Zeitschrift für Kristallographie - New Crystal Structures

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Zeitschrift für Kristallographie - New Crystal Structures

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Zeitschrift für Kristallographie - New Crystal Structures

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Frontmatter

26. Dezember 2022

Seiten: i-vi

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New Crystal Structures
Open Access
Crystal structure of undecacalcium decaarsenide, Ca₁₁As₁₀

11. Oktober 2022

Andrea V. Hoffmann, Viktor Hlukhyy, Thomas F. Fässler

Seiten: 1-3

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Ca 11 As 10 , tetragonal, I 4/ mmm (no. 139), a = 11.2532(1) Å, c = 16.2351(4) Å, and V = 2055.92(6) Å 3 , Z = 4, R gt ( F ) = 0.0347, wR ref ( F 2 ) = 0.0931, T = 150 K.
Open Access
Crystal structure of catena-poly[diiodido-(μ₂-1,5-dimethyl-2-phenyl-4-((pyridin-4- ylmethylene)amino)-1,2-dihydro-3H -pyrazol-3-one-κ² N: O)zinc(II)], C₁₇H₁₆I₂N₄OZn

1. November 2022

Ben Li, Yujiao Huang, Weicheng Qian, Haixia Pang, Qiang Tang

Seiten: 5-7

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C 17 H 16 I 2 N 4 OZn, monoclinic, P 2 1 / n , a = 7.4827(5) Å, b = 14.9521(10) Å, c = 18.2838(13) Å, β = 99.251(1)°, V = 2019.0(2) Å 3 , Z = 4, R gt ( F ) = 0.0404, wR ref ( F 2 ) = 0.787, T = 298 K.
Open Access
The crystal structure of 5,10,15,20-tetrakis(4-(tert-butyl)phenyl)porphyrin-21,23-diido-κ⁴ N ⁴-naphthalocyanido-κ⁴ N ⁴-neodymium(IV) - chloroform (1/6) C₁₁₄H₉₀N₁₂Cl₁₈Nd

1. November 2022

Yang Liguo, Wang Xin, Fu Jiaqi, Ji Xinyu

Seiten: 9-12

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C 114 H 90 N 12 Cl 18 Nd, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 17.3389(7) Å, b = 18.7671(5) Å, c = 19.1454(8) Å, α = 79.600(3)°, β = 68.752(4)°, γ = 68.572(3)°, V = 5396.7(4) Å 3 , Z = 2, R gt ( F ) = 0.0722, wR ref ( F 2 ) = 0.1979, T = 298 K.
Open Access
The crystal structure of 1-(4-bromophenyl)-3-(2-chlorobenzyl)urea, C₁₄H₁₂BrClN₂O

4. November 2022

Zhihong Zhu, Lilei Zhang

Seiten: 13-14

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C 14 H 12 BrClN 2 O, monoclinic, P 2 1 / c (no. 14), a = 13.4072(6) Å, b = 8.6103(5) Å, c = 12.3824(6) Å, β = 100.475(4), V = 1405.60(12) Å 3 , Z = 4, R gt ( F ) = 0.0499, wR ref ( F 2 ) = 0.1215, T = 173 K.
Open Access
Crystal structure of bis[benzyl(methyl)carbamodithioato-κ ² S,S′]-di-n-butyltin(IV), C₂₆H₃₈N₂S₄Sn

24. Oktober 2022

Nurul Amalina Abd Aziz, Normah Awang, Kok Meng Chan, Nurul Farahana Kamaludin, Nur Najmi Mohamad Anuar, Nur Atiyah Nadhrah Jamaludin, Yee Seng Tan, Edward R. T. Tiekink

Seiten: 15-18

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C 26 H 38 N 2 S 4 Sn, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 9.6272(1) Å, b = 12.1043(2) Å, c = 13.3584(2) Å, α = 82.296(1)°, β = 86.611(1)°, γ = 66.912(1)°, V = 1419.02(4) Å 3 , Z = 2, R gt ( F ) = 0.0235, wR ref ( F 2 ) = 0.0612, T = 100 K.
Open Access
Crystal structure of (E)-3-(2-(4-(diethylamino)-2-hydroxystyryl)-3,3-dimethyl-3H-indol-1-ium-1-yl)propane-1-sulfonate – methanol (1/2), C₂₅H₃₂N₂O₄S⋅2CH₃OH

