Zeitschrift für Kristallographie - New Crystal Structures

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Zeitschrift für Kristallographie - New Crystal Structures

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Zeitschrift für Kristallographie - New Crystal Structures

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Frontmatter

January 4, 2024

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New Crystal Structures
Open Access
Crystal structure of poly[diaqua-(μ₄-3,3′-di(1H-1,2,4-triazol-1-yl)-[1,1′-biphenyl]-4,4′-dicarboxylate-N:N′:O:O′)cadmium(II)], C₁₈H₁₄N₆O₆Cd

November 15, 2023

Jin-Bo Guo, Long Zhang

Page range: 1-2

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C 18 H 14 N 6 O 6 Cd, monoclinic, C 2/ c (no. 15), a = 27.000(3) Å, b = 7.0750(8) Å, c = 10.5576(11) Å, β = 110.080(2)°, Z = 4, V = 1894.2(4) Å 3 , R gt ( F ) = 0.0370, wR ref ( F 2 ) = 0.0584, T = 296 K.
Open Access
Crystal structure of (8R,8′S,13S,13′R)-8,8′-bis(hydroxymethyl)-9,9′,10,10′-tetramethoxy-5,5′,6,6′,8,8′,13,13′-octahydro-[13,13′-bi[1,3]dioxolo[4,5-g]isoquinolino[3,2-a]isoquinoline]-7,7′-diium chloride-methanol (1/2), C₄₆H₅₈N₂O₁₄Cl₂

November 8, 2023

Wei Han, Mei Li, Xiang Geng, Guoshun Zhang

Page range: 3-5

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C 46 H 58 N 2 O 14 Cl 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 7.5623(2) Å, b = 10.87056(17) Å, c = 13.90486(15) Å, α = 105.7122(12)°, β = 98.907(2)°, γ = 91.067(2)°, V = 1084.88(4) Å 3 , Z = 1, R gt ( F ) = 0.0341, wR ref ( F 2 ) = 0.0935, T = 100(2) K.
Open Access
The crystal structure of 8-methoxy-2,2-diphenyl-tosyl-1,2-dihydro-2λ⁴,3λ⁴-[1,3,2]diazaborolo[4,5,1-ig]quinoline, C₂₉H₂₅BN₂O₃S

November 8, 2023

Siyi Ding

Page range: 7-9

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C 29 H 25 BN 2 O 3 S, monoclinic, P 2 1 / c (no. 14), a = 14.4345(6) Å, b = 9.7073(5) Å, c = 18.3873(8) Å, β = 107.766°, V = 2453.56(19) Å 3 , Z = 4, R gt ( F ) = 0.0587, w R ref ( F 2 ) = 0.1592, T = 193 K.
Open Access
Crystal structure of aqua-(5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ⁴N,N′,N″,N‴)copper(II) 5-carboxyisophthalate tetrahydrate, C₂₅H₅₀N₄CuO₁₁

December 6, 2023

Qin-Guo Quan, Guang-Chuan Ou

Page range: 11-13

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C 25 H 50 N 4 CuO 11 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 10.553(6) Å, b = 12.099(7) Å, c = 12.674(8) Å, α = 86.258(6) ° , β = 78.131(6) ° , γ = 81.408(6) ° , V = 1564.8(16) Å 3 , Z = 2, R gt ( F ) = 0.0332, wR ref ( F 2 ) = 0.0927, T = 296(2) K.
Open Access
The crystal structure of 1-(naphthalen-2-ylsulfonyl)-2,2-diphenyl-1,2-dihydro-2λ⁴,3λ⁴-[1,3,2]diazaborolo[4,5,1-ij]quinoline, C₃₁H₂₃BN₂O₂S

November 8, 2023

Jing Zhou, Siyi Ding

Page range: 15-17

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C 31 H 23 BN 2 O 2 S, monoclinic, P 2 1 / c (no. 14), a = 9.1784(5) Å, b = 9.1168(6) Å, c = 28.7021(16) Å, β = 93.439°, V = 2397.4(2) Å 3 , Z = 4, R gt ( F ) = 0.0489, wR ref ( F 2 ) = 0.1191, T = 193 K.
Open Access
Crystal structure of iodido-(η⁶-benzene) (1-(pyridin-2-yl)-N-(p-fluoro-methanamine)-κ²N,Nʹ)ruthenium(II) hexaflourophosphate, (C₁₈H₁₅F₇IN₂RuP)

