Zeitschrift für Kristallographie - New Crystal Structures

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Volume 218, Issue 3

February 2014

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Zeitschrift für Kristallographie - New Crystal Structures

Contents

Open Access
Refinement of the crystal structure of silver(I) thiocyanate, AgSCN

February 17, 2014

H.-L. Zhu, G.-F. Liu, F.-J Meng

Page range: 263-264

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AgCNS, monoclinic, C 12/ c 1 (No. 15), a = 8.792(5) Å, b = 7.998(5) Å, c = 8.207(5) Å, β= 93.75(1)°, V = 575.9 Å 3 , Z = 8, R gt (F) = 0.049, wR ref (F 2 ) = 0.086, T = 293 K.
Open Access
Crystal structure of Tutton’s salts, Rb₂[M^II(H2O)6](SeO4)2, MII = Mg, Co, Mn, Zn

February 17, 2014

H. Euler, B. Barbier, A. Meents, A. Kirfel

Page range: 265-268

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H 12 MgO 14 Rb 2 Se 2 , monoclinic, P 12 1 / a 1 (No. 14), a = 9.401(1) Å, b = 12.658(2) Å, c = 6.339(1) Å, β = 105.25(1)°, V = 727.8 Å 3 , Z = 2, R gt (F) = 0.020, wR ref (F 2 ) = 0.040, T = 293 K. CoH 12 O 14 Rb 2 Se2, monoclinic, P 12 1 / a 1 (No. 14), a = 9.363(1) Å, b = 12.618(1) Å, c = 6.3562(7) Å, β = 105.238(9)°, V = 724.5Å 3 , Z = 2, R gt (F) = 0.018, wR ref (F 2 ) = 0.037, T = 293 K. H 12 MnO 14 Rb 2 Se 2 , monoclinic, P 12 1 / a 1 (No. 14), a = 9.4496(8) Å, b = 12.760(1) Å, c = 6.3794(7) Å, β = 105.189(7)°, V = 742.4Å 3 , Z = 2, R gt (F) = 0.025, wR ref (F 2 ) = 0.056, T = 293 K. H 12 O 14 Rb 2 Se 2 Zn, monoclinic, P 12 1 / a 1 (No. 14), a = 9.352(1) Å, b = 12.626(2) Å, c = 6.360(1) Å, β = 105.195(8)°, V = 724.7 Å 3 , Z = 2, R gt (F) = 0.024, wR ref (F 2 ) = 0.048, T = 293 K.
Open Access
Crystal structure of ammonium triiodidomercurate(II) monohydrate, NH₄HgI₃ · H₂O

February 17, 2014

M. Loukil, A. Kabadou, I. Svoboda, A. B. Salah, H. Fuess

Page range: 269-270

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H 6 HgI 3 NO, monoclinic, C 1 c 1 (No. 9), a = 11.1235(9) Å, b = 9.8046(8) Å, c = 8.7430(8) Å, β = 90.185(7)°, V = 953.5Å 3 , Z = 4, R gt (F) = 0.033, wR ref (F 2 ) = 0.072, T = 299 K.
Open Access
Crystal structure of dicaesium oxopentachloromolybdate(V), Cs₂(MoOCl₅)

February 17, 2014

J.-X. Mi, X.-C. Feng, S.-Y. Mao, J.-T. Zhao, H. Zhang

Page range: 271-272

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Cl 5 Cs 2 MoO, cubic, Fm 3̅ m (No. 225), a = 10.2276(2) Å, V = 1069.8 Å 3 , Z =4, R gt (F) = 0.027, wR ref (F 2 ) = 0.058, T = 295K
Open Access
Crystal structure of lithium cadmium diaqua catena-[monoborodiphosphate]- monohydrate, LiCd(H₂O)₂[BP₂O₈] · H₂O

February 17, 2014

M.-H. Ge, J.-X. Mi, Y.-X. Huang, J.-T. Zhao, R. Kniep

Page range: 273-274

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BCdH 6 LiO 11 P 2 , hexagonal, P 6 5 (No. 170), a = 9.7111(6) , c = 16.012(1) Å, V = 1307.7 Å 3 , Z = 6, R gt (F) = 0.055, wR ref (F 2 ) = 0.126, T = 293 K.
Open Access
Crystal structure of sodium alumosilicate cyanide, Na₈[AlSiO₄]₆(CN)₂

