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Zeitschrift für Kristallographie - New Crystal Structures

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Cover and Frontmatter

2. März 2018

Seiten: i-vii

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Open Access
Crystal structure and optical properties of diaqua-tris(nitrato-κ²O,O′)-bis(4,4,5,5-tetramethyl-2-(p-pyridyl)imidazoline-1-oxyl 3-oxide-κN)praseodymium(III), C₂₄H₃₆N₉O₁₅Pr

1. Februar 2018

Dongjiao Li, Zhiyuan Zhao, Xiuxiu Yao, Zhen Chen, Xiaoqiang Wu, Xiuwen Zheng

Seiten: 163-164

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C 24 H 36 N 9 O 15 Pr, monoclinic C 2/ c (no. 15), a = 23.686(9) Å, b = 11.727(5) Å, c = 12.001(5) Å, β = 94.852(4) V = 3322(2) Å 3 , Z = 4, R gt ( F ) = 0.0282, wR ref ( F 2 ) = 0.0769, T = 293 K.
Open Access
Crystal structure of dimethanol-bis(μ₂-methanol-κ²O:O)-bis{3-((4-methoxy-2-oxidobenzylidene)amino)-2-oxo-2H-chromen-4-olato-κ³O,N,O′}dimanganese(II), C₃₈H₃₈Mn₂N₂O₁₄

15. Januar 2018

Jing Li, Hao-Ran Jia, Yin-Xia Sun

Seiten: 165-167

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C 38 H 38 Mn 2 N 2 O 14 , triclinic, P 1̅ (no. 2), a = 8.2828(12) Å, b = 10.428(2) Å, c = 12.152(3) Å, α = 113.44(2)°, β = 93.369(16)°, γ = 107.890(16)°, Z = 1, V = 896.5(3) Å 3 , R gt ( F ) = 0.0578, wR ref ( F 2 ) = 0.1288, T = 293(2) K.
Open Access
Crystal structure of catena-poly[diaqua-bis(μ₂-2-(2-((2,6-dichlorophenyl)amino)phenyl)acetato-κ³O,O′:O′)calcium(II)], C₅₆H₄₈N₄Ca₂Cl₈O₁₂

7. Februar 2018

Ying Duan, Shi-Hui Li

Seiten: 169-171

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C 56 H 48 N 4 Ca 2 Cl 8 O 12 , monoclinic, P 2 1 / c , a = 16.776(8) Å, b = 24.193(12) Å, c = 7.657(4) Å, β = 101.110(7)°, V = 3050(3) Å 3 , Z = 2, R gt ( F ) = 0.0685, wR ref ( F 2 ) = 0.1663, T = 296(2) K.
Open Access
Crystal structure of catena-poly[triaqua-(isophthalato-κO)-(μ₂-1,6-di(1H-imidazol-1-yl)hexane-κ²N:N′)]nickel(II), C₂₀H₂₈N₄NiO₇

10. Februar 2018

Wei Song, Shi-Hui Li, Xue-Li Xu

Seiten: 173-175

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C 20 H 28 N 4 NiO 7 , monoclinic, P 2 1 / c (no. 14), a = 8.6404(5) Å, b = 21.0392(12) Å, c = 12.2580(6) Å, β = 96.839(5)°, V = 2212.5(2) Å 3 , Z = 4, R gt ( F ) = 0.0476, wR ref ( F 2 ) = 0.1092, T = 293(2) K.
Open Access
Crystal structure of cyclo[hexaqua-bis[1-[(2-ethyl-1H-imidazol-1-yl) methyl]-1H-benzotriazole-κ²N:N′]-bis(sulfato-κ¹O)dicadmium(II)] monohydrate, C₂₄H₄₂Cd₂N₁₀O₁₆S₂

29. Januar 2018

Xia Wang, Han-Bing Li, Di Cheng, Shu-Ling Zhang

Seiten: 177-178

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{[Cd 2 (C 12 H 13 N 5 ) 2 (H 2 O) 6 (SO 4 ) 2 ](H 2 O) 2 }, triclinic, P 1̅, a = 8.2977(5) Å, b = 10.2955(6) Å, c = 12.0979(9) Å, α = 103.879(6)°, β = 100.039(6)}°, γ = 104.567(5) V = 940.32(11) Å 3 , Z = 1, R gt ( F ) = 0.0282, wR ref ( F 2 ) = 0.0745, T = 291 K.
Open Access
Crystal Structure of bis(2-fluorbenzoato-κO)-bis(1,10-phenanthroline-κ²N,N′)manganese(II) dihydrate, C₃₈H₂₈F₂MnN₄O₆

7. Februar 2018

Zhu-Nian Jin, Bi-Song Zhang

Seiten: 179-181

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C 38 H 28 F 2 MnN 4 O 6 , monoclinic, P 2 1 / c (no. 14), a = 11.0710(3) Å, b = 25.4046(7) Å, c = 11.7681(3) Å, β = 93.496(1)°, V = 3303.67(15) Å 3 , Z = 4, R gt ( F ) = 0.0540, wR ref ( F 2 ) = 0.1504, T = 293 K.
Open Access
Crystal structure of tetrapropylammonium 5-hydroxyisophthalate tetrahydrate, C₂₀H₄₁NO₉

29. Januar 2018

Yalin Liu, Qiufang Li

Seiten: 183-184

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C 20 H 41 NO 9 , monoclinic, P 2 1 / n (no. 14), a = 16.475(7) Å, b = 8.582(4) Å, c = 17.579(8) Å, β = 103.371(5)°, V = 2418.1(18) Å 3 , Z = 4, R gt ( F ) = 0.0456, wR ref ( F 2 ) = 0.1378, T = 296(2) K.
Open Access
Crystal structural of 2-amino-4-(3-bromophenyl)-3-cyano-7,7-dimethyl-5-oxo-4H-5,6,7,8-tetrahydrobenzo[b]pyran, C₁₈H₁₇BrN₂O₂

