Zeitschrift für Kristallographie - New Crystal Structures

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Volume 239, Issue 4

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Zeitschrift für Kristallographie - New Crystal Structures

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Zeitschrift für Kristallographie - New Crystal Structures

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Frontmatter

July 4, 2024

Page range: i-vii

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New Crystal Structures
Open Access
The crystal structure of hexaquazinc(II) poly[hexakis(μ₂-4-methylbenzenesulfinato-κ²O:O′) dizinc(II)]

May 31, 2024

Tai Xi-Shi, Yan Xi-Hai, Wang Yuan-Fang, Wang Li-Hua

Page range: 589-590

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C 42 H 54 O 18 S 6 Zn 3 , trigonal, P 3 ‾ 1 m $P\overline{3}1m$ (no. 162), a = 9.2916(13) Å, c = 18.121(4) Å, V = 1354.9(5) Å 3 , Z = 0.99996, R gt ( F ) = 0.0490, w R ref ( F 2 ) = 0.1330, T = 293(2) K.
Open Access
The crystal structure of poly[((2-(4,5-dihydro-1H-pyrazol-4-yl)-1,3-dioxoisoindoline-5-carbonyl)oxy)(1-(dimethylamino)ethoxy)zinc[II]], C₁₆H₁₄ZnN₄O₅

May 24, 2024

Zong-Wen Mo, Jie-Wei Liu, Gang Liang, Guo-Zhu Liu

Page range: 591-592

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C 16 H 14 ZnN 4 O 5 , orthorhombic, Pbcn (no. 60), a = 19.0280(5) Å, b = 9.0707(2) Å, c = 20.0081(6) Å, V = 3453.34(16) Å 3 , Z = 8, R gt ( F ) = 0.0396, wR ref ( F 2 ) = 0.0953, T = 230(2) K.
Open Access
Crystal structure of bis[(triaqua-4-iodopyridine-2,6-dicarboxylato-κ ³ N,O,O ^″)cobalt(II)] trihydrate, C₁₄H₂₂N₂O₁₇I₂Co₂

May 24, 2024

Liye Wang, Xiaofan Zhang, Hongxu Dong

Page range: 593-595

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C 14 H 22 N 2 O 17 I 2 Co 2 , monoclinic, P 2 1 / c (no. 14), a = 7.13476(14) Å, b = 11.1853(2) Å, c = 32.5727(5) Å, β = 93.5815(16)°, Z = 4, V = 2594.38(8) Å 3 , R gt ( F ) = 0.0447, wR ref ( F 2 ) = 0.0865, T = 293.0 K.
Open Access
Crystal structure of bis(methanol-κO)-bis(nitrato-kO)-bis(1-((2-(2-chloro-4-(4-chlorophenoxy)phenyl)-4-methyl-1,3-dioxolan-2-yl)methyl)-1H-1,2,4-triazole-κN)cadmium(II), C₄₀H₄₂O₁₄N₈Cl₄Cd

May 1, 2024

Le-le Zhou, Yi-wen Rao, Ze-jing Fan, Hong-ya Li, Biao Yan

Page range: 597-599

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C 40 H 42 O 14 N 8 Cl 4 Cd, triclinic, P 1̄ (no. 2), a = 7.5892(16) Å, b = 7.6583(15) Å, c = 20.629(4) Å, α = 79.620(4)°, β = 84.594(3)°, γ = 79.427(4)°, V = 1157.0(4) Å 3 , Z = 1, R gt ( F ) = 0.0721, w R ref ( F 2 ) = 0.1967, T = 296(2) K.
Open Access
Crystal structure of poly[μ₂-dichlorido-(μ₂-1-[(2,4-dimethyl-1H-triazole-1-yl)methyl]-1H-benzotriazole-κ²N:N′)cadmium(II)], C₁₁H₁₂CdN₆Cl₂

May 24, 2024

Tan-Peng Zhou, Meng-Meng Cao, Jun-Ya Du, Jing Yang, Xia Wang

Page range: 601-603

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C 11 H 12 CdN 6 Cl 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 6.8644(8) Å, b = 10.4577(8) Å, c = 10.6304(12) Å, α = 112.218(9)°, β = 94.638(9)°, γ = 93.289(8)°, Z = 2, V = 700.93(13) Å 3 , R gt ( F ) = 0.0427, wR ref ( F 2 ) = 0.1137, T = 293(2) K.
Open Access
The crystal structure of (3aS, 4R, 7S, 7aR)-hexahydro-4, 7-methano-1H-isoindole-1, 3-(2H)-dione, C₉H₁₁NO₂

April 23, 2024

Xueli Cao, Xiao Guo

Page range: 605-606

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C 9 H 11 NO 2 , monoclinic, P 2 1 / c (no. 14), a = 11.293(4) Å, b = 6.998(3) Å, c = 10.932(4) Å, β = 104.175(7)°, V = 837.6(5) Å 3 , Z = 4, R gt ( F ) = 0.0578, wR ref ( F 2 ) = 0.1330, T = 296 K.
Open Access
The crystal structure of N-(acridin-9-yl)-4-chloro-N-(4-chloro-butanoyl) butanamide, C₂₁H₂₀Cl₂N₂O₂