February 17, 2014

Th. M. Gesing, J.-Ch. Buhl

Page range: 275-275

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Al 6 C 2 N 2 Na 8 O 24 Si 6 , cubic, P 4̅3 n (No. 218), a = 8.9192(1) Å, V = 709.5 Å 3 , Z = 1, R(P) = 0.036, R(I) = 0.020, T = 293 K.
Open Access
Crystal structure of dialuminum difluorotetraoxogermanate, Al₂GeO₄F₂

February 17, 2014

M. D. Mathews, A. K. Tyagi, J. Köhler

Page range: 276-276

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Al 2 F 2 GeO 4 , orthorhombic, Pnma (No. 62), a = 8.985(1) Å, b = 8.521(1) Å, c = 4.755(1) Å, V = 364.0 Å 3 , Z = 4, R(P) = 0.095, R(I) = 0.061, T = 295 K.
Open Access
Crystal structure of dieuropium trisulfate octahydrate, Eu₂(SO₄)₃ · 8H₂O

February 17, 2014

D.-Y. Wei, Y.-Q. Zheng

Page range: 277-278

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Eu 2 H 16 O 20 S 3 , monoclinic, C 12/ c 1 (No. 15), a = 13.555(2) Å, b = 6.757(1) Å, c = 18.317(2) Å, β = 102.27(1)°, V = 1639.4Å 3 , Z = 4, R gt (F) = 0.042, wR ref (F 2 ) = 0.105, T = 293 K.
Open Access
Crystal structure of trieuropium octacopper tetrastannide, Eu₃Cu₈Sn₄

February 17, 2014

M. L. Fornasini, P. Manfrinetti, D. Mazzone

Page range: 279-280

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Cu 8 Eu 3 Sn 4 , hexagonal, P 6 3 mc (No. 186), a = 9.251(2) Å, c = 7.801(1) Å, V = 578.2 Å 3 , Z = 2, R gt (F) = 0.026, wR all (F 2 ) = 0.062, T = 293 K.
Open Access
Crystal structure of dilanthanum pentaiodide, La₂I₅

February 17, 2014

Hj. Mattausch, O. Oeckler, A. Simon

Page range: 281-281

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I 5 La 2 , monoclinic, P 121/ m 1(No. 11), a = 8.618(2)Å, b = 4.4038(9)Å, c = 14.580(3) Å, β = 90.20(3)°, V = 553.3 Å 3 , Z = 2, R gt (F) = 0.026, wR ref (F 2 ) = 0.059, T = 293 K.
Open Access
Crystal structure of tetraterbium hexabromide monosilicide, Tb₄Br₆Si

February 17, 2014

Hj. Mattausch, O. Oeckler, A. Simon

Page range: 282-282

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Br 6 SiTb 4 , orthorhombic, Pbam (No. 55), a = 13.061(1) Å, b = 13.859(2) Å, c = 4.0407(4) Å, V = 731.4 Å 3 , Z = 2, R gt (F) = 0.029, wR ref (F 2 ) = 0.071, T = 293 K.
Open Access
Crystal structure of dekalanthanum tetrabromide pentaaluminide, La₁₀Br₄Al₅

February 17, 2014

Hj. Mattausch, O. Oeckler, A. Simon

Page range: 283-284

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Al 5 Br 4 La 10 , tetragonal, I 4/ mcm (No. 140), a = 8.2713(8) Å, c = 32.835(5) Å, V = 2246.4 Å 3 , Z = 4, R gt (F) = 0.027, wR ref (F 2 ) = 0.058, T = 293 K.
Open Access
Crystal structure of digadolinium(III) oxide disulfide, Gd₂OS₂

February 17, 2014

J. Wontcheu, Th. Schleid

Page range: 285-286

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Gd 2 OS 2 , monoclinic, P 12 1 / c 1 (No. 14), a = 8.3365(6) Å, b = 6.9872(5) Å, c = 6.9231(5) Å, β = 99.463(6)°, V = 397.8Å 3 , Z = 4, R gt (F) = 0.022, wR ref (F 2 ) = 0.047, T = 293 K.
Open Access
Crystal structure of pentacaesium hexacosatelluridopentazirconate, Cs₅Zr₅Te₂₆, a new polyanionic chalcogenometalate

February 17, 2014

N. A. Harringer, K. O. Klepp

Page range: 287-288

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Cs 5 Te 26 Zr 5 , monoclinic, P 12 1 / c 1 (No. 14), a = 19.39(2) Å, b = 9.548(2) Å, c = 28.06(5) Å, β = 98.51(5)°, V = 5137.7 Å 3 , Z = 4, R gt (F) = 0.045, wR ref (F) = 0.047, T = 294 K.
Open Access
Crystal structure of distrontium lithium magnesium trisilicide, Sr₂(Li_xMg_2-x)Si₃ (x = 1)

