Volume 218, Issue 2

BiKP 2 S 6 , monoclinic, P 12 1 1 (No. 4), a = 6.6200(6) Å, b = 7.4058(7) Å, c = 9.9002(9) Å, β = 92.108(1)°, V = 485.0Å 3 , Z = 2, R gt (F) = 0.027, wR ref (F 2 ) = 0.060, T = 293 K.

C 12 H 36 Li 4 N 8 Si 2 , monoclinic, C 12/ c 1 (No. 15), a = 19.468(4) Å, b = 12.870(3) Å, c = 20.568(4) Å, β = 117.88(3)°, V = 4555.3Å 3 , Z = 8, R gt (F) = 0.052, wR ref (F 2 ) = 0.148, T = 293 K.

B 2 Hg 3 O 6 , trigonal, R 3 c (No. 167), a = 8.8936(9) Å, c = 13.052(3) Å, V = 894.1 Å3, Z = 6, R gt (F) = 0.021, wR ref (F 2 ) = 0.053, T = 293 K.

C 14 H 28 MnN 6 O 4 S 2 , triclinic, P 1 (No. 2), a = 7.27(2) Å, b = 9.55(2) Å, c = 9.68(2) Å, α = 82.12(3)°, β = 68.90(3)°, = 67.61(2)°, V = 580.0 Å 3 , Z = 1, R gt (F) = 0.069, wR ref (F 2 ) = 0.190, T = 298 K.

B 6 ErTa 0.23 V 1.77 , orthorhombic, Pbam (No. 55), a = 11.280(2) Å, b = 8.940(2) Å, c = 3.390(1) Å, V = 341.9 Å 3 , Z = 4, R gt (F) = 0.034, wR obs (F) = 0.034, T = 293 K.

CeNi 10 P 4 , orthorhombic, Pnma (No. 62), a = 9.263(1) Å, b = 3.6654(5) Å, c = 22.092(3) Å, V = 750.1 Å3, Z = 4, R gt (F) = 0.030, wR ref (F 2 ) = 0.068, T = 293 K.

CrN 4 Sr 3 , orthorhombic, Pbca (No. 61), a = 10.199(1) Å, b = 9.566(1) Å, c = 11.169(2) Å, V = 1089.6 Å 3 , Z = 8, R(P) = 0.082, R(I) = 0.053, T = 293 K.

C 6 H 24 FeI 2 O 6 , trigonal, P 3(No. 147), a = 8.2947(8)Å, c = 7.0884(6)Å, V = 422.4Å 3 , Z = 1, R gt (F) = 0.023, wR ref (F 2 ) = 0.065, T = 193 K.

BCdH 6 NaO 10.8 P 2 , hexagonal, P 6 1 22 (No. 178), a = 9.713(1) Å, c = 16.136(3) Å, V = 1318.4 Å 3 , Z = 6, R gt (F) = 0.047, wR ref (F 2 ) = 0.105, T = 273 K.

CsGaHO 10 P 3 , monoclinic, C 121 (No. 5), a = 9.061(1) Å, b = 8.7105(9) Å, c = 6.2195(8) Å, β = 111.993(6) 0 , V = 455.2 Å 3 , Z = 2, R gt (F) = 0.018, wR ref (F 2 ) = 0.046, T = 295 K.

CsGaHO 10 P 3 , monoclinic, P 12 1 / n 1 (No. 13), a = 8.843(1) Å, b = 4.9523(5) Å, c = 11.084(1) Å, β = 108.793(6) 0 , V = 459.5 Å 3 , Z = 2, R gt (F) = 0.042, wR ref (F 2 ) = 0.123, T = 295 K.

BCsGaHO 9 P 2 , monoclinic, P 12 1 / c 1 (No. 14), a = 9.259(1) Å, b = 8.6462(9) Å, c = 9.615(1) Å, = 103.059(6) 0 , V = 749.8 Å 3 , Z = 4, R gt (F) = 0.050, wR ref (F 2 ) = 0.104, T = 295 K.

B 8 Si 1.87 Y 5 , tetragonal, P 4/ mbm (No. 127), a = 7.2234(2) Å, c = 8.0961(3) Å, V = 422.4 Å 3 , Z = 2, R gt (F) = 0.040, wR ref (F 2 ) = 0.095, T = 293 K.

C 16 H 15 NO, monoclinic, P 12 1 / a 1 (No. 14), a = 7.085(1) Å, b = 18.587(3) Å, c = 9.080(2) Å, β = 95.30(2) 0 , V = 1190.5 Å 3 , Z = 4, R gt (F) = 0.068, wR ref (F 2 ) = 0.239, T = 293 K.