April 22, 2024

Dan Zhou, Chen Yang Jing, Hong-ji Li, Xinyi Zhang, Pei Rong Zhao, Wen Li

Page range: 607-609

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C 21 H 20 Cl 2 N 2 O 2 , orthorhombic, P 2 1 (no. 4), a = 8.3667(14) Å, b = 15.444(3) Å, c = 15.105(2) Å, V = 1951.9(6) Å 3 , Z = 4, R gt ( F ) = 0.0481, wR ref ( F 2 ) = 0.1574, T = 292 K.
Open Access
Crystal structure of 3,3′-dimethoxy-4,4′-oxy-di-benzaldehyde, C₁₆H₁₄O₅

April 24, 2024

Shiyin Huang, Minlei Yin, Yuxin Lin, Heyi Yang, Jie Chen, Ting Qiu

Page range: 611-612

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C 16 H 14 O 5 , monoclinic, P 2 1 / c (no. 14), a = 11.1420(17) Å, b = 8.4700(12) Å, c = 15.429(2) Å, β = 104.624(4)°, V = 1408.9(4) Å 3 , Z = 4, R gt ( F ) = 0.0513, w R ref ( F 2 ) = 0.1243, T = 296(2) K.
Open Access
The crystal structure of tetrakis(μ ₂-2-amino-3,5-dibromobenzoate-κ ² O:O′)-octakis(n-butyl-κ ¹ C)-bis(μ ₃-oxo)tetratin(II), C₆₀H₉₂Br₈N₄O₁₀Sn₄

April 29, 2024

Kaoxue Li, Ailing Zhang, Shuhua Cao, Jianmin Wang

Page range: 613-615

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C 60 H 92 Br 8 N 4 O 10 Sn 4 , orthorhombic, Pccn (no. 56), a = 16.5363(14) Å, b = 20.3146(17) Å, c = 22.7452(19) Å, V = 7640.8(11) Å 3 , Z = 4, R gt ( F ) = 0.0424, wR ref ( F 2 ) = 0.1254, T = 298 K.
Open Access
Crystal structure of methyl-1-(naphthalen-1-yl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b] indole-3-carboxylate, C₂₃H₂₀N₂O₂

April 29, 2024

Xiaofeng Yang, Mo Du, Bin Liu, Wenqiang Tang, Hongjuan Tong

Page range: 617-618

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C 23 H 20 N 2 O 2 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 10.1373(13) Å, b = 10.137 Å, c = 18.093(2) Å, V = 1859.3(3) Å 3 , Z = 4, R gt ( F ) = 0.0507, wR ref ( F 2 ) = 0.1108, T = 150 K.
Open Access
Crystal structure of tetrapropylammonium bicarbonate–1-(diaminomethylene)thiourea(1/1)

April 22, 2024

Yunyun Wang, Yimin Hou, Huahui Zeng

Page range: 619-621

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C 60 H 140 N 20 O 12 S 4 , monoclinic, P 2/ n (no. 13), a = 15.6996 Å, b = 8.5361 Å, c = 15.8896 Å, β = 94.722°, V = 2122.19(10) Å 3 , Z = 4, R gt ( F ) = 0.0440, wR ref ( F 2 ) = 0.1366, T = 296(2) K.
Open Access
Crystal structure of 6,6′-((1E,1′E)-((2-phenylpyrimidine-4,6-diyl)bis(hydrazin-2-yl-1-ylidene))bis(methaneylylidene))bis(2-methoxyphenol)monohydrate, C₂₆H₂₆N₆O₅

May 1, 2024

Yating Hao, Pan Pan, Hairong Lan, Jiaxing Lu, Yan Wan, Yixin Chu

Page range: 623-625

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C 26 H 26 N 6 O 5 , monoclinic, P 2 1 / c (no. 14), a = 10.9393(1) Å, b = 16.8724(2) Å, c = 13.5836(2) Å, β = 102.843(1)°, V = 2444.43(5) Å 3 , Z = 4, R gt ( F ) = 0.0318, wR ref ( F 2 ) = 0.0827, T = 173 K.
Open Access
Crystal structure of bis(N,N,N-trimethylbutanaminium) tetrathiotungstate(VI), (BuMe₃N)₂[WS₄]

April 22, 2024

Kang-Woo Kim, Young-Hyun Yoo

Page range: 627-629

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C 14 H 36 N 2 S 4 W, monoclinic, C 2/ c (no. 15), a = 16.175(3) Å, b = 9.7755(15) Å, c = 15.452(3) Å, β = 115.183(7)°, V = 2211.0(7) Å 3 , Z = 4, R gt ( F ) = 0.0190, wR ref ( F 2 ) = 0.0490, T = 223 K.
Open Access
The crystal structure of 2,3,9-triphenyl-9-(2-phenylbenzofuran-3-yl)-9H-9λ ⁵-benzo[4,5][1,2]oxaphospholo[2,3-b][1,2,5]oxadiphosphole 2-oxide, C₄₀H₂₈O₄P₂

May 27, 2024

Longgen Sun, Zhichao Mei, Chao Chen, Haiyang Huang, Fangfang Kong, Jiang Bai

Page range: 631-633

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C 40 H 28 O 4 P 2 , monoclinic, P 2 1 / c (no. 4), a = 10.651(3) Å, b = 16.702(5) Å, c = 11.352(4) Å, β = 112.985(5)°, V = 1859.1(10) Å 3 , Z = 2, R gt ( F ) = 0.0807, wR ref ( F 2 ) = 0.2281, T = 296 K.
Open Access
Crystal structure of 1–methyl-3-propyl-4-nitro-1H-pyrazole-5-carboxylic acid, C₈H₁₁N₃O₄