1. November 2022

Wen-Ze Zhao

Seiten: 19-21

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C 27 H 40 N 2 O 6 S, monoclinic, P 2 1 / c (no. 14), a = 11.2654(15) Å, b = 21.630(3) Å, c = 12.2868(17) Å, β = 111.422(3)°, V = 2787.1(7) Å 3 , Z = 4, R gt ( F ) = 0.0493, w R ref ( F 2 ) = 0.1313, T = 198(2) K.
Open Access
Synthesis and crystal structure of {(N′,N″-(((ethane-1,2-diylbis(oxy))bis(2,1-phenylene))-bis(methaneylylidene))bis(2-hydroxybenzohydrazonato)-κ⁶ N ² O ⁴}copper(II), C₃₀H₂₄CuN₄O₆

1. November 2022

Jie-Qiong Cai

Seiten: 23-25

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C 30 H 24 CuN 4 O 6 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 10.8014(2) Å, b = 10.8211(2) Å, c = 13.4530(3) Å, α = 100.308(1)°, β = 113.075(1)°, γ = 99.989(1)°, Z = 2, V = 1370.76(5) Å 3 , R gt ( F ) = 0.0365, wR ref ( F 2 ) = 0.0937, T = 297 K.
Open Access
The crystal structure of ((E)-2,4-dibromo-6-(((5-(nitro)-2-oxidophenyl)imino)methyl)phenolato-κ ³ N,O,O′)tris(pyridine-κN)manganese(II), C₂₈H₂₁Br₂MnN₅O₄

28. Oktober 2022

Ting Li, Keying Qiu, Yuxing Tan, Wujiu Jiang

Seiten: 27-29

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C 28 H 21 Br 2 MnN 5 O 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.9193(14) Å, b = 9.2271(15) Å, c = 17.933(3) Å, α = 103.574(2)°, β = 91.518(2)°, γ = 98.762(2)°, V = 1415.0(4) Å 3 , Z = 2, R gt ( F ) = 0.0347, wR ref ( F 2 ) = 0.0864, T = 296(2) K.
Open Access
Synthesis and crystal structure of 1-((3R,10S,13R,17S)-10,13-dimethyl-3-(p-tolylamino)hexadecahydro-1H-cyclopenta-[a]phenanthren-17-yl)ethan-1-one, C₂₈H₄₁NO

1. November 2022

Hua Huang, Wen-Wen Zhang, Jiang-Hai Ye, Juan Zou, Kang He

Seiten: 31-33

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C 28 H 41 NO, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 10.5758(10) Å, b = 12.3659(9) Å, c = 18.0301(16) Å, V = 2358.0(4) Å 3 , Z = 4, R gt ( F ) = 0.0524, wR ref ( F 2 ) = 0.1220, T = 273(2) K.
Open Access
The crystal structure of 3-nitrobenzene-1,2-dicarboxylic acid—pyrazine-2-carboxamide(1/1), C₁₃H₁₀N₄O₇

1. November 2022

Cheng-Jun Jiang, Die Cheng, Ying-Fan Xia, Jia-rong Zhang, Shu-ting Lin

Seiten: 35-37

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C 13 H 10 N 4 O 7 , monoclinic, P 2 1 / n (no. 14), a = 10.7017(7) Å, b = 7.1240(5) Å, c = 19.0878(13) Å, β = 99.280(3)°, V = 1436.19(17) Å 3 , Z = 4, R gt ( F ) = 0.0586, wR ref ( F 2 ) = 0.1746, T = 296.15 K.
Open Access
Crystal structure of poly[tetrakis(μ₃-2-aminonicotinato-κ³N,O,O′)-(μ₂-oxalato-κ⁴ O,O′:O″,O′″)-(μ₄-oxalato-κ⁶ N:N′:O,O′:O″,O′″)dicopper(I)-disamarium(III)], [SmCu(C₆N₂H₅O₂)₂(C₂O₄)]_n