C 27 H 43 N 3 O 7 , orthorhombic, P 2 1 2 1 2 (No. 18), a = 12.202(1) Å, b = 27.790(1) Å, c = 9.128(1) Å, V = 3095.2 Å 3 , Z = 4, R gt (F) = 0.054, wR ref (F 2 ) = 0.180, T = 293 K.

C 20 H 27 NO 4 , monoclinic, P 12 1 1 (No. 4), a = 12.689(6) Å, b = 7.539(2) Å, c = 19.490(3) Å, β = 105.87(3) 0 , V = 1793.4 Å 3 , Z = 4, R gt (F) = 0.032, wR ref (F 2 ) = 0.081, T = 218 K.

C 66 H 54 Fe 6 , monoclinic, P 12 1 / c 1 (No. 14), a = 12.4201(4) Å, b = 20.0247(6)Å, c = 19.8328(3) Å, β = 93.054(2) 0 , V = 4925.6 Å 3 , Z = 4, R gt (F) = 0.039, wR ref (F 2 ) = 0.074, T = 223 K.

C 41 H 56 Br 2 N 2 Ni, orthorhombic, P 212 1 2 1 (No. 19), a = 10.121(2) Å, b = 17.115(2) Å, c = 22.835(2) Å, V = 3955.5 Å 3 , Z = 4, R gt (F) = 0.037, wR ref (F 2 ) = 0.086, T = 218 K.

C 24 H 16 N 6 O 5.50 Pb, triclinic, P 1 (No. 2), a = 7.805(2) Å, b = 11.332(2) Å, c = 13.184(3) Å, α = 94.934(3) 0 , β = 99.471(3) 0 , γ = 101.504(3) 0 , V = 1118.6 Å 3 , Z = 2, R gt (F) = 0.028, wR ref (F 2 ) = 0.066, T = 110 K.

C 22 H 32 Cl 2 N 4 O 4 , triclinic, P 1 (No. 2), a = 7.081(1) Å, b = 13.247(3) Å, c = 13.923(3) Å, α = 102.90(3) 0 , β = 96.90(3) 0 , γ = 98.36(3) 0 , V = 1243.7 Å 3 , Z = 2, R gt (F) = 0.066, wR ref (F 2 ) = 0.241, T = 293 K.

C 24 H 28 F 3 N 3 O 6 , monoclinic, P 12 1 / c 1 (No. 14), a = 9.677(4) Å, b = 11.005(5) Å, c = 24.858(7) Å, β = 92.12 0 , V = 2645.5 Å 3 , Z = 4, R gt (F) = 0.064, wR ref (F 2 ) = 0.199, T = 293 K.

C 10 H 10 Cl 2 CuN 2 , monoclinic, P 12 1 / n 1 (No. 14), a = 3.7911(2) Å, b = 8.5205(3) Å, c = 16.9910(7) Å, β = 91.973(3)°, V = 548.5 Å 3 , Z = 2, R gt (F) = 0.033, wR ref (F 2 ) = 0.086, T = 100 K.

C 25 H 50 N 5 Ta, monoclinic, P 12 1 / c 1 (No. 14), a = 15.3542(9) Å, b = 9.9150(6) Å, c = 18.141(1) Å, β = 108.109(1)°, V = 2624.9 Å 3 , Z = 4, R gt (F) = 0.053, wR ref (F 2 ) = 0.142, T = 100 K.

C 12 H 32 N 4 Si, monoclinic, C 121 (No. 5), a = 19.041(4) Å, b = 5.211(1) Å, c = 9.187(2) Å, β = 111.60(2)°, V = 847.6 Å 3 , Z = 2, R gt (F) = 0.051, wR ref (F 2 ) = 0.061, T = 293 K.

C 38 H 24 O, monoclinic, P 121/ n 1 (No. 14), a = 10.737(2) Å, b = 16.963(3) Å, c = 15.246(3) Å, β = 109.30(3)°, V = 2620.8 Å 3 , Z = 4, R gt (F) = 0.088, wR ref (F 2 ) = 0.252, T = 293 K.

C 22 H 44 N 2 NiS 4 , monoclinic, P 121/ n 1 (No. 14), a = 10.402(2) Å, b = 13.261(3) Å, c = 10.701(2) Å, β = 114.79(3)°, V = 1340.1 Å 3 , Z = 2, R gt (F) = 0.049, wR ref (F 2 ) = 0.118, T = 120 K.

C 10 H 11 Cl 5 N 2 Re, monoclinic, P 121/ m 1 (No. 11), a = 7.193(1) Å b = 6.991(1) Å, c = 15.142(3) Å, β = 103.14(3)°, V = 741.5 Å 3 , Z = 2, R gt (F) = 0.041, wR ref (F 2 ) = 0.092, T = 100 K.

