
Crystal structure of poly[μ₃-5-(4-(2,6-di(pyridine-2-yl)pyridine-4-yl)phenoxy)isophthalato-κ⁵O:O′,O′′:N,N′,N′′cobalt(II)], C₂₉H₁₇CoN₃O₅

April 27, 2018

Xue-Guo Liu, Wei-Hong Yan, Xiao-Jing Xing, Hui-Tao Fan

Page range: 625-627

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C 29 H 17 CoN 3 O 5 , monoclinic, P 2 1 / c (no. 14), a = 11.1893(6) Å, b = 13.9922(10) Å, c = 14.1772(7) Å, β = 94.544(5)°, V = 2212.6(2) Å 3 , Z = 4, R gt ( F ) = 0.0460, wR ref ( F 2 ) = 0.0975, T = 293(2) K.
Open Access
Crystal structure of poly[μ₃-5-(4-(2,6-di(pyridine-2-yl)pyridine-4-yl)phenoxy)isophthalato-κ⁶O:O′,O′′:N,N′,N′′)cobalt(II)] C₂₉H₁₇CoN₃O₅

May 3, 2018

Xue-Guo Liu, Wei-Hong Yan, Xiao-Jing Xing, Hui-Tao Fan

Page range: 629-630

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C 29 H 17 CoN 3 O 5 , monoclinic, P 2 1 (no. 4), a = 7.7751(6) Å, b = 12.8081(14) Å, c = 12.4032(15) Å, β = 103.79(1)°, V = 1199.6(2) Å 3 , Z = 2, R gt ( F ) = 0.0627, wR ref ( F 2 ) = 0.0940, T = 293(2) K.
Open Access
Crystal structure of diaqua-(acetato-κ³O,O′:O′′)-(μ₃-4,6-di(1H-imidazol-1-yl)isophthalato-κ⁴O:O′:O′′,O′′′)lanthanum(III), C₁₆H₁₅LaN₄O₈

May 3, 2018

Xue-Guo Liu, Wei-Hong Yan, Xiao-Jing Xing, Hui-Tao Fan

Page range: 631-632

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C 16 H 15 LaN 4 O 8 , monoclinic, P 2 1 / c (no. 14), a = 13.2370(6) Å, b = 15.4658(5) Å, c = 9.5723(4) Å, β = 108.834(4)°, V = 1854.72(14) Å 3 , Z = 4, R gt ( F ) = 0.0342, wR ref ( F 2 ) = 0.0814, T = 293(2) K.
Open Access
Synthesis and crystal structure of 6-carboxy-1-(3,5-dicarboxyphenyl)-1H-benzo[d]imidazol-3-ium-5-carboxylate dihydrate, C₁₈H₁₂N₂O₈

April 7, 2018

Meng Yun, Xiu-Yan Dong

Page range: 633-634

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C 18 H 12 N 2 O 8 , triclinic, P 1̄ (no. 2), a = 8.4592(10) Å, b = 9.8442(11) Å, c = 11.2565(12) Å, α = 66.892(3)°, β = 86.069(3)°, γ = 81.658(4)°, V = 852.97(17) Å 3 , Z = 2, R gt ( F ) = 0.0609, wR ref ( F 2 ) = 0.1557, T = 153(2) K.
Open Access
Crystal structure of (E)-2-hydroxybenzaldehyde O-(2-(((E)-(4-(dimethylamino)benzylidene)amino)oxy)ethyl)oxime, C₁₈H₂₁N₃O₃

May 18, 2018

Yun-Dong Peng, Yang Zhang, Zong-Li Ren, Li Wang, Wen-Kui Dong

Page range: 635-636

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C 18 H 21 N 3 O 3 , monoclinic, P 2 1 / n , a = 5.3025(3) Å, b = 9.7824(7) Å, c = 33.3847(19) Å, β = 93.699(6)°, V = 1728.10(19) Å 3 , Z = 4, R gt (F) = 0.0677, wR ref (F 2 ) = 0.1892, T = 290.7(3) K.
Open Access
Crystal structure of bis{2-((E)-((4-((E)-1-(methoxyimino)ethyl)phenyl)imino)methyl)phenolato-κ²N,O}zinc(II), C₃₂H₃₀N₄O₄Zn

