Startseite Microstructure of a Damascene sabre after annealing
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Microstructure of a Damascene sabre after annealing

  • Marianne Reibold , Alexander A. Levin , Dirk C. Meyer , Peter Paufler EMAIL logo und Werner Kochmann
Veröffentlicht/Copyright: 12. Januar 2022
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Abstract

X-ray phase analysis combined with high-resolution electron microscopy of samples taken from a genuine Damascus sabre after annealing for 24 hat 400 °C and 800 °C followed by slow cooling down to room temperature has led to a better insight into the nature of cementite nanowires, which have been discovered recently. According to the present study, nanowires remained after 400 °C annealing, but disappeared after heat treatment at 800 °C and subsequent cooling down. On the other hand, perlitic cementite has been retained qualitatively after the same treatment. Knowing that the exceptional mechanical properties of Damascene blades disappear after annealing, the present results suggest a significant influence of the nanowires upon these features.


Prof. Dr. Peter Paufler Institut für Strukturphysik Fachrichtung Physik Technische Universität Dresden D-01062 Dresden, Germany Tel.: +49 351 4633 4670 Fax: +49 351 4633 7048

  1. The authors express their gratitude to Ms. Heide Müller for experimental help.

References

[1] W. Kochmann, M. Reibold, R. Goldberg, W. Hauffe, A.A. Levin, D.C. Meyer, T. Stephan, H. Müller, A. Belger, P. Paufler: J. Alloys Comp. 372 (2004) L15.10.1016/j.jallcom.2003.10.005Suche in Google Scholar

[2] A.A. Levin, D.C. Meyer, M. Reibold, W. Kochmann, N. Pätzke, P. Paufler: Crystal Res. Technol. 40 (2005) 905.10.1002/crat.200410456Suche in Google Scholar

[3] B. Zschokke: Revue de Métallurgie 21 (1924) 635.10.1051/metal/192421110635Suche in Google Scholar

[4] TOPAS. General profile and structure analysis software for powder diffraction data. Version 2.0, Bruker AXS GmbH, Germany (2000).Suche in Google Scholar

[5] P. Villars, L.D. Calvert: Pearson’s Handbook of Crystallographic Data for Intermetallic Phases, 2nd ed., Vols. 1–4, Am. Soc. for Metals, Metals Park, Ohio (1991).Suche in Google Scholar

[6] H.L. Jr. Yakel: Intern. Met. Rev. 30 (1985) 17; ICSD code 42542.10.1179/imr.1985.30.1.17Suche in Google Scholar

[7] J.P. Bouchard: Ann. Chim. (Paris) 1967 (1967) 353; ICSD code 31018.10.7326/0003-4819-66-2-353Suche in Google Scholar

[8] A.J.C. Wilson (Ed.): International Tables for Crystallography, Vol. C, Kluwer Academic Publishers, Dordrecht/Boston/London (1992).Suche in Google Scholar

[9] R.E. Young (Ed.): The Rietveld Method, Oxford University Press, New York (1995).Suche in Google Scholar

[10] W.A. Dollase: J. Appl. Cryst. 19 (1986) 267.10.1107/S0021889886089458Suche in Google Scholar

[11] J.-F. Bérar, P. Lelann: J. Appl. Cryst. 24 (1991) 1.10.1107/S0021889890008391Suche in Google Scholar

[12] P.A. Stadelmann: Ultramicroscopy 21 (1987) 131.10.1016/0304-3991(87)90080-5Suche in Google Scholar

[13] H. Schumann, H. Oettel: Metallografie, 14th ed., Wiley-VCH, Weinheim (2004)Suche in Google Scholar

[14] R.J. Hill, H.D. Flack: J. Appl. Cryst. 20 (1987) 356.10.1107/S0021889887086485Suche in Google Scholar

Received: 2005-09-13
Accepted: 2005-11-15
Published Online: 2022-01-12

© 2006 Carl Hanser Verlag, München

Artikel in diesem Heft

  1. Contents
  2. Extended editorial with anecdotes
  3. Anelastic relaxation and structure of ternary Fe–Al–Me alloys with Me = Co, Cr, Ge, Mn, Nb, Si, Ta, Ti, Zr
  4. Kinetic study of the β → α + γ transformation reaction in a CuZnAl alloy
  5. Calorimetric investigation of the binary Cu–In system
  6. Thermodynamic properties of liquid Cu–In–Zn alloys
  7. Comparing the thermodynamic behaviour of Al(l) + ZrO2(4% Y2O3) and Al(l) + Al2O3
  8. Failure-mode dependence of the strengthening effect in Ti3AlC2/10 vol.% Al2O3 composite
  9. Investigation of Cu-graphite composites prepared by electroforming
  10. Neutron diffraction analysis of martensite ageing in high-carbon FeCMnSi steel
  11. Effect of reinforcement size hybridization on the wear properties of SiCp/Cu Composites
  12. Temperature dependence of lattice mismatch and γ′ volume fraction of a fourth-generation monocrystalline nickel-based superalloy
  13. Novel combinatorial microstructures in Ti-6Al-4V alloy achieved by an electric-current-pulse treatment
  14. The Effect of Ti–B and Sr on the mechanical behaviour of the Zinc–Aluminum-based ZA-12 alloy produced by gravity casting
  15. Determination of retained austenite in multiphase steels by magnetic force microscopy
  16. Filtration resistance during pressure filtration tests of liquid aluminium alloys
  17. Microstructure of a Damascene sabre after annealing
  18. Effect of tin added to the zinc bath on the formation and the microstructure of hot-dip galvanized coatings
  19. Personal
  20. Conferences
  21. Contents
  22. Editorial
  23. Extended editorial with anecdotes
  24. Basic
  25. Anelastic relaxation and structure of ternary Fe–Al–Me alloys with Me = Co, Cr, Ge, Mn, Nb, Si, Ta, Ti, Zr
  26. Kinetic study of the β → α + γ transformation reaction in a CuZnAl alloy
  27. Calorimetric investigation of the binary Cu–In system
  28. Thermodynamic properties of liquid Cu–In–Zn alloys
  29. Comparing the thermodynamic behaviour of Al(l) + ZrO2(4% Y2O3) and Al(l) + Al2O3
  30. Failure-mode dependence of the strengthening effect in Ti3AlC2/10 vol.% Al2O3 composite
  31. Investigation of Cu-graphite composites prepared by electroforming
  32. Neutron diffraction analysis of martensite ageing in high-carbon FeCMnSi steel
  33. Applied
  34. Effect of reinforcement size hybridization on the wear properties of SiCp/Cu Composites
  35. Temperature dependence of lattice mismatch and γ′ volume fraction of a fourth-generation monocrystalline nickel-based superalloy
  36. Novel combinatorial microstructures in Ti-6Al-4V alloy achieved by an electric-current-pulse treatment
  37. The Effect of Ti–B and Sr on the mechanical behaviour of the Zinc–Aluminum-based ZA-12 alloy produced by gravity casting
  38. Determination of retained austenite in multiphase steels by magnetic force microscopy
  39. Filtration resistance during pressure filtration tests of liquid aluminium alloys
  40. Microstructure of a Damascene sabre after annealing
  41. Effect of tin added to the zinc bath on the formation and the microstructure of hot-dip galvanized coatings
  42. Notifications
  43. Personal
  44. Conferences
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