1. November 2022

Wei-Wei Zhou, Wang Zhao, Jing Wang, Ming-Jun Song

Seiten: 39-41

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[SmCu(C 6 N 2 H 5 O 2 ) 2 (C 2 O 4 )] n , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 9.457(6) Å, b = 9.482(4) Å, c = 11.013(4) Å, α = 75.87(4)°, β = 89.853(12)°, γ = 62.786(11)°, V = 844.8(7) Å 3 , Z = 2, R gt ( F ) = 0.0292, wR ref ( F 2 ) = 0.0691, T = 296 K.
Open Access
The crystal structure of 2,3,4-trihydroxybenzoic- acid—pyrazine-2-carboxamide—water (1/1/1), C₁₂H₁₃N₃O₇

1. November 2022

Cheng-Jun Jiang, Zhi-Hua Wang, Ying-Fan Xia, Chao-Feng Li, Shu-ting Lin, Jia-rong Zhang

Seiten: 43-44

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C 12 H 13 N 3 O 7 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 6.9878(9) Å, b = 7.0956(8) Å, c = 13.8113(15) Å, α = 88.745(5)°, β = 87.764(5)°, γ = 75.785(5)°, V = 663.27(14) Å 3 , Z = 2, R gt ( F ) = 0.0455, wR ref ( F 2 ) = 0.1264, T = 296.15 K.
Open Access
Crystal structure of N-ethyl-4-[3-(trifluoromethyl)-phenyl]piperazine-1-carbothioamide, C₁₄H₁₈F₃N₃S

28. Oktober 2022

Lamya H. Al-Wahaibi, Olivier Blacque, Nora H. Al-Shaalan, Edward R. T. Tiekink, Ali A. El-Emam

Seiten: 45-47

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C 14 H 18 F 3 N 3 S, monoclinic, P 2 1 / c (no. 14), a = 4.61919(4) Å, b = 29.1507(3) Å, c = 11.27803(10) Å, β = 94.4768(8)°, V = 1513.99(3) Å 3 , Z = 4, R gt ( F ) = 0.0588, wR ref ( F 2 ) = 0.1579, T = 160 K.
Open Access
The crystal structure of 3-anilino-1,4-diphenyl-4H-1,2,4-triazol-1-ium iodide, C₂₀H₁₇N₄I

1. November 2022

Hon Man Lee, Hsiu-Yu Hung

Seiten: 49-50

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C 20 H 17 N 4 I, monoclinic, P 2 1 / n (no. 14), a = 7.304(3) Å, b = 14.830(7) Å, c = 16.482(7) Å, β = 98.202(12)°, V = 1767.2(14) Å 3 , Z = 4, R gt ( F ) = 0.0568, wR ref ( F 2 ) = 0.1359, T = 150 K.
Open Access
The crystal structure of (tris(2-benzimidazolylmethyl)amine)-benzoato-copper(II) perchlorate monohydrate, CuC₃₁H₂₈N₇O₇Cl

28. Oktober 2022

Ji Li, Mingzhi Miao

Seiten: 51-53

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CuC 31 H 28 N 7 O 7 Cl, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 10.1386(6) Å, b = 12.1155(8) Å, c = 14.1972(8) Å, α = 100.297(2)°, β = 98.411(2)°, γ = 112.744(2)°, V = 1536.78(16) Å 3 , Z = 2, R gt ( F ) = 0.0613, wR ref ( F 2 ) = 0.1519, T = 250(2) K.
Open Access
Crystal structure of [2-hydroxy-3-methyl-benzoato-k¹ O-triphenyltin(IV)], C₂₆H₂₂O₃Sn

