Zeitschrift für Kristallographie - New Crystal Structures

Issue Open Access

Volume 240, Issue 2

Published by

Become an author with De Gruyter Brill

Submit Manuscript Author Information

Zeitschrift für Kristallographie - New Crystal Structures

This issue is in the journal

Zeitschrift für Kristallographie - New Crystal Structures

Contents

Publicly Available
Frontmatter

February 27, 2025

Page range: i-vii

Download PDF
New Crystal Structures
Open Access
The crystal structure of N-(3-bromo-4-fluorophenyl)-N′-hydroxy-4-{[2-(4-methylphenyl)ethyl]amino}-1,2,5-oxadiazole-3-carboximidamide, C₁₈H₁₇BrFN₅O₂

January 13, 2025

Limin Zuo, Xia Zhou, Yitong Liu, Yongsheng Gu, Yifei Jiang, Xiaofang Lian, Huiyi Liu, Qingying Jia, Guangzhi Shan

Page range: 175-177

Download PDF

C 18 H 17 BrFN 5 O 2 , monoclinic, P 2 1 / c (no. 14), a = 19.3571(8) Å, b = 13.4295(12) Å, c = 7.3036(5) Å, β = 93.372(5)°, V = 1895.3(2) Å 3 , Z = 4, R gt ( F ) = 0.0407, wR ref ( F 2 ) = 0.0939, T = 293(2) K.
Open Access
Synthesis and crystal structure of ethyl (2S,4aS,6aS,6bR,8aR,12aS,12bR,14bR,E)-10-(((3,4-dichlorobenzyl)oxy)imino)-2,4a,6a,6b,9,9,12a-heptamethyl-13-oxo-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,12b,13,14b-icosahydropicene-2-carboxylate

January 13, 2025

Zhang-Chao Dong, Hui Shen, Ze-Bo Mu, Kai-Hua Xu

Page range: 179-181

Download PDF

C 39 H 53 Cl 2 NO 4 , monoclinic, P 2 1 (no. 4), a = 7.55730(10) Å, b = 11.0989(2) Å, c = 20.9222(3) Å, β = 91.426(1)°, V = 1754.36(5) Å 3 , Z = 2, R gt ( F ) = 0.0360, wR ref ( F 2 ) = 0.1028, T = 169.98(10) K.
Open Access
The crystal structure of pyrazole nitrate

January 8, 2025

Feng Qingxin, Zhang Mian, Liu Jikai, Cheng Jun, Sheng Fanfan, Zhao Linxiu, Ren Fude, Cao Duanlin

Page range: 183-184

Download PDF

C 3 H 5 N 3 O 3 , monoclinic, P 2 1 / c (no. 14), a = 3.702(2) Å, b = 11.109(7) Å, c = 13.105(8) Å, β = 94.21(2)°, V = 537.5(6) Å 3 , Z = 4, R gt ( F ) = 0.0731, wR ref ( F 2 ) = 0.2217, T = 170 K.
Open Access
Crystal structure of tetramethyl-bis(μ₂-2-(2-hydroxy-3-methoxybenzylidene)-1-(6-(2-(2-hydroxy-3-methoxybenzylidene)hydrazine-1-carbonyl)picolinoyl)hydrazin-1-ido-κ⁴O,N,O′:O′)ditin(II) ─ ethanol (1/2), C₅₄H₆₂N₁₀O₁₄Sn₂

January 8, 2025

Yan–Ling Qiao, Ji–Chun Cui

Page range: 185-187

Download PDF

C 54 H 62 N 10 O 14 Sn 2 , triclinic, P 1̄ (no. 2), a = 8.9238(14) Å, b = 10.6950(19) Å, c = 16.506(2) Å, α = 81.653(3)°, β = 75.444(2)°, γ = 70.354(2)°, V = 1432.8(4) Å 3 , Z = 1, R gt ( F ) = 0.0309, wR ref ( F 2 ) = 0.0824, T = 298(2) K.
Open Access
Crystal structure of catena-poly[μ₃-iodido-(4-bromopyridine-κ¹N)copper(I)], C₅H₄BrNCuI

January 7, 2025

Qingjia Liu, Litong Wang, Fanchao Meng, Quanxiang Han, Bingyu Xu, Xiaoxin Zheng

Page range: 189-190

Download PDF

C 5 H 4 BrNCuI, orthorhombic, Pna 2 1 (no. 33), a = 11.3879(4) Å, b = 16.3292(5) Å, c = 4.2274(1) Å, V = 786.11(4) Å 3 , Z = 4, R gt ( F ) = 0.0304, wR ref ( F 2 ) = 0.0579, T = 273(2) K.
Open Access
The crystal structure of cyclopentadienyl Co–P–C complexes by benzylideneacetone addition, C₃₈H₃₈CoO₂P

February 6, 2025

Shengnan Zhang, Lumin Wang, Zengli Zhai, Zihui Zhu

Page range: 191-193

Download PDF

C 38 H 38 CoO 2 P, triclinic, P 1̄ (no. 2), a = 10.5200(6) Å, b = 10.5216(6) Å, c = 15.3394(7) Å, α = 102.038(4)°, β = 105.984(4)°, γ = 100.225(5)°, V = 1545.69(15) Å 3 , Z = 2, R gt ( F ) = 0.0498, wR ref ( F 2 ) = 0.1120, T = 173.0(10) K.
Open Access
Synthesis and crystal structure of-(3S,10S,13S,17S)-N-(2-methoxyphenyl)-10,13-dimethyl-17-((R)-1-(phenylamino)ethyl)hexadecahydro-1H-cyclopenta[α]phenanthren-3-amine, C₃₄H₄₈N₂O