12. Februar 2018

Jing Song

Seiten: 185-186

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C 18 H 17 BrN 2 O 2 , monoclinic, C 2/ c (no. 15), a = 23.554(2) Å, b = 9.3060(8) Å, c = 15.7691(15) Å, β = 93.372(9)°, V = 3450.5(5) Å 3 , Z = 8, R gt ( F ) = 0.0521, wR ref ( F 2 ) = 0.1686, T = 293 K.
Open Access
Crystal structural of 2-amino-4-(4-methoxyphenyl)-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile, C₁₇H₁₆N₂O₃

6. Februar 2018

Yi-Yan Su

Seiten: 187-188

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C 17 H 16 N 2 O 3 , monoclinic, P 2 1 / c (no. 14), a = 8.6539(4) Å, b = 16.7491(9) Å, c = 10.5511(5) Å, β = 104.304(5)°, V = 1481.92(13) Å 3 , Z = 4, R gt ( F ) = 0.043, wR ref ( F 2 ) = 0.121, T = 293 K.
Open Access
Crystal structure of catena-poly[aqua(μ₂-1,3-bis(1H-benzo[d]imidazol-1-yl)propane-κ²N:N′)-(μ₂-5-(tert-butyl)isophthalate-κ³O,O′:O′′)nickel(II)], C₂₉H₃₀N₄NiO₅

6. Februar 2018

Zhan Zhou, Zhe Zhou, Peng-Jing Jing

Seiten: 189-191

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C 29 H 30 N 4 NiO 5 , triclinic, P 1̅ (no. 2), a = 10.0887(15) Å, b = 11.2076(17) Å, c = 13.277(2) Å, α = 87.780(2)°, β = 72.138(2)°, γ = 67.129(2)°, V = 1311.0(3) Å 3 , Z = 2, R gt ( F ) = 0.0461, wR ref ( F 2 ) = 0.1048, T = 296.15 K.
Open Access
Crystal structure of catena-poly[(μ₂-dicyanamido-κ²N:N′)-(μ₂-2-(pyridin-2-yl)ethan-1-olato-κ³N,O:O′)copper(II)], C₉H₈CuN₄O

6. Februar 2018

Fang Xiangqing, Xu Jiajia, Wu Qi, Yang Liguo, Li Ya

Seiten: 193-194

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C 9 H 8 CuN 4 O, triclinic, P 1̅ (no. 2), a = 7.6740(6) Å, b = 8.6401(8) Å, c = 8.8869(9) Å, α = 109.201(2)°, β = 106.629(1)°, γ = 105.410(1)°, V = 489.21(8) Å 3 , Z = 2, R gt ( F ) = 0.0406, wR ref ( F 2 ) = 0.0993, T = 298(2) K.
Open Access
Crystal structure of bis(5,5′-((butane-1,4-diylbis(azanylylidene))bis(methanylylidene))bis(3-(ethoxycarbonyl)-2,4-dimethylpyrrol-1-ido-k⁴N,N′,N′′,N′′′)copper(II), C₂₄H₃₂CuN₄O₄

9. Februar 2018

Wan-Wan Wang, Wei-Na Wu, Yuan Wang

Seiten: 195-197

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C 24 H 32 CuN 4 O 4 , monoclinic, Cc , a = 11.8142(10) Å, b = 45.481(4) Å, c = 9.2540(8) Å, β = 97.886(2)°, V = 4925.4(8) Å 3 , Z = 8, R gt ( F ) = 0.0501, wR ref ( F 2 ) = 0.1188, T = 296(2) K.
Open Access
The crystal structure of the formamide solvate of (17b)-estra-1,3,5(10)-triene-3,17diol, C₁₉H₂₇NO₃

29. Januar 2018

Hui P. Wang, Juan Xu, Li F. Ning, Peng Li, Xiao F. Chen

Seiten: 199-201

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C 19 H 27 NO 3 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 8.1564(16) Å, b = 16.937(3) Å, c = 24.686(10) Å, V = 3410.3(12) Å 3 , Z = 8, R gt ( F ) = 0.0651, wR ref ( F 2 ) = 0.1345, T = 153(2) K.
Open Access
Crystal structure of catena-poly[diaqua-bis(μ₂-1H-benzo[d]imidazole-5-carboxylato-κ²N:O)nickel(II)] dihydrate, C₁₆H₁₈N₄NiO₈

6. Februar 2018

Wang Xin, Liu Qingyun, Yang Liguo, Liu Nana, Dai Yuqiang

Seiten: 203-204

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C 16 H 18 N 4 NiO 8 , monoclinic, C 2/ c (no. 15), a = 16.1598(8) Å, b = 8.7803(5) Å, c = 14.1809(11) Å, β = 118.197(1)°, V = 1773.32(19) Å 3 , Z = 4, R gt ( F ) = 0.0220, wR ref ( F 2 ) = 0.0598, T = 273(2) K.
Open Access
Crystal structure of dibromido[(1,2-bis(diisopropylphosphino)-1,2-dicarba-closo-dodecaborane-κ²P,P′]nickel(II), C₁₄H₃₈B₁₀NiBr₂P₂