November 13, 2023

Sizwe J. Zamisa, Joel M. Gichumbi, Holger B. Friedrich

Page range: 19-21

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C 18 H 15 F 7 IN 2 RuP, triclinic, P 1̄ (no. 2), a = 7.3761(3) Å, b = 9.8737(4) Å, c = 14.3439(6) Å, α = 92.996(2) ° , β = 95.590(2) ° , γ = 104.992 (2) ° , V = 10001.03(7) Å 3 , Z = 2, R gt ( F ) = 0.0212, wR ref ( F 2 ) = 0.0527, T = 173 K.
Open Access
The crystal structure of 1-(3-oxo-1-phenyl-3-(p-tolyl) propylidene)-1,3-dihydro-2H-inden-2-one, C₂₅H₂₀O₂

November 8, 2023

Mengdan Wang, Weiwei Lu, Junling Wang, Mengyang Li, Yuanyuan Feng, Jun-Ying Ma

Page range: 23-24

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C 25 H 20 O 2 , triclininc, P 1 ‾ $\overline{1}$ (no. 2), a = 9.821(2) Å, b = 10.141(2) Å, c = 10.679(2) Å, α = 61.688(4) ° , β = 86.002(4) ° , γ = 84.220(4) ° , V = 931.3(3) Å 3 , Z = 2, R gt ( F ) = 0.0522, wR ref ( F 2 ) = 0.1437, T = 293 K.
Open Access
Crystal structure of tricyclohexyl[4-(4H-1,2,4-triazol-4-yl)-benzoato-κO]tin(IV), C₂₇H₃₉N₃O₂Sn

November 7, 2023

Jingjing Qing, Jie Tian, Xin Deng, Fuxing Zhang

Page range: 25-27

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C 27 H 39 N 3 O 2 Sn, monoclinic, P 2 1 / c (no. 14), a = 10.3317(6) Å, b = 15.8067(9) Å, c = 16.5497(9) Å, β = 90.5380(10) ° , V = 2702.6(3) Å 3 , Z = 4, R gt ( F ) = 0.0370, w R ref ( F 2 ) = 0.0954, T = 296(2) K.
Open Access
Crystal structure of [triaqua-(8-carboxymethoxy-quinoline-2-carboxylate-κ⁴N,O,O,O)cadmium(II)]monohydrate, C₁₂H₁₅NO₉Cd

November 3, 2023

Wang Li-Hua, Yan Xi-Hai, Wang Yuan-Fang, Tai Xi-Shi

Page range: 29-31

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C 12 H 15 NO 9 Cd, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 7.5263(5) Å, b = 8.0953(3) Å, c = 12.4005(8) Å, α = 86.814(4)°, β = 79.845(5)°, γ = 86.140(4)°, V = 741.28(7) Å 3 , Z = 2, R gt ( F ) = 0.0759, wR ref ( F 2 ) = 0.2248, T = 295 K.
Open Access
Crystal structure of ethyl 2-((4-(3,5-dimethylisoxazol-4-yl)-2,6-difluorophenyl)amino)benzoate, C₂₀H₁₈F₂N₂O₃

November 8, 2023

Wenqiang Tang, Yanrong Gao, Xiaona Xu, Zhoujing Zhu

Page range: 33-35

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C 20 H 18 F 2 N 2 O 3 , monoclinic, P 2 1 / n (no. 14), a = 7.5573(10) Å, b = 14.519(2) Å, c = 16.245(2) Å, β = 98.187(3)°, V = 1764.4(4) Å 3 , Z = 4, R gt ( F ) = 0.0420 w R ref ( F 2 ) = 0.1142, T = 205 K.
Open Access
The crystal structure of 2-(hydroxymethyl)-2-(4H-1,2,4-triazol-4-yl)propane-1,3-diol, C₆H₁₁N₃O₃

November 7, 2023

Jing-Jing Guo, Chao Feng, Zi-Jie Chen

Page range: 37-38

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C 6 H 11 N 3 O 3 , monoclinic, P 2 1 / n (no. 14), a = 6.1802(3) Å, b = 12.6623(5) Å, c = 10.0897(4) Å, β = 93.328(2) ° , V = 760.10(6) Å 3 , Z = 4, R gt ( F ) = 0.0341, w R ref ( F 2 ) = 0.0864, T = 150 K.
Open Access
The crystal structure of 1,2-bis(2,4-dinitrophenyl) hydrazine, C₁₂H₈N₆O₈

