The superplasticity of friction stir processed Al-5Mg alloy with additions of scandium and zirconium
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Anton Smolej
, Damjan Klobčar , Brane Skaza , Aleš Nagode , Edvard Slaček , Vukašin Dragojević und Samo Smolej
Abstract
The paper describes the effect of minor additions of scandium and zirconium on the superplastic behaviour of friction stir processed Al-5Mg based alloy. The measurements included the flow curves and tensile elongations of (in wt.%) Al-5Mg-0.1Zr, Al-5Mg-0.2Sc, and Al-5Mg-0.2Sc-0.15Zr alloys at initial strain rates ranging from 1 × 10−3 to 1 × 10−1 s−1, and at forming temperatures from 350 to 500°C. The inclusion of friction stir processing at tool rotation rates of 95 and 475 rpm considerably enhanced the superplastic behaviour of the Al-5Mg-0.2Sc-0.15Zr alloy, which was reflected in elongations without failure of over 1900%. Other friction stir processed alloys, treated at lower tool rotation rates, did not achieve superplasticity due to abnormal grain growth. The results yielded by the friction stir processed alloys are compared with the superplastic behaviour of the same alloys produced conventionally by cold rolling.
References
[1] J.S.Vetrano, C.A.Lavender, C.H.Hamilton, M.T.Smith, S.M.Bruemmer: Scr. Metall. Mater.30 (1994) 565. 10.1016/0956-716X(94)90430-8Suche in Google Scholar
[2] R.Verma, A.K.Gosh, S.Kim, C.Kim: Mater. Sci. Eng.A191 (1995) 143. 10.1016/0921-5093(94)09622-4Suche in Google Scholar
[3] H.Iwasaki, H.Hosokawa, T.Mori, T.Tagata, K.Higashi: Mater. Sci. Eng.A252 (1998) 199. 10.1016/S0921-5093(98)00678-9Suche in Google Scholar
[4] P.A.Friedman, W.B.Copple: J. Mater. Eng. Perform.13 (2004) 335. 10.1361/10599490419162Suche in Google Scholar
[5] M.A.Kulas, P.E.Krajewski, J.R.Bradley, E.M.Taleff: J.Mater. Eng. Perform.16 (2007) 308. 10.1007/s11665-007-9057-Suche in Google Scholar
[6] T.G.Langdon: Mater. Trans. JIM40 (1999) 1320. 10.2320/matertrans1989.40.716Suche in Google Scholar
[7] C.Hsiao, J.C.Huang: Metall. Mater. Trans.33 A (2002) 1373. 10.1007/s11661-002-0062-0Suche in Google Scholar
[8] T.G.Langdon: Mater. Trans. JIM40 (1999) 716. 10.2320/matertrans1989.40.716Suche in Google Scholar
[9] Z.Horita, M.Furukawa, M.Nemoto, A.J.Barnes, T.G.Langdon: Acta Mater.48 (2000) 3633. 10.1016/S1359-6454(00)00182-8Suche in Google Scholar
[10] Z.Horita, M.Furukawa, M.Nemoto, T.G.Langdon: Mater. Sci. Technol.16 (2000) 1239. 10.1179/026708300101507091Suche in Google Scholar
[11] S.Komura, Z.Horita, M.Furukawa, M.Nemoto, T.G.Langdon: Metall. Mater. Trans.A32 (2001) 707. 10.1007/s11661-001-0087-9Suche in Google Scholar
[12] M.Kawasaki, R.B.Figueiredo, C.Xu, T.G.Langdon: Metall. Mater. Trans.A38 (2007) 1891. 10.1007/s11661-006-9000-xSuche in Google Scholar
[13] T.G.Langdon: J. Mater. Sci.42 (2007) 3388. 10.1007/s10853-006-1475-8Suche in Google Scholar
[14] E.Avtokratova, O.Sitdikov, M.Markushev, R.Mulyukov: Mater. Sci. Eng.A538 (2012) 386. 10.1016/j.msea.2012.01.041Suche in Google Scholar
[15] Z.Horita, T.G.Langdon: Scr. Mater.58 (2008) 1029. 10.1016/j.scriptamat.2008.01.043Suche in Google Scholar
[16] N.Tsuji, K.Shiotsuki, Y.Saito: Mater. Trans. JIM40 (1999) 765. 10.2320/matertrans1989.40.765Suche in Google Scholar