15. Januar 2018

Yang Liguo, Liu Qingyun, Wang Xin, Gao Qianqian, Dai Yuqiang

Seiten: 205-207

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C 14 H 38 B 10 NiBr 2 P 2 , monoclinic, P 2 1 / c (no. 14), a = 10.1920(14) Å, b = 19.055(2) Å, c = 13.5243(17) Å, β = 103.394(2)°, V = 2555.1(6) Å 3 , Z = 4, R gt ( F ) = 0.0461, wR ref ( F 2 ) = 0.0869, T = 298 K.
Open Access
The crystal structure of catena-poly[aquachlorido(3,3′-([4,4′-bipyridine]-1,1′-diium-1,1′-diylbis(methylene))dibenzoato-κ²O:O′)copper(II)] chloride dihydrate, C₂₆H₂₆Cl₂CuN₂O₇

9. Februar 2018

Xiaoli Gao, Kai Zhu, Wenmin Wang, Liping Lu

Seiten: 209-211

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{[Cu(C 26 H 20 N 2 O 4 )Cl(H 2 O)] + ⋅ Cl − ⋅ 2H 2 O} n , monoclinic, Cc (no. 9), a = 17.225(4), b = 14.918(3), c = 11.589(3) Å, β = 118.957(3)°, V = 2605.6(10) Å 3 , Z = 4, R gt ( F ) = 0.0334, ω R ref ( F 2 ) = 0.0819, T = 293 K.
Open Access
The crystal structure of N′-(2-nitrobenzylidene)-2-phenylacetohydrazide, C₁₅H₁₃N₃O₃

4. Januar 2018

Wang Li-Hua, Liu Qing-Yun, Tai Xi-Shi

Seiten: 213-214

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C 15 H 13 N 3 O 3 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 8.6321(17) Å, b = 12.120(2) Å, c = 13.540(3) Å, V = 1416.6(5) Å 3 , Z = 4, R gt ( F ) = 0.0453, wR ref ( F 2 ) = 0.1141, T = 293(2) K.
Open Access
Crystal structure of dichlorido bis[1-[(2-methyl-1H-benzoimidazol-1-yl)methyl]-1H-benzotriazole-κ¹N]cadmium(II), C₃₀H₂₆CdCl₂N₁₀

9. Februar 2018

Xia Wang, Ning Ling, Yu-Xian Li, Shu-Ling Zhang

Seiten: 215-216

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[Cd(C 15 H 13 N 5 ) 2 Cl 2 ], monoclinic, C 2/ c (no. 15), a = 15.6291(6) Å, b = 12.8859(4) Å, c = 14.7622(5) Å, β = 97.781(3)°, V = 2945.65(18) Å 3 , Z = 4, R gt ( F ) = 0.0381, ω R ref (F 2 ) = 0.0738, T = 293(2) K.
Open Access
Crystal structure of aqua-bis(3-(2-pyridyl)-5-(4-pyridyl)-1H-1,2,4-triazole-κ²N,N′)copper(II) sulfate tetrahydrate, C₂₄H₂₈CuN₁₀O₉S

9. Februar 2018

Ai-Yun Fu

Seiten: 217-219

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C 24 H 28 CuN 10 O 9 S, monoclinic, P 2 1 / c (no. 14), a = 16.3499(16) Å, b = 14.0411(13) Å, c = 12.7069(13) Å, β = 104.019(2)°, V = 2830.2(5) Å 3 , Z = 4, R gt ( F ) = 0.0472, wR ref ( F 2 ) = 0.1165, T = 293(2) K.
Open Access
Crystal structure of dibromido-carbonyl-(η⁶-p-cymene)osmium(II), C₁₁H₁₄Br₂OOs

6. Februar 2018

Hadley S. Clayton

Seiten: 221-222

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C 11 H 14 Br 2 OOs, monoclinic, P 2 1 / c (no. 14), a = 10.3844(5) Å, b = 6.7833(3) Å, c = 19.0379(9) Å, β = 102.143(2)°, V = 1311.03(11) Å 3 , Z = 4, R gt ( F ) = 0.0258, wR ref ( F 2 ) = 0.0582, T = 173(2) K.
Open Access
Crystal structure of catena-poly[chlorido-(μ₂-chlorido)-bis(imidazole-κN)copper(II)] C₆H₈Cl₂CuN₄

15. Januar 2018

Hong Zhang

Seiten: 223-224

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C 6 H 8 Cl 2 CuN 4 , orthorhombic, Cmc 2 1 (no. 26), a = 12.915(3) Å, b = 10.784(3) Å, c = 6.8037(18) Å, V = 947.6(4) Å 3 , Z = 4, R gt ( F ) = 0.0368, wR ref ( F 2 ) = 0.0905, T = 293(2) K, Flack parameter: 0.05(4).
Open Access
Crystal structure of [(1,2-bis(dicyclohexylphosphino)-1,2-dicarba-closo-dodecaborane-κ²P,P′]dibromidonickel(II)), C₂₆H₅₄B₁₀NiBr₂P₂

12. Februar 2018

Yang Liguo, Liu Qingyun, Wang Xin, Liu Nana, Dai Yuqiang

Seiten: 225-227

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C 26 H 54 B 10 NiBr 2 P 2 , monoclinic, C 2/ c (no. 15), a = 13.064(7) Å, b = 15.655(8) Å, c = 16.652(9) Å, β = 95.830(7)°, V = 3388(3) Å 3 , Z = 4, R gt ( F ) = 0.0603, wR ref ( F 2 ) = 0.1364, T = 298(2) K.
Open Access
Crystal structure of dichlorido[1,1′-bis(diphenylphosphanyl)ferrocene-κ²P,P′]zinc(II), C₃₄H₂₈FeCl₂P₂Zn