January 13, 2025

Lu-Lu Li, Peng Wei, Jiang-Hai Ye, Juan Zou, Kang He

Page range: 195-197

Download PDF

C 34 H 48 N 2 O, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 6.4541(3) Å, b = 12.5937(5) Å, c = 34.8855(12) Å, V = 2835.5(2) Å 3 , Z = 4, R gt ( F ) = 0.0665, wR ref ( F 2 ) = 0.1961, T = 297(2) K.
Open Access
The crystal structure of (E)-3-((E)-3-(4-ethoxy-3-methoxyphenyl)-1-hydroxyallylidene) chroman-2,4-dione, C₂₁H₁₈O₆

December 23, 2024

Suzana C. Janićević, Vidoslav S. Dekić, Biljana R. Dekić, Emilija T. Pecev Marinković, Niko S. Radulović, Milica G. Bogdanović, Marko V. Rodić

Page range: 199-201

Download PDF

C 21 H 18 O 6 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 7.2187(4) Å, b = 9.3833(7) Å, c = 13.6874(13) Å, α = 85.933(7)°, β = 81.991(7)°, γ = 69.983(7)°, V = 862.35(12) Å 3 , Z = 2, R gt ( F ) = 0.0418, wR ref ( F 2 ) = 0.1233, T = 295(2) K.
Open Access
The crystal structure of trans–L/D-[bis-(2-methyl-8-hydroxyquinoline-κ² N,O) bis-(1,3,5-triaza-7-phosphaadamantane-κ² P)cobalt(III)] tetrafluoroborate

January 7, 2025

Orbett T. Alexander, Andreas Roodt

Page range: 203-206

Download PDF

C 32 H 40 BCoF 4 N 8 O 2 P 2 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 10.682(4) Å, b = 12.900(5) Å, c = 13.453(4) Å, α = 76.214(9) ∘ , β = 70.490(9) ∘ , γ = 70.449(10) ∘ , V = 1629.80(10) Å 3 , Z = 2, R gt ( F ) = 0.0799, wR ref ( F 2 ) = 0.1820, T = 100 K.
Open Access
Crystal structure of 9-chloro-2,3,4,4a,5,6-hexahydro-1H-pyrido [1′,2′:1,6]pyrazino[2,3-b]quinoxaline, C₁₄H₁₅ClN₄

January 8, 2025

Qiang Chen, Xian Wu Fu, Yu Yu

Page range: 207-208

Download PDF

C 14 H 15 ClN 4 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 7.4938(4) Å, b = 9.1046(5) Å, c = 11.0448(5) Å, α = 113.516(5)°, β = 91.811(4)°, γ = 109.583(5)°, V = 638.98(6) Å 3 , Z = 2, R gt ( F ) = 0.0700, wR ref ( F 2 ) = 0.1909, T = 100 K.
Open Access
Crystal structure of 7-(diethylamino)-3-(benzoyl)-2 H -chromen-2-one, C₂₀H₁₉NO₃

January 13, 2025

Yahong Chen, Jing Wang, Ruoya Wang

Page range: 209-212

Download PDF

C 20 H 19 NO 3 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 8.2965(7) Å, b = 12.5111(11) Å, c = 16.2899(15) Å, V = 1,690.9(3) Å 3 , Z = 4, R gt ( F ) = 0.0582, wR ref ( F 2 ) = 0.1257, T = 298.8(6) K.
Open Access
The crystal structure of 4–bromo-3,5-dinitropyrazole

January 8, 2025

Wang Xiaolei, Xin Xianping, Sheng Fanfan, Zhao Linxiu, Cao Duanlin, Ren Fude

Page range: 213-214

Download PDF

C 3 HBrN 4 O 4 , monoclinic, P 2 1 / c (no. 14), a = 11.9791(4) Å, b = 5.9291(2) Å, c = 9.8188(4) Å, β = 96.520(1) ∘ , V = 692.87(4) Å 3 , Z = 4, R gt ( F ) = 0.0291, wR ref ( F 2 ) = 0.0676, T = 170 K.
Open Access
Crystal structure of 8-hydroxy-3,5,8a-trimethyl-7,8,8a,9-tetrahydronaphtho[2,3-b]furan-4,6-dione, C₁₅H₁₆O₄

January 8, 2025

Mei-Ling Wang, Jie Wu, Pan-Feng Cai, Jiang-Hai Ye, Juan Zou, Qi-Ji Li, Ya-Hua Liu, Ji-Xin Li

Page range: 215-216

Download PDF

C 15 H 16 O 4 , monoclinic, P 2 1 / c (no. 14), a = 11.4430(15) Å, b = 7.6794(7) Å, c = 15.598(2) Å, β = 111.52°, V = 1275.1(3) Å 3 , Z = 4, R gt ( F ) = 0.0587, w R ref ( F 2 ) = 0.1820, T = 273 K.
Open Access
Crystal structure of 5-hydroxy-3,5,8a-trimethyl-4a,5,6,7,8a,9-hexahydronaphtho[2,3-b]furan-4,8-dione, C₁₅H₁₈O₄

January 10, 2025

Mei-Ling Wang, Jie Wu, Pan-Feng Cai, Jiang-Hai Ye, Juan Zou, Qi-Ji Li, Ya-Hua Liu, Ji-Xin Li

