Startseite Influence of SPS parameters on the density and hardness of zinc selenide
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Influence of SPS parameters on the density and hardness of zinc selenide

  • Saman Safian , Mohammad Zakeri , Mohammad Reza Rahimipour , Ali Rahbari und Elnaz Irom
Veröffentlicht/Copyright: 29. September 2016
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International Journal of Materials Research
Aus der Zeitschrift International Journal of Materials Research Band 107 Heft 10

Abstract

In the present study, zinc selenide powder was successfully sintered using spark plasma sintering. The effect of spark plasma sintering temperature and pressure on the densification, microstructure and hardness were investigated. Relative density, microstructure, hardness and crystallographic properties of specimens were evaluated by means of the Archimedes method, optical microscopy/scanning electron microscopy, micro-Vickers and X-ray diffraction, respectively. The results indicated that temperature and pressure were the most effective parameters affecting the process. The maximum relative density (99.3%) and hardness (163 kg mm−2) were obtained using conditions of 1100°C for 5 min under 70 MPa. The crystallographic orientation (twinning) observed by optical microscopy was confirmed by X-ray diffraction results.

Keywords: Spark plasma sintering; ZnSe; Density; Hardness; Orientation
*Correspondence address, Mr. Saman Safian, Ceramic Department, Materials and Energy Research Center (MERC), Karaj P.O. Box 14155-4777, Iran, Tel.: +982636204131-4, Fax: +982636201888, E-mail:

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Received: 2016-02-02
Accepted: 2016-06-20
Published Online: 2016-09-29
Published in Print: 2016-10-14

© 2016, Carl Hanser Verlag, München

Artikel in diesem Heft

  1. Contents
  2. Contents
  3. Original Contributions
  4. A metastable phase diagram for the dynamic transformation of austenite at temperatures above the Ae3
  5. Experimental investigation of phase equilibria in the Co–Ni–Zr ternary system
  6. Phase equilibria of the Ni–Sb–Zn system at 600 °C
  7. High frequency cycling behaviour of three AZ magnesium alloys – microstructural characterisation
  8. Influence of auxetic foam in quasi-static axial crushing
  9. Electrochemical behaviour of iron and AISI 304 stainless steel in simulated acid rain solution
  10. Mechanochemical synthesis of CaMoO4 nanoparticles: kinetics and characterization
  11. Synthesis and characterization of iron oxide nanoparticles prepared hydrothermally at different reaction temperatures and pH
  12. Influence of SPS parameters on the density and hardness of zinc selenide
  13. Investigation into the kinetic behavior of molten aluminum pressureless infiltration into SiC preforms
  14. Review
  15. Centrifugal casting technique baseline knowledge, applications, and processing parameters: overview
  16. People
  17. Prof. Dr.-Ing. Jürgen Hirsch on the occasion of his 65th birthday
  18. DGM News
  19. DGM News
https://doi.org/10.3139/146.111413
Schlagwörter für diesen Artikel
Spark plasma sintering; ZnSe; Density; Hardness; Orientation

Artikel in diesem Heft

  1. Contents
  2. Contents
  3. Original Contributions
  4. A metastable phase diagram for the dynamic transformation of austenite at temperatures above the Ae3
  5. Experimental investigation of phase equilibria in the Co–Ni–Zr ternary system
  6. Phase equilibria of the Ni–Sb–Zn system at 600 °C
  7. High frequency cycling behaviour of three AZ magnesium alloys – microstructural characterisation
  8. Influence of auxetic foam in quasi-static axial crushing
  9. Electrochemical behaviour of iron and AISI 304 stainless steel in simulated acid rain solution
  10. Mechanochemical synthesis of CaMoO4 nanoparticles: kinetics and characterization
  11. Synthesis and characterization of iron oxide nanoparticles prepared hydrothermally at different reaction temperatures and pH
  12. Influence of SPS parameters on the density and hardness of zinc selenide
  13. Investigation into the kinetic behavior of molten aluminum pressureless infiltration into SiC preforms
  14. Review
  15. Centrifugal casting technique baseline knowledge, applications, and processing parameters: overview
  16. People
  17. Prof. Dr.-Ing. Jürgen Hirsch on the occasion of his 65th birthday
  18. DGM News
  19. DGM News
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