May 7, 2024

Wen-Chao Fang, Xiao-Fei Liao, Yuan-Zhen Xiong, Ping Zhao, Jian-Ping Huang

Page range: 635-637

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[C 8 H 11 N 3 O 4 ], monoclinic, P 2 1 / c (no. 14), a = 4.5811(16) Å, b = 19.734(7) Å, c = 11.812(4) Å, β = 101.181(11)°, V = 1047.6(6) Å 3 , Z = 4, R gt ( F ) = 0.0742, wR ref ( F 2 ) = 0.1176, T = 296(2) K.
Open Access
Crystal structure of N-(benzo[d]thiazol-2-yl)-2-chloroacetamide, C₉H₇ClN₂OS

April 30, 2024

Yi-Ding Geng, Ming-Yu Huang, Yi-Xiu Zhang, Yi-Xia Gong, Ya-Lu Zhang

Page range: 639-640

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C 9 H 7 ClN 2 OS, monoclinic, P 2 1 / n (no. 14), a = 8.3507(3) Å, b = 12.3768(4) Å, c = 10.2340(4) Å, β = 96.857(4)°, V = 1050.17(7) Å 3 , Z = 4, R gt ( F ) = 0.0673, wR ref ( F 2 ) = 0.2013, T = 296(2) K.
Open Access
The crystal structure of N-benzyl-2-chloro-N-(p-tolyl) acetamide, C₁₆H₁₆ClNO

April 24, 2024

Yi-Ding Geng, De-Qi Kong, Ya-Lu Zhang, Yi-Xiu Zhang, Yi-Xia Gong

Page range: 641-643

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C 16 H 16 ClNO, monoclinic, P 2 1 / n (no. 14), a = 9.2566 Å, b = 9.2270(7) Å, c = 17.2231(14) Å, β = 103.745(8)°, V = 1428.9(2) Å 3 , Z = 4, R gt ( F ) = 0.0655, wR ref ( F 2 ) = 0.2113, T = 293 K.
Open Access
Crystal structure of 3,4-dimethoxybenzyl 2-(6-methoxynaphthalen-2-yl)propanoate, C₂₃H₂₄O₅

April 29, 2024

Dong-li Jiang, Yang Liu, Ying Cui, Rui Li

Page range: 645-647

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C 23 H 24 O 5 , monoclinic, C 2 (no. 4), a = 23.958(2) Å, b = 5.8145(5) Å, c = 17.839(3) Å, β = 129.974(3)°, V = 1904.3(4) Å 3 , Z = 4, R gt ( F ) = 0.0435, wR ref ( F 2 ) = 0.1140, T = 153(2) K.
Open Access
Crystal structure of 2,5-bis(2,5-dimethoxybenzyl)-3,6-dimethyl-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione, C₂₆H₂₈N₂O₆

April 23, 2024

Lin-Li Tang, Fei Zeng

Page range: 649-651

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C 26 H 28 N 2 O 6 , monoclinic, P 2 1 / c (no. 14), a = 15.962(9) Å, b = 14.828(8) Å, c = 9.929(5) Å, β = 93.303°, V = 2346(2) Å 3 , Z = 4, R gt ( F ) = 0.0515, w R ref ( F 2 ) = 0.1621, T = 296(2) K.
Open Access
Crystal structure of poly[(μ₃-5-bromoisophthalato-κ⁴ O,O′ :O″,O‴)-(μ₂-1,2-bis(1,2,4-triazole-1-ylmethyl)benzene-κ² N:N′)cobalt(II)], C₂₀H₁₅BrCoN₆O₄

May 7, 2024

Yao Xin-Tong, Cai Jin, Liu Yang, Chen Man-Sheng

Page range: 653-655

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C 20 H 15 BrCoN 6 O 4 , monoclinic, P 2 1 / n (no. 14), a = 8.7395(7) Å, b = 16.1423(11) Å, c = 14.9519(12) Å, β = 103.694(3)°, V = 2049.4(3) Å 3 , Z = 4, R gt ( F ) = 0.0514, wR ref ( F 2 ) = 0.1079, T = 193(2) K.
Open Access
The crystal structure of bis(2-(piperidin-1-ium-4-yl)-1Hbenzo[d]imidazol-3-ium) dihydrogen decavanadate, C₂₄H₃₆N₆O₂₈V₁₀

May 24, 2024

Qiu-Chen Mao, Xiao-Jie Gong, Si-Yu Zhou, Bao-Kuan Chen

Page range: 657-659

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C 24 H 36 N 6 O 28 V 10 , monoclinic, P 2 1 / c (no. 14), a = 10.4869(6) Å, b = 11.5123(7) Å, c = 17.4627(9) Å, β = 108.459(3)°, V = 1999.8(2) Å 3 , Z = 2, R gt ( F ) = 0.0209, wR ref ( F 2 ) = 0.0582, T = 296 K.
Open Access
Crystal structure of diaqua-bis(1-(3-carboxyphenyl)-5-methyl-4-oxo-1,4-dihydropyridazine3-carboxylato-O,O′)-cobalt(ii)dihydrate, C₂₆H₃₆N₄O₁₄Co

May 27, 2024

Hui-Bin Pan, Meng-Qi Tuo, Xia Gao, Jin Liu, Jiu-Fu Lu

Page range: 661-663

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C 26 H 36 N 4 O 14 Co, triclinic, P 1̄ (no. 2), a = 7.1895(7) Å, b = 8.7773(9) Å, c = 10.9067(11) Å, α = 98.180(2)°, β = 104.0480(10)°, γ = 90.180(2)°, V = 660.37(11) Å 3 , Z = 1, R gt ( F ) = 0.0287, wR ref ( F 2 ) = 0.0751, T = 296.15 K.
Open Access
Crystal structure of poly[(μ₂-5-bromoisophthalato-κ⁴ O,O ^′:O ^″,O ^‴)-(μ₂-1,4-bis(2-methylimidazol-1-ylmethyl)benzene-N:N^′)cadmium(II)], C₂₄H₂₁BrCdN₄O₄