Page range: 217-219

Download PDF

C 15 H 18 O 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 6.7517(6) Å, b = 9.0117(8) Å, c = 11.5876(10) Å, α = 108.039(2), β = 100.136(2)°, γ = 90.748(2), V = 658.20(10) Å 3 , Z = 2, R gt ( F ) = 0.0608, wR ref ( F 2 ) = 0.1634, T = 273 K.
Open Access
Synthesis and crystal structure of-(3S,10S,13S,17S)-N-(2-methoxyphenyl)-10,13-dimethyl-17-((R)-1-(p-tolylamino)ethyl)hexadecahydro-1H-cyclopenta[α]phenanthren-3-amine, C₃₅H₅₀N₂O

January 8, 2025

Mei Yang, Peng Wei, Yi-Chun Sun, Jiang-Hai Ye, Juan Zou, Kang He

Page range: 221-223

Download PDF

C 35 H 50 N 2 O, orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 6.7114 Å, b = 19.6699(9) Å, c = 22.7057(10) Å, V = 2,997.4(2) Å 3 , Z = 4, R gt ( F ) = 0.0401, wR ref ( F 2 ) = 0.0995, T = 297(2) K.
Open Access
The crystal structure of catena-poly((μ₂-1,3,5-tri(1H- imidazol-1-yl)benzene κ²N:N′)-bis(4-hydroxbenzoato-κ¹O)-zinc(II) monohydrate), C₂₉H₂₄N₆O₇Zn

January 9, 2025

Wentao Chen, Zhongjie Lai, Hangyi An, Yani Luo, Airong Wang, Yan Li, Jiaming Li

Page range: 225-229

Download PDF

C 29 H 24 N 6 O 7 Zn, monoclinic, Cc (no. 9), a = 10.8388(9) Å, b = 20.8648(12) Å, c = 13.0363(13) Å, β = 111.921(11)°, V = 2735.0 Å 3 , Z = 4, R gt ( F ) = 0.0406, wR ref ( F 2 ) = 0.0946, T = 298.15 K.
Open Access
Crystal structure of 2-(benzo[d]oxazol-2-yl)acetonitrile, C₉H₆N₂O

January 16, 2025

Juan Wang, Lei Feng, Dongrun Li, Litong Wang, Fanchao Meng, Quanxiang Han, Jinke Jiang, Xiaoxin Zheng, Xing Gao

Page range: 231-232

Download PDF

C 9 H 6 N 2 O, monoclinic, P 2 1 (no. 4), a = 5.3241(3) Å, b = 7.1833(5) Å, c = 10.3407(7) Å, β = 99.811(6)°, V = 389.69(4) Å 3 , Z = 2, R gt ( F ) = 0.0763, R ref ( F 2 ) = 0.1836, T = 293(2) K.
Open Access
Crystal structure of 1,3-dihydroxy-6,8-dimethoxy-2-(6-methyltetrahydro-2Hpyran-2-yl)-4a,9a-dihydroanthracene-9,10-dione, C₂₂H₂₂O₇

January 8, 2025

Shu-jun Shan, Yao-yao Cao, Ping Yao, Pei-pei Du, Sai Chen, Hong-lei Li

Page range: 233-235

Download PDF

C 22 H 22 O 7 , monoclinic, P 2 1 / n (no. 14), a = 7.8761(5) b = 17.0563(11) Å, c = 14.0504(10) Å, β = 95.563(4)°, V = 1878.6(2) Å 3 , Z = 4, R gt ( F ) = 0.0504, wR ref ( F 2 ) = 0.1475, T = 296(2) K.
Open Access
The crystal structure of the double salt potassium 1-methylpiperazine-1,4-di-ium trinitrate, C₅H₁₄KN₅O₉

February 7, 2025

Yi-Ping Shang, Jun-Ying Wu, Yu-Le Yao, Rui-Zheng Liu, Dan-Yang Liu, Lang Chen

Page range: 237-238

Download PDF

C 5 H 14 KN 5 O 9 , orthorhombic, Pbca (no. 61), a = 10.4760(3) Å, b = 14.0476(4) Å, c = 17.3708(5) Å, V = 2,556.33(13) Å 3 , Z = 8, T = 100 K, R gt ( F ) = 0.0226, wR ref ( F 2 ) = 0.0607.
Open Access
Crystal structure of 5′-hydroxy-6′-methoxy-1′-methyl-2′,3′,8′,8a′-tetrahydro-1′H-spiro[cyclohexane-1,7′-cyclopenta[ij]isoquinoline]-2,5-dien-4-one, C₁₈H₁₉NO₃

February 5, 2025

Li-Qiong Yang, Jie Wu, Hai-Long Qin, Pan-Feng Cai, Ya-Hua Liu, Ji-Xin Li

Page range: 239-241

Download PDF

C 18 H 19 NO 3 , monoclinic, P 2 1 (no. 4), a = 10.0669(6) Å, b = 6.9690(4) Å, c = 11.9051(7) Å, β = 113.011(2)°, V = 768.76(8) Å 3 , Z = 2, R gt ( F ) = 0.0344, wR ref ( F 2 ) = 0.0849, T = 170 K.
Open Access
The crystal structure of 1,1′-(2,3,5,6-tetramethylpyrazine-1,4-diyl)bis(ethan-1-one), C₁₂H₁₈N₂O₂