November 3, 2023

Yunlu Li, Mei Xue, Xinzhong Wang

Page range: 39-40

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C 12 H 8 N 6 O 8 , orthorhombic, Pbcn (no. 60), a = 11.9333(5) Å, b = 9.2524(4) Å, c = 12.8675(7) Å, V = 1420.72(12) Å 3 , Z = 8, R gt ( F ) = 0.0468, wR ref ( F 2 ) = 0.1159, T = 170 K.
Open Access
Crystal structure of 1-(2,6-dichloro-4-(3,5-dimethylisoxazol-4-yl)phenyl)-1,2-dihydro-4H-benzo[d][1,3]oxazin-4-one, C₁₉H₁₄Cl₂N₂O₃

November 13, 2023

Zhoujing Zhu, Cuiya Zhang, Xiaona Xu, Wenqiang Tang

Page range: 41-42

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C 19 H 14 Cl 2 N 2 O 3 , monoclinic, P 2 1 / c (no. 14), a = 10.635(3) Å, b = 8.772(3) Å, c = 19.656(6) Å, β = 98.256(10)°, V = 1814.8(10) Å 3 , Z = 4, R gt ( F ) = 0.0602, wR ref ( F 2 ) = 0.1547, T = 205 K.
Open Access
The crystal structure of 5-amino-5-oxo-4-(1-oxo-4-(2-oxopyrrolidin-1-yl)isoindolin-2-yl)pentanoic acid, C₁₇H₁₉N₃O₅

November 15, 2023

Qing Wang, Yanrong Gao, Hongjuan Tong, Wenqiang Tang

Page range: 43-45

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C 17 H 19 N 3 O 5 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 8.3683(3) Å, b = 9.1873(3) Å, c = 11.3782(4) Å, α = 96.553(1) ° , β = 108.368(1) ° , γ = 92.429(1) ° , V = 821.94(5) Å 3 , Z = 2, R gt ( F ) = 0.0450, wR ref ( F 2 ) = 0.1175, T = 170 K.
Open Access
Crystal structure of N²,N⁶-bis(2-(((Z)-5-bromo-2-hydroxybenzylidene)amino) phenyl)pyridine-2,6-dicarboxamide, C₃₃H₂₃Br₂N₅O₄

November 29, 2023

Wen-Ze Zhao, Lei Zhang, Na Zhang

Page range: 47-49

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C 33 H 23 Br 2 N 5 O 4 , triclinic, P 1̄ (no. 2), a = 10.649(3) Å, b = 11.244(3) Å, c = 14.301(4) Å, α = 68.254(7)°, β = 72.939(7)°, γ = 81.125(7)°, V = 1518.5(7) Å 3 , Z = 2, R gt ( F ) = 0.0514, w R ref ( F 2 ) = 0.1327, T = 273(2) K.
Open Access
The crystal structure of (E)-2-methoxy-6-(((5-methyl-1,3,4-thiadiazol-2-yl)imino)methyl)phenol, C₁₁H₁₁N₃O₂S

November 21, 2023

Qiuping Huang, Zhenfang Zeng, Qiuchan Huang

Page range: 51-52

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C 11 H 11 N 3 O 2 S, orthorhombic, Pna 2 1 (no. 33), a = 22.6572(9) Å, b = 10.0205(4) Å, c = 4.9023(2) Å, V = 1113.01(8) Å 3 , Z = 5, R gt ( F ) = 0.0341, w R ref ( F 2 ) = 0.0857, T = 297 K.
Open Access
The crystal structure of 3-((tert-butyldiphenylsilyl)methyl)-5,5-diphenyl-6-(p-tolyl) tetrahydro-2H-pyran-2-one, C₄₁H₄₂O₂Si