February 17, 2014

Q.-X. Xie, R. Nesper

Page range: 289-290

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LiMgSi 3 Sr 2 , orthorhombic, Cmcm (No. 63), a = 4.6179(5) Å, b = 19.488(2) Å, c = 7.1618(8) Å, V = 644.5 Å 3 , Z = 4, R gt (F) = 0.029, wR ref (F 2 ) = 0.063, T = 293 K.
Open Access
Crystal structure of sodium strontium monogermanide, Na_xSr₁_–xGe (x = 0.14)

February 17, 2014

Q.-X. Xie, R. Nesper

Page range: 291-292

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GeNa 0.14 Sr 0.86 , orthorhombic, Cmcm (No. 63), a = 4.828(1) Å, b = 11.309(3) Å, c = 4.124(1) Å, V = 225.2 Å 3 , Z = 4, R gt (F) = 0.049, wR ref (F 2 ) = 0.115, T = 293 K.
Open Access
Refinement of the crystal structure of zirconium tritellurate(IV), ZrTe₃O₈

February 17, 2014

O. Noguera, P. Thomas, O. Masson, J.-C. Champarnaud-Mesjard

Page range: 293-294

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O 8 Te 3 Zr, cubic, Ia 3̅ (No. 206), a = 11.308(1) Å, V = 1446.0Å 3 , Z = 8, ρ m = 5.50(3) g·cm -3 , R gt (F) = 0.024, wR ref (F 2 ) = 0.049, T = 293 K.
Open Access
Crystal structure of tetraaquasamarium(III) tri(2-chlorofumarate) hexahydrate, Sm₂(COOCHCClCOO)₃(H₂O)₄ · 6H₂O, with two-dimensional net structure

February 17, 2014

M.-G. Zhao, J.-M. Shi, W.-T. Yu

Page range: 295-296

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C 12 H 23 Cl 3 O 22 Sm 2 , triclinic, P 1 (No. 2), a = 8.877(3) Å, b = 9.413(3) Å, c = 9.554(3) Å, α = 103.778(5)°, β = 101.31 (5)°, ϒ = 93.954(5)°, V = 754.7 Å 3 , Z = 1, R gt (F) = 0.056, wR ref (F 2 ) = 0.152, T = 293 K.
Open Access
Crystal structure of nitratodi(1,3-propanediamine)cobalt(II) mononitrate monohydrate, [Co(C₃H₁₀N₂)₂(NO₃)]NO₃ · H₂O

February 17, 2014

C.-Q. Liu, J.-M. Shi, C.-J. Wu

Page range: 297-298

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C 6 H 22 CoN 6 O 7 , monoclinic, P 12 1 / c 1 (No. 14), a = 8.76(1) Å, b = 10.22(1) Å, c = 15.83(2) Å, β = 93.45(2)°, V = 1414.3 Å 3 , Z = 4, R gt (F) = 0.053, wR ref (F 2 ) = 0.131, T = 293 K.
Open Access
Crystal structure of diaqua-bis[N-(2-pyridyl)carbonylaniline]copper(II) diperchlorate, Cu(C₁₂H₁₆N₂O)₂(H₂O)₂(ClO₄)₂, at 120K

February 17, 2014

A. Ramazani, A. Morsali

Page range: 299-300

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C 24 H 24 Cl 2 CuN 4 O 12 , monoclinic, P 12 1 / n 1 (No. 14), a = 8.245(2) Å, b = 11.852(2) Å, c = 14.882(3) Å, β = 104.927(4)°, V = 1405.2 Å 3 , Z = 2, R gt (F) = 0.051, wR ref (F 2 ) = 0.132, T = 120 K.
Open Access
Crystal structure of 1,2-ethylenediaminesilver(I) bis(4-nitrobenzoato)- silver(I), C₁₆H₁₆Ag₂N₄O₈

February 17, 2014

S.-H. Chen, H.-L. Zhu, Y.-J. Pan, X.-J. Wang, D.-Q. Wang

Page range: 301-302

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C 16 H 16 Ag 2 N 4 O 8 , triclinic, P 1̅ (No. 2), a = 6.346(3) Å, b = 7.022(3) Å, c = 23.04(1) Å, α = 82.638(7)°, β = 83.169(6)°, ϒ = 67.880(6)°, V = 940.6 Å 3 , Z = 2, R gt (F) = 0.031, wR ref (F 2 ) = 0.070, T = 298 K.
Open Access
Crystal structure of 1,2-diaminopropanesilver(I) 3,5-dinitrobenzoate hydrate, Ag(C₃H₁₀N₂)(C₇H₃N₂O₆) · 1.5H₂O