April 20, 2018

Qing-Lin Li, Peng-Peng Li, Jin-Xia Ma, Ji-Xing Zhao, Li Zhao

Page range: 637-639

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C 32 H 30 N 4 O 4 Zn, triclinic, P 1̅ (no. 2), a = 8.6632(8) Å, b = 12.7133(10) Å, c = 14.2719(12) Å, α = 98.585(3)°, β = 94.985(3)°, γ = 92.916(3)°, Z = 2, V = 1545.1(2) Å 3 , R gt ( F ) = 0.0714, wR ref ( F 2 ) = 0.1740, T = 296(2) K.
Open Access
Crystal structure of bis(9-aminoacridin-10-ium) tetrachloridocuprate(II) monohydrate, C₂₆H₂₄Cl₄CuN₄O

April 27, 2018

Artur Sikorski

Page range: 641-642

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C 26 H 24 Cl 4 CuN 4 O, triclinic, P 1̄ (no. 2), a = 9.967(1) Å, b = 11.853(1) Å, c = 13.370(2) Å, α = 101.981(8)°, β = 106.586(8)°, γ = 113.856(9)°, V = 1287.0(3) Å 3 , Z = 2, R gt ( F ) = 0.0300, wR ref ( F 2 ) = 0.0771, T = 295(2) K.
Open Access
The crystal structure of 4-tert-butyl-N′-[(E)-(4-fluoro-3-methoxyphenyl)methylidene]benzohydrazide, C₁₉H₂₁F₁N₂O₂

May 3, 2018

Muhammad Ikram, Momin Khan, Sajjad Ahmad, Sadia Rehman, Carola Schulzke

Page range: 643-645

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C 19 H 21 F 1 N 2 O 2 , monoclinic, Cc (no. 9), a = 14.337(3) Å, b = 15.549(3) Å, c = 8.0212(16) Å, β = 103.33(3)°, V = 1740.0(6) Å 3 , Z = 4, R gt ( F ) = 0.0796, wR ref ( F 2 ) = 0.2192, T = 170 K.
Open Access
Crystal structure of (E)-3-(3-(5-methyl-1-4-tolyl-1H-1,2,3-triazol-4-yl)-1-phenyl-1H-pyrazol-4-yl)-1-(5-methyl-1-phenyl-1H-1,2,3-triazol-4-yl)prop-2-en-1-one, C₃₁H₂₆N₈O

April 20, 2018

Mohammad Hayal Alotaibi, Hanan A. Mohamed, Bakr F. Abdel-Wahab, Mohammed Abu Bakr Abu El-Enin, Hazem A. Ghabbour, Gamal A. El-Hiti

Page range: 647-648

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C 31 H 26 N 8 O, triclinic, P 1̄ (no. 2), a = 6.6046(3) Å, b = 15.1056(8) Å, c = 15.2115(8) Å, α = 61.996(2)°, β = 80.390(3)°, γ = 87.579(2)°, V = 1319.97(12) Å 3 , Z = 2, R int = 0.108, wR ( F 2 ) = 0.143, T = 296(2) K.
Open Access
Crystal structure of (E)-N′-(4-methoxybenzylidene)-5-methyl-1-(4-tolyl)-1H-1,2,3-triazole-4-carbohydrazide, C₁₉H₁₉N₅O₂

April 20, 2018

Mohammad Hayal Alotaibi

Page range: 649-650

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C 19 H 19 N 5 O 2 , triclinic, P 1̄ (no. 2), a = 6.6320(3) Å, b = 10.3272(5) Å, c = 13.0832(6) Å, α = 102.751(2)°, β = 96.130(2)°, γ = 103.079(2)°, V = 839.63(7) Å 3 , Z = 2, R gt = 0.0553, wR ref ( F 2 ) = 0.1521, T = 100(2) K.
Open Access
Crystal structure and molecular packing of O-ethyl (2-chlorophenyl)carbamothioate, C₉H₁₀ClNOS

April 7, 2018

Chien Ing Yeo, Edward R.T. Tiekink

Page range: 651-653

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C 9 H 10 ClNOS, triclinic, P 1̄ (no. 2), a = 7.2277(3) Å, b = 9.9791(3) Å, c = 14.7725(7) Å, α = 81.007(3)°, β = 82.268(4)°, γ = 73.210(3)°, V = 1003.01(7) Å 3 , Z = 4, R gt ( F ) = 0.0364, wR ref ( F 2 ) = 0.0828, T = 100(2) K.
Open Access
Crystal structure of pyrene-2-carbaldehyde, C₁₇H₁₀O