[17] R.S.Mishra, Z.Y.Ma: Mater. Sci. Eng. R50 (2005) 1. 10.1016/j.mser.2005.07.001Suche in Google Scholar
[18] R.S.Mishra, M.W.Mahoney, in: R.S.Mishra, M.W.Mahoney (Eds.) Friction Stir Welding and Processing, Materials Park, OH, ASM International (2007) 309.Suche in Google Scholar
[19] R.R.Sawtell, G.L.Jansen: Metall. Trans.A21 (1990) 421. 10.1007/BF02782422Suche in Google Scholar
[20] T.G.Nieh, L.M.Hsiung, J.Wadsworth, R.Kaibyshev: Acta Mater.46 (1998) 2789. 10.1016/S1359-6454(97)00452-7Suche in Google Scholar
[21] M.Furukawa, A.Utsunomiya, K.Matsubara, Z.Horita, T.L.Langdon: Acta Mater.49 (2001) 3829. 10.1016/S1359-6454(01)00262-2Suche in Google Scholar
[22] F.Musin, R.Kaibyshev, Y.Motohashi, G.Itoh: Metall. Mater. Trans.A35 (2004) 2383. 10.1007/s11661-006-0218-4Suche in Google Scholar
[23] A.Smolej, B.Skaza, V.Dragojević: J. Mater. Eng. Perform.19 (2010) 221. 10.1007/s11665-009-9450-6Suche in Google Scholar
[24] Z.Y.Ma, M.S.Mishra, M.W.Mahoney, R.Grimes: Mater. Sci. Eng.A351 (2003) 148. 10.1016/S0921-5093(02)00824-9Suche in Google Scholar
[25] S.Lee, A.Utsunomiya, H.Akamatsu, K.Neishi, M.Furukawa, Z.Horita, T.G.Langdon: Acta Mater.50 (2002) 553. 10.1016/S1359-6454(01)00368-8Suche in Google Scholar
[26] Y.Peng, Z.Yin, B.Nie, L.Zhong: Trans. Nonferr. Met. Soc. China17 (2007) 744. 10.1016/S1003-6326(07)60167-8Suche in Google Scholar
[27] A.Smolej, D.Klobčar, B.Skaza, A.Nagode, E.Slaček, V.Dragojević, S.Smolej: Mater. Sci. Eng.A590 (2014) 421. 10.1016/j.msea.2013.10.027Suche in Google Scholar
[28] Z.Y.Ma, F.C.Lui, R.S.Mishra: Acta Mater.58 (2010) 4693. 10.1016/j.actamat.2009.10.059Suche in Google Scholar
[29] W.M.Thomas, E.D.Nicholas, J.C.Needham, M.G.Murch, P.Templesmith, G.J.Dawes: GB Patent Application No. 9125978.8 (1991).Suche in Google Scholar
[30] F.C.Lui, Z.Y.Ma: Scr. Mater.58 (2008) 667. 10.1016/j.scriptamat.2007.11.044Suche in Google Scholar
[31] R.S.Mishra, M.W.Mahoney, S.X.McFadden, N.A.Mara, A.K.Mukherjee: Scr. Mater.42 (2000) 163. 10.1016/S1359-6462(99)00329-2Suche in Google Scholar
[32] Z.Y.Ma, R.S.Mishra, M.W.Mahoney: Acta Mater.50 (2002) 4419. 10.1016/S1359-6454(02)00261-6Suche in Google Scholar
[33] I.Charit, R.S.Mishra: Mater. Sci. Eng.A359 (2003) 290. 10.1016/S0921-5093(03)00367-8Suche in Google Scholar
[34] I.Charit, R.S.Mishra, M.W.Mahoney: Scr. Mater.47 (2002) 631. 10.1016/S1359-6462(02)00257-9Suche in Google Scholar
[35] S.Jana, R.S.Mishra, J.A.Baumann, G.Grant: Mater. Sci. Eng.A528 (2010) 189. 10.1016/j.msea.2010.08.049Suche in Google Scholar
[36] I.Charit, R.S.Mishra: Acta. Mater.53 (2005) 4211. 10.1016/j.actamat.2005.05.021Suche in Google Scholar
[37] M.A.Garcia-Bermal, R.S.Mishra, R.Verma, D.Hernándes-Silva: Scr. Mater.60 (2009) 850. 10.1016/j.scriptamat.2009.01.030Suche in Google Scholar
[38] I.Charit, R.S.Mishra: J. Mater. Res.19 (2004) 3329. 10.1557/JMR.2004.0429Suche in Google Scholar
[39] Z.Y.Ma, R.S.Mishra: Scr. Mater.53 (2005) 75. 10.1016/j.scriptamat.2005.03.018Suche in Google Scholar
[40] Z.Y.Ma, R.S.Mishra, M.W.Mahoney: Metall. Mater. Trans.A36 (2005) 1447. 10.1007/s11661-005-0237-6Suche in Google Scholar
[41] F.C.Lui, Z.Y.Ma, I.Q.Chen: Scr. Mater.60 (2009) 968. 10.1016/j.scriptamat.2009.02.021Suche in Google Scholar
[42] F.C.Lui, Z.Y.Ma: Scr. Mater.59 (2008) 882. 10.1016/j.scriptamat.2008.06.035Suche in Google Scholar