January 9, 2025

Yuwen Wang, Ruolin Cui, Chunteng Zhang

Page range: 243-244

Download PDF

C 12 H 18 N 2 O 2 , monoclinic, P 2 1 / n (no. 14), a = 9.2113(4) Å, b = 11.9224(6) Å, c = 11.4469(4) Å, β = 96.413(2)°, V = 1249.24(9) Å 3 , Z = 4, R gt ( F ) = 0.0589, wR ref ( F 2 ) = 0.1869, T = 655 K.
Open Access
Crystal structure of [μ₂-piperazine-1,4-bis(2-hydroxypropanesulfonato-κ²O:O′)] bis(μ₂-4,4′-trimethylenedipyridyl-κ²N:N′)disilver(I), C₁₈H₂₄AgN₃O₄S

January 9, 2025

Chaohong Ma, Xianwu Dong, Jinke Jiang, Hui Jiang

Page range: 245-246

Download PDF

C 18 H 24 AgN 3 O 4 S, monoclinic, P 2 1 / n (no. 14), a = 10.5522(10) Å, b = 9.4295(6) Å, c = 19.2298(12) Å, β = 95.606(7)°, V = 1904.3(2) Å 3 , Z = 4, R gt ( F ) = 0.0401, wR ref ( F 2 ) = 0.0959, T = 293(2) K.
Open Access
Crystal structure of bis ((1-((E)-((4-methoxyphenyl)imino)methyl)naphthalen-2-yl)oxy) copper(II), C₃₆H₂₈CuN₂O₄

January 8, 2025

Haneen Fadhil Abbas, Basil A. Saleh, Faris A. J. Al-Doghachi, Benson M. Kariuki, Gamal A. El-Hiti

Page range: 247-249

Download PDF

C 36 H 28 CuN 2 O 4 , tetragonal, P 4̄2 1 c (no. 114), a = 18.9249(5) Å, c = 7.9571(5) Å, V = 2,849.9(2) Å 3 , Z = 4, R gt ( F ) = 0.0538, wR ref ( F 2 ) = 0.1336, T = 293 K.
Open Access
Synthesis and crystal structure of 6,6′-((1E,11E)-5,8-dioxa-2,11-diazadodeca-1,11-diene-1,12-diyl) bis(2,4-di-tert-butylphenol), C₃₆H₅₆N₂O₄

January 9, 2025

Ya-Fang Zhang, Ji-Xing Zhao

Page range: 251-253

Download PDF

C 36 H 56 N 2 O 4 , monoclinic, P 2 1 / c (no. 14), a = 18.1240(10) Å, b = 17.1409(9) Å, c = 11.3102(6) Å, β = 95.659(2)°, V = 3,496.5(3) Å 3 , Z = 4, R gt ( F ) = 0.0638, wR ref ( F 2 ) = 0.1634, T = 173 K.
Open Access
The crystal structure of barium hexahydroxidoiridate(IV) dihydroxide, Ba₂[Ir(OH)₆](OH)₂

February 7, 2025

Jörn Bruns, Désirée Badea

Page range: 255-256

Download PDF

Ba 2 [Ir(OH) 6 ](OH) 2 , orthorhombic, Pbca (no. 61), a = 8.5717(4) Å, b = 8.6814(4) Å, c = 10.3683(5) Å, V = 771.55(6) Å 3 , Z = 4, R gt ( F ) = 0.0154, wR ref ( F 2 ) = 0.0304, T = 100(2) K.
Open Access
Crystal structure of cinnamoyl ferrocene, C₁₉H₁₆FeO

January 27, 2025

Qiaru Wang, Xiaona Xu, Mo Du, Wenqiang Tang, Bin Liu

Page range: 257-259

Download PDF

C 19 H 16 FeO, orthorhombic, Pna 2 1 (no. 33), a = 40.8379(12) Å, b = 5.7993(2) Å, c = 11.9680(3) Å, V = 2834.40(15) Å 3 , Z = 8, R gt ( F ) = 0.0397, wR ref ( F 2 ) = 0.0834, T = 170 K. CCDC no.: 2403075.
Open Access
Crystal structure of (E)-3-(4-butoxyphenyl)acryloylferrocene, C₂₃H₂₄FeO₂

January 29, 2025

Mo Du, Xiaona Xu, Qiaru Wang, Wenqiang Tang, Bin Liu

Page range: 261-263

Download PDF

C 23 H 24 FeO 2 , monoclinic, P 2 1 / c (no. 14), a = 13.8934(19) Å, b = 5.8012(7) Å, c = 23.011(4) Å, β = 97.160(5)°, V = 1840.2(4) Å 3 , Z = 4, R gt ( F ) = 0.0915, w R ref ( F 2 ) = 0.2115, T = 170 K.
Open Access
Crystal structure of 7-(dimethylamino)-2-hydroxy-2-(trifluoromethyl)-2H-chromene-3-ethyl carboxylate, C₁₅H₁₆F₃NO₄

January 27, 2025

Ruifeng Yue, Ruiying Wang, Hang Shu, Dayong Fu, Zhuanghui Qi

Page range: 265-269

Download PDF

C 15 H 16 F 3 NO 4 , triclinic, P 1 ‾ $P\overline{1}$ (no. 2), a = 6.7000(2) Å, b = 11.7844(4) Å, c = 19.3039(6) Å, α = 83.581(3)°, β = 86.015(3)°; γ = 87.713(3)°; V = 1510.14 Å 3 , Z = 4, R gt ( F ) = 0.0459, w R ref ( F 2 ) = 0.1389, T = 294.95 K.
Open Access
The crystal structure of 1-phenylethan-1-aminium 4-hydroxy-3,5-dimethoxybenzoate C₁₇H₂₁NO₅