June 19, 2024

Yao Xin-Tong, Chen Xiang-Yu, Liu Yang, Chen Man-Sheng

Page range: 665-667

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C 24 H 21 BrCdN 4 O 4 , orthorhombic, Pnna (no. 52), a = 7.4860(5) Å, b = 17.7424(13) Å, c = 17.2241(12) Å, V = 2,287.7(3) Å 3 , Z = 4, R gt ( F ) = 0.0363, w R ref ( F 2 ) = 0.0866, T = 296(2) K.
Open Access
The crystal structure of dimethyl 8-(3-methoxy-2-(methoxycarbonyl)-3-oxoprop-1-en-1-yl)-4-methyl-1-(p-tolyl)-1,3a,4,8b-tetrahydro-3H-furo[3,4-b]indole-3,3-dicarboxylate. C₂₈H₂₉NO₉

May 27, 2024

Du Yuchang, Li Guoxiang, Zeng Guimei, He Xiaobing, Zou Shengqin, Chen Zuliang

Page range: 669-671

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C 28 H 29 NO 9 , triclinic, P 1̄ (no. 2), a = 9.1736(7) Å, b = 12.4005(9) Å, c = 13.0593(9) Å, α = 67.098(7)°, β = 72.187(6)°, γ = 88.103(6)°, V = 1296.61(19) Å 3 , Z = 2, R gt ( F ) = 0.0444, wR ref ( F 2 ) = 0.1119, T = 200 K.
Open Access
Crystal structure of (3R)-1-(3,5-dimethoxyphenyl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole-3-carboxylate chloride, C₂₁H₂₃ClN₂O₄

April 24, 2024

Hongjuan Tong, Xiaona Xu, Zhoujing Zhu, Bin Liu

Page range: 673-675

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C 21 H 23 ClN 2 O 4 , monoclinic, P 2 1 (no. 4), a = 10.9270(4) Å, b = 8.0274(3) Å, c = 12.9691(6) Å, β = 114.914(1)°, V = 1031.73(7) Å 3 , Z = 2, R gt ( F ) = 0.0362 wR ref ( F 2 ) = 0.0898, T = 150 K.
Open Access
Synthesis and crystal structure of 3-(4,5-dihydroisoxazol-3-yl)-2-methyl-4-(methylsulfonyl)benzoic acid, C₁₂H₁₃NO₅S

May 31, 2024

Zeng Rong, Hu Ying, Zeng Xiao-Yan, Peng Da-Yong, Zhang Ji

Page range: 677-679

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C 12 H 13 NO 5 S, triclinic, P 1̄ (no. 2), a = 9.7095(6) Å, b = 11.9632(6) Å, c = 12.4335(5) Å, α = 86.456(4)°, β = 73.532(4)°, γ = 69.272(5)°, V = 1294.15(12) Å 3 , Z = 4, R gt ( F ) = 0.0445, wR ref ( F 2 ) = 0.1113, T = 296(2) K.
Open Access
The crystal structure of hexaaquamagnesium(II) bis-3-(1,2,3,4-tetrahydrobenzo[4,5]imidazo[1,2-α]pyridin-1-yl)benzoate, C₃₆H₄₂N₄O₁₀Mg

May 27, 2024

Zhao Zeng-Bing, Cheng Lan-Xing, Yang Shu-Cheng, Chai Yong-Li, Tai Xi-Shi

Page range: 681-683

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C 36 H 42 N 4 O 10 Mg, monoclinic, C 2/ c (no. 15), a = 16.4977(12) Å, b = 16.3866(10) Å, c = 12.5814(10) Å, β = 101.922(8)°, V = 3327.9(4) Å 3 , Z = 4, R gt ( F ) = 0.0794, wR ref ( F 2 ) = 0.2021, T = 260 K.
Open Access
Crystal structure of 4-formyl-2-methoxyphenyl 2-acetoxybenzoate, C₁₇H₁₄O₆

April 30, 2024

Li-Na Gao, Ying Cui, Xing Chai

Page range: 685-687

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C 17 H 14 O 6 , monoclinic, P 2 1 / n (no. 14), a = 13.9003(10) Å, b = 7.6509(6) Å, c = 14.4694(11) Å, β = 105.300(3)°, V = 1484.3(2) Å 3 , Z = 4, R gt ( F ) = 0.0357, w R ref ( F 2 ) = 0.0947, T = 100(2) K.
Open Access
Crystal structure of poly[octakis(μ-oxido)-tris(μ-1,1′-[[1,1′-biphenyl]-4,4′-diylbis(methylene)]bis(1H-imidazole))-tetrakis(oxido)-tetra-vanadium-dimanganese(II)dihydrate], C₃₀H₂₉MnN₆O₇V₂

May 9, 2024

Ling-Ling Dai, Xiao-Jie Wang, Yu-Cai Qin

Page range: 689-691

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C 30 H 29 MnN 6 O 7 V 2 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 9.0806(3) Å, b = 11.1937(3) Å, c = 16.3585(5) Å, α = 102.2430(10)°, β = 100.090(1)°, γ = 97.7410(10)°, V = 1574.09(8) Å 3 , Z = 2, R gt ( F ) = 0.0335, wR ref ( F 2 ) = 0.0886, T = 100 K.
Open Access
Crystal structure of 4,8a-bis(4-chlorophenyl)-1,5,6-tris(4-fluorobenzyl)-1,4,4a,4b,5,6,8a,8b-octahydrocyclobuta[1,2-b:3,4-c′]dipyridine-3,8-dicarbonitrile, C₄₅H₃₃Cl₂F₃N₄