[43] R.S.Mishra: Adv. Mater. Process.162 (2004) 45.Suche in Google Scholar
[44] Z.Y.Ma, A.L.Pilchak, M.C.Juhas, J.C.Williams: Scr. Mater.58 (2008) 361. 10.1016/j.scriptamat.2007.09.009Suche in Google Scholar
[45] I.Charit, R.S.Mishra: Scr. Mater.58 (2008) 367. 10.1016/j.scriptamat.2007.09.052Suche in Google Scholar
[46] P.B.Barbon, S.Komura, A.Utsonomiya, Z.Horita, M.Furukawa, M.Nemoto, T.G.Langdon: Mater. Trans. JIM40 (1999) 772. 10.2320/matertrans1989.40.772Suche in Google Scholar
[47] Z.Y.Ma, R.S.Mishra: Acta Mater.51 (2003) 3551. 10.1016/S1359-6454(03)00173-3Suche in Google Scholar
[48] S.Fujikawa: J. Japan. Inst. Metals.49 (1999) 128. 10.2464/jilm.49.128Suche in Google Scholar
© 2014, Carl Hanser Verlag, München
Artikel in diesem Heft
- Contents
- Contents
- Original Contributions
- On the orientation dependence of grain boundary triple line energy in Cu
- Hydrogen storage kinetics of as-cast and spun (Mg24Ni10Cu2)100–xNdx (x = 0–20) alloys
- Segregation of phosphorus to ferrite grain boundaries during transformation in an Fe–P alloy
- A study on the pseudoelasticity of low temperature aged and thermomechanically treated Ti-51.5 at.% Ni shape memory alloy
- Experimental determination and thermodynamic calculation of the phase equilibria in the Co–Mn–Ta system
- 800°C isothermal section of the Co–Cr–Mo–Si quaternary system
- Phase fraction mapping in the as-cast microstructure of extrudable 6xxx aluminum alloys
- Effect of thixoforming on morphological changes in iron-bearing intermetallics and mechanical properties of Al–Si–Cu alloys
- The superplasticity of friction stir processed Al-5Mg alloy with additions of scandium and zirconium
- Short Communications
- Anti-corrosion behaviour of VE/GF coatings on mild steel
- Intermetallic phase stabilized Al/Pb metallic emulsion
- Synthesis of ultrafine powder (W,Ti)C by microwave heating in a stream of argon
- Fabrication and properties of porous silicon nitride ceramics via microwave sintering
- DGM News
- Personal
Artikel in diesem Heft
- Contents
- Contents
- Original Contributions
- On the orientation dependence of grain boundary triple line energy in Cu
- Hydrogen storage kinetics of as-cast and spun (Mg24Ni10Cu2)100–xNdx (x = 0–20) alloys
- Segregation of phosphorus to ferrite grain boundaries during transformation in an Fe–P alloy
- A study on the pseudoelasticity of low temperature aged and thermomechanically treated Ti-51.5 at.% Ni shape memory alloy
- Experimental determination and thermodynamic calculation of the phase equilibria in the Co–Mn–Ta system
- 800°C isothermal section of the Co–Cr–Mo–Si quaternary system
- Phase fraction mapping in the as-cast microstructure of extrudable 6xxx aluminum alloys
- Effect of thixoforming on morphological changes in iron-bearing intermetallics and mechanical properties of Al–Si–Cu alloys
- The superplasticity of friction stir processed Al-5Mg alloy with additions of scandium and zirconium
- Short Communications
- Anti-corrosion behaviour of VE/GF coatings on mild steel
- Intermetallic phase stabilized Al/Pb metallic emulsion
- Synthesis of ultrafine powder (W,Ti)C by microwave heating in a stream of argon
- Fabrication and properties of porous silicon nitride ceramics via microwave sintering
- DGM News
- Personal