1. November 2022

Shaoliang Zhang, Shanshan Li

Seiten: 55-56

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C 26 H 22 O 3 Sn, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 10.8480(9) Å, b = 11.3511(11) Å, c = 11.4109(12) Å, α = 114.431(3)°, β = 96.994(2)°, γ = 108.207(3)°, V = 1162.94(19) Å 3 , Z = 2, R gt ( F ) = 0.0357, wR ref ( F 2 ) = 0.0667, T = 298 K.
Open Access
Crystal structure of diaqua-bis(4-(hydroxymethyl)-benzoato-k¹ O)zinc(II), C₁₆H₁₈O₈Zn

1. November 2022

Yujiao Huang, Ben Li, Siyi Miao, Linhui Luo, Haixia Pang, Qiang Tang

Seiten: 57-59

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C 16 H 18 O 8 Zn, monoclinic, I 2/ a (no. 15), a = 12.152(2) Å, b = 5.0051(8) Å, c = 27.273(5) Å, β = 101.536(7)°, V = 1625.3(5) Å 3 , Z = 4, R gt ( F ) = 0.052, w R ref ( F 2 ) = 0.143, T = 296 K.
Open Access
The crystal structure of dicarbonyl-(N-nitroso-N-oxido-phenylamine-κ ² O,O)-rhodium(I), C₈H₅N₂O₄Rh

10. November 2022

Mohammed A. Elmakki, Wesley Abdul Gafoor, Orbett T. Alexander, Johan A. Venter, Andreas Roodt

Seiten: 61-63

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C 8 H 5 N 2 O 4 Rh, monoclinic, P 2 1 / c (no. 14), a = 14.1998(9) Å, b = 3.6516(2) Å, c = 17.7458(11) Å, β = 92.801(2)°, V = 919.06(10) Å 3 , Z = 4, R gt ( F ) = 0.0281, wR ref ( F 2 ) = 0.0702, T = 100 K.
Open Access
The crystal structure of oxalic acid – 2-ethoxybenzamide (2/1), C₂₀H₂₄N₂O₈

1. Dezember 2022

Ying-Fan Xia, Shu-Ting Lin, Jia-Rong Zhang, Cheng-Jun Jiang

Seiten: 65-67

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C 20 H 24 N 2 O 8 , monoclinic, P 2 1 / n (no. 14), a = 3.8981(3) Å, b = 16.0675(11) Å, c = 16.2908(10) Å, β = 94.537(3)°, V = 1017.14(12) Å 3 , Z = 2, R gt ( F ) = 0.0634, wR ref ( F 2 ) = 0.1746, T = 170 K.
Open Access
The crystal structure of ethyl 7-ethyl-5-methyl-4,7-dihydrotetrazolo[1,5-a]pyrimidine-6-carboxylate, C₁₀H₁₅N₅O₂

10. November 2022

Wenxiang Wang, Jiahui Mou, Yue Sun

Seiten: 69-70

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C 10 H 15 N 5 O 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.0501(16) Å, b = 8.6163(17) Å, c = 9.6654(19) Å, α = 69.74(3)°, β = 75.79(3)°, γ = 87.43(3)°, V = 609.1(2) Å 3 , Z = 2, R gt ( F ) = 0.0593, w R ref ( F 2 ) = 0.1821, T = 293 K.
Open Access
Crystal structure of poly[(N,N-dimethylacetamide-κO) (μ₄-2-nitroisophthalato-κ ⁴ O:O′:O″:O′″)manganese(II)], C₁₁H₁₀N₂O₇Mn

16. November 2022

Xiao-Ming Shi, Yu-Jia Fu, Zhi-Chao Zhang

Seiten: 71-73

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C 11 H 10 N 2 O 7 Mn, monoclinic, P 2 1 / c (no. 14), a = 8.1501(5) Å, b = 10.8198(7) Å, c = 15.2391(9) Å, β = 91.921(5)°, V = 1343.07(14) Å 3 , Z = 4, R gt ( F ) = 0.0363, wR ref ( F 2 ) = 0.0783, T = 293 K.
Open Access
Crystal structure of 14-O-acetyldelcosine, C₂₆H₄₁NO₈