November 14, 2023

Xiao-Feng Zhai, Shi-Hong Lin, Zhao-Zhao Zhou, Haixin Ding

Page range: 53-55

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C 41 H 42 O 2 Si, monoclinic, P 2 1 / n (no. 14), a = 14.1100(17) Å, b = 15.8352(19) Å, c = 16.644(2) Å, β = 110.659(2)°, V = 3479.7(7) Å 3 , Z = 4, R gt ( F ) = 0.0540, wR ref ( F 2 ) = 0.1633, T = 296.15 K.
Open Access
Crystal structure of 9-fluoro-4-(6-methoxypyridin-3-yl)-5,6-dihydrobenzo[h]quinazolin-2-amine, C₁₈H₁₅FN₄O

November 7, 2023

Xiao-Qing Yun, Yun Hou, Feng-Lan Zhao, Qing-Guo Meng

Page range: 57-59

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C 18 H 15 FN 4 O, triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 8.8914(5) Å, b = 10.5705(7) Å, c = 16.4831(9) Å, α = 96.673(5)°, β = 99.397(5)°, γ = 95.062(5)°, V = 1508.93(16) Å 3 , Z = 4, R gt ( F ) = 0.0477, w R ref ( F 2 ) = 0.1232, T = 293 K.
Open Access
The crystal structure of 2-bromo-5-(4-cyanophenoxy)benzyl 1-methyl-1,2,5,6-tetrahydropyridine-3-carboxylate, C₂₁H₁₉BrN₂O₃

November 20, 2023

Xianwu Liu, Yifan Li, Changzhou Liao, Yanping Luo, Lanying Wang

Page range: 61-63

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C 21 H 19 BrN 2 O 3 , orthorhombic, Pna 2 1 (no. 33) a = 25.412(3) Å, b = 21.329(2) Å, c = 7.0020(8) Å, V = 3795.2(7) Å 3 , Z = 8, R gt ( F ) = 0.0390, wR ref ( F 2 ) = 0.1009, T = 100(2) K.
Open Access
Crystal structure of 3,3′-(1,4-phenylenebis(methylene))bis(1-isopropyl-1H-imidazol-3-ium) bis(hexafluorophosphate(V)), C₁₀H₁₄F₆N₂P

December 6, 2023

Yi-Chen Zou, Nian-Cheng Lin, Wan-Ming Xiong, Xu-Liang Nie, Su-Qin Wu

Page range: 65-67

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C 10 H 14 F 6 N 2 P, orthorhombic, Pbca (no. 61), a = 9.5929(10) Å, b = 15.9201(16) Å, c = 17.8640(19) Å, V = 2728.2(5) Å 3 , Z = 8, R gt ( F ) = 0.0587, wR ref ( F 2 ) = 0.1735, T = 296(2) K.
Open Access
The crystal structure of 2,2-di(thiophen-3-yl)-1-tosyl-1,2-dihydro-2λ⁴,3λ⁴-[1,3,2]diazaborolo[4,5,1-ig]quinoline, C₂₄H₁₉BN₂O₂S₃

December 6, 2023

Siyi Ding

Page range: 69-71

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C 24 H 19 BN 2 O 2 S 3 , P 2 1 / n (no. 14), a = 13.9768(6) Å, b = 9.0258(4) Å, c = 18.3256(8) Å, β = 104.763°, V = 2235.49(18) Å 3 , Z = 4, R gt ( F ) = 0.0406, w R ref ( F 2 ) = 0.1156, T = 193 K.
Open Access
Crystal structure of 5-bromo-1-(2-iodobenzoyl)-1H-indole-3-carbaldehyde, C₁₆H₉BrINO₂

November 23, 2023

Yue Zhang, Qian-Qian Tang, Jia-Cheng Yuan, Cheng-Sheng Sheng, Wei Cong

Page range: 73-75

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C 16 H 9 BrINO 2 , triclinic, P 1̄ (no. 2), a = 7.9305(12) Å, b = 8.2051(10) Å, c = 11.3141(13) Å, α = 85.384(10)°, β = 85.619(11)°, γ = 87.745(11)°, V = 731.27(17) Å 3 , Z = 2, R gt ( F ) = 0.0397, wR ref ( F 2 ) = 0.0819, T = 293(2) K.
Open Access
The crystal structure of monocarbonyl-2-carboxypyridinato-κ²N,O-triphenylphosphine-rhodium(I) acetonitrile solvate, C₂₆H_20.50N_1.50O₃PRh

November 9, 2023

Mohammed A. Elmakki, Thato N. Taoana, Setjhaba V. Mosese, Alice Brink, Johan A. Venter

