Greener route for synthesis of cerium oxide and Fe-doped cerium oxide nanoparticles using acacia concinna fruit extract
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Sthitiprajna Muduli
Abstract
Nanomaterials have enabled extraordinary technical breakthroughs relative to bulk materials because of their unique properties. In this study, we have synthesized CeO2 and Ce1−xFe x O2 (x = 0.02, 0.04 and 0.06 w/w) nanoparticles by the sol–gel method using acacia concinna fruit extract. The crystallite size of 22.7 nm for CeO2 and varied from 32.47 nm to 62.95 nm for Fe-doped CeO2 nanoparticles as calculated from the X-ray diffraction pattern. Scanning electron microscope images showed a porous network-like morphology for both the samples. Fourier transform infrared spectroscopy showed a characteristic absorption band for Ce–O at 849 cm−1. Raman spectra indicated the vibrational mode of the cubic fluorite type structure of CeO2 nanoparticles at 464 cm−1. The specific surface area of CeO2 nanoparticles, was observed to be 58 m2 g−1, while that for 2%, 4%, and 6% Fe-doped CeO2 nanoparticles was 45 m2 g−1, 34 m2 g−1, 24 m2 g−1 respectively.
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Author contributions: All the authors have accepted responsibility for the entire content of this submitted manuscript and approved submission.
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Research funding: None declared.
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Conflict of interest statement: The authors declare no conflicts of interest regarding this article.
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© 2023 Walter de Gruyter GmbH, Berlin/Boston
Artikel in diesem Heft
- Frontmatter
- Review
- Preparations and applications of organic conducting polymers/graphene composites in heavy metal ion sensing: a review
- Original Papers
- Complex dielectric, electric modulus, impedance, and optical conductivity of Sr3−x Pb x Fe2TeO9 (x = 1.50, 1.88 and 2.17)
- Complex permittivity and predominance of non-overlapping small-polaron tunneling conduction process in copper indium selenide compound
- Effect of Bacillus and Pseudomonas biofilms on the corrosion behavior of AISI 304 stainless steel
- Fabrication of magnesium oxide nanoparticles using Eucalyptus tereticornis seed extract and their characterisation
- Greener route for synthesis of cerium oxide and Fe-doped cerium oxide nanoparticles using acacia concinna fruit extract
- Phase equilibria of Ni–Al–Pd and Ni–Cr–Pd ternary systems and Ni–Al–Cr–Pd quaternary system at 1423 K
- Effect of grain size on oxidation behaviour of Ag-20Cu-30Cr alloys in 0.1 MPa pure O2 at 700 and 800 °C
- News
- DGM – Deutsche Gesellschaft für Materialkunde
Artikel in diesem Heft
- Frontmatter
- Review
- Preparations and applications of organic conducting polymers/graphene composites in heavy metal ion sensing: a review
- Original Papers
- Complex dielectric, electric modulus, impedance, and optical conductivity of Sr3−x Pb x Fe2TeO9 (x = 1.50, 1.88 and 2.17)
- Complex permittivity and predominance of non-overlapping small-polaron tunneling conduction process in copper indium selenide compound
- Effect of Bacillus and Pseudomonas biofilms on the corrosion behavior of AISI 304 stainless steel
- Fabrication of magnesium oxide nanoparticles using Eucalyptus tereticornis seed extract and their characterisation
- Greener route for synthesis of cerium oxide and Fe-doped cerium oxide nanoparticles using acacia concinna fruit extract
- Phase equilibria of Ni–Al–Pd and Ni–Cr–Pd ternary systems and Ni–Al–Cr–Pd quaternary system at 1423 K
- Effect of grain size on oxidation behaviour of Ag-20Cu-30Cr alloys in 0.1 MPa pure O2 at 700 and 800 °C
- News
- DGM – Deutsche Gesellschaft für Materialkunde