February 17, 2014

H.-L. Zhu, X.-J. Wang, Y.-J. Pan, D.-Q. Wang

Page range: 303-304

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C 10 H 16 AgN 4 O 7.50 , monoclinic, C 12/ c 1 (No. 15), a = 28.123(8) Å, b = 5.241(2) Å, c = 24.723(7) Å, β = 122.958(4)°, V = 3057.9Å 3 , Z = 8, R gt (F) = 0.037, wR ref (F 2 ) = 0.070, T = 298 K.
Open Access
Crystal structure of ethylenediaminesilver(I) di(3,5-dinitrobenzoato)- silver(I) dihydrate, Ag₂(C₂H₈N₂)(C₇H₃N₂O₆)₂ · 2H₂O

February 17, 2014

H.-L. Zhu, X.-J. Sun, X.-J. Wang, D.-Q. Wang

Page range: 305-306

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C 16 H 18 Ag 2 N 6 O 14 , triclinic, P 1̅ (No. 2), a = 6.978(2) Å, b = 12.919(5) Å, c = 15.029(5) Å, α = 84.320(6)°, β = 76.81 (5)°, ϒ = 79.612(6)°, V = 1295.1 Å 3 , Z = 2, R gt (F) = 0.065, wR ref (F 2 ) = 0.091, T = 298 K.
Open Access
Crystal structure of ethylenediaminesilver(I) perchlorate, C₂H₈N₂Ag(ClO₄)

February 17, 2014

H.-L. Zhu, X.-M. Zhang, Q. Yu, D.-Q. Wang

Page range: 307-308

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C 2 H 8 AgClN 2 O 4 , monoclinic, P 12 1 / n 1 (No. 14), a = 8.676(3) Å, b = 9.869(3) Å, c = 8.822(3) Å, β = 111.240(4)°, V = 704.1 Å 3 , Z = 4, R gt (F) = 0.032, wR ref (F 2 ) = 0.063, T = 293 K.
Open Access
Crystal structure of 1,2-diaminopropanesilver(I) 3,5-dinitrobenzoate — ammonia (1:1), Ag(C₃H₁₀N₂)(C₇H₃N₂O₆) · NH₃

February 17, 2014

H.-L. Zhu, X.-M. Zhang, X.-J. Wang, D.-Q. Wang

Page range: 309-310

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C 10 H 16 AgN 5 O 6 , triclinic, P 1̅ (No. 2), a = 5.640(5)Å, b = 9.499(8)Å, c = 14.84(2) Å, α = 84.24(1)°, β = 79.05(2)°, ϒ = 2.731(8)°, V = 744.8 Å 3 , Z = 2, R gt (F) = 0.044, wR ref (F 2 ) = 0.111, T = 298 K.
Open Access
Crystal structure of dinitrato-dimethanol-bis[N-(2-aminopropyl)- salicylaldiminato]dicadmium(II), Cd₂(C₁₀H₁₃N₂O)₂(NO₃)2(CH₃OH)₂

February 17, 2014

D.-S. Xia, Y.-F. Wang, W.-J. Liu, D.-Q. Wang, H.-L. Zhu

Page range: 311-312

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C 22 H 34 Cd 2 N 6 O 10 , triclinic, P 1̅ (No. 2), a = 7.832(2) Å, b = 9.275(3) Å, c = 10.497(3) Å, α = 85.445(4)°, β = 71.174(4)°, ϒ = 88.390(4)°, V = 719.4 Å 3 , Z = 1, R gt (F) = 0.041, wR ref (F 2 ) = 0.113, T = 293 K.
Open Access
Crystal structure of diaqua-di(2-methoxyacetato)cobalt(II), C₆H₁₄CoO₈

February 17, 2014

H.-L. Zhu, Q.-F. Zeng, D.-S. Xia, X. Liu, X.-L. Zhu, D.-Q. Wang

Page range: 313-314

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C 6 H 14 CoO 8 , monoclinic, P 12 1 / n 1 (No. 14), a = 6.985(1) Å, b = 10.102(2) Å, c = 7.132(1) Å, β = 97.15(1)°, V = 499.3 Å 3 , Z = 2, R gt (F) = 0.028, wR ref (F 2 ) = 0.072, T = 292 K.
Open Access
Crystal structure of diaqua-di(2-methoxyacetato)copper(II), C₆H₁₄CuO₈