April 18, 2018

Miao Bao-Xi, Tang Xin-Xue, Zhang Li-Fang

Page range: 655-657

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C 17 H 10 O, monoclinic, P 2 1 /c (no. 14), a = 8.1312(16) Å, b = 7.8252(16) Å, c = 17.231(3) Å, β = 92.47(3)°, V = 1095.3(4) Å 3 , Z = 4, R gt ( F ) = 0.0517, wR ref ( F 2 ) = 0.1281, T = 293(2) K.
Open Access
Crystal structure of (E)-2,4-diiodo-6-(4-methyl-2-nitrostyryl)phenol, C₁₄H₁₀I₂N₂O₃

April 20, 2018

Yong Hong, Wei Liu, Heping Yan

Page range: 659-660

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C 14 H 10 I 2 N 2 O 3 , monoclinic, P 2 1 / c (no. 14), a = 13.5219(8) Å, b = 7.2772(4) Å, c = 15.2709(8) Å, β = 96.1761(18)°, V = 1493.96(14) Å 3 , Z = 4, R gt ( F ) = 0.0716, wR ref ( F 2 ) = 0.1888, T = 293(2) K.
Open Access
Crystal structure of (E)-2,4-dichloro-6-(((4-methoxy-2-nitrophenyl)imino)methyl)phenol, C₁₄H₁₀Cl₂N₂O₄

May 29, 2018

Yong Hong

Page range: 661-662

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C 14 H 10 Cl 2 N 2 O 4 , monoclinic, P 2 1 / c , a = 14.2599(10) Å, b = 6.9970(4) Å, c = 15.0779(10) Å, β = 108.245(2)°, V = 1428.79(16) Å 3 , Z = 4, R gt ( F ) = 0.0355, wR ref ( F 2 ) = 0.0860, T = 150(2) K.
Open Access
Crystal structure of (E)-2-bromo-4-chloro-6-(4-methoxy-2-nitrostyryl)phenol, C₁₄H₁₀BrClN₂O₄

May 29, 2018

Yong Hong

Page range: 663-664

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C 14 H 10 BrClN 2 O 4 , monoclinic, P 2 1 / c (no. 14), a = 14.2726(16) Å, b = 6.9919(9) Å, c = 15.1927(15) Å, β = 107.308(5)°, V = 1447.5(3) Å 3 , Z = 4, R gt ( F ) = 0.0362, wR ref ( F 2 ) = 0.0831, T = 150(2) K.
Open Access
Crystal structure of (E)-4,6-diiodo-2-(((4-methoxy-2-nitrophenyl)imino)methyl)-3-methylphenol, C₁₄H₁₀I₂N₂O₄

April 27, 2018

Yong Hong

Page range: 665-666

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C 14 H 10 I 2 N 2 O 4 , triclinic, P 1̄ (no. 2), a = 9.2216(4) Å, b = 9.7072(5) Å, c = 10.0628(5) Å, α = 61.778(2)°, β = 77.716(2)°, γ = 79.144(2)°, V = 771.49(7) Å 3 , Z = 2, R gt ( F ) = 0.0184, wR ref ( F 2 ) = 0.0542, T = 150(2) K.
Open Access
The crystal structure of 7-bromo-1-cyclopropyl-8-methyl-4-oxo-1,4-dihydroquinoline-3-carboxylic acid an intermediate of the ozenoxacin synthesis, C₁₄H₁₂BrNO₃

April 18, 2018

Xiao-Li Yang, Xu Qian, Rui Cao, Hao Xu, Qi Wang

Page range: 667-668

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C 14 H 12 BrNO 3 , triclinic, P 1̅ (no. 2), a = 8.4134(5) Å, b = 9.5365(6) Å, c = 9.6154(7) Å, α = 60.728(2)°, β = 83.130(2)°, γ = 66.331(2)°, V = 613.52(7) Å 3 , Z = 2, R gt ( F ) = 0.0393, wR ref ( F 2 ) = 0.0709, T = 296(2) K.
Open Access
Crystal structure of bis(N-(1-(pyrazin-2-yl)ethylidene)nicotinohydrazonato-κ³N,N′,O)copper(II) C₂₄H₂₀N₁₀O₂Cu