January 8, 2025

Chen-Yu Ruan, Zi-Wei Ai, Gong-Yi Liang, Pan-Yue Cao, Ke-Fan Yu, Cheng-Jun Jiang

Page range: 271-272

Download PDF

C 17 H 21 NO 5 , monoclinic, P 2 1 (no. 4), a = 6.0322(2) Å, b = 16.0271(6) Å, c = 9.0421(3) Å, β = 105.568(2)°, V = 842.11(5) Å 3 , Z = 2, R gt ( F ) = 0.0384, wR ref ( F 2 ) = 0.1008, T = 170 K.
Open Access
The crystal structure of 1,3,5-trichloro-2-nitrobenzene

January 23, 2025

Bai Sha, Liu Qiaoe, Lu Zhiyan, Wang Fan, Wang Jianlong, Chen Lizhen

Page range: 273-274

Download PDF

C 6 H 2 NCl 3 O 2 , monoclinic, C 2/ c (no. 15), a = 8.161(4) Å, b = 12.192(6) Å, c = 8.903(4) Å, β = 110.664(10)°, V = 828.8(7) Å 3 , Z = 4, R gt ( F ) = 0.0513, wR ref ( F 2 ) = 0.1384, T = 193 K.
Open Access
The crystal structure of tris(μ₂-bromido)-bis(η⁶-p-cymene)-diosmium(II) tetrafluoroborate, C₂₀H₂₈BBr₃F₄Os₂

February 4, 2025

Kgaugelo C. Tapala, Hadley S. Clayton

Page range: 275-277

Download PDF

C 20 H 28 BBr 3 F 4 Os 2 , orthorhombic, Pccn (no. 56), a = 10.9714(15) Å, b = 13.3784(17) Å, c = 16.7710(2) Å, V = 2,461.7(6) Å 3 , Z = 4, R gt ( F ) = 0.0188, w R ref ( F 2 ) = 0.0442, T = 173(2) K.
Open Access
Crystal structure of new barium lithium manganese fluorides: Ba₁₄Li_1.87Mn_14.13F₆₈ with a Jarlite–related structure

January 8, 2025

Hong Young Chang, Sun Woo Kim

Page range: 279-280

Download PDF

Ba 14 Li 1.87 Mn 14.13 F 68 , monoclinic, C 2/ m (no. 12), a = 16.9675(7) Å, b = 11.5326(5) Å, c = 7.5783(3) Å, β = 102.4190(10)°, V = 1448.22(10) Å 3 , Z = 1, R gt ( F ) = 0.0177, wR ref ( F 2 ) = 0.0454, T = 296(2) K.
Open Access
Crystal structure of (4-fluorobenzyl)triphenylphosphonium chloride, C₂₅H₂₁ClFP

January 23, 2025

Xue Li, Guangyao Wang

Page range: 281-282

Download PDF

C 25 H 21 ClFP, monoclinic, P 2 1 / n (no. 14), a = 9.5700(2) Å, b = 13.9963(2) Å, c = 15.8793(4) Å, β = 101.024(2)°, V = 2087.70(8) Å 3 , Z = 4, R gt ( F ) = 0.0401, wR ref ( F 2 ) = 0.1112, T = 150 K.
Open Access
The crystal structure of calcitriol–chloroform (1/1), C₂₇H₄₄O₃⋅CHCl₃

January 24, 2025

Yue-Ting Deng, Zhong-Yan Hao, Xi Liu, Kang Pan, An Zhao, Wen-Yang Zheng, Wei Xiang, Wen-Jing Ma

Page range: 283-285

Download PDF

C 27 H 44 O 3 ⋅CHCl 3 , monoclinic, P 2 1 (no. 4), a = 11.2800(7) Å, b = 8.4193(4) Å, c = 16.6951(10) Å, β = 109.593(4)°, V = 1493.72(15) Å 3 , Z = 2, R gt ( F ) = 0.0561, wR ref ( F 2 ) = 0.1550, T = 299 K.
Open Access
The crystal structure of (E)-1-((3)-nitrophenyl)pyren-3-(pyren-1-yl)prop-2-en-1-one, C₂₅H₁₅NO₃

January 27, 2025

Claudio Barrientos, J. Arturo Squella, Silvana Moris

Page range: 287-289

Download PDF

C 25 H 15 NO 3 , triclinic, P 1̄ (no. 2), a = 8.4899(3) Å, b = 10.1383(4) Å, c = 11.3806(5) Å, α = 78.373(1)°, β = 72.020(1)°, γ = 73.381(1)°, V = 885.89(6) Å 3 , Z = 2, R gt ( F ) = 0.0439, wR ref ( F 2 ) = 0.1290, T = 296.15 K.
Open Access
Crystal structure of (E)-2-hydroxy-N′-(1-(4-hydroxyphenyl)propylidene)benzohydrazide, C₁₆H₁₆N₂O₃

February 7, 2025

Xiaona Xu, Hongjuan Tong, Bin Liu

Page range: 291-293

Download PDF

C 16 H 16 N 2 O 3 , monoclinic, P 2 1 / c (no. 14), a = 8.9406(3) Å, b = 9.3999(3) Å, c = 17.1101(6) Å, β = 98.8190(10)°, V = 1420.95(8) Å 3 , Z = 4, R gt ( F ) = 0.0468, wR ref ( F 2 ) = 0.1213, T = 298 K.
Open Access
Crystal structure of (E)-(3-(thiophen-2-yl)acryloyl)ferrocene, C₁₇H₁₄FeOS