February 17, 2014

H.-L. Zhu, Q.-F. Zeng, D.-S. Xia, X.-L. Zhu, X. Liu, D.-Q. Wang

Page range: 315-316

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C 6 H 14 CuO 8 , monoclinic, P 12 1 / n 1 (No. 14), a = 6.955(1) Å, b = 10.123(2) Å, c = 7.226(1) Å, β = 96.57(1)°, V = 505.4 Å 3 , Z = 2, R gt (F) = 0.026, wR ref (F 2 ) = 0.069, T = 292 K.
Open Access
Crystal structure of 4-di(2-pyridinoamino)methylbenzaldehyde, C₁₈H₁₆N₄O

February 17, 2014

H.-L. Zhu, Q.-X. Liu, A. Usman, H.-K. Fun

Page range: 317-318

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C 18 H 16 N 4 O, monoclinic, P 12 1 / c 1 (No. 14), a = 10.7420(6) Å, b = 12.7228(7)Å, c = 11.8769(7)Å, β = 105.495(1)°, V = 1564.2Å 3 , Z = 4, R gt (F) = 0.045, wR ref (F 2 ) = 0.125, T = 298 K.
Open Access
Crystal structure of bis(diaquamanganese(II))hexaacetatomanganese(II) octahydrate, ((H₂O)₂Mn)₂(C₂H₃O₂)₆Mn · 8H₂O

February 17, 2014

S.-Y. Li, Y.-H. Li, H.-L. Liu, H.-L. Zhu, D.-Q. Wang

Page range: 319-320

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C 12 H 42 Mn 3 O 24 , monoclinic, P 12 1 / c 1 (No. 14), a = 10.409(8) Å, b = 17.52(1) Å, c = 9.059(7) Å, β = 110.93(1)°, V = 1543.3 Å 3 , Z = 2, R gt (F) = 0.032, wR ref (F 2 ) = 0.089, T = 298 K.
Open Access
Crystal structure of µ₂-hydroxyl-bis(5-methyl-1,4,9-triazanonanezinc(II)) triperchlorate, C₁₄H₃₉Cl₃N₆O₁₃Zn₂

February 17, 2014

H.-L. Zhu, F.-J. Meng, F. Yang, Z.-D. Wang

Page range: 321-322

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C 14 H 39 Cl 3 N 6 O 13 Zn 2 , monoclinic, P 12 1 / m 1 (No. 11), a = 7.802(2) Å, b = 12.121(3) Å, c = 15.662(3)Å, β = 104.29(2)°, V = 1435.3 Å 3 , Z =2, R gt (F) = 0.055, wR ref (F 2 ) = 0.152, T = 293 K.
Open Access
Crystal structure of 4,5-(ethoxyethylenedithio)-1,3-dithiole-2-thione, C₇H₈OS₅

February 17, 2014

G. Xue, W.-T. Yu, Q. Fang

Page range: 323-324

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C 7 H 8 OS 5 , monoclinic, P 12 1 / c 1 (No. 14), a = 8.3699(7) Å, b = 17.573(2) Å, c = 7.5305(7) Å, β = 103.584(7)°, V = 1076.6 Å 3 , Z =4, R gt (F) = 0.033, wR ref (F 2 ) = 0.082, T = 293 K.
Open Access
Crystal structure of tetra-n-butylammonium (1,3-dithiol-2-thione-4,5-dithiolato)-( diethyldithiocarbamato-S,S')-nickelate(II), (C₁₆H₃₆N)(C₈H₁₀NNiS₇)

February 17, 2014

W. Xu, Q. Fang, G. Xue, W.-T. Yu

Page range: 325-327

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C 24 H 46 N 2 NiS 7 , monoclinic, C 1 c 1 (No. 9), a = 8.846(2) Å, b = 24.702(6) Å, c = 15.392(3) Å, β = 95.12(1)°, V = 3349.9Å 3 , Z = 4, R gt (F) = 0.059, wR ref (F 2 ) = 0.166, T = 293 K.
Open Access
Crystal structure of 5,19-bis(acetyloxy)-13-deoxy-10-deoxy-20- (ethylthio)-2,20-dihydro-(2α,5β,19R)-enmein, C₂₈H₃₈O₁₀S