May 7, 2018

Qingqing Li, Kaichuang Jiao, Zhouqing Xu

Page range: 669-670

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C 24 H 20 N 10 O 2 Cu, orthorhombic, Aba 2 (no. 41), a = 12.2281(16) Å, b = 19.176(3) Å, c = 9.8689(13) Å, V = 2314.1(5) Å 3 , Z = 4, R gt ( F ) = 0.0381, wR ref ( F 2 ) = 0.0752, T = 296(3) K.
Open Access
Crystal structure of diaqua-dinitrato-k²O,O′((Z)-N-((E)-1-(pyrazin-2-yl)ethylidene)nicotinohydrazonato-k³N,N′,O)europium(II), C₁₂H₁₄N₇O₉Eu

May 7, 2018

He Yaling, Zeng Shilin, Zhang Peiling, Xu Zhouqing

Page range: 671-672

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C 12 H 14 N 7 O 9 Eu, monoclinic, P 2 1 / c (no. 14), a = 16.770(3) Å, b = 7.7185(16) Å, c = 15.165(3) Å, β = 108.409(3)°, V = 1862.5(7) Å 3 , Z = 4, R gt ( F ) = 0.0174, wR ref ( F 2 ) = 0.0453, T = 296(2) K.
Open Access
Crystal structure of ethyl 4-amino-5-(5-methyl-1-(4-tolyl)-1H-1,2,3-triazole-4-carbonyl)-2-(phenylamino)thiophene-3-carboxylate, C₂₄H₂₃N₅O₃S

June 4, 2018

Mohammed H. Geesi, Hanan A. Mohamed, Bakr F. Abdel-Wahab, Amany S. Hegazy, Benson M. Kariuki, Gamal A. El-Hiti

Page range: 673-674

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C 24 H 23 N 5 O 3 S, triclinic, P 1̅ (no. 2), a = 9.1704(9) Å, b = 10.1253(11) Å, c = 12.2182(14) Å, α = 83.686(10)°, β = 89.542(9)°, γ = 76.982(9)°, V = 1098.5(2) Å 3 , Z = 2, R gt ( F ) = 0.0551, wR ref ( F 2 ) = 0.1510, T = 296(2) K.
Open Access
The crystal structure of acridin-10-ium2-carboxybenzoate, C₂₁H₁₅NO₄

May 16, 2018

Kornelia Fennig, Artur Sikorski

Page range: 675-676

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C 21 H 15 NO 4 , monoclinic, P 2 1 / n (no. 14), a = 7.2223(3) Å, b = 9.1850(4) Å, c = 25.2304(10) Å, β = 92.604(3)°, V = 1671.97(11) Å 3 , Z = 4, R gt ( F ) = 0.0498, wR ref ( F 2 ) = 0.1205, T = 295(2) K.
Open Access
The crystal structure of 3-((phenylamino)methylene)-1,5-dioxaspiro[5.5]undecane-2,4-dione, C₁₆H₁₇N₁O₄

May 18, 2018

Jiang Jin-He, Zeng Wu-Lan, Yang Yong-Mei

Page range: 677-678

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C 16 H 17 N 1 O 4 , triclinic, P 1̅ (no. 2), a = 7.0971(3) Å, b = 7.6638(4) Å, c = 13.2375(6) Å, α = 92.116(10)°, β = 99.690(10)°, γ = 95.196(10)° V = 705.81(6) Å 3 , Z = 2, R gt ( F ) = 0.0529, wR ref ( F 2 ) = 0.1489, T = 296(2) K.
Open Access
Crystal structure of 12-chloro-5,6,7,12-tetrahydrodibenzo[c,f][1,5]oxastibocine, C₁₄H₁₂ClOSb

May 10, 2018

Nianyuan Tan, Donghui Lan, Shuisheng Wu, Chak-Tong Au, Bing Yi

Page range: 679-681

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C 14 H 12 ClOSb, triclinic, P 1̄ (no. 2), a = 9.3453(14) Å, b = 10.9826(16) Å, c = 13.303(2) Å, α = 90.823(3)°, β = 90.394(3)°, γ = 108.307(2)°, V = 1296.0(3) Å 3 , Z = 4, R gt ( F ) = 0.0587, wR(F 2 ) = 0.1767, T = 293(2) K.
Open Access
Crystal structure of 4-((1,3-dioxoisoindolin-2-yl)methyl)phenethyl 4-methylbenzenesulfonate, C₂₄H₂₁NO₅S