February 7, 2025

Fangfang Ding, Xiaona Xu, Zhoujing Zhu, Hongjuan Tong, Wenqiang Tang

Page range: 295-297

Download PDF

C 17 H 14 FeOS, monoclinic, P 2 1 / n (no. 14), a = 5.8315(3) Å, b = 19.9325(13) Å, c = 11.9563(7) Å, β = 90.11(5)°, V = 1389.75(14) Å 3 , Z = 4, R gt ( F ) = 0.0386 wR ref ( F 2 ) = 0.0858, T = 170 K.
Open Access
Crystal structure of (E)-(3-(furan-2-yl)acryloyl)ferrocene, C₁₇H₁₄FeO₂

February 6, 2025

Zhoujing Zhu, Xiaona Xu, Hongjuan Tong, Wenqiang Tang

Page range: 299-301

Download PDF

C 17 H 14 FeO 2 , orthorhombic, Pbca (no. 61), a = 9.1480(2) Å, b = 10.2745(2) Å, c = 27.8889(6) Å, V = 2621.31(10) Å 3 , Z = 8, R gt ( F ) = 0.0287, wR ref ( F 2 ) = 0.0760, T = 170 K.
Open Access
Synthesis and crystal structure poly[diaqua(μ₃-3-(((7-hydroxy-3-(4-methoxy-3-sulfonatophenyl)-4-oxo-4H-chromen-8-yl) methyl)ammonio)propanoate-κ³ O:O′:O″) sodium(I)] monohydrate, C₂₀H₂₄NNaO₁₂S

February 12, 2025

Hai-Lin Chen, Yan-Ping Wang, Qing-Yan Sun, Ze-Ping Luo

Page range: 303-305

Download PDF

C 20 H 24 NNaO 12 S, monoclinic, P 2 1 / c (no. 14), a = 16.3424(5) Å, b = 9.2619(2) Å, c = 16.1782(5) Å, β = 115.163(4)°, V = 2216.38(13) Å 3 , Z = 4, R gt ( F ) = 0.0368, wR ref ( F 2 ) = 0.1024, T = 100 K.
Open Access
Crystal structure of 9-methoxy-4-(2-methoxypyridin-3-yl)-5,6-dihydrobenzo[h]quinazolin-2-amine C₁₉H₁₈N₄O₂

February 11, 2025

Mei-Lin Song, Xian-Rui Xie, Gui-Ge Hou

Page range: 307-309

Download PDF

C 19 H 18 N 4 O 2 , triclinic, P 1¯ (no. 2), a = 8.3712(10) Å, b = 9.6699(11) Å, c = 10.5323(12) Å, α = 77.24(1)°, β = 74.576(10)°, γ = 81.126(9)°, V = 797.42(17) Å 3 , Z = 2, R gt ( F ) = 0.0564, wR ref ( F 2 ) = 0.1540, T = 293.0 K.
Open Access
Synthesis and crystal structure of 4-(difluoromethyl)-1-methyl-N-(pyridin-3-yl)-1H-pyrazole-3-carboxamide hydrate, C₁₁H₁₂F₂N₄O₂

February 7, 2025

Hao-Wen Huang, Hao-Hong Liu, Si-Tong Lin, Xian-Nv Gan, Ji Zhang

Page range: 311-313

Download PDF
Open Access
The crystal structure of caesalfurfuric acid B, C₂₂H₃₂O₄

February 17, 2025

Xiuyuan Li, Guoyong Luo, Jianghai Ye, Tiantian Li, Tianqiong Lang

Page range: 315-317

Download PDF

C 22 H 32 O 4 , monoclinic, P 2 1 (no. 4), a = 12.0894(10) Å, b = 6.4123(5) Å, c = 13.9418(12) Å, β = 112.621(3), V = 997.63(14) Å 3 , Z = 2, R gt ( F ) = 0.0517, wR ref ( F 2 ) = 0.1312, T = 170 K.
Open Access
The crystal structure of 2-bromo-2-(5-bromo-2-methyl-4-nitro-1H-imidazol-1-yl)-1-phenylethanone, C₁₂H₉Br₂N₃O₃

February 3, 2025

Sadeekah O. Saber, Yaseen A. Al-Soud, Raed A. Al-Qawasmeh, Monther A. Khanfar

Page range: 319-321

Download PDF

C 12 H 9 Br 2 N 3 O 3 , monoclinic, P 2 1 / c (no. 14), a = 9.0255(5) Å, b = 14.9112(5) Å, c = 10.9438(5) Å, β = 109.223(5)°, V = 1390.71(12) Å 3 , Z = 4, R gt ( F ) = 0.0482, wR ref ( F 2 ) = 0.0948, T = 293(2) K.
Open Access
The crystal structure of bis{chlorido-[μ₂-(1-oxidopyridin-2-yl)(pyridin-2-yl)amido-κ³ O,N, N′]copper(II)}, C₂₀H₁₆Cl₂Cu₂N₆O₂

February 18, 2025

Yinqiu Liu

Page range: 323-324

Download PDF

C 20 H 16 Cl 2 Cu 2 N 6 O 2 , monoclinic, C 2/ c (no. 15), a = 22.705(4) Å, b = 7.6810(13) Å, c = 14.287(3) Å, β = 119.813(5) ∘ , V = 2161.9(7) Å 3 , Z = 8, R gt ( F ) = 0.0203, wR ref ( F 2 ) = 0.0551, T = 293 K.
Open Access
The crystal structure of 3-amino-2-formyl-1-phenyl-9,10-dihydrophenanthrene-4-carbonitrile, C₂₂H₁₆N₂O