February 17, 2014

Y.-W. Guo, J.-L. Yu, J. Sun

Page range: 328-330

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C 28 H 38 O 10 S, orthorhombic, P 2 1 2 1 2 1 (No. 19), a = 9.1243(6) Å, b = 9.3896(7) Å, c = 33.962(2) Å, V = 2909.6 Å 3 , Z = 4, R gt (F) = 0.058, wR ref (F 2 ) = 0.149, T = 293 K.
Open Access
Crystal structure of 1,1,5,5-tetramethyl-1,2,5,6-tetrahydro-3a,4,7a,8-tetraaza- s-indacene-3,7-dione, C₁₂H₁₆N₄O₂

February 17, 2014

A. Mrozek, J. Karolak-Wojciechowska, K. Wejroch, J. Lange

Page range: 331-332

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C 12 H 16 N 4 O 2 , monoclinic, P 12 1 / c 1 (No. 14), a = 9.306(2) Å, b = 5.755(1) Å, c = 11.499(2) Å, β = 98.15(3)°, V = 609.6 Å 3 , Z = 2, R gt (F) = 0.045, wR ref (F 2 ) = 0.075, T = 294 K.
Open Access
Crystal structure of diaqua-(2-carboxyethylene-8-hydroxyquinolinato)- copper(II) monohydrate, Cu(C₁₂H₉O₃N)(H₂O)₂ · H₂O

February 17, 2014

J.-I. Tanaka, K. Itoh, J.-I. Setsune

Page range: 333-334

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C 12 H 15 CuNO 6 , triclinic, P 1̅ (No. 2), a = 7.363(2) Å, b = 8.985(2) Å, c = 10.349(2) Å, α = 97.438(4)°, β = 100.846(4)°, ϒ = 106.334(4)°, V = 633.1 Å 3 , Z = 2, R gt (F) = 0.029, wR obs (F 2 ) = 0.073, T = 298 K
Open Access
Crystal structure of 1,2-bis(salicylideneiminato)propanechromium(III) nitrate, C₁₇H₂₀CrN₃O₇

February 17, 2014

H.-L. Zhu, X. Liu, X.-L. Zhu, D.-Q. Wang

Page range: 335-336

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C 17 H 20 CrN 3 O 7 , monoclinic, C 12/ c 1 (No. 15), a = 18.905(7) Å, b = 13.915(5) Å, c = 14.822(6) Å, β = 97.246(7)°, V = 3868.0Å 3 , Z = 8, R gt (F) = 0.052, wR ref (F 2 ) = 0.125, T = 298 K.
Open Access
Crystal structure of pimolin, C₂₆H₂₀O₈

February 17, 2014

A. Pal, P. Pradhan, A. Banerji, T. P. Singh

Page range: 337-338

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C 26 H 20 O 8 , triclinic, P ̅1̅ (No. 2), a = 9.002(2) Å, b = 9.140(2) Å, c = 14.501(3) Å, α = 104.90(3)°, β = 95.34(3)°, ϒ = 113.83(3)°, V = 1028.2Å 3 , Z = 2, R gt (F) = 0.074, wR ref (F 2 ) = 0.250, T = 293 K.
Open Access
Crystal structure of bis(2-pyrimidylthio)methane, C₉H₈N₄S₂

February 17, 2014

L.-H. Liu, Y.-S. Fu, Q.-F. Zhang

Page range: 339-340

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C 9 H 8 N 4 S 2 , monoclinic, P 12/ c 1 (No. 13), a = 18.757(4) Å, b = 3.9876(8) Å, c = 14.668(3) Å, β = 112.15(3)°, V = 1016.1 Å 3 , Z = 4, R gt (F) = 0.030, wR ref (F 2 ) = 0.080, T = 100 K.
Open Access
Crystal structure of 4,4'-bipyridin-1-ium bi(trihydrogen- 1,2,4,5-benzenetetracarboxylate), C₃₀H₂₀N₂O₁₆

February 17, 2014

N.-W. Zhu, R.-Q. Zhang, T.-H. Sun

Page range: 341-342

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C 30 H 20 N 2 O 16 , monoclinic, C 12/ c 1 (No. 15), a = 12.021(6) Å, b = 15.469(7) Å, c = 15.436(7) Å, β = 110.806(7)°, V = 2683.2Å 3 , Z = 4, R gt (F) = 0.063, wR ref (F 2 ) = 0.143, T = 298 K.
Open Access
Crystal structure of bis(1-phenylimidazolium) tetrachlorocuprate(II), (C₉H₉N₂)₂(CuCl₄)