Page range: 77-79

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C 26 H 20.50 N 1.50 O 3 PRh, monoclinic, C 2/ c (no. 15), a = 30.5215(9) Å, b = 8.7529(2) Å, c = 22.4219(11) Å, β = 132.137(1) ∘ , V = 4441.9(3) Å 3 , Z = 8, R gt ( F ) = 0.0305, wR ref ( F 2 ) = 0.0615, T = 100 K.
Open Access
Crystal structure of dichlorido-tetrakis(1-(2,4-dichlorophenyl)-4,4-dimethyl-2-(1,2,4-triazol-1-yl)pent-1-en-3-ol-κ¹N)manganese(II), C₆₀H₆₈O₄N₁₂Cl₁₀Mn

December 5, 2023

Ze-Jing Fan, Hong-Ya Li, Biao Yan

Page range: 81-83

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C 60 H 68 O 4 N 12 Cl 10 Mn, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 8.9262(11) Å, b = 13.7013(18) Å, c = 15.330(2) Å, α = 91.414(2)°, β = 98.951(2)°, γ = 106.688(2)°, V = 1769.3(4) Å 3 , Z = 1, R gt ( F ) = 0.0443, wR ref ( F 2 ) = 0.1222, T = 296(2) K.
Open Access
Crystal structure of 3-(tert-butyldiphenylsilyl)-1-(2,6-dichlorophenyl)-2,2-diphenylpropan-1-ol, C₃₇H₃₆Cl₂OSi

December 13, 2023

Shu-Liang Zhang, Zhao-Zhao Zhou, Xi Chen

Page range: 85-87

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C 37 H 36 Cl 2 OSi, monoclinic P 2 1 / n (no. 14), a = 10.4363(14) Å, b = 17.128(2) Å, c = 17.875(3) Å, β = 90.934(2)°, V = 3194.8(8) Å 3 , Z = 4, R gt ( F ) = 0.0491, wR ref ( F 2 ) = 0.1449, T = 296.15 K.
Open Access
Crystal structure of langite from Mine du Pradet (France)

December 7, 2023

Christian Paulsen, Valérie Galéa-Clolus, Rainer Pöttgen

Page range: 89-91

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Cu 4 (OH) 6 SO 4 ·2H 2 O, monoclinic, Pc (no. 7), a = 7.1026(2) Å, b = 6.0143(1) Å, c = 11.1645(3) Å, β = 90.1103(8)°, V = 476.91(2) Å 3 , Z = 2, R gt ( F 2 ) = 0.0206, wR ref ( F 2 ) = 0.0563, T = 100 K.
Open Access
The crystal structure of 5′-(furan-2-yl)-3′-((4-methylphenyl)sulfonamido)-3′,4′,5′,6′-tetrahydro-[1,1′:3′,1″-terphenyl]-4′-carboxylic acid, C₃₀H₂₇NO₅S

December 8, 2023

Xulan Wang, Guoyong Luo, Jianghai Ye, Jiangping Wang, Yunlong Liu, Tianqiong Lang

Page range: 93-95

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C 30 H 27 NO 5 S, monoclinic, P 2 1 (no. 4), a = 10.4329(16) Å, b = 11.6208(18) Å, c = 11.8268(18) Å, β = 114.257(5)°, V = 1307.3(4) Å 3 , Z = 2, R gt ( F ) = 0.0685, wR ref ( F 2 ) = 0.1547, T = 273(2) K.
Open Access
Synthesis and crystal structure of bis{2-(((4-acetophenone)imino)methyl)-4-fluorophenolato-κ²N,O}zinc(II), C₃₀H₂₂F₂N₂O₄Zn

December 29, 2023

Ji-Xing Zhao, Lei-Fang Wu, Da-Qun Chen

Page range: 97-98

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C 30 H 22 F 2 N 2 O 4 Zn, monoclinic, P 2/ c (no. 13), a = 9.5936(8) Å, b = 11.2561(10) Å, c = 11.9682(10) Å, β = 104.598(3)°, V = 1250.68(19) Å 3 , Z = 2, R gt ( F ) = 0.0661, wR ref ( F 2 ) = 0.1259, T = 173(2) K.
Open Access
The crystal structure of poly[(tripyridine-κ³N,N′,N″) μ₃-(pyridine-3,4-dicarboxylate-κ³N:O:O′) manganese(II)], C₂₂H₂₂N₄O₈Mn