February 14, 2025

Longdie Cheng, Guoyong Luo, Xulan Wang, Jianghai Ye, Tianqiong Lang

Page range: 325-327

Download PDF

C 22 H 16 N 2 O, monoclinic, P 2 1 / c , (no. 14), a = 9.689(7) Å, b = 16.800(10) Å, c = 10.379(7) Å, β = 92.229(17), V = 1,688.22(18) Å 3 , Z = 4, R gt ( F ) = 0.0584, wR ref ( F 2 ) = 0.1572, T = 273(2) K.
Open Access
The crystal structure of 1,1′-(2,5-dimethylpyrazine-1,4-diyl)bis(ethan-1-one), C₁₀H₁₄N₂O₂

February 13, 2025

Jinfeng Wang

Page range: 329-330

Download PDF

C 10 H 14 N 2 O 2 , monoclinic, C 2/c (no. 15), a = 15.7853(7) Å, b = 8.5036(4) Å, c = 31.4964(17) Å, β = 90.371(2)°, V = 4,227.7(4) Å3, Z = 8, R gt ( F ) = 0.0451, wR ref (F 2 ) = 0.1611, T = 655 K.
Open Access
Crystal structure of 5′-(9-phenyl-9H-carbazol-3-yl)-[2,2′-bithiophene]-5-carbaldehyde, C₂₇H₁₇NOS₂

February 13, 2025

Wen-Ze Zhao, Feng-Jun Lu

Page range: 331-333

Download PDF

C 27 H 17 NOS 2 , monoclinic, P 2 1 / c (no. 14), a = 17.5582(11) Å, b = 12.4355(8) Å, c = 10.0535(5) Å, β = 103.391(2)°, V = 2135.5 Å 3 , Z = 4, R gt ( F ) = 0.0555, w R ref ( F 2 ) = 0.1093, T = 273 K.
Open Access
The crystal structure of the double salt dipyridin-1-ium bromide tribromide

February 12, 2025

Wang Bo, Pan Hongxia, Chen Jun, Li Yunlu, Chen Lizhen, Wang Jianlong

Page range: 335-336

Download PDF

C 10 H 12 Br 4 N 2 , orthorhombic, Pbcn (no. 60), a = 13.3150(2) Å, b = 13.8478(2) Å, c = 15.7803(2) Å, V = 2909.63(7) Å 3 , Z = 8, R gt ( F ) = 0.0302, wR ref ( F 2 ) = 0.0948, T = 220 K.
Open Access
Crystal structure of (E)-(3-(3-methylthiophen-2-yl)acryloyl)ferrocene, C₁₈H₁₆FeOS

February 11, 2025

Yanjiao Wang, Haoliang Zheng, Keyi Zhang, Xiaohua Li, Bin Liu

Page range: 337-339

Download PDF

C 18 H 16 FeOS, monoclinic, Cc (no. 6), a = 13.4809(7) Å, b = 13.3262(7) Å, c = 9.5652(6) Å, β = 120.604(2)°, V = 1479.02(15) Å 3 , Z = 4, R gt ( F ) = 0.0364 wR ref ( F 2 ) = 0.0882, T = 170 K.
Open Access
Crystal structure of (E)-(3-(4-phenoxyphenyl)acryloyl)ferrocene, C₂₅H₂₀FeO₂

February 7, 2025

Jie Gao, Shuang Zhang, Yanan Wang, Yucong Guo, Bin Liu

Page range: 341-343

Download PDF

C 25 H 20 FeO 2 , monoclinic, P 2 1 / c (no. 14), a = 15.9672(10) Å, b = 5.7830(4) Å, c = 20.9889(15) Å, β = 104.017(3)°, V = 1880.4(2) Å 3 , Z = 4, R gt ( F ) = 0.0565 wR ref ( F 2 ) = 0.1227, T = 173 K.
Open Access
Crystal structure of (E)-(3-(3,4-dimethylphenyl)acryloyl)ferrocene, C₂₁H₂₀FeO

February 11, 2025

Yanrong Gao, Xiaona Xu, Zhoujing Zhu, Wenqiang Tang

Page range: 345-348

Download PDF

C 21 H 20 FeO, monoclinic, P 2 1 / c (no. 14), a = 27.666(3) Å, b = 5.9979(5) Å, c = 21.0340(19) Å, β = 112.226(3)°, V = 3231.0(5) Å 3 , Z = 8, R gt ( F ) = 0.1155 wR ref ( F 2 ) = 0.3122, T = 170 K.
Open Access
Crystal structure of [(1,4,8,11-tetraazacyclotetradecane-κ⁴N,N′,N′′,N‴)tetracyanidodiplatinum(II)] dimethyl sulfoxide solvate, C₁₈H₃₆N₈O₂Pt₂S₂

February 3, 2025

Kwang Ha

Page range: 349-351

Download PDF

C 18 H 36 N 8 O 2 Pt 2 S 2 , monoclinic, P 2 1 / c (no. 14), a = 12.0848(16) Å, b = 14.1725(18) Å, c = 8.1065(9) Å, β = 97.603(4)°, V = 1376.2 Å 3 , Z = 2, R gt ( F ) = 0.0279, wR ref ( F 2 ) = 0.0749, T = 223 K.
Open Access
Crystal structure of (4-ethoxybenzyl)triphenylphosphonium bromide ethanol solvate, C₂₉H₃₂BrO₂P