9. Februar 2018

Yang Liguo, Wang Xin, Liu Qingyun, Liu Nana, Dai Yuqiang

Seiten: 229-231

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C 34 H 28 FeCl 2 P 2 Zn, triclinic, P 1̅ (no. 2), a = 9.6794(11) Å, b = 9.7989(10) Å, c = 18.2141(19) Å, α = 95.8740(10)°, β = 99.9350(10)°, γ = 115.596(2)°, V = 1503.9(3) Å 3 , Z = 2, R gt ( F ) = 0.0362, wR ref ( F 2 ) = 0.0964, T = 298 K.
Open Access
Crystal structure of tris(μ₂-2-(pyridin-2-yl)ethan-1-olato-κ³N,O:O)-trithiocyanato-κN-dicobalt(III), C₂₄H₂₄Co₂N₆O₃S₃

9. Februar 2018

Wang Yanfei, Liu Nana, Liu Qingyun, Yang Liguo, Wei Aimin

Seiten: 233-234

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C 24 H 24 Co 2 N 6 O 3 S 3 , triclinic, P 1̅ (no. 2), a = 10.5658(9) Å, b = 11.1693(11) Å, c = 11.7054(14) Å, α = 79.200(1)°, β = 84.714(1)°, γ = 89.519(2)°, V = 1351.1(2) Å 3 , Z = 2, R gt ( F ) = 0.0482, wR ref ( F 2 ) = 0.1213, T = 298 K.
Open Access
The crystal structure of diaqua-2,2′-((cyclohexane-1,2-diylbis(azanylylidene))bis(methanylylidene))diphenolato-κ⁴N,N′,O,O′)manganese(III) perchlorate, C₂₀H₂₄MnClN₂O₄

13. Februar 2018

Hongping Ju, Zihao Chen, Jing Qin, Yu Lang, Yunhui Ren, Ping Li, Nan Li, Kaihua Zhou

Seiten: 235-237

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C 20 H 24 MnClN 2 O 4 , triclinic, P 1̅ (no. 2), a = 7.9912(8) Å, b = 11.8174(9) Å, c = 12.7781(15) Å, α = 112.855(9)°, β = 97.649(9)°, γ = 91.215(7)°, V = 1098.6(2) Å 3 , Z = 2; R gt ( F ) = 0.0491, wR ref ( F 2 ) = 0.1319, T = 250(2) K.
Open Access
Crystal structure of bis(μ₃-chlorido)-bis(μ₂-chlorido)-tetrakis(μ₂-2,6-bis (diphenylmethyl)-4-t-butylphenolato)tetralithium(I)dicobalt(II) toluene solvate, C_75.5H₇₀Cl₂CoLi₂O₂

7. Februar 2018

Donglei Bu, Xiaodan Chen, Miao Meng, Feifeng Zhu, Hao Lei

Seiten: 239-241

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C 75.5 H 70 Cl 2 CoLi 2 O 2 , triclinic, P 1̅ (no. 2), a = 13.1085(7) Å, b = 13.4704(7) Å, c = 18.8367(10) Å, α = 88.604(5)°, β = 88.255(4)°, γ = 68.282(5)°, V = 3088.3(3) Å 3 , Z = 1, R gt ( F ) = 0.0666, wR ref ( F 2 ) = 0.1743, T = 150 K.
Open Access
The crystal structure of hexaaqua-bis(μ₂-3-(3-(pyridin-4-yl)-1,2,4-oxadiazol-5-yl)propanoato-κ²O:O′)-tetrakis(3-(3-(pyridin-4-yl)-1,2,4-oxadiazol-5-yl)propanoato-κO)dierbium(III) octahydrate, C₆₀H₇₆N₁₈O₃₂Er₂

9. Februar 2018

Fang Zhang, Fang Huang, Xiaodong Huang, Yanhua Lu, Qifan Chen, Fei Liu

Seiten: 243-245

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C 60 H 76 N 18 O 32 Er 2 , monoclinic, P 2 1 / n (no. 14), a = 10.5441(4) Å, b = 31.1092(9) Å, c = 12.0993(4) Å, β = 114.398(4)°, V = 3614.4(2) Å 3 , Z = 2, R gt ( F ) = 0.0431, wR ref ( F 2 ) = 0.0805, T = 296(2) K.
Open Access
Crystal structure of dimethylammonium bis(naphthalene-2,3-diolato)borate, C₂₂H₂₀BNO₄

16. Februar 2018

Mustafa Tombul, Kutalmış Güven, Adnan Bulut, Ingrid Svoboda, Hartmut Fuess

Seiten: 247-249

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C 22 H 20 BNO 4 , monoclinic, C 2/ c (no. 15), a = 32.303(4) Å, b = 8.2703(6) Å, c = 7.3876(6) Å, β = 92.889(8)°, V = 1971.1(3) Å 3 , Z = 4, R gt ( F ) = 0.0978, wR ref ( F 2 ) = 0.2063, T = 298 K.
Open Access
Crystal structure of 2-amino-4-(4-nitro-phenyl)-7,7-dimethyl-5-oxo-5,6,7,8-tetrahydro-4H-chromene-3-carbonitrile, C₁₈H₁₇N₃O₄

29. Januar 2018

Jing Song

Seiten: 251-252

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C 18 H 17 N 3 O 4 , monoclinic, P 2 1 / n (no. 14), a = 9.5820(6) Å, b = 16.5417(11) Å, c = 10.6951(7) Å, β = 111.060(8)°, V = 1581.97(18) Å 3 , Z = 4, R gt ( F ) = 0.0437, wR ref ( F 2 ) = 0.1307, T = 293 K.
Open Access
The crystal structure of (E)-4-chloro-2-(((5-methylpyridin-2-yl)imino)methyl)phenol, C₁₃H₁₁ClN₂O

