Home Effects of sintering temperature on pore characterization and strength of porous cordierite–mullite ceramics by a pore-forming in-situ technique
Article
Licensed
Unlicensed Requires Authentication

Effects of sintering temperature on pore characterization and strength of porous cordierite–mullite ceramics by a pore-forming in-situ technique

  • Wen Yan , Hao Luo , Jun Tong and Nan Li
Published/Copyright: March 26, 2012
Become an author with De Gruyter Brill

Abstract

Porous cordierite–mullite ceramics with high strength were prepared by a pore-forming in-situ technique. The phase compositions, pore characteristics, and strength were investigated through X-ray diffractometry, scanning electron microscopy, and a microscopy measurement method. It is found that the sintering temperature strongly affects the formation of cordierite and mullite and the sintering, and thus changes the pore characteristics and strength. The formation of cordierite and mullite takes place on a large scale at 1430°C. The pore size distributions are bimodal in specimens sintered at 1370°C, 1400°C, and 1430°C, and mono-modal in a specimen sintered at 1450°C. The strength increases slightly when the sintering temperature increases from 1370°C to 1400°C, and increases significantly when the sintering temperature is increased to 1430°C. The most appropriate mode is a specimen sintered at 1430°C which has high cordierite (42 wt.%) and mullite content (53 wt.%), high apparent porosity (44%), high compressive strength (30.6 MPa) and a relatively homogeneous pore-size distribution.


2 Correspondence address: Wen Yan, Heping Road 947#, Qingshan DistrictWuhan City, Hubei Province, 430081China, Tel.: +86-027-68862511, Fax: +86-027-68862121, E-mail:

Refrences

[1]M.Fukushima, M.Nakata, Y.Y.Wa: J. Ceram. Soc. Jpn.116 (2008) 1322. 10.2109/jcersj2.116.1322Search in Google Scholar

[2]H.M.Alves, G.Tarì, A.T.Fonseca, J.M.F.Ferreira: Mater. Res. Bull.33 (1998) 1439. 10.1016/S0025-5408(98)00131-7Search in Google Scholar

[3]W.Yan, N.Li, B.Q.Han, J.Liu, G.P.Liu: Trans. Indian Ceram. Soc.70 (2011) 65.Search in Google Scholar

[4]J.Takahashi, M.Natsuisaka, S.Shimada: J. Eur. Ceram. Soc.22 (2002) 479. 10.1016/S0955-2219(01)00312-0Search in Google Scholar

[5]T.Ebadzadeh: Br. Ceram. Trans.102 (2003) 66. 10.1179/096797803225001542Search in Google Scholar

[6]D.N.Boccaccini, C.Leonelli, M.R.Rivasi, M.Romagnoli, A.R.Boccaccini: Ceram. Int.31 (2005) 417. 10.1016/j.ceramint.2004.06.005Search in Google Scholar

[7]J.H.She, T.Ohji: Mater. Chem. Phys.80 (2003) 610. 10.1016/S0254-0584(03)00080-4Search in Google Scholar

[8]Y.F.Liu, X.Q.Liu, H.Wei, G.Y.Meng: Ceram. Int.27 (2001) 1. 10.1016/S0272-8842(00)00034-1Search in Google Scholar

[9]W.Yan, N.Li, B.Q.Han: J. Ceram. Process. Res.11 (2010) 388.Search in Google Scholar

[10]W.Yan, N.Li: Am. Ceram. Soc. Bull.85 (2006) 9401.Search in Google Scholar

[11]E.M.M.Ewais, Y.M.Z.Ahmed, A.M.M.Ameen: J. Ceram. Process. Res.10 (2009) 721.Search in Google Scholar

[12]R.Barea, M.I.Osendi, P.Miranzo, J.M.F.Ferreira: J. Am. Ceram. Soc.88 (2005) 777. 10.1111/j.1551-2916.2005.00092.xSearch in Google Scholar

[13]J.H.She, T.Ohji: Mater. Chem. Phys.80 (2003) 610. 10.1016/S0254-0584(03)00080-4Search in Google Scholar

[14]M.Fukushima, M.Nakata, Y.Y.Wa: J. Ceram. Soc. Jpn.116 (2008) 1322. 10.2109/jcersj2.116.1322Search in Google Scholar

[15]Y.Wen, L.Nan, B.Q.Han: Am. Ceram. Soc. Bull.84 (2005) 9201.Search in Google Scholar

[16]N.Li, H.Z.Gu, H.Z.Zhao: Refractories Fundamental and Technology (in Chinese), Metallurgical Industry Press, Beijing (2010).Search in Google Scholar

Received: 2011-5-1
Accepted: 2012-2-6
Published Online: 2012-03-26
Published in Print: 2012-10-01

© 2012, Carl Hanser Verlag, Munich

Articles in the same Issue

  1. Contents
  2. Contents
  3. Original Contributions
  4. Phase equilibria in the Gd–Ni binary and Mg–Ni–Gd ternary systems
  5. Thermodynamics of dilute binary solid solutions using the cluster variation method
  6. Thermal stability of coherent Pd/TiAl interfaces studied from first-principles calculations and experiments
  7. Electropulsing-induced phase transformations and their effects on the single point diamond turning of a tempered alloy AZ91
  8. Study of the mechanism of ductile-regime grinding of SiCp/Al composites using finite element simulation
  9. Investigations on laser welding of magnesium alloys
  10. Investigation of the surface of a laser-treated cast iron cylinder bore
  11. Solidification behaviour of an AA5754 Al alloy ingot cast with high impurity content
  12. Study of the structural evolution of crystalline zinc oxide films prepared by PLD
  13. Effects of sintering temperature on pore characterization and strength of porous cordierite–mullite ceramics by a pore-forming in-situ technique
  14. Sol–gel synthesis of Eu3+, Tb3+ co-doped Y2O3 scintillating nanopowders
  15. Morphological study of SiC coating developed on 2D carbon composites using MTS precursor in a hot-wall vertical reactor
  16. Self-assembling behavior and corrosion inhibition properties of TDPA films on differently structured surfaces of 2024 and 1060 aluminum alloys
  17. Photocatalytic activity of MnWO4 powder in highly effective hydrogen generation from H2O and H2O2
  18. Rheology and microstructure of polymer-modified asphalt nanocomposites
  19. Short Communications
  20. Microstructure and phase composition in a die cast Mg–Nd alloy containing Zn and Zr
  21. DGM News
  22. DGM News
Downloaded on 26.10.2025 from https://www.degruyterbrill.com/document/doi/10.3139/146.110757/html?lang=en
Scroll to top button