May 31, 2024

Zhuo-Jun Li, Lu-Yao Xiao, Wei-Kang Shi, Kai-Yin Yang

Page range: 693-695

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C 45 H 33 Cl 2 F 3 N 4 , monoclinic, P 2 1 / c (no. 14), a = 11.7076(13) Å, b = 11.8186(13) Å, c = 27.473(3) Å, β = 91.188(2)°, V = 3800.6(7) Å 3 , Z = 4, R gt ( F ) = 0.0591, wR ref ( F 2 ) = 0.1856, T = 293 K.
Open Access
Crystal structure of benzo[d][1,3]dioxol-5-ylmethyl 2-(6-methoxynaphthalen-2-yl)propanoate, C₂₂H₂₀O₅

April 23, 2024

Yang Bai, Xin-Ru Zhang, Duo Hao, Ye Gu

Page range: 697-699

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C 22 H 20 O 5 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 5.8585(3) Å, b = 16.2727(10) Å, c = 18.4886(11) Å, V = 1762.59(18) Å 3 , Z = 4, R gt ( F ) = 0.0276, wR ref ( F 2 ) = 0.0700, T = 100(2) K.
Open Access
Crystal structure of N-benzoyl-N-phenylhydroxylaminato-dicarbonylrhodium(I), [Rh(BNA)CO₂]

May 27, 2024

Mokete Motente, Alice Brink, Johan A. Venter, Dumisani Kama

Page range: 701-703

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[Rh(BNA)(CO) 2 ], monoclinic, P 2 1 / c (no. 14), a = 12.095(3) Å, b = 17.199(4) Å, c = 6.778(15) Å, β = 90.519(7)°, V = 1398.5(6) Å 3 , Z = 4, R gt ( F ) = 0.0241, wR ref ( F 2 ) = 0.0616, T = 100 K.
Open Access
The crystal structure of N-(2-((2-methoxynaphthalen-1-yl)ethynyl)phenyl)-4-methylbenzenesulfonamide, C₂₆H₂₁NO₃S

May 27, 2024

Yi-Ning Li, Yi Liu, Shaoliang Zhang

Page range: 705-708

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C 26 H 21 NO 3 S, triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 11.7598(11) Å, b = 12.7434(12) Å, c = 17.0020(16) Å, α = 104.146(3)°, β = 103.926(3)°, γ = 102.322(3)°, V = 2295.5(4) Å 3 , Z = 4, R gt ( F ) = 0.0453, wR ref ( F 2 ) = 0.1320, T = 293 K.
Open Access
The crystal structure of methyl ((4-aminobenzyl)sulfonyl)-d-prolinate, C₁₃H₁₈N₂O₄S

May 31, 2024

Kuo Cheng, Qing-Guo Meng, Bao-Gang Wang, Yun Hou, Ya-Bin Song

Page range: 709-711

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C 13 H 18 N 2 O 4 S, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 6.8690(1) Å, b = 12.0694(2) Å, c = 16.6748(3) Å, V = 1382.42(4) Å 3 , Z = 4, R gt ( F ) = 0.0278, wR ref ( F 2 ) = 0.0729, T = 150 K.
Open Access
The crystal structure of dichlorido-(N-isopropyl-N-(pyridin-2-ylmethyl)propan-2-amine-κ ² N, N′)palladium(II), C₁₂H₂₀N₂PdCl₂

May 27, 2024

Deng-Zheng Lin, Zi-Yang Zhan, Jia-jun Liang, Zong-Wen Mo, Hai-Ping Wang

Page range: 713-714

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C 12 H 20 N 2 PdCl 2 , monoclinic, P 2 1 / c (no. 14), a = 16.2780(2) Å, b = 6.97160(10) Å, c = 13.07070(10) Å, β = 102.780(1)°, V = 1446.56(3) Å 3 , Z = 4, R gt ( F ) = 0.0261, wR ref ( F 2 ) = 0.0707, T = 291 K.
Open Access
Crystal structure of poly[(μ ₂-5-hydroxyisophthalato-κ⁴ O,O′:O″,O‴)-(μ ₂-1,4-bis(2-methylimidazolyl)-1-butene-N:N′)nickel(II)], C₂₀H₂₀NiN₄O₅

May 27, 2024

Yao Xin-Tong, Cai Jin, Chen Man-Sheng

Page range: 715-717

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C 20 H 20 NiN 4 O 5 , monoclinic, P 2 1 / n (no. 14), a = 8.8571(7) Å, b = 20.4827(14) Å, c = 10.9374(8) Å, β = 101.235(3)°, V = 1946.2(2) Å 3 , Z = 4, R gt ( F ) = 0.0697, wR ref ( F 2 ) = 0.1486, T = 193(2) K.
Open Access
The crystal structure of {hexakis(1-methyl-1H-imidazole-κ ¹ N)cobalt(II)}(μ ₂-oxido)-hexaoxido-dimolybdenum(VI)— 1-methyl-1H-imidazole (1/2), C₃₂H₄₈CoMo₂N₁₆O₇