10. Januar 2018

Xiaohua Pu

Seiten: 253-254

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C 13 H 11 ClN 2 O, monoclinic, P 2 1 / n (no. 14), a = 13.997(5) Å, b = 4.6734(15) Å, c = 18.019(7) Å, β = 102.714(5)°, V = 1149.7(7) Å 3 , Z = 4, R gt ( F ) = 0.0481, wR ref ( F 2 ) = 0.1141, T = 153(2) K.
Open Access
Crystal structure of bis(N,N,N-trimethylbutanaminium) poly[heptaselenidotristannate(IV)], C₁₄H₃₆N₂Se₇Sn₃

29. Januar 2018

Kang-Woo Kim, Man-Young Heo

Seiten: 255-257

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C 14 H 36 N 2 Se 7 Sn 3 , monoclinic, C 2/ c (no. 15), a = 23.950(4) Å, b = 13.760(2) Å, c = 20.011(3) Å, β = 114.565(7)°, V = 5997.9(17) Å 3 , Z = 8, R gt ( F ) = 0.0546, wR ref ( F 2 ) = 0.1393, T = 223 K.
Open Access
The crystal structure of N-((3,5-di-tert-butyl-4-hydroxyphenyl)(phenyl)methyl)-4-methylbenzenesulfonamide, C₂₈H₃₅N₃S

10. Januar 2018

Xiao-Yu Guan, Sheng-Shu Liu, Liang-Dong Zhang, Xin Guo, Xuebing Ma, Zhang-Qin Liu

Seiten: 259-261

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C 28 H 35 NO 3 S, triclinic, P 1̄ (no. 2), a = 10.3965(4) Å, b = 10.7525(5) Å, c = 12.2772(6) Å, α = 86.651(4)°, β = 86.653(4)°, γ = 75.323(4)°, V = 1324.05(11) Å 3 , Z = 2, R gt ( F ) = 0.0472, wR ref ( F 2 ) = 0.1298, T = 291 K.
Open Access
Crystal structure of 2-(4-chlorophenyl)-2,3-dihydro-1H-perimidine, C₁₇H₁₃Cl₁N₂

10. Januar 2018

Zhong-Yan Li, Min Zhang, Xian-You Yuan, Lin Yuan

Seiten: 263-264

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C 17 H 13 Cl 1 N 2 , monoclinic, P 2 1 / c (no. 14), a = 7.830(2) Å, b = 26.688(8) Å, c = 7.362(2) Å, β = 115.366(3)°, V = 1390.1(7) Å 3 , Z = 4, R gt ( F ) = 0.0604, wR ref ( F 2 ) = 0.1761, T = 296(2) K.
Open Access
The Crystal structure of 2-iodo-1-(p-tolyl)propan-1-one, C₁₀H₁₁IO

15. Januar 2018

Hui Liu, Linglan Li, Shu Zhang, Junfeng Miao

Seiten: 265-266

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C 10 H 11 IO, monoclinic, P 2 1 / c (no. 14), a = 6.5799(5) Å, b = 10.1508(9) Å, c = 15.0983(12) Å, β = 92.313(7)°, V = 1007.61(14) Å 3 , Z = 4, R gt ( F ) = 0.0343, wR ref ( F 2 ) = 0.0860, T = 297 K.
Open Access
Crystal structure of ethyl 1-(4-bromobenzyl)-3-phenyl-1H-pyrazole-5-carboxylate, C₁₉H₁₇BrN₂O₂

7. Februar 2018

Zhen-Zhen Wang, Jin-Zong You, Yi-Ping Zhang, Sheng-Yue Tong, Ke-Ji Yu, Qiong Hu, Yan-Qi Guo, Dan Liu, De-Qiang Qi

Seiten: 267-268

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C 19 H 17 BrN 2 O 2 , triclinic, P 1̅ (no. 2), a = 8.3979(11) Å, b = 10.4083(14) Å, c = 11.1696(15) Å, α = 69.270(2)°, β = 89.401(2)°, γ = 73.709(2)°, V = 872.1(2) Å 3 , Z = 2, R gt ( F ) = 0.0422, wR ref ( F 2 ) = 0.1138, T = 296.15 K.
Open Access
Crystal structure of ethyl 1-(4-fluorobenzyl)-3-phenyl-1H-pyrazole-5-carboxylate, C₁₉H₁₇FN₂O₂

7. Februar 2018

Sheng-Yue Tong, Jin-Zong You, Yi-Ping Zhang, Zhen-Zhen Wang, Ke-Ji Yu, Qiong Hu, Hui-Juan Pan, Cheng-Jie Wu, De-Qiang Qi

Seiten: 269-270

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C 19 H 17 FN 2 O 2 , triclinic, P 1̅ (no. 2), a = 7.8593(19) Å, b = 10.3322(18) Å, c = 10.9747(19) Å, α = 108.914(18)°, β = 92.931(3)°, γ = 99.544(3)°, V = 826.1(3) Å 3 , Z = 2, R gt ( F ) = 0.0431, wR ref ( F 2 ) = 0.1170, T = 296.15 K.
Open Access
Crystal structure of catena-poly[diaqua-(μ₂-2,5-dihydroxyterephthalato-κ⁴O,O′:O′′,O′′′)cadmium(II)], C₈H₈O₈Cd

1. Februar 2018

Li-ping Xue

Seiten: 271-272

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C 8 H 8 O 8 Cd, monoclinic, C 2/ c (no. 15), a = 16.5170(11) Å, b = 5.4639(3) Å, c = 11.5875(9) Å, β = 108.992(8)°, V = 988.81(12) Å 3 , Z = 4, R gt ( F ) = 0.0196, w R ref ( F 2 ) = 0.0510, T = 286.74(11) K.
Open Access
Crystal structure of tetraaqua-bis[6-(1H-imidazol-1-yl-κN)nicotinato]zinc(II), C₁₈H₂₀N₆O₈Zn