C 28 H 19 BrO 3 , monoclinic, P 121/ c 1 (No. 14), a = 13.769(1) Å, b = 19.058(2) Å, c = 8.716(1) Å, β = 107.964(6)°, V = 2175.7 Å 3 , Z = 4, R gt (F) = 0.059, wR ref (F 2 ) = 0.164, T = 293 K.

C 20 H 14 N 3 O 9 Sm, triclinic, P 1 (No. 2), a = 9.981(4) Å, b = 10.266(5) Å, c = 11.082(5) Å, α = 85.556(8)°, β = 75.913(8)°, γ = 70.087(7)°, V = 1035.5 Å 3 , Z = 2, R gt (F) = 0.029, wR ref (F 2 ) = 0.070, T = 293 K.

C 37 H 35 N 2 NdO 12 , triclinic, P 1 (No. 2), a = 10.9793(5) Å, b = 12.0965(5) Å, c = 15.3714(9) Å, α = 67.072(1)°, β = 83.799(2)°,γ = 72.887(2)°, V = 1796.9 Å 3 , Z = 2, R gt (F) = 0.037, wR ref (F 2 ) = 0.058, T = 293 K.

C 4 H 8 Cl 2 N 2 , orthorhombic, P 2 1 2 1 2 1 (No. 19), a = 4.828(2) Å, b = 10.497(3) Å, c = 14.830(4) Å, V = 751.6 Å 3 , Z = 4, R gt (F) = 0.052, wR ref (F 2 ) = 0.132, T = 193 K.

C 22 H 15 FO 3 S, monoclinic, P 12 1 / c 1 (No. 14), a = 8.739(1) Å, b = 15.948(3) Å, c = 12.993(1) Å, β = 94.99(1)°, V = 1804.0 Å 3 , Z = 4, R gt (F) = 0.045, wR ref (F 2 ) = 0.119, T = 298 K.

C 15 H 18 N 2 O 4 S 2 , monoclinic, P 12 1 / c 1 (No. 14), a = 8.754(3) Å, b = 12.499(2) Å, c = 15.599(3) Å, β = 95.09(2)°, V = 1700.1Å 3 , Z = 4, R gt (F) = 0.049, wR ref (F 2 ) = 0.128, T = 294 K.

C 18 H 52 Co 2 O 20 , orthorhombic, P bam (No. 55), a = 6.573(1) Å, b = 12.533(3) Å, c = 19.934(4) Å, V = 1642.2 Å 3 , Z = 2, R gt (F) = 0.037, wR ref (F 2 ) = 0.116, T = 293 K.

C 16 H 14 CoN 2 O 5 , triclinic, P 1 (No. 2), a = 7.499(1) Å, b = 10.270(1) Å, c = 10.490(1) Å, α = 97.65(1)°, β = 106.80(1)°, γ = 100.57(1)°, V = 745.3 Å 3 , Z = 2, R gt (F) = 0.058, wR ref (F 2 ) = 0.151, T = 293 K.

C 19 H 20 N 2 O 5 Pb, triclinic, P 1 (No. 2), a = 7.488(2) Å, b = 11.543(2) Å, c = 11.742(2) Å, α = 83.50(3)°, β = 82.54(3)°, γ = 81.94(3)°, V = 991.7 Å 3 , Z = 2, R gt (F) = 0.046, wR ref (F 2 ) = 0.128, T = 293 K.

C 10 H 14 MnN 2 O 7 S, monoclinic, P 12 1 / c 1 (No. 14), a = 20.924(3) Å, b = 6.667(2) Å, c = 20.107(2) Å, β = 95.21(1)°, V = 2793.4 Å 3 , Z = 8, R gt (F) = 0.047, wR ref (F 2 ) = 0.107, T = 293 K.

C 14 H 28 N 2 O 12 Zn, triclinic, P 1 (No. 1), a = 7.189(1) Å, b = 7.764(2) Å, c = 9.843(2) Å, α = 79.16(3)°, β = 87.80(3)°, γ = 71.29(3)°, V = 510.9 Å 3 , Z = 1, R gt (F) = 0.032, wR ref (F 2 ) = 0.095, T = 293 K.

C 8 H 20 NiO 8 , triclinic, P 1 (No. 2), a = 4.874(1) Å, b = 6.329(1) Å, c = 10.560(1) Å, α = 76.78(1)°, β = 87.79(1)°, γ = 76.97(1)°, V = 308.9 Å 3 , Z = 2, R gt (F) = 0.024, wR ref (F 2 ) = 0.065, T = 293 K.

C 48 H 88 N 6 O 26 P 6 , triclinic, P 1 (No. 2), a = 10.759(3) Å, b = 10.351(9) Å, c = 15.914(6) Å, α = 99.82(6)°, β = 98.02(2)°, γ = 75.96(5)°, V = 1685.2 Å 3 , Z = 1, R gt (F) = 0.060, wR ref (F) = 0.060, T = 296 K.