May 10, 2018

Huang Cuicui, Maojian Shi, Jing Liu, Lin Ding, Jinhui Zhou

Page range: 683-684

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C 24 H 21 NO 5 S, monoclinic, P 2 1 / c (no. 14), a = 7.7790(16) Å, b = 22.726(5) Å, c = 12.755(3) Å, β = 107.15(3)°, V = 2154.6(9) Å 3 , Z = 4, R gt ( F 2 ) = 0.0453, wR ref ( F 2 ) = 0.1371, T = 293.15 K.
Open Access
Crystal structure of 3-methyl-2,3-dihydro-2-thioxoquinazolin-4(1H)-one, C₉H₈N₂OS

May 18, 2018

Hao Wu, Hai-Tao Zong

Page range: 685-686

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C 9 H 8 N 2 OS, monoclinic, C 2/ c (no. 15), a = 24.273(5) Å, b = 9.026(2) Å, c = 8.2852(19) Å, β = 108.818(4)°, V = 1718.2(7) Å 3 , Z = 8, R gt ( F ) = 0.0438, wR ref ( F 2 ) = 0.1190, T = 296(2) K.
Open Access
Crystal structure of tert-butyl (2-(4-oxo-2-thioxo-1,4-dihydroquinazolin-3(2H)-yl)ethyl)carbamate, C₁₅H₁₉N₃O₃S

May 18, 2018

Hai-Tao Zong, Lin-Yan Bian, Ling-Ling Yan

Page range: 687-688

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C 15 H 19 N 3 O 3 S, triclinic, P 1̅ (no. 2), a = 8.682(8) Å, b = 9.700(8) Å, c = 11.273(10) Å, α = 90.681(14)°, β = 112.624(13)°, γ = 112.632(13)°, V = 794.5(12) Å 3 , Z = 2, R gt ( F ) = 0.0405, wR ref ( F 2 ) = 0.1171, T = 296(2) K.
Open Access
Crystal structure of ethyl 5-formyl-3,4-dimethylpyrrole-2-carboxylate–1-(propan-2-ylidene)thiosemicarbazide (1/1), C₁₄H₂₂N₄O₃S

May 16, 2018

Wan-Wan Wang, Hai-Tao Zong, Wei-Na Wu

Page range: 689-690

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C 13 H 17 N 3 OS, triclinic, P 1̄ (no. 2), a = 6.9906(9) Å, b = 8.0075(11) Å, c = 16.057(2) Å, α = 81.822(2)°, β = 89.151(2)°, γ = 70.735(2)°, V = 839.4(2) Å 3 , Z = 2, R gt ( F ) = 0.0444, wR ref ( F 2 ) = 0.1299, T = 296(2) K.
Open Access
Crystal structure of bis-(N′-(5-ethoxycarbonyl-3,4-dimethyl-pyrrol-2-yl-methylidene)-3-hydroxybenzohydrazide-κ²O,N)copper(II) – dimethylformamide (1/2), C₄₀H₅₀N₈O₁₀Cu

May 22, 2018

Wei-Guo Duan, Yi-Peng Guo, Long Lin, Wei-Na Wu

Page range: 691-692

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C 40 H 50 N 8 O 10 Cu, triclinic, P 1̄ (no. 2), a = 6.8237(9) Å, b = 12.9229(17) Å, c = 13.3275(18) Å, α = 104.949(2)°, β = 104.049(2)°, γ = 99.538(2)°, V = 1068.3(2) Å 3 , Z = 1, R gt ( F ) = 0.0497, wR ref ( F 2 ) = 0.1343, T = 296(2) K.
Open Access
Crystal structure of bis(acetato-κO)bis{2-((1H-tetrazol-1-yl)methyl)-1H-benzo[d]imidazole-κN}zinc(II), C₂₂H₂₂N₁₂O₄Zn

May 18, 2018

Shan-Shan Li, Xiao-Yang Zhao, Qiu-Ying Huang, Xiang-Ru Meng

Page range: 693-695

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C 22 H 22 N 12 O 4 Zn, monoclinic, P 2 1 / c (no. 14), a = 9.864(2) Å, b = 8.6657(17) Å, c = 30.803(8) Å, β = 106.67(3)°, V = 2522.3(10) Å 3 , Z = 4, R gt ( F ) = 0.0630, wR ref ( F 2 ) = 0.1625, T = 293(2) K.
Open Access
Crystal structure of 4-phenyl-3-((4-phenyl-1H-1,2,3-triazol-1-yl)methyl)-1H-1,2,4-triazole-5(4H)-thione, C₁₇H₁₄N₆S