16. Februar 2018

Zhao-Hao Li

Seiten: 273-274

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C 18 H 20 N 6 O 8 Zn, triclinic, P 1̅, a = 6.2576(6) Å, b = 6.9645(8) Å, c = 12.1262(15) Å, α = 78.536(10)°, β = 86.677(9)°, γ = 72.340(9)°, Z = 1, V = 493.52(10) Å 3 , R gt ( F ) = 0.0603, w R ref (F 2 ) = 0.1290, T = 291(2) K.
Open Access
Crystal structure of dichlorido-bis(N-phenyl-2-(quinolin-8-yloxy)acetamide-κ²N,O) – acetone (2/1), C_35.5H₃₁N₄O_4.5Cl₂Cu

9. Februar 2018

Liang Chen, Wei-Na Wu

Seiten: 275-277

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C 35.5 H 31 N 4 O 4.5 Cl 2 Cu, monoclinic, P 2 1 / c (no. 14), a = 14.8239(3) Å, b = 16.2169(2) Å, c = 15.6515(3) Å, β = 109.889(1)°, V = 3538.16(11) Å 3 , Z = 4, R gt ( F ) = 0.0499, wR ref ( F 2 ) = 0.1577, T = 296(2) K.
Open Access
Crystal Structure of ethyl (E)-3,4-dimethyl-5-((2-(4-methylbenzoyl)hydrazono)methyl)-1H-pyrrole-2-carboxylate — water — ethanol (1/1/1), C₂₀H₂₉N₃O₅

4. Januar 2018

Hao Wu, Qiang Hu, Yuan Wang

Seiten: 279-280

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C 20 H 29 N 3 O 5 , triclinic, P 1̅ (no. 2), a = 9.1571(18) Å, b = 10.505(2) Å, c = 11.576(2) Å, α = 94.509(4)°, β = 92.570(4)°, γ = 102.312(3)°, V = 1082.4(4)) Å 3 , Z = 2, R gt ( F ) = 0.0543, wR ref ( F 2 ) = 0.1704, T = 296(2) K.
Open Access
Crystal structure of 5-((4-(1H-benzo[d]imidazol-2-yl)-2-methoxyphenoxy)methyl)-2-chlorothiazole - trichloromethane - methanol (1/1/1), C₂₀H₁₉Cl₄N₃O₃S

9. Februar 2018

An-Jia Wang, Yun-Hui Zhang, Zhi Zhang, Ai-Zhen Weng, Liu-Yang Wang, Dong-Mei She, Jun Ning, Wei-Jie Si, Xiang-Dong Mei

Seiten: 281-282

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C 20 H 19 Cl 4 N 3 O 3 S, monoclinic, P 2 1 / c (no. 14), a = 14.2134(9) Å, b = 21.4083(13) Å, c = 7.6709(5) Å, β = 99.260(6)°, V = 2303.7(2) Å 3 , Z = 4, R gt ( F ) = 0.0659, wR ref ( F 2 ) = 0.1682, T = 180 K.
Open Access
The crystal structure of a matrine derivative: 4¹S,7aS,12S,13aR,13bR)-12-(4-methylpiperazin-1-yl)dodecahydro-1H,5H,10H-dipyrido[2,1-f:3′,2′,1′-ij][1,6]naphthyridin-10-one, C₂₀H₃₄N₄O

9. Februar 2018

Xing-An Cheng, Liu Zhan-Mei, Wu Bo, Huang Su-Qing, Xiong Xia-Ling, Jiang Xu-Hong

Seiten: 283-285

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C 20 H 34 N 4 O, triclinic, P 1 (no. 1), a = 7.8545(6) Å, b = 10.8802(9) Å, c = 12.3714(9) Å, α = 73.200(7)°, β = 75.372(6)°, γ = 71.091(7)°, V = 942.65(13) Å 3 , Z = 2, R gt ( F ) = 0.0591, wR ref ( F 2 ) = 0.1641, T = 293(2) K.
Open Access
Crystal structure of cesium beryllophosphate, Be₃Cs₂P₄O₁₄

14. Februar 2018

Wang Fang, Chen Yigang

Seiten: 287-288

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Be 3 Cs 2 P 4 O 14 , orthorhombic, Pnma (no. 62), a = 15.0612(3) Å, b = 11.0386(2) Å, c = 15.5316(3) Å, V = 2582.19(8) Å 3 , Z = 8, R gt ( F ) = 0.0229, wR ref ( F 2 ) = 0.0594, T = 293(2) K.
Open Access
Crystal Structure of 3-((3-hydroxybenzyl)ammonio)-3-phenylpropanoate, C₁₆H₁₇NO₃

1. Februar 2018

Wan-Wan Wang, Xing-Ying Chen, Wei-Na Wu

Seiten: 289-290

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C 16 H 17 NO 3 , orthorhombic, Pna 2 1 (no. 33), a = 10.3470(3) Å, b = 7.9347(2) Å, c = 17.0947(4) Å, V = 403.48(6) Å 3 , Z = 4, R gt ( F ) = 0.0427, wR ref ( F 2 ) = 0.1044, T = 296(2) K.
Open Access
Crystal structure of 9,10-dimethoxy-5,6-dihydro-[1,3]dioxolo[4,5-g]isoquinolino[3,2-a]isoquinolin-7-ium chloride — 4-hydroxy-3-methoxybenzoic acid — water (2/1/5), C₄₈H₅₄N₂Cl₂O₁₇