February 17, 2014

U. Casellato, R. Ettorre, R. Graziani

Page range: 343-344

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C 18 H 18 Cl 4 CuN 4 , monoclinic, C 121 (No. 5), a = 14.109(3) Å, b = 10.263(2) Å, c = 15.290(3) Å, β = 102.61(3)°, V = 2160.6Å 3 , Z = 4, R gt (F) = 0.040, wR all (F 2 ) = 0.124, T = 293 K.
Open Access
Crystal structure of trans-diaqua-di(bis(pyrazolylmethane)copper(II) dinitrate, Cu(C₇H₁₀N₄)₂(OH₂)₂(NO₃)₂

February 17, 2014

K. A. Van Langenberg, B. Moubaraki, K. S. Murray, E. R. T. Tiekink

Page range: 345-346

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C 14 H 20 CuN 10 O 8 , triclinic, P 1̅ (No. 2), a = 8.498(1) Å, b = 9.167(2) Å, c = 8.323(3) Å, α = 103.41(3)°, β = 101.87(3)°, ϒ = 117.10(1)°, V = 523.9 Å 3 , Z = 1, R gt (F) = 0.041, wR ref (F 2 ) = 0.122, T = 293 K.
Open Access
Crystal structure of N-(2-(aminoethyl)pyridyl)(salicylaldiminato)- copper(II) perchlorate dimer, [Cu(C₁₄H₁₃N₂O)]₂(ClO₄)₂

February 17, 2014

M. Burns, B. Moubaraki, E. R. T. Tiekink

Page range: 347-348

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C 14 H 13 ClCuN 2 O 5 , monoclinic, P 12 1 / n 1 (No. 14), a = 9.559(2) Å, b = 11.024(2) Å, c = 14.397(4) Å, β = 104.75(2)°, V = 1467.1Å 3 , Z = 4, R gt (F) = 0.034, wR ref (F 2 ) = 0.089, T = 293 K.
Open Access
Crystal structure of μ₂-oxo-bis-μ₂-formato-bis(tris(pyrazolyl)- methane)diiron(III) perchlorate, C₂₂H₂₂Cl₂Fe₂N₁₂O₁₃

February 17, 2014

B. Moubaraki, K. S. Murray, E. R. T. Tiekink

Page range: 349-350

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C 11 H11ClFeN 6 O 6.50 , orthorhombic, Pnnm (No. 58), a = 12.733(6) Å, b = 15.315(9) Å, c = 16.260(5) Å, V = 3170.8Å 3 , Z = 8, R gt (F) = 0.058, wR ref (F 2 ) = 0.200, T = 293 K.
Open Access
Crystal structure of [bis-tris(pyrazolyl)methanecopper(II)] [chlorobis( η2-benzoato)-η¹-benzoato-manganate(II)] hydrate, Cu(C₁₀H₁₀N₆)Mn(C₇H₅O₂)₃Cl · H₂O

February 17, 2014

B. Moubaraki, K. S. Murray, Tiekink

Page range: 351-353

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C 41 H 37 ClCuMnN 12 O 7 , monoclinic, P 12 1 / n 1 (No. 14), a = 15.946(3) Å, b = 13.26(2) Å, c = 20.766(5) Å, β = 106.49(2)°, V = 4209.3 Å 3 , Z = 4, R gt (F) = 0.060, wR ref (F 2 ) = 0.155, T = 293 K.
Open Access
Crystal structure of [bis-tris(pyrazolyl)methanecobalt(II)] [chlorobis( η²-benzoato)-η¹-benzoato-manganate(II)] hydrate, Co(C₁₀H₁₀N₆)Mn(C₇H₅O₂)₃Cl · H₂O

February 17, 2014

B. Moubaraki, K. S. Murray, E. R. T. Tiekink

Page range: 354-356

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C 41 H 37 ClCoMnN 12 O 7 , monoclinic, P 12 1 / n 1 (No. 14), a = 16.024(5) Å, b = 13.23(1) Å, c = 20.833(4) Å, β = 106.54(2)°, V = 4233.8Å3, Z = 4, R gt (F) = 0.054, wR ref (F 2 ) = 0.138, T = 293 K.
Open Access
Crystal structure of di-μ₂-benzoato-di-[tris(pyrazolyl)methane-aquamanganese( II)] benzoate, C₂₄H₂₂N₆MnO₅