21. November 2022

Huan-Ni Liu, Yi-Kun Hao, Neng-Hua Chen, Lai-Ming Li

Seiten: 75-77

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C 26 H 41 NO 8 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 8.24370(10) Å, b = 13.1867(2) Å, c = 22.8490(4) Å, V = 2483.85(6) Å 3 , Z = 4, R gt ( F ) = 0.0357, wR ref ( F 2 ) = 0.0975, T = 169.99(10) K.
Open Access
The crystal structure of poly[(1,10-phenanthroline-κ² N,N′)-(μ ₄-2-chlorobenzene-1,3-dicarboxylato-κ⁵ O:O′:O″:O‴) cadmium(II)] monohydrate, C₂₀H₁₃CdClN₂O₅

24. November 2022

Guang Huang

Seiten: 79-81

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C 20 H 13 CdClN 2 O 5 , monoclinic, P 2 1 / n (no. 14), a = 11.4994(9) Å, b = 13.1171(10) Å, c = 13.0233(10) Å, β = 109.126(8)°, V = 1856.0(3) Å 3 , Z = 4, R gt ( F ) = 0.0341, wR ref ( F 2 ) = 0.0779, T = 293 K.
Open Access
Crystal structure of propane-1,3-diylbis(diphenylphosphine sulfide) ethanol solvate, C₂₇H₂₆P₂S₂

21. November 2022

Kgaugelo C. Tapala, Hadley S. Clayton

Seiten: 83-85

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C 27 H 26 P 2 S 2 , tetragonal, I 4 (no. 79), a = 16.9196(12) Å, c = 9.4187(8) Å, V = 2696.3(4) Å 3 , Z = 4, R gt ( F ) = 0.0341, wR ref ( F 2 ) = 0.0726, T = 173(2) K.
Open Access
Crystal structure of bis{[(4-diethylamino-2-hydroxy-benzylidene)-hydrazinocarbonylmethyl]-trimethylammonium} tetrabromozincate, C₃₂H₅₄N₈O₄ZnBr₄

25. November 2022

Shi-Lin Zhang

Seiten: 87-89

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C 32 H 54 N 8 O 4 ZnBr 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.250(5) Å, b = 12.289(10) Å, c = 20.954(14) Å, α = 82.36(2)°, β = 81.977(14)°, γ = 86.96(2)°, V = 2084(2) Å 3 , Z = 2, R gt ( F ) = 0.0525, w R ref ( F 2 ) = 0.1419, T = 150(2) K.
Open Access
Synthesis and crystal structure of dimethyl 2,2′-(2,5-bis(4-hydroxyphenyl)-2,5-dihydrofuran-3,4-diyl)dibenzoate, C₃₄H₃₀O₇

18. November 2022

Yun-Yee Low, Siew-Huah Lim

Seiten: 91-93

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C 34 H 30 O 7 , monoclinic, C 2/ c (no. 15), a = 29.4446(6) Å, b = 12.4393(3) Å, c = 14.9807(3) Å, β = 90.390(1)°, V = 5486.9(2) Å 3 , Z = 8, R gt ( F ) = 0.0408, w R ref ( F 2 ) = 0.1023, T = 100 K.
Open Access
Synthesis and crystal structure of 2-(2-oxo-2-phenylethyl)-4H-chromen-4-one, C₁₇H₁₂O₃

22. November 2022

Feng Liu, Yi Liu, Yang Chen, Xiaolong Yan, Tao Xiao

Seiten: 95-96

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C 17 H 12 O 3 , monoclinic, P 2 1 / c (no. 14), a = 9.2911(15) Å, b = 17.525(3) Å, c = 8.5586(15) Å, β = 109.358(7)° V = 1314.8(4) Å 3 , Z = 4, R gt ( F ) = 0.0550, w R ref ( F 2 ) = 0.1789, T = 296(2) K.
Open Access
The crystal structure of tetra(imidazole-κ¹ N)zinc(II) μ₂-oxido-hexaoxido-divanadium(VI) C₁₂H₁₆N₈O₆V₂Zn