6. Februar 2018

Mei Zhang, Benyong Lou, Xiaodong Huang, Yali Huang

Seiten: 291-293

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C 48 H 54 N 2 Cl 2 O 17 , orthorhombic, Pnma (no. 62), a = 28.3651(8) Å, b = 22.8464(6) Å, c = 7.1341(2) Å, V = 4623.2(2) Å 3 , Z = 4, R gt ( F ) = 0.0437, wR ref ( F 2 ) = 0.1225, T = 100(2) K.
Open Access
The crystal structure of (1R, 2R)-N¹,N²-diferrocenyl-1,2-cyclohexanedicarboxamide, C₂₈H₃₀Fe₂N₂O₂

18. Januar 2018

Martin Zábranský, Zdeněk Leitner, Petr Štěpnička

Seiten: 295-298

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C 28 H 30 Fe 2 N 2 O 2 , monoclinic, P 2 1 (no. 4), a = 10.7490(10) Å, b = 9.8370(8) Å, c = 11.9621(13) Å, β = 113.030(4)°, V = 1164.04(19) Å 3 , Z = 2, R gt ( F ) = 0.0358, wR ref ( F 2 ) = 0.0612, Flack parameter = −0.007(11), T = 150(2) K.
Open Access
Crystal structure of N-(2-methylphenyl)ethoxycarbothioamide, C₁₀H₁₃NOS

29. Januar 2018

Chien Ing Yeo, Edward R.T. Tiekink

Seiten: 299-301

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C 10 H 13 NOS, triclinic, P 1̅ (no. 2), a = 7.2099(5) Å, b = 9.9751(6) Å, c = 15.0463(9) Å, α = 80.560(5)°, β = 81.827(5)°, γ = 73.887(6)°, V = 1020.19(12) Å 3 , Z = 4, R gt ( F ) = 0.055, wR ref ( F 2 ) = 0.186, T = 100 K.
Open Access
Crystal Structure of ethyl (E)-2,4-dimethyl-5-((2-tosylhydrazono)methyl)-1H-pyrrole-3-carboxylate monohydrate, C₁₇H₂₃N₃O₅

1. Februar 2018

Zhongliang Lu, Jingzhang Ren, Wei-Na Wu

Seiten: 303-305

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C 17 H 23 N 3 O 5 , monoclinic, P 2 1 / n (No. 14), a = 12.8132(12) Å, b = 21.4531(19) Å, c = 15.3438(14) Å, β = 114.308(2)°, V = 3843.8(6) Å 3 , Z = 8, R gt ( F ) = 0.0652, wR ref ( F 2 ) = 0.2297, T = 296(2) K.
Open Access
Crystal structure of Diiodo-(N′-((quinolin-8-yl)methylene)isonicotinohydrazide κ³N,N′,O)cadium(II) – dimethylformamide (1/1), C₁₉H₁₉N₅O₂CdI₂

13. Februar 2018

Zhi-Hong Xu, Wei-Na Wu

Seiten: 307-308

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C 19 H 19 N 5 O 2 CdI 2 , monoclinic, P 2 1 / c (no. 14), a = 12.32(1) Å, b = 8.952(7) Å, c = 21.533(16) Å, β = 92.892(13)°, V = 2372(3) Å 3 , Z = 4, R gt ( F ) = 0.0373, wR ref ( F 2 ) = 0.0771, T = 296(2) K.
Open Access
Crystal structure of dinitrato-(N′-((quinolin-8-yl)methylene)isonicotinohydrazide κ³-N,N′,O)copper(II), C₁₆H₁₂N₆O₇Cu

9. Februar 2018

Zhi-Hong Xu, Ye Shen, Wei-Na Wu

Seiten: 309-310

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C 16 H 12 N 6 O 7 Cu, monoclinic P 2 1 / n , a = 7.832(4) Å, b = 15.641(9) Å, c = 14.747(8) Å, β = 101.365(9)°, V = 1770.9(17) Å 3 , Z = 4, R gt ( F ) = 0.0338, wR ref ( F 2 ) = 0.0885, T = 296(2) K.
Open Access
Crystal structure of benzoato-κO-bis(1,3,5-triaza-7-phosphaadamantane-κP)silver(I) monohydrate C₁₉H₃₁AgN₆O₃P₂

9. Februar 2018

Francois J.F. Jacobs, Gertruida J.S. Venter, Alice Brink

Seiten: 311-313

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C 19 H 31 AgN 6 O 3 P 2 , monoclinic, P 2 1 / c (no. 14), a = 16.5661(8) Å, b = 6.1644(3) Å, c = 23.8822(10) Å, β = 114.553(3)°, V = 2218.32(18) Å 3 , Z = 4, R gt ( F ) = 0.0188, wR ref ( F 2 ) = 0.0525, T = 100(2) K.
Open Access
Crystal structure of (E)-2-(anthracen-9-ylmethylene)hydrazine-1-carbothioamide, C₁₆H₁₃N₃S

7. Februar 2018

Chao Liu

Seiten: 315-316

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C 16 H 13 N 3 S, monoclinic, P 2 1 / c (no. 14), a = 19.0479(17) Å, b = 4.7282(4) Å, c = 16.7554(15) Å, β = 114.309(1)°, V = 1375.2(2) Å 3 , Z = 4, R gt ( F ) = 0.0412, wR ref ( F 2 ) = 0.1436, T = 293(2) K.
Open Access
The crystal structure of 8-chloro-7-ethyl-1,3-dimethyl-1H-purine-2,6(3H,7H)-dione, C₉H₁₁ClN₄O₂