May 22, 2018

Mohamed Reda Aouad, Mouslim Messali, Nadjet Rezki, Naveen Shivalingegowda, Ismail Warad

Page range: 697-698

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C 17 H 14 N 6 S, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 7.3832(3) Å, b =14.4702(7) Å, c = 15.2806(7) Å, V = 1632.52(13) Å 3 , Z = 4 and with R int = 0.0577, R gt ( F ) = 0.0358, wR ref ( F 2 ) = 0.0944, T = 296(2) K.
Open Access
Crystal structure of (Z)-N-(4-nitrophenyl)-3-phenyl-3-(phenylamino)acrylamide, C₂₁H₁₇N₃O₃

May 18, 2018

Xin-Sheng Xiao, Guo-Kai Jia, Wen-Yi Li, Xiu-Wen Chen

Page range: 699-700

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C 21 H 17 N 3 O 3 , orthorhombic, Pbca (no. 61), a = 14.3606(4) Å, b = 7.4250(2) Å, c = 34.2840(9) Å, V = 3655.62(17) Å 3 , Z = 8, R gt ( F ) = 0.0399, wR ref ( F 2 ) = 0.1178, T = 571(2) K.
Open Access
Crystal structure of 1,1′-(pentane-1,5-diyl)bis(3-methyl-1H-imidazol-3-ium)bis(hexafluorophosphate), C₁₃H₂₂F₁₂N₄P₂

May 22, 2018

Xiong Wan-Ming, Zhou Long, Lv Shen-Ming, Nie Xu-Liang, Chen Jing, Huang Chang-Gan

Page range: 701-703

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C 13 H 22 F 12 N 4 P 2 , monoclinic, P 2 1 / c , a = 12.9171(13) Å, b = 13.3953(13) Å, c = 12.5808(12) Å, β = 97.766(1)°, V = 2156.9(4) Å 3 , Z = 4, R gt ( F ) = 0.0583, wR ref ( F 2 ) = 0.1557, T = 296(2) K.
Open Access
Synthesis and crystal structure of bis(furan-2-ylmethanaminium)-catena-[bis(μ₂-phthalato-κ²O:O′)cobalt(II)], C₂₆H₂₄CoN₂O₁₀

May 30, 2018

Musa A. Said, David L. Hughes, Rayees Ahmad Shiekh

Page range: 705-707

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C 26 H 24 CoN 2 O 10 , monoclinic, F 2/ d (equiv. to no. 15), a = 23.7125(7) Å, b = 10.7325(4) Å, c = 39.5740(15) Å, β = 90.324(3)°, V = 10071.2(6) Å 3 , Z = 16, R gt ( F ) = 0.0514, wR ref ( F 2 ) = 0.1048, T = 140(1) K.
Open Access
Crystal structure of methyl (R)-4-(o-chlorobenzoyl)-1-thia-4-azaspiro[4.5]decane-3-carboxylate, C₁₇H₂₀ClNO₃S

May 22, 2018

Li-Xia Zhao, Qing-Rui Wang, Yue-Li Zou, Hao Wu, Fei Ye

Page range: 709-710

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C 17 H 20 ClNO 3 S, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 6.1984(2) Å, b = 14.3940(5) Å, c = 18.9651(6) Å, V = 1692.06(10) Å 3 , Z = 4, R gt ( F ) = 0.0263, wR ref ( F 2 ) = 0.0683, T = 293(2) K.
Open Access
Crystal structure of 2-[[4-[2-[4-(4-methoxyphenyl)-1-piperazinyl]ethyl]phenyl] methyl]-1H-isoindole-1,3(2H)-dione, C₂₈H₂₉N₃O₃

May 29, 2018

Jinhui Zhou, Cuicui Huang, Maojian Shi, Jing Liu, Lin Ding

Page range: 711-714

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C 28 H 29 N 3 O 3 , triclinic, P 1̄ (no. 2), a = 8.2887(3) Å, b = 14.1977(5) Å, c = 21.3385(7) Å, α = 107.142(3)°, β = 92.773(3)°, γ = 104.240(3)°, V = 2305.97(15) Å 3 , Z = 4, R gt ( F 2 ) = 0.0555, wR ref ( F 2 ) = 0.1620, T = 100(1) K.
Open Access
The crystal structure of benzenaminium 5,7-dihydroxy-4-oxo-2-phenyl-4H-chromene-8-sulfonate hydrate, C₂₁H₁₉NO₈S