December 7, 2023

Wen-Jie Bi, Hu Chen, Shi-Wei Yang, Xiao-Hong Wang

Page range: 99-101

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C 22 H 22 N 4 O 8 Mn, monoclinic, P 2 1 / c (no. 14), a = 12.7620(10) Å, b = 14.980(2) Å, c = 13.2910(11) Å, β = 120.070(5)°, V = 2198.9(4) Å 3 , Z = 4, R gt ( F ) = 0.0594, wR ref ( F 2 ) = 0.1345, T = 293(2) K.
Open Access
The crystal structure of (E)-4-chloro-N′-(1-(4-hydroxyphenyl)propylidene)benzohydrazide, C₁₆H₁₅ClN₂O₂

December 6, 2023

Yanjiao Wang, Chao Wang, Xuguang Gao, Bin Liu

Page range: 103-104

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C 16 H 15 ClN 2 O 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 7.9715(8) Å, b = 8.2727(8) Å, c = 11.5105(12) Å, α = 90.296(8)°, β = 100.566(9)°, γ = 102.603(9)°, V = 727.41(13) Å 3 , Z = 2, R gt ( F ) = 0.0522, wR ref ( F 2 ) = 0.1257, T = 293 K.
Open Access
Synthesis and crystal structure of bis{2-(tert-butyl)-6-((E)-((4-((E)-1-(methoxyimino) ethyl)phenyl)imino)methyl)phenolato-κ²N,O}cobalt(II), C₄₀H₄₆CoN₄O₄

December 29, 2023

Ji-Xing Zhao, Da-Qun Chen, Lei-Fang Wu

Page range: 105-107

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C 40 H 46 CoN 4 O 4 , monoclinic, P 2 1 / n (no. 14), a = 12.0084(5) Å, b = 28.1263(10) Å, c = 12.0351(5) Å, β = 110.800(1) ° , V = 3800.0(3) Å 3 , Z = 4, R gt ( F ) = 0.0575, wR ref ( F 2 ) = 0.1150, T = 173(2) K.
Open Access
Crystal structure of tetraaqua-[(1-(carboxymethyl)-1H-pyrazole-3-carboxylato-κ²N,O)cobalt(II)], C₆H₁₂CoN₂O₈

December 4, 2023

Ling-Feng Zhang

Page range: 109-110

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C 6 H 12 CoN 2 O 8 , monoclinic, P 2 1 / c (no. 14), a = 12.573(5) Å, b = 7.212(3) Å, c = 11.652(5) Å, β = 98.045(6)°, V = 1046.1(7) Å 3 , Z = 4, R gt ( F ) = 0.0310, wR ref ( F 2 ) = 0.0674, T = 293 K.
Open Access
(6R,7S)-2,3,13-trimethoxy-6,7-dimethyl-5,6,7,8-tetrahydrobenzo[3′,4′]cycloocta [1′,2′:4,5]benzo[1,2-d][1,3]dioxol-1-ol, C₂₂H₂₆O₆

November 23, 2023

Chen-Yu Lu, Jiang-Hai Ye, Yu-Ling Luo, Ren-Song Chen, Chen-Liang Zhao, Jing-Jie Zhang

Page range: 111-113

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C 22 H 26 O 6 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 7.6648(5) Å, b = 11.2663(6) Å, c = 22.7321(7) Å, V = 1963.0(2) Å 3 , Z = 4, R gt ( F ) = 0.0652, wR ref ( F 2 ) = 0.1399, T = 273(2) K.
Open Access
Crystal structure of 2-((2,6-dichloro-4-(3,5-dimethylisoxazol-4-yl)phenyl)amino)benzoic acid, C₁₈H₁₄Cl₂N₂O₃