17. November 2022

Yueyang Huo, Shiqi Fu, Yanqi Shi, Yingying Duan, Meiyu Zhang

Seiten: 97-99

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C 12 H 16 N 8 O 6 V 2 Zn, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 9.5397(4) Å, b = 10.2457(4) Å, c = 11.0920(4) Å, α = 92.848(1)°, β = 110.314(1)°, γ = 94.421(1)°, V = 1010.29(7) Å 3 , Z = 2, R gt ( F ) = 0.0358, wR ref ( F 2 ) = 0.0932, T = 293 K.
Open Access
Crystal structure of S-2-(1-(5-methylpyridin-2-ylamino)octyl)-3-hydroxynaphthalene-1,4-dione, C₂₄H₂₈N₂O₃

16. November 2022

Qing-Gang Chen, Wei Wan, Guo-Ying Peng, Chang-gan Huang

Seiten: 101-103

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[C 24 H 28 N 2 O 3 ], monoclinic, P 12 1 / n , a = 12.8878(5) Å, b = 27.5641(11) Å, c = 13.0517(6) Å, β = 111.908(2) ∘ , V = 4301.7(3) Å 3 , Z = 4, R gt ( F ) = 0.0576, wR ref ( F 2 ) = 0.1749, T = 296(2) K.
Open Access
Crystal structure of bis(μ₂-5-chloro-2-oxido-N-(1-oxido-2-oxo-2-phenylethylidene)-benzohydrazonato-κ⁵ N,O,O′:N′,O′′)-oktakis(pyridine-κ¹ N)trinickel(II) – methanol – pyridine (1/1/1) C₇₆H₆₅N₁₃C_l2Ni₃O₉

18. November 2022

Zhou Zhongyuan, Yang Liguo, Zou Kun, Fu Jiaqi, Ji Xinyu

Seiten: 105-108

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C 76 H 65 N 13 Cl 2 Ni 3 O 9 , monoclinic, P 2 1 / n , a = 15.937(4) Å, b = 16.805(4) Å, c = 27.463(7) Å, β = 94.613(3)°, V = 7332(3) Å 3 , Z = 4, R gt ( F ) = 0.0490, wR ref ( F 2 ) = 0.1596, T = 298 K.
Open Access
The crystal structure of methyl 3,5-diaminobenzoate, C₈H₁₀N₂O₂

14. Dezember 2022

John M. Gardiner, James Raftery, Ian G. Beadham, Jannat N. Azarah, Mohammed Y. Abu-Foul, Adel M. Awadallah, Rami Y. Morjan

Seiten: 109-110

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C 8 H 10 N 2 O 2 , orthorhombic, Pbca (no. 61), a = 11.0571(2) Å, b = 8.1172(2) Å, c = 17.6080(4) Å, V = 1580.37(6) Å 3 , Z = 8, R gt ( F ) = 0.0324, wR ref ( F 2 ) = 0.0872, T = 100(2) K.
Open Access
Crystal structure of 10-(9H-carbazol-9-yl)-5H-dibenzo[a,d][7]annelen-5-one, C₂₇H₁₇NO

14. Dezember 2022

Yunlu Li, Xinzhong Wang

Seiten: 111-112

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C 27 H 17 NO, monoclinic, P 2 1 (no. 4), a = 9.8945(6) Å, b = 8.1838(5) Å, c = 12.2042(7) Å, β = 107.539(6)°, V = 942.29(10) Å 3 , Z = 2, R gt ( F ) = 0.0306, wR ref ( F 2 ) = 0.0698, T = 149.99(10)
Open Access
Crystal structure of ethyl 1-(2-hydroxyethyl)-4-((4-methoxyphenyl)amino)-5-oxo-2,5-dihydro-1H-pyrrole-3-carboxylate, C₁₆H₂₀N₂O₅

13. Dezember 2022

Fatin Nur Ain Abdul Rashid, Muhamad Zulfaqar Bacho, Alexandra M. Z. Slawin, Mohd Abdul Fatah Abdul Manan, Saiful Azmi Johari, Mohd Fazli Mohammat