May 7, 2018

Wu-Wu Li, Min-Yan Zheng, Zun-Ting Zhang

Page range: 715-717

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C 21 H 19 NO 8 S, triclinic, P 1̄ (no. 2), a = 7.2884(9) Å, b = 11.9469(15) Å, c = 12.2002(16) Å, α = 95.862(2)°, β = 106.659(2)°, γ = 93.189(2)°, V = 1008.4(2) Å 3 , Z = 2, R gt ( F ) = 0.0659, wR ref ( F 2 ) = 0.1831, T = 296(2) K.
Open Access
Crystal structure of semiconducting potassium poly[(μ₂-tetraselenido-κ²Se¹:Se⁴)(μ₂-pentaselenido-κ¹Se¹:Se¹)argentate(I)], K₃AgSe₉

May 7, 2018

Kang-Woo Kim, Hyoungjoong Kim

Page range: 719-720

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K 3 AgSe 9 , monoclinic, P 2 1 / c (no. 14), a = 11.094(2) Å, b = 9.7164(15) Å, c = 14.223(3) Å, β = 90.738(9)°, V = 1533.0(5) Å 3 , Z = 4, R gt ( F ) = 0.0377, wR ref ( F 2 ) = 0.0832, T = 223(2) K.
Open Access
Crystal structure of 2-isopropyl-8-methyl-phenanthrene-3,4-dione, C₁₈H₁₆O₂

May 16, 2018

Jichun Wu, Guoyong Luo, Yuchen Liu, Wude Yang

Page range: 721-722

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C 18 H 16 O 2 , orthorhombic, Pnma (no. 62), a = 14.474(6) Å, b = 6.815(3) Å, c = 13.738(6) Å, V = 1355.1(10) Å 3 , Z = 4, R gt ( F ) = 0.0583, wR ref ( F 2 ) = 0.1759, T = 173 K.
Open Access
Crystal structure of 2-isopropyl-8,8-dimethyl-5,6,7,8-tetrahydrophenanthrene-3,4-dione, C₁₉H₂₂O₂

May 18, 2018

Jichun Wu, Guoyong Luo, Yuchen Liu, Wude Yang

Page range: 723-724

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C 19 H 22 O 2 , triclinic, P 1̄ (no. 2), a = 8.4768(13) Å, b = 8.7667(14) Å, c = 11.1282(17) Å, α = 73.284(3)°, β = 73.041(3)°, γ = 83.391(3)°, V = 757.1(2) Å 3 , Z = 2, R gt ( F ) = 0.0509, wR ref ( F 2 ) = 0.1613, T = 173 K.
Open Access
Crystal structure of (E)-2-(1-((2-aminophenyl)imino)ethyl)-4-bromophenol, C₁₄H₁₃BrN₂O

May 10, 2018

Yong Hong, Wei Liu

Page range: 725-726

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C 14 H 13 BrN 2 O, monoclinic, P 2 1 (no. 4), a = 6.8679(5) Å, b = 7.7096(5) Å, c = 12.4043(7) Å, β = 101.332(2)°, V = 643.99(7) Å 3 , Z = 2, R gt ( F ) = 0.0294, wR ref ( F 2 ) = 0.0691, T = 293(2) K.
Open Access
Crystal structure of 1,1-di(4-cyanophenyl)-2,2-diphenylethene, C₂₈H₁₈N₂

May 22, 2018

Miao Bao-Xi, Sun Hao, Ni Zhong-Hai

Page range: 727-729

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C 28 H 18 N 2 , orthorhombic, Pccn (no. 56), a = 9.8955(6) Å, b = 11.0163(6) Å, c = 19.9752(14) Å, V = 2177.5(2) Å 3 , Z = 4, R gt ( F ) = 0.0402, wR ref ( F 2 ) = 0.1012, T = 123(2) K.
Open Access
Crystal structure of bis(hydroxylamido-κ²O,N)-oxido(1H-pyrazole-3-carboxylato-κ²O,N)vanadium(V), C₄H₇N₄O₅V

May 18, 2018

Heng-Qiang Zhang, Qiong Wu, Qi-Ying Zhang, Xue Yang, Hong-Li Chen

Page range: 731-732

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C 4 H 7 N 4 O 5 V, monoclinic, P 2 1 / c (no. 14), a = 9.6179(8) Å, b = 8.3133(7)(11) Å, c = 10.8235(9) Å, β = 102.253(2)°, V = 845.69(12) Å 3 , Z = 8, R gt ( F ) = 0.0242, wR ref ( F 2 ) = 0.0718, T = 296(2) K.
Open Access
The crystal structure of In_1.2B₃O_5.6(OH)_1.4