May 27, 2024

Zou-Guang Han, Wei-Na Cai, Si-Yu Zhou, Bao-Kuan Chen

Page range: 719-721

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C 32 H 48 CoMo 2 N 16 O 7 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 10.425(2) Å, b = 10.517(2) Å, c = 11.187(2) Å, α = 94.671(7)°, β = 112.270(6)°, γ = 104.108(7)°, V = 1080.0(3) Å 3 , Z = 1, R gt ( F ) = 0.0407, wR ref ( F 2 ) = 0.1015, T = 273 K.
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Synthesis, crystal structure and nonlinear optical property of 1-((propan-2-ylideneamino)oxy)propan-2-yl-4-methylbenzenesulfonate, C₁₃H₁₉O₄NS

June 20, 2024

Guo-Ling Li, Ran Zhang

Page range: 723-725

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C 13 H 19 O 4 NS, monoclinic, Cc (no. 9), a = 11.4661(6) Å, b = 11.7180(7) Å, c = 12.1509(7) Å, β = 115.395(2)°, V = 1474.84(15) Å 3 , Z = 4, R gt ( F ) = 0.0253, wR ref ( F 2 ) = 0.0643, T = 200(2) K. The title compound crystallizes in a non-centrosymmetric space group.
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The crystal structure of N,N-(ethane-1,1-diyl)dibenzamide, C₁₆H₁₆N₂O₂

May 27, 2024

Zhen-Xiang Liu, Zheng-Ye Yu, Hui Mao, Tai-Jin Cheng, Hang-Cheng Ni

Page range: 727-729

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C 16 H 16 N 2 O 2 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 9.370(2) Å, b = 10.265(2) Å, c = 15.863(4) Å, V = 1525.8(6) Å 3 , Z = 4, R gt ( F ) = 0.0753, wR ref ( F 2 ) = 0.198, T = 273 K.
Open Access
Crystal structure of 1-(4-bromophenyl)-3-(diphenylphosphoryl)-3-hydroxypropan-1-one, C₂₁H₁₈BrO₃P

June 3, 2024

Yifan Liu, Ronghai Cui, Jialing Kang, Xin Jin, Qiang Huang, Jian Zhang

Page range: 731-733

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C 21 H 18 BrO 3 P, monoclinic, P 2 1 / c (no. 14), a = 20.2890(9) Å, b = 5.9736(2) Å, c = 16.1577(8) Å, β = 105.371(2)°, V = 1888.24(14) Å 3 , Z = 4, R gt ( F ) = 0.1359, w R ref ( F 2 ) = 0.1414, T = 298.00 K.
Open Access
The crystal structure of fac-tricarbonyl(bis(3,5-dimethyl-4H-pyrazole)-κ¹ N)-((nitrato)-κ¹ O)-rhenium(I)— 3,5-dimethyl-4H-pyrazole(1/1), C₁₈H₂₃N₇O₆Re

June 19, 2024

Lesetja V. Ramoba, Orbett T. Alexander, Frederick P. Malan, Amanda-Lee E. Manicum

Page range: 735-737

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C 18 H 23 N 7 O 6 Re, triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 10.527(2) Å, b = 10.849(2) Å, c = 11.215(2) Å, α = 72.798(2)°, β = 69.767(2)°, γ = 87.496(10)°, V = 1145.52(4) Å 3 , Z = 2, R gt ( F ) = 0.0273, w R ref ( F 2 ) = 0.0727, T = 150(2) K.
Open Access
The crystal structure of 4′-chloro-griseofulvin: (2S,6′R)-4′,7-dichloro-4,6-dimethoxy-6′-methyl-3H-spiro[benzofuran-2,1′-cyclohexan]-3′-ene-2′,3-dione, C₁₆H₁₄Cl₂O₅

May 31, 2024

Kai-Ming Yang, Meng Zhang, Yi-Xiang Li, Liang-Zhu Huang, Yu Zhao, Hua Yang, Yu-Bin Bai

Page range: 739-741

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C 16 H 14 Cl 2 O 5 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 8.6429 (4) Å, b = 11.3361 (6) Å, c = 33.9029 (11) Å, V = 3321.7 (3) Å 3 , Z = 8, R gt ( F ) = 0.0635, w R ref ( F 2 ) = 0.1630, T = 293(2) K.
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Crystal structure of tetraethylammonium bicarbonate–1-(diaminomethylene)thiourea(1/1)

June 5, 2024

Zheng Zhang, Peiyu Wang, Xin Zhu

Page range: 743-745

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C 44 H 108 N 20 O 12 S 4 , monoclinic, P 2 1 / n (no. 14), a = 8.0480(3) Å, b = 18.6415(7) Å, c = 11.9008(4) Å, β = 103.242(2)°, V = 1737.97(11) Å 3 , Z = 4, R gt ( F ) = 0.0471, wR ref ( F 2 ) = 0.1422, T = 296(2) K.
Open Access
Crystal structure of 1-cyclohexyl-4-p-tolyl-1,4-dihydropyridine-3,5-dicarboxylic acid dimethyl ester, C₂₂H₂₇NO₄

June 18, 2024

Yucong Liu, Zhihui Zhang, Ran Zhou, Yannan Ji, Yanlong Lan, Ruixia Guo, Haixia Wu, Jingyu He

Page range: 747-749

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C 22 H 27 NO 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 9.3356(8) Å, b = 10.2842(11) Å, c = 11.5902(12) Å, α = 103.266(4)°, β = 106.189(3)°, γ = 97.779(4)°, V = 1016.20(18) Å 3 , Z = 2, R gt ( F ) = 0.0413, w R ref ( F 2 ) = 0.0928, T = 293 K.
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The crystal structure of catena-poly(μ₂-1,4-bis-(1H-imidazol-1-yl)benzene-copper(I)) dichloridocopper(I), {[CuC₁₂H₁₀N₄]⁺[CuCl₂]⁻}_n