November 29, 2023

Xiaolin Dang, Kai Zhang, Xiaohua Li, Yanrong Gao, Wenqiang Tang

Page range: 115-116

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C 18 H 14 Cl 2 N 2 O 3 , monoclinic, C 2/ c (no. 15), a = 26.989(7) Å, b = 8.414(2) Å, c = 14.642(4) Å, β = 99.651(8)°, V = 3300.7(16) Å 3 , Z = 8, R gt ( F ) = 0.0636, w R ref ( F 2 ) = 0.1877, T = 205 K.
Open Access
Crystal structure of (5aS,6aS,8aR,9R,11aS, 11bS,13R,13aS)-1,1,8a,11a-tetramethyl-9-((S)-1-((S)-5-methyl-6-oxo-3,6-dihydro-2H-pyran-2-yl)ethyl)-3-oxo-1,7,8,8a,9,10,11,11a,11b,12,13,13a-dodecahydro-3H,6H-cyclopenta[5,6]cyclopropa[1,8a]naphtho[2,1-c]oxepin-13-yl acetate, C₃₂H₄₄O₆

December 1, 2023

Cheng-Hong Jian, Ren-Song Chen, Jie-Jing Zhang, Chen-Liang Zhao, Neng-Wu Zhao, Jiang-Hai Ye

Page range: 117-120

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C 32 H 44 O 6 , monoclinic, P 2 1 (no. 4), a = 12.2561 Å, b = 10.3674(4) Å, c = 23.3835(8) Å, β = 98.463°, V = 2938.85(19) Å 3 , Z = 2, R gt ( F ) = 0.0602, wR ref ( F 2 ) = 0.1537, T = 273(2) K.
Open Access
Crystal structure of catena-poly[triaqua-(μ₂-1-(4-carboxylatophenyl)-4-oxo-1,4-dihydropyridazine-3-carboxylato-O,O′:O″)cobalt(II)], C₁₂H₁₂N₂O₈Co

December 5, 2023

Wen-Jun Liu, Dai-Fang Wang, Xiao Cao, Qian-Wen Wang, Li-Gong Shen

Page range: 121-123

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C 12 H 12 N 2 O 8 Co, orthorhombic, Pbca (no. 61), a = 11.4542(10) Å, b = 9.2421(8) Å, c = 25.501(2) Å, V = 2699.6(4) Å 3 , Z = 2, R gt ( F ) = 0.0342, wR ref ( F 2 ) = 0.0888, T = 296 K.
Open Access
Crystal structure of 3-[(furan-2-ylmethyl)-amino]-2-(2,3,4,5-tetrafluoro-benzoyl)-acrylic acid ethyl ester, C₁₇H₁₃F₄NO₄

December 14, 2023

Zheng-Bao Qi, Man-Jing Zhu, Xu-Liang Nie, Guo-Ping Huang, Jian-Ping Huang

Page range: 125-127

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C 17 H 13 F 4 NO 4 , monoclinic, P 2 1 / n (no. 14), a = 5.470(4) Å, b = 26.141(17) Å, c = 11.689(8) Å, β = 90.01°, V = 1671.3(19) Å 3 , Z = 4, R gt ${R}_{\mathit{gt}}$ ( F ) = 0.0612, w R ref $w{R}_{\mathit{ref}}$ ( F 2 ) = 0.1650, T = 296(2) K.
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Crystal structure of methyl 4-(2-ethoxy-2-oxoethoxy)-3-methoxybenzoate, C₁₃H₁₆O₆

December 4, 2023

Liu Shu-Juan, Guo Chun-Mei, Wang Gui-Shu, Li Wen-Jing, Nie Xu-Liang

Page range: 129-130

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C 13 H 16 O 6 , monoclinic, P 2 1 / c (no. 14), a = 12.180(3) Å, b = 13.813(4) Å, c = 7.842(2) Å, β = 93.917(4) ° , V = 1316.2(6) Å 3 , Z = 4, R gt ( F ) = 0.0442, wR ref ( F 2 ) = 0.1375, T = 296(2) K.
Open Access
Crystal structure of 4-bromo-2-(4-chlorophenyl)-1-methyl-5-(trifluoromethyl)-1H-pyrrole-3-carbonitrile, C₁₃H₇BrClF₃N₂

December 8, 2023

Jia-Rui Qin, Wen-Hao Tang, Kai Li, Hai-Yu Pan

Page range: 131-132

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C 13 H 7 BrClF 3 N 2 , monoclinic, P 2 1 / c (no. 14), a = 9.4183(18) Å, b = 15.185(3) Å, c = 13.1826(18) Å, β = 133.905(8)°, V = 1358.4(4) Å 3 , Z = 4, R gt ( F ) = 0.0420, wR ref ( F 2 ) = 0.1015, T = 293 K.
Open Access
The crystal structure of triaqua-(8-carboxymethoxy-quinoline-2-carboxylate-κ³N,O,O)nickel(II) monohydrate, C₁₂H₁₅NO₉Ni

