Startseite Technik Synthesis of ultrafine powder (W,Ti)C by microwave heating in a stream of argon
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Synthesis of ultrafine powder (W,Ti)C by microwave heating in a stream of argon

  • Irina Nikolaenko , Nikolay Kedin und Gennadii Shveikin
Veröffentlicht/Copyright: 5. Dezember 2014
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Abstract

In this article, a new method of synthesis of ultrafine powder solid solution (Ti,W)C by a combination of classical liquid-phase precipitation on a carbon support and low-temperature microwave heat treatment is proposed. An entire spectrum of intermediates obtained during thermolysis, reduction, and carbidization precursor to the final product has been obtained. The structure, particle morphology, phase structure and surface area values for the samples are shown.


* Correspondence address, Dr. Irina Nikolaenko, Institute of Solid State Chemistry, Ural Branch of the Russian Academy of Sciences, 91 Pervomaiskaya str., 620990 Ekaterinburg, Russia, E-mail:

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Received: 2014-06-03
Accepted: 2014-07-25
Published Online: 2014-12-05
Published in Print: 2014-12-08

© 2014, Carl Hanser Verlag, München

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