Seiten: 113-115

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C 16 H 20 N 2 O 5 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 7.9179(7) Å, b = 10.1982(9) Å, c = 10.4144(8) Å, α = 76.184(7)°, β = 87.090 (7)°, γ = 73.500(8)°, V = 782.86(12) Å 3 , Z = 2, R gt ( F ) = 0.0458, w R ref ( F 2 ) = 0.1333, T = 93 K.
Open Access
The crystal structure of 1-(4-bromophenyl)-3-cycloheptylurea, C₁₄H₁₉BrN₂O

14. Dezember 2022

Kai Gao, Su-E. Zha, Chang-Ying Liu, Qiao-Juan Wang, Er-Qiang Wang

Seiten: 117-118

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C 14 H 19 BrN 2 O, monoclinic, P 2 1 / c (no. 14), a = 12.9782(8) Å, b = 9.1447(6) Å, c = 11.8842(8) Å, β = 98.214(6)°, V = 1395.97(16) Å 3 , Z = 4, R gt ( F ) = 0.0637, wR ref ( F 2 ) = 0.1876, T = 293 K.
Open Access
The crystal structure of 1,4-bis(1,2,3,4,5-pentamethylcyclopenta-2,4-dien-1-yl)-3,6-bis ((4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methylene)-1,4-dialuminacyclohexane – benzene (1/2), C₅₀H₇₂Al₂B₂O₄

14. Dezember 2022

Bing Wang, Bo-Han Hu, Di Wu

Seiten: 119-121

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C 50 H 72 Al 2 B 2 O 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.7261(2) Å, b = 11.1827(3) Å, c = 13.8599(4) Å, α = 112.7800(10)°, β = 102.5410(10)°, γ = 93.8340(10)°, V = 1199.98(6) Å 3 , Z = 1, R gt ( F ) = 0.0365, wR ref ( F 2 ) = 0.1037, T = 170 K.
Open Access
Crystal structure of bis(μ ₃-diphenylphosphinato)-tetrakis(μ ₂-diphenylphosphinato)-bis(diphenylphosphinato)-bis(μ ₂-hydroxo)dicopper(II)-ditin(IV), C₁₀₄H₁₀₀O₁₈P₈Cu₂Sn₂

5. Dezember 2022

Sun Xiaolin, Guo Yuhua, Yu Youzhu

Seiten: 123-125

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C 104 H 100 O 18 P 8 Cu 2 Sn 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 13.8254(6) Å, b = 14.1283(6) Å, c = 15.1940(7) Å, α = 112.571(1)°, β = 104.707(1)°, γ = 104.433(1)°, V = 2442.87(19) Å 3 , Z = 1, R gt ( F ) = 0.0256, wR ref ( F 2 ) = 0.0955, T = 296(2) K.
Open Access
Crystal structure of 3-((3,4-dichloroisothiazol-5-yl)methoxy)benzo[d] isothiazole 1,1-dioxide, C₁₁H₆Cl₂N₂O₃S₂

14. Dezember 2022

Huang Cong, Xiao Shu-Zhen, Zhong Liang, Chen Shang-Xing, Peng Da-Yong

Seiten: 127-128

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C 11 H 6 Cl 2 N 2 O 3 S 2 , triclinic, P 1‾ (no. 2), a = 6.974(3) Å, b = 8.132(3) Å, c = 12.349(5) Å, α = 86.123(4)°, β = 78.299(4)°, γ = 85.715(4)°, V = 682.9(4) Å 3 , Z = 2, R gt ( F ) = 0.0410, wR ref ( F 2 ) = 0.1058, T = 296(2) K.
Open Access
Synthesis and crystal structure of 2-(2-(2-fluorophenyl)-2-oxoethyl)-4H-chromen-4-one, C₁₇H₁₁FO₃