December 7, 2023

Tai Xi-Shi, Yan Xi-Hai, Wang Yuan-Fang, Wang Li-Hua

Page range: 133-135

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C 12 H 15 NO 9 Ni, triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 7.3184(3) Å, b = 8.1941(3) Å, c = 12.1015(5) Å, α = 85.603(3)°, β = 79.719(3)°, γ = 84.790(3)°, V = 709.74(5) Å 3 , Z = 2, R gt ( F ) = 0.0437, wR ref ( F 2 ) = 0.1243, T = 290.1(3) K.
Open Access
Crystal structure of dihydroxy(2,4,6-triisopro-pylphenyl)telluronium trifluoromethanesulfonate, C₁₆H₂₅F₃O₅STe

December 29, 2023

Yuga Shibuya, Aya Mihoya, Shinichi Koguchi, Makoto Oba

Page range: 137-139

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C 16 H 25 F 3 O 5 STe, monoclinic, P 2 1 / c (no. 14), a = 5.8214(2) Å, b = 16.0059(5) Å, c = 21.9311(7) Å, β = 94.760(3)°, V = 2036.42(12) Å 3 , Z = 4, R gt ( F ) = 0.0282, w R ref ( F 2 ) = 0.0598, T = 293 K.
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The crystal structure of 1-(carboxymethyl)-1H-imidazole 3-oxide

December 29, 2023

Zhongzhen Yang, Dongrun Tang, Haifang Wang

Page range: 141-142

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C 5 H 6 O 3 N 2 , monoclinic, P 2 1 / c (no. 14), a = 11.3451(10) Å, b = 4.9505(5) Å, c = 10.3200(8) Å, β = 99.220(3)°, V = 572.12(9) Å 3 , Z = 4, R gt ( F ) = 0.0429, wR ref ( F 2 ) = 0.1031, T = 170 K.
Open Access
The crystal structure of 1,3,5-tris(dibromomethyl)benzene, C₉H₆Br₆

December 29, 2023

Chao-Bo Yang, Jia-Lu Chen, Tian-Yu Zhang, Kai-Long Zhong

Page range: 143-145

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C 9 H 6 Br 6 , hexagonal, P 6 3 / m (no. 176), a = 8.8911(3) Å, c = 10.6847(5) Å, V = 731.48(6) Å 3 , Z = 2, R gt ( F ) = 0.0441, wR ref ( F 2 ) = 0.1094, T = 293 K.
Open Access
Crystal structure of (Z)-3-(4-methoxyphenyl)-4-(5-methyl-1-phenyl-1H-1,2,3-triazol-4-yl)-N-phenylthiazol-2(3H)-imine, C₂₅H₂₁N₅OS

December 29, 2023

Bakr F. Abdel-Wahab, Saud A. Alanazi, Emad Yousif, Benson M. Kariuki, Gamal A. El-Hiti

Page range: 147-149

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C 25 H 21 N 5 OS, monoclinic, P 2 1 / n (no. 14), a = 12.9303(5) Å, b = 9.1111(4) Å, c = 18.7111(8) Å, β = 97.879(4)°, V = 2183.53(16) Å 3 , Z = 4, R gt ( F ) = 0.0487, wR ref ( F 2 ) = 0.1327, T = 293(2) K.
Open Access
Crystal structure of (Z)-3-(3-(4-hydroxyphenyl)-2-(phenylimino)-2,3-dihydrothiazol-4-yl)-2H-chromen-2-one, C₂₄H₁₆N₂O₃S

December 29, 2023

Bakr F. Abdel-Wahab, Saud A. Alanazi, Emad Yousif, Benson M. Kariuki, Gamal A. El-Hiti

Page range: 151-153

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C 24 H 16 N 2 O 3 S, triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 6.7738(3) Å, b = 11.6072(6) Å, c = 13.6060(9) Å, α = 69.197(6)°, β = 87.025(5)°, γ = 76.990(4)°, V = 973.90(10) Å 3 , Z = 2, R gt ( F ) = 0.0482, wR ref ( F 2 ) = 1191, T = 293(2) K.

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