February 14, 2025

Shuyan Chen, Xiangbin Nan, Haoqi Yang, Yiheng Xue, Hui Jiang

Page range: 353-355

Download PDF

C 29 H 32 BrO 2 P, monoclinic, P 2 1 / c (no. 14), a = 8.52420(10) Å, b = 13.5027(5) Å, c = 23.3580(4) Å, β = 95.359(1)°, V = 2676.75(11) Å 3 , Z = 4, R gt ( F ) = 0.0386, w R ref ( F 2 ) = 0.1039, T = 298(2) K.
Open Access
Crystal structure of (1-naphthalen-1-yl-methyl)triphenylphosphonium chloride ethanol solvate, C₃₁H₃₀ClOP

February 17, 2025

Jinke Jiang, Hui Jiang

Page range: 357-359

Download PDF

C 31 H 30 ClOP, orthorhombic, Pna 2 1 (no. 33), a = 16.4933(2) Å, b = 9.8603(2) Å, c = 16.1472(3) Å, V = 2626.00(8) Å 3 , Z = 4, R gt ( F ) = 0.0770, wR ref ( F 2 ) = 0.2238, T = 298 K.
Open Access
Crystal structure of (1,4,8,11-tetraazacyclotetradecane-κ⁴N,N′,N″,N‴)platinum(II) bis[tribromido(dimethyl sulfoxide-κS)platinate(II)], C₁₄H₃₆Br₆N₄O₂Pt₃S₂

February 3, 2025

Kwang Ha

Page range: 361-362

Download PDF

C 14 H 36 Br 6 N 4 O 2 Pt 3 S 2 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 8.985(3) Å, b = 9.384(3) Å, c = 9.672(3) Å, α = 68.419(7)°, β = 87.691(9)°, γ = 77.166(8)°, V = 738.5(3) Å 3 , Z = 1, R gt ( F ) = 0.0232, wR ref ( F 2 ) = 0.0616, T = 223 K.
Open Access
Crystal structure of (2-methylbenzyl)triphenylphosphonium chloride ethanol solvate, C₂₈H₃₀ClOP

February 14, 2025

Chaohong Ma, Xianwu Dong, Jinke Jiang, Hui Jiang

Page range: 363-365

Download PDF

C 28 H 30 ClOP, monoclinic, P 2 1 / n (no. 14), a = 9.0999(1) Å, b = 14.7077(2) Å, c = 18.5420(3) Å, β = 95.281(1)°, V = 2471.10(6) Å 3 , Z = 4, R gt ( F ) = 0.0450, wR ref ( F 2 ) = 0.1261, T = 293 K.
Open Access
Crystal structure of bis(η², σ¹-8-methoxycyclooct-4-enyl)(μ₂-1,4,8,11-tetraazacyclotetradecane-κ⁴ N, N′, N″, N‴)diplatinum(II) dibromide, C₂₈H₅₄Br₂N₄O₂Pt₂

February 4, 2025

Kwang Ha

Page range: 367-369

Download PDF

C 28 H 54 Br 2 N 4 O 2 Pt 2 , monoclinic, P 2 1 / n (no. 14), a = 9.798(5) Å, b = 11.389(5) Å, c = 15.228(7) Å, β = 107.148(14)°, V = 1623.6(12) Å 3 , Z = 2, R gt ( F ) = 0.0273, wR ref ( F 2 ) = 0.0529, T = 223 K.
Open Access
Crystal structure of (1,4,8,11-tetraazacyclotetradecane-κ⁴N,N^′,N^″,N^‴)palladium(II) tetrabromidopalladate(II), C₁₀H₂₄Br₄N₄Pd₂

February 3, 2025

Kwang Ha

Page range: 371-372

Download PDF

C 10 H 24 Br 4 N 4 Pd 2 , monoclinic, C 2/ c (no. 15), a = 13.784(7) Å, b = 8.985(5) Å, c = 16.006(12) Å, β = 113.429(17)°, V = 1819.0(19) Å 3 , Z = 4, R gt ( F ) = 0.0388, wR ref ( F 2 ) = 0.1202, T = 223 K.
Open Access
Crystal structure of (1,4,8,11-tetraazacyclotetradecane-κ⁴N,N′,N″,N‴)palladium(II) bis[trichlorido(dimethyl sulfoxide-κS)platinate(II)], C₁₄H₃₆Cl₆N₄O₂PdPt₂S₂

February 3, 2025

Kwang Ha

Page range: 373-374

Download PDF

C 14 H 36 Cl 6 N 4 O 2 PdPt 2 S 2 , triclinic, P 1 ‾ $\overline{1}$ (no. 2), a = 8.714(2) Å, b = 9.270(2) Å, c = 9.525(2) Å, α = 68.940(6)°, β = 87.786(7)°, γ = 77.327(7)°, V = 699.9(3) Å 3 , Z = 1, R gt ( F ) = 0.0153, wR ref ( F 2 ) = 0.0351, T = 223 K.
Open Access
Crystal structure of (1,4,8,11-tetraazacyclotetradecane-κ⁴N,N′,N″,N‴)palladium(II) tetraiodidopalladate(II), C₁₀H₂₄I₄N₄Pd₂

February 7, 2025

Kwang Ha

Page range: 375-377

Download PDF

C 10 H 24 I 4 N 4 Pd 2 , monoclinic, P 2 1 / n (no. 14), a = 8.955(7) Å, b = 15.587(13) Å, c = 14.752(12) Å, β = 95.63(2)°, V = 2049(3) Å 3 , Z = 4, R gt ( F ) = 0.0564, wR ref ( F 2 ) = 0.1562, T = 223 K.

Issues in this Volume

Search the content of this journal

This issue

All issues

Issues in this Volume

Institutional Access

How does access work?

Downloaded on 4.10.2025 from https://www.degruyterbrill.com/journal/key/ncrs/240/2/html