June 19, 2024

Airong Wang, Hangyi An, Xiaoli Wang, Zhongfeng Shi, Jiaming Li

Page range: 751-754

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[CuC 12 H 10 N 4 ]⋅[CuCl 2 ], triclinic, P 1̄ (no. 2), a = 4.2957(9) Å, b = 8.718(2) Å, c = 9.878(3) Å, α = 67.58(2)°, β = 78.97(2)°, γ = 80.043(19)°, V = 333.63(15) Å 3 , Z = 1, R gt ( F ) = 0.0360, wR ref ( F 2 ) = 0.0998, T = 296 K.
Open Access
The crystal structure of propane-1-aminium-2-carbamate, C₄H₁₀N₂O₂

June 21, 2024

Yujiu Wu, Yangling Ji, Xusen Gong, Shouwen Jin, Xinyi Hong

Page range: 755-757

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C 4 H 10 N 2 O 2 , monoclinic, Cc (no. 9), a = 9.5726(8) Å, b = 9.2271(9) Å, c = 7.4577(7) Å, β = 115.295(3)°, V = 595.56(9) Å 3 , Z = 4, R gt ( F ) = 0.0520, wR ref ( F 2 ) = 0.1436, T = 298 K .
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Crystal structure of 5,6,3′,4′,5′-pentamethoxy-flavone dihydrate, C₂₀H₂₄O₉

June 19, 2024

Abubakar Siddiq Salihu, Wan Mohd Nuzul Hakimi Wan Salleh, Amalina Mohd Tajuddin, Nurunajah Ab Ghani

Page range: 759-761

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C 20 H 24 O 9 , monoclinic, P 2 1 / c (no. 14), a = 9.7647(2) Å, b = 7.3098(10) Å, c = 27.7075(4) Å, β = 92.138(10)°, V = 1976.33(6) Å 3 , Z = 4, R gt ( F ) = 0.0479, wR ref ( F 2 ) = 0.1504, T = 300(2) K.
Open Access
Crystal structure of (E)-N-(2-bromophenyl)-4-(4-(3,5-dimethoxystyryl)phenoxy)pyrimidin-2-amine, C₂₆H₂₂BrN₃O₃

June 20, 2024

Wuji Sun, Lixin Sun, Hong Yan

Page range: 763-765

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C 26 H 22 BrN 3 O 3 , monoclinic, P 2 1 / c (no. 14), a = 17.7467(15) Å, b = 10.7974(8) Å, c = 11.9136(8) Å, β = 96.084°, V = 2270.0(3) Å 3 , Z = 4, R gt ( F ) = 0.0375, wR ref ( F 2 ) = 0.1205, T = 293 K.
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Crystal structure of methyl (3R)-1-(2-bromo-4-fluorophenyl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole-3-carboxylate hydrochloride hydrate, C₁₉H₁₉BrClFN₂O₃

June 5, 2024

Feijuan Wang, Yanjiao Wang, Xiaojuan Han, Wenqiang Tang

Page range: 767-769

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C 19 H 19 BrClFN 2 O 3 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 9.4940(6) Å, b = 10.8303(9) Å, c = 17.7300(14) Å, V = 1823.0(2) Å 3 , Z = 2, R gt ( F ) = 0.0615 wR ref ( F 2 ) = 0.1077, T = 150 K.
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The crystal structure of 1-(2-chlorophenyl)-3-(p-tolyl)urea, C₁₄H₁₃ClN₂O

June 5, 2024

Lei Han, Mo Du, Xiaohua Li, Wenqiang Tang

Page range: 771-772

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C 14 H 13 ClN 2 O, monoclinic, P 2 1 / c (no. 14), a = 23.904(2) Å, b = 4.6173(3) Å, c = 11.6906(13) Å, β = 96.895(9)°, V = 1281.0(2) Å 3 , Z = 4, R gt ( F ) = 0.0646, w R ref ( F 2 ) = 0.1314, T = 293 K.
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The crystal structure of 1-cyclohexyl-3-(p-tolyl)urea, C₁₄H₂₀N₂O

June 5, 2024

Jiayuan Dou, Wenqiang Tang, Yanrong Gao

Page range: 773-775

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C 14 H 20 N 2 O, monoclinic, P 2 1 / c (no. 14), a = 12.6793(11) Å, b = 9.0970(7) Å, c = 11.4964(10) Å, β = 98.008(8)°, V = 1,313.11(19) Å 3 , Z = 4, R gt ( F ) = 0.0585, w R ref ( F 2 ) = 0.1595, T = 293 K.
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Crystal structure of ((benzyl(hydroxy)-amino)(4-chlorophenyl)methyl)-diphenylphosphine oxide, C₂₆H₂₃ClNO₂P

June 18, 2024

Chongning Jiang, Pengfei Zhao

Page range: 777-778

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C 26 H 23 ClNO 2 P, triclinic, P 1̄ (no. 2), a = 9.6023(16) Å, b = 9.9881(17) Å, c = 13.406(2) Å, α = 77.627(2)°, β = 70.524(2)°, γ = 73.294(2)°, V = 1151.0(3) Å 3 , Z = 2, R gt ( F ) = 0.0439, wR ref ( F 2 ) = 0.1452, T = 296(2) K.
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The crystal structure of ethyl 3-(1-methyl-1H-indole-2-carbonyl)-2-phenylquinoline-4-carboxylate, C₂₈H₂₂N₂O₃