April 12, 2018

Daniela Vitzthum, Hubert Huppertz

Page range: 733-734

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In 1.4 B 3 O 5.6 (OH) 1.4 , tetragonal, P 4̄2 1 m (no. 113), a = 6.6969(9) Å, c = 4.4865(9) Å, V = 201.21(7) Å 3 , Z = 2, R gt ( F ) = 0.0117, wR ref ( F 2 ) = 0.0297, T = 293(2) K.
Open Access
The crystal structure of chlorido(2-(1H-pyrazol-3-yl)phenolato-κ²N,O)(2-(1H-pyrazol-3-yl)phenol-κN)copper(II), C₁₈H₁₅ClCuN₄O₂

May 22, 2018

Wu-Wu Li, Min-Yan Zheng, Zun-Ting Zhang

Page range: 735-737

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C 18 H 15 ClCuN 4 O 2 , triclinic, P 1̄ (no. 2), a = 8.938(3) Å, b = 9.228(3) Å, c = 12.127(6) Å, α = 105.478(7)°, β = 110.358(8)°, γ = 99.727(6)°, V = 865.0(6) Å 3 , Z = 2, R gt ( F ) = 0.0504, wR ref ( F 2 ) = 0.1447, T = 296(2) K.
Open Access
Crystal structure of 1-heptylpyridazin-1-ium iodide, C₁₁H₁₉N₂I

June 9, 2018

Musa A. Said, Mohamed R. Aouad, Saud M. Almutairi, David L. Hughes, Mouslim Messali

Page range: 739-741

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C 11 H 19 N 2 I, triclinic, P 1̄ (no. 2), a = 5.7074(3) Å, b = 8.9811(5) Å, c = 14.4312(8) Å, α = 100.989(4)°, β = 94.768(4)°, γ = 97.327(4)°, V = 715.83(7) Å 3 , Z = 2, R gt ( F ) = 0.0386, wR ref ( F 2 ) = 0.0913, T = 295(2) K.
Open Access
The crystal structure of N-butylpyridinium bis(μ₂-dichlorido)-tetrachloridodicopper(II), C₁₈H₂₈N₂Cu₂Cl₆

June 22, 2018

A. Abouserie, U. Schilde, A. Taubert

Page range: 743-746

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C 9 H 14 Cl 3 CuN, monoclinic, P 2 1 /n (no. 14), a = 9.6625(6) Å, b = 9.3486(3) Å, c = 14.1168(8) Å, β = 102.288(5)°, V = 1245.97(11) Å 3 , Z = 4, R gt ( F ) = 0.0182, wR ref ( F 2 ) = 0.0499, T = 210(2) K.
Open Access
Crystal structure of 6-hydroxy-5-((2-hydroxy-6-oxocyclohex-1-en-1-yl)(4-methoxyphenyl)methyl)-1,3-dimethylpyrimidine-2,4(1H,3H)-dione, C₂₀H₂₂N₂O₆

May 18, 2018

Mezna Saleh Altowyan, M. Ali, Saied M. Soliman, Almoqbl A. Naser, Abdullah Mohammed Al-Majid, Assem Barakat

Page range: 747-749

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C 20 H 22 N 2 O 6 , monoclinic, P 2 1 / c (no. 14), a = 8.6657(6) Å, b = 18.6201(14) Å, c = 22.3583(18) Å, β = 91.808(3)°, V = 3605.9(5) Å 3 , Z = 8, R gt ( F ) = 0.067, wR ref ( F 2 ) = 0.177, T = 100(2) K.
Open Access
Crystal structure of bis(acetonitrile)-diaqua-dichloridoiron(II), C₄H₁₀Cl₂N₂O₂Fe

May 29, 2018

Jian Zuo

Page range: 751-752

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C 4 H 10 Cl 2 N 2 O 2 Fe, monoclinic, P 21/ c (no. 14), a = 7.8501(10) Å, b = 7.8289(10) Å, c = 8.2974(17) Å, β = 97.840(2), V = 505.17(14) Å 3 , Z = 2, R gt ( F ) = 0.0447, wR ref ( F 2 ) = 0.1237, T = 298(2) K.

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