2. Dezember 2022

Yi Liu, Feng Liu, Yang Chen, Xiaolong Yan, Tao Xiao

Seiten: 129-131

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C 17 H 11 FO 3 , monoclinic, P 2 1 / c (no. 14), a = 9.1987(2) Å, b = 17.5458(3) Å, c = 8.5802(2) Å, β = 108.193(3)°, V = 1315.60(5) Å 3 , Z = 4, R gt ( F ) = 0.0346, wR ref ( F 2 ) = 0.1196, T = 293(2) K.
Open Access
The crystal structure of tris(carbonyl)-bis(carbonyl)-[μ-propane-1,2- dithiolato]-(benzyldiphenylphosphine)diiron (Fe—Fe), C₂₇H₂₃Fe₂O₅PS₂

14. Dezember 2022

Ming-Gang Wu, Xu-Feng Liu

Seiten: 133-135

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C 27 H 23 Fe 2 O 5 PS 2 , monoclinic, P 2 1 / c (no. 14), a = 11.3170(5) Å, b = 16.1774(8) Å, c = 15.2170(7) Å, β = 92.933(1)°, V = 2782.3(2) Å 3 , Z = 4, R gt ( F ) = 0.0537, wR ref ( F 2 ) = 0.1636, T = 296(2) K.
Open Access
Crystal structure of 1-(2-(4-chlorophenethyl)-2-hydroxy-3,3-dimethylbutyl)-1H-1,2,4-triazol-4-ium nitrate, C₁₆H₂₃N₄O₄Cl

15. Dezember 2022

Hua Wang, Guo-tao Zhang, Hong-ya Li

Seiten: 137-139

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C 16 H 23 N 4 O 4 Cl, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 7.609(2) Å, b = 9.287(3) Å, c = 13.511(4) Å, α = 90.530(7)°, β = 102.028(5)°, γ = 97.774(6)°, V = 924.4(5) Å 3 , Z = 2, R gt ( F ) = 0.0625, w R ref ( F 2 ) = 0.1634, T = 296(2) K.
Open Access
The crystal structure of 3,3′-disulfanediyldi(1H-1,2,4-triazol-5-amine) monohydrate, C₄H₈N₈OS₂

14. Dezember 2022

Giyosiddin Khayrullaev, Batirbay Torambetov, Shakhnoza Kadirova, Yevhenii Vaksler

Seiten: 141-144

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C 4 H 8 N 8 OS 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 7.4377(5) Å, b = 7.5032(5) Å, c = 10.0964(6) Å, α = 91.481(5)°, β = 108.906(5)°, γ = 110.678(6)°, V = 492.41(6) Å 3 , Z = 2, R gt ( F ) = 0.0653, wR ref ( F 2 ) = 0.1888, T = 293 (2) K.
Open Access
The crystal structure of trans-[bis(4-methylpyridine-κN)bis(quinoline-2-carboxylato- κ ² N,O)cadmium(II)], C₃₂H₂₆CdN₄O₄

14. Dezember 2022

Boris-Marko Kukovec, Vesna Sokol, Zora Popović

Seiten: 145-147

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C 32 H 26 CdN 4 O 4 , tetragonal, P 4 1 2 1 2 (no. 92), a = 13.7308(6) Å, c = 15.1806(7) Å, V = 2862.1(3) Å 3 , Z = 4, R gt ( F ) = 0.0359, wR ref ( F 2 ) = 0.0693, T = 296(2) K.
Open Access
The crystal structure of ethyl 2′-hydroxy-4′,6′-dimethoxy-3-(4-methoxynaphthalen-1-yl)-5-oxo-2,3,4,5-tetrahydro-[1,1′-biphenyl]-4-carboxylate, C₂₈H₂₈O₇

14. Dezember 2022

Soon Young Shin, Ha-Jin Lee, Dongsoo Koh

Seiten: 149-151

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C 28 H 28 O 7 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 11.0746(18) Å, b = 11.4312(17) Å, c = 11.552(2) Å, α = 77.148(8)°, β = 62.164(8)°, γ = 67.858(8)°, V = 1195.9(4) Å 3 , Z = 2, R gt ( F ) = 0.0522, wR ref ( F 2 ) = 0.1862, T = 223(2) K .

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