June 5, 2024

Mengdan Wang, Junling Wang, Yinhai Zhou, Jianyue Li, Zhenquan Han, Jinlong Wang, Jun-Ying Ma

Page range: 779-781

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C 28 H 22 N 2 O 3 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 9.7431(6) Å, b = 12.2795(6) Å, c = 12.6009(6) Å, α =71.454(2)°, β =68.694(2)°, γ =72.563(2)°, V = 1,302.36(12) Å 3 , Z = 2, R gt ( F ) = 0.0655, wR ref ( F 2 ) = 0.1988, T = 293(2) K.
Open Access
The crystal structure of 1,4-bis(1H-imidazol-3-ium-1-yl)benzene dinitrate, C₁₂H₁₂N₄ ²⁺·2(NO₃ ⁻)

June 5, 2024

Hangyi An, Xiaoli Wang, Airong Wang, Zhongfeng Shi, Jiaming Li

Page range: 783-786

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[H 2 (C 12 H 10 N 4 )] 2+ ·2(NO 3 ) − , monoclinic, P 2 1 / c (no. 14), a = 3.6937(3) Å, b = 15.5641(10) Å, c = 12.3322(8) Å, β = 93.201(7)°, V = 707.86(9) Å 3 , Z = 2, R gt ( F ) = 0.0377, wR ref ( F 2 ) = 0.1076, T = 298.15 K.
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Crystal structure of tris(hexafluoroacetylacetonato-κ²O,O′) bis(triphenylphosphine oxide-κ¹O)samarium(III), C₅₁H₃₃F₁₈O₈P₂Sm

June 18, 2024

Wanbin Li, Jinke Jiang, Xin Wang, Qiang Liu

Page range: 787-789

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C 51 H 33 F 18 O 8 P 2 Sm, monoclinic, P 2 1 / c (no. 14), a = 12.8193(9) Å, b = 13.4721(8) Å, c = 30.280(2) Å, β = 91.227(3)°, V = 5,228.2(6) Å 3 , Z = 4, R gt ( F ) = 0.0370, wR ref ( F 2 ) = 0.1025, T = 100.0 K.
Open Access
Crystal structure of 1-(4-(dimethylamino)phenyl)-2,3-bis(diphenylphosphoryl)propan-1-one, C₃₅H₃₃NO₃P₂

June 10, 2024

Qianlu Xing, Junhao Ao, Xin Jin, Qiang Huang

Page range: 791-793

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C 35 H 33 NO 3 P 2 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 5.9926(3) Å, b = 20.7065(10) Å, c = 23.5675(12) Å, V = 2924.4(3) Å 3 , Z = 4, T = 300 K, R gt ( F ) = 0.0440, wR ref ( F 2 ) = 0.1232.
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Crystal structure of diaqua[bis(μ ₂-pyridine 2,6-dicarboxylato) bismuth(III) potassium(I)], C₁₄H₁₀BiKN₂O₁₀

June 21, 2024

Lu Wei-Hong, Hong Zu-Chen, Li Jia-Hui, Huang Miao

Page range: 795-797

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C 14 H 10 BiKN 2 O 10 , triclinic, P 1̄ (no. 2), a = 7.029(8) Å, b = 10.460(9) Å, c = 11.891(9) Å, α = 71.19(2)°, β = 80.57(3)°, γ = 85.18(4)°, V = 815.9(13) Å 3 , R gt ( F ) = 0.0512, wR ref ( F 2 ) = 0.1410, Z = 2, T = 296(2) K.
Open Access
Crystal structure of (R)-N, N ^′-dimethyl-[1, 1′-binaphthalene]-2, 2′-diamine, C₂₂H₂₀N₂

June 19, 2024

Jinke Jiang, Xue Li, Guangyao Wang, Hui Jiang

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C 22 H 20 N 2 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 13.4475(3) Å, b = 14.6000(3) Å, c = 17.3708(4) Å, V = 3,410.47(13) Å 3 , Z = 8, R gt ( F ) = 0.0414, wR ref ( F 2 ) = 0.1026, T = 173(2) K.
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Crystal structure of 1-phenyl-4-(2-furoyl)-3-furyl-1H-pyrazol-5-ol, C₁₈H₁₂N₂O₄

June 19, 2024

Tong-Yin Jin, Xue-Mei Lin, Bi-He Zhu, Heng-Qiang Zhang, Chuang Ma

Page range: 803-805

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C 18 H 12 N 2 O 4 , monoclinic, P 2 1 / c (no. 14), a = 12.3075(7) Å, b = 6.5075(3) Å, c = 18.4929(9) Å, β = 92.883(4)°, V = 1,479.24(13) Å 3 , Z = 4, R gt ( F ) = 0.0394, wR ref ( F 2 ) = 0.1047, T = 173 K.
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Crystal structure of bis(14,34-dimethyl[11,21:23,31-terphenyl]-22-yl)diselane, C₄₀H₃₄Se₂

June 21, 2024

Ling-Yu Zhao, Shuang Lü, Guo-Dong Shen

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C 40 H 34 Se 2 , monoclinic, P 2 1 / c (no. 14), a = 13.377(3) Å, b = 14.843(3) Å, c = 16.003(4) Å, β = 93.922(4)°, V = 3170.0(12) Å 3 , Z = 4, R gt ( F ) = 0.0336, w R ref ( F 2 ) = 0.0717, T = 113(2) K.

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