C 24 H 24 CuN 6 O 10 , monoclinic, P 12 1 / c 1 (No. 14), a = 7.441(2) Å, b = 11.458(2) Å, c = 14.850(3) Å, β = 95.941(5)°, V = 1259.4 Å 3 , Z = 2, R gt (F) = 0.049, wR ref (F 2 ) = 0.126, T = 120 K.

C 16 H 20 ErNO 11 , orthorhombic, Pnma (No. 62), a = 7.744(2) Å, b = 21.929(4) Å, c = 11.013(2) Å, V = 1870.2 Å 3 , Z = 4, R gt (F) = 0.020, wR ref (F 2 ) = 0.083, T = 293 K.

C 19 H 24 O 2 , monoclinic, P 12 1 / n 1 (No. 14), a = 8.408(2) Å, b = 13.915(3) Å, c = 14.456(3) Å, β = 93.15(3)°, V = 1688.8 Å 3 , Z = 4, R gt (F) = 0.042, wR ref (F 2 ) = 0.111, T = 293 K.

C 9 H 13 AgN 3 O 4.50 , monoclinic, C 12/ c 1 (No. 15), a = 8.331(2) Å, b = 11.645(2) Å, c = 23.947(5) Å, β = 94.845(3)°, V = 2314.8 Å 3 , Z = 8, R gt (F) = 0.030, wR ref (F 2 ) = 0.072, T = 298 K.

C 23 H 20 Cl 2 CuFN 3 O 5 , triclinic, P 1 (No. 2), a = 10.329(2) Å, b = 11.417(4) Å, c = 10.225(3) Å, α = 95.77(3)°, β = 99.10(2)°, γ = 98.65(2)°, V = 1167.5 Å 3 , Z = 2, R gt (F) = 0.050, wR obs (F) = 0.061, T = 293 K.

C 16 H 18 Cl 2 N 2 O 4 , monoclinic, C 12/ c 1 (No. 15), a = 21.92(1) Å, b = 9.015(5) Å, c = 8.620(5) Å, β = 96.151(9)°, V = 1693.3 Å 3 , Z = 4, R gt (F) = 0.064, wR ref (F 2 ) = 0.186, T = 298 K.

C 10 H 18 AgN 3 O 6 , triclinic, P 1 (No. 2), a = 7.139(2) Å, b = 7.509(2) Å, c = 14.007(4) Å, α = 78.505(5)°, β = 78.789(4)°, γ = 82.023(4)°, V = 717.8 Å 3 , Z = 2, R gt (F) = 0.036, wR ref (F 2 ) = 0.096, T = 298 K.

C 14 H 10 Ag 2 N 2 O 9 , monoclinic, C 12/ c 1 (No. 15), a = 21.164(6) Å, b = 6.451(2) Å, c = 12.219(4) Å, β = 104.646(4)°, V = 1614.1 Å 3 , Z = 4, R gt (F) = 0.035, wR ref (F 2 ) = 0.074, T = 298 K.

C 6 H 6 AgNO 3 S, monoclinic, P 12 1 / c 1 (No. 14), a = 9.109(5) Å, b = 8.910(5) Å, c = 9.546(6) Å, β = 100.076(7)°, V = 762.8 Å 3 , Z = 4, R gt (F) = 0.030, wR ref (F 2 ) = 0.078, T = 293 K.

C 20 H 26 ClCoN 4 O 6 , monoclinic, P 12 1 / c 1 (No. 14), a = 9.703(4) Å, b = 24.323(9) Å, c = 10.289(4) Å, β = 111.561(6)°, V = 2258.4 Å 3 , Z = 4, R gt (F) = 0.049, wR ref (F 2 ) = 0.110, T = 298 K

C 22 H 30 CoN 5 O 7 , orthorhombic, Fdd 2 (No. 43), a = 18.576(8) Å, b = 56.96(2) Å, c = 9.874(4) Å, V = 10448 Å 3 , Z = 16, R gt (F) = 0.057, wR ref (F 2 ) = 0.123, T = 298 K.

C 18 H 36 CuN 6 S 2 , monoclinic, P 12 1 / c 1 (No. 14), a = 7.691(1) Å, b = 9.449(3) Å, c = 16.380(2) Å, β = 101.08(2)°, V = 1168.1 Å 3 , Z = 2, R gt (F) = 0.037, wR ref (F 2 ) = 0.098, T = 293 K.

C 36 H 36 Cu 2 O 12, orthorhombic, Pbca (No. 61), a = 10.992(1) Å, b = 7.706(1) Å, c = 41.770(5) Å, V = 3538.0 Å 3 , Z = 4, R gt (F) = 0.109, wR ref (F 2 ) = 0.269, T = 293 K.