6. Februar 2018

Syed Saeed Ali, Abdulrahman M. Al-Obaid, Eric C. Hosten, Ahmed Bari

Seiten: 317-318

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C 9 H 11 ClN 4 O 2 , orthorhombic, Pbca (no. 61), a = 8.9735(4) Å, b = 12.2946(7) Å, c = 19.3751(11) Å, V = 2137.6(2) Å 3 , Z = 8, R gt ( F ) = 0.0355, wR ref ( F 2 ) = 0.1087, T = 200(2) K.
Open Access
Crystal structure of {5,5′-((propane-1,3-diylbis(azanylylidene))bis(methanylylidene))bis(3-(ethoxycarbonyl)-2,4-dimethylpyrrol-1-ido)-κ⁴N,N′,N′′,N′′′}zinc(II), C₂₃H₃₀N₄O₄Cu

6. Februar 2018

Xue-Feng Han, Qing-Wen Yang, Miao Yang, Wei-Na Wu

Seiten: 319-320

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C 13 H 17 N 3 OS, monoclinic, P 1̅ (no. 2), a = 7.746(6) Å, b = 12.344(9) Å, c = 12.655(9) Å, α = 95.766(7)°, β = 98.007(7)°, γ = 101.595(13)°, V = 1163.4(15) Å 3 , Z = 2, R gt ( F ) = 0.0550, wR ref ( F 2 ) = 0.1616, T = 296(2) K.
Open Access
Crystal structure of bis(4-dimethylamino-pyridin-1-ium)tetrafluorosuccinate, C₁₈H₂₂F₄N₄O₄

28. Dezember 2017

Kuanguan Liu, Jing Nie

Seiten: 321-323

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C 18 H 22 F 4 N 4 O 4 , triclinic, P 1̄ (no. 2), a = 7.3295(9) Å, b = 8.6026(9) Å, c = 8.8041(11) Å, α = 77.240(4)°, β = 72.215(4)°, γ = 71.531(4)°, V = 496.61(10) Å 3 , Z = 1, R gt ( F ) = 0.1022, wR ref ( F 2 ) = 0.1587, T = 294(2) K.
Open Access
Crystal structure of dimethyl 3,9-dibenzyl-6,12-dicyclohexyl-3,9-diazahexacyclo [6.4.0.0^2,7.0^4,11.0^5,10]-dodecane-1,11-dicarboxylate, C₄₀H₅₀N₂O₄

12. Februar 2018

Hao Zhu, Yi-Fan Li, Ying-Ying Guo, Shan Liu, Han-Yang Lan, Peng-Yu Zhuang, Qi-Di Zhong

Seiten: 325-326

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C 40 H 50 N 2 O 4 , monoclinic, P 2 1 / c (no. 14), a = 10.355(2) Å, b = 17.809(4) Å, c = 8.9354(16) Å, β = 97.101(4)°, V = 1635.2(5) Å 3 , Z = 2, R gt ( F ) = 0.0453, wR ref ( F 2 ) = 0.1270, T = 113 K.
Open Access
Crystal structure of diethyl 3,9-diphenyl-6,12-bis(3-methoxyphenyl)-3,9-diazahexacyclo[6.4.0.0^2,7.0^4,11.0^5,10]dodecane-1,11-dicarboxylate, C₄₂H₄₂N₂O₆

8. Februar 2018

Hao Zhu, Ying-Ying Guo, Shan Liu, Yi-Fan Li, Han-Yang Lan, Peng-Yu Zhuang, Qi-Di Zhong

Seiten: 327-328

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C 42 H 42 N 2 O 6 , monoclinic, P 2 1 / c (no. 14), a = 6.9848(14) Å, b = 20.816(4) Å, c = 11.543(2) Å, β = 99.745(5)°, V = 1654.1(6) Å 3 , Z = 2, R gt ( F ) = 0.0377, wR ref ( F 2 ) = 0.1019, T = 113(2) K.
Open Access
Crystal structure of bis(acetato-κO)-bis(1-(pyridin-2-yl)ethan-1-one oxime-κ²N,N′)nickel(II), C₁₈H₂₂N₄NiO₆

1. Februar 2018

Jian Zuo

Seiten: 329-330

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C 18 H 22 N 4 NiO 6 , triclinic, P 1̅ (no. 2), a = 9.3398(13) Å, b = 9.9707(11) Å, c = 12.0063(18) Å, α = 89.829(3)°, β = 71.931(2)°, γ = 74.243(2)°, V = 1019.0(2) Å 3 , Z = 2, R gt ( F ) = 0.0472, wR ref ( F 2 ) = 0.1305, T = 298(2) K.
Open Access
Crystal structure of (N-(3-ethoxy-2-oxidobenzylidene)-4-fluorobenzohydrazonato-κ³N,O,O′)-diphenyltin(IV), C₂₈H₂₃FN₂O₃Sn

12. Februar 2018

Yee Seng Tan, See Mun Lee, Edward R.T. Tiekink

Seiten: 331-333

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C 28 H 23 FN 2 O 3 Sn, orthorhombic, Pbca (no. 61), a = 16.0887(2) Å, b = 14.5333(2) Å, c = 20.5550(2) Å, V = 4806.21(10) Å 3 , Z = 8, R gt ( F ) = 0.0199, wR ref ( F 2 ) = 0.0596, T = 100(2) K.
Open Access
Crystal structure of {N-(3-ethoxy-2-oxidobenzylidene)-4-fluorobenzohydrazonato-κ³O,N,O′}dimethyltin(IV), C₁₈H₁₉FN₂O₃Sn

13. Februar 2018

See Mun Lee, Yee Seng Tan, Edward R.T. Tiekink

Seiten: 335-337

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C 18 H 19 FN 2 O 3 Sn, monoclinic, C 2/ c (no. 15), a = 27.1120(3) Å, b = 9.5721(1) Å, c = 13.3072(1) Å, β = 98.271(1)°, V = 3417.55(6) Å 3 , Z = 8, R gt ( F ) = 0.016, wR ref ( F 2 ) = 0.043, T = 100(2) K.

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