February 17, 2014

B. Moubaraki, K. S. Murray, E. R. T. Tiekink

Page range: 357-358

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C 24 H 22 MnO 5 N 6 , triclinic, P 1̅ (No. 2), a = 11.126(1) Å, b = 12.953(1) Å, c = 9.0895(9) Å, α = 109.241(8)°, β = 102.835(8)°, ϒ = 71.273(8)°, V = 1161.3 Å 3 , Z = 2, R gt (F) = 0.042, wR ref (F 2 ) = 0.136, T = 293 K.
Open Access
Crystal structure of meso-dimethyl 2,3-dibenzamido-2,3-dimethylbutanedioate, C₂₂H₂₄N₂O₆

February 17, 2014

D. R. Coghlan, C. J. Easton, E. R. T. Tiekink

Page range: 359-360

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C 22 H 24 N 2 O 6 , monoclinic, P 12 1 / n 1 (No. 14), a = 14.455(3) Å, b = 10.239(2) Å, c = 14.991(5) Å, β = 101.01(2)°, V = 2177.9Å 3 , Z = 4, R gt (F) = 0.068, wR ref (F 2 ) = 0.244, T = 293 K.
Open Access
Crystal structure of dl-dimethyl 2,3-dibenzamido-2,3-dimethylbutanedioate, C₂₂H₂₄N₂O₆

February 17, 2014

D. R. Coghlan, C. J. Easton, E. R. T. Tiekink

Page range: 361-362

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C 22 H 24 N 2 O 6 , monoclinic, P 12 1 / c 1 (No. 14), a = 10.982(2) Å, b = 9.440(1) Å, c = 10.375(3) Å, β = 111.06(1)°, V = 1003.7Å 3 , Z = 2, R gt (F) = 0.074, wR ref (F 2 ) = 0.222, T = 293 K.
Open Access
Crystal structure of 3-(2,6-dichlorophenyl)-6,7-dihydro-4Hpyrano[ 3,4-d]isoxazol-4-one, C₁₂H₇Cl₂NO₃

February 17, 2014

C. M. M. Hughes, E. R. T. Tiekink, C. J. Easton

Page range: 363-364

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C 12 H 7 Cl 2 NO 3 , monoclinic, P 12 1 / c 1 (No. 14), a = 13.518(1) Å, b = 5.987(1) Å, c = 14.3838(8) Å, β = 99.736(5)°, V = 1147.4Å 3 , Z = 4, R gt (F) = 0.039, wR ref (F 2 ) = 0.110, T = 293 K.
Open Access
Crystal structure of 3-(2,6-dichlorophenyl)-4,5-dihydro-7Hpyrano[ 4,3-d]isoxazol-7-one, C₁₂H₇Cl₂NO₃

February 17, 2014

C. J. Easton, C. M. M. Hughes, E. R. T. Tiekink

Page range: 365-366

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C 12 H 7 Cl 2 NO 3 , monoclinic, P 12 1 / n 1 (No. 14), a = 7.499(4) Å, b = 14.450(4) Å, c = 21.559(3) Å, β = 96.89(2)°, V = 2319.3Å 3 , Z = 8, R gt (F) = 0.054, wR ref (F 2 ) = 0.134, T = 293 K.
Open Access
Crystal structure of di(3,5-dinitrobenzoato-O,O')tetra(μ-3,5- dinitrobenzoato-O,O') di(1,10-phenanthroline-N,N')dieuropium(III), Eu₂(C₇H₃N₂O₆)₆(C₁₂H₈N₂)₂

February 17, 2014

M.-L. Hu, X.-H. Li, H.-P. Xiao

Page range: 367-369

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C 66 H 34 Eu 2 N 16 O 36 , monoclinic, P 12 1 / n 1 (No. 14), a = 11.889(2) Å, b = 22.660(4) Å, c = 13.491(2) Å, β = 101.710(2)°, V = 3558.9Å 3 , Z = 2, R gt (F) = 0.029, wR ref (F 2 ) = 0.064, T = 293 K.
Open Access
Crystal structure of di[K(18-crown-6)]dirubidium nonagermanide(4–) diethylenediamine, [K(C₁₂H₂₆N₂O₄)]₂Rb₂[Ge₉] · 2C₂N₂H₈

February 17, 2014

R. Hauptmann, T. F. Fässler

Page range: 370-372

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C 28 H 68 Ge 9 K 2 N 8 O 8 Rb 2 , monoclinic, P 12 1 / c 1 (No. 14), a = 16.864(3) Å, b = 12.091(2) Å, c = 26.466(5) Å, β = 97.28(3)°, V = 5353.0Å3, Z = 4, R gt (F) = 0.058, wR ref (F 2 ) = 0.176, T = 153 K.

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