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Direct measurement of nanoindentation area function by metrological AFM

  • G. Aldrich-Smith EMAIL logo , N. M. Jennett und U. Hangen
Veröffentlicht/Copyright: 4. Februar 2022
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Abstract

Both the hardness and modulus values obtained by nanoindentation depend on knowledge of the area of contact between the test material and the indenter. Significant errors can be introduced into the measurement if the projected area of the indentation contact is not known with sufficient accuracy. The state-of-the-art for user validation of indenter area function is to use materials of known Young’s modulus in the ‘two reference materials method’. However, the area function is best measured directly by traceably calibrated metrological atomic force microscopy. An area function for a standard Hysitron indenter was generated, using both atomic force microscopy and indentation. The results are compared, and the effect of data fitting techniques and measurement uncertainty are discussed.


Dr. Giles Aldrich-Smith National Physical Laboratory Hampton Road, Teddington, Middlesex, TW11 0LW, UK Tel.: +44 20 8943 6353 Fax: +44 20 8614 0534

References

[1] K. Herrmann, N.M. Jennett, W. Wegener, J. Meneve, K. Hasche, R. Seemann: Thin Solid Films 377 –378 (2000) 394.10.1016/S0040-6090(00)01367-5Suche in Google Scholar

[2] W.C. Oliver, G.M. Pharr: J. Mater. Res. 7 (1992) 1564.10.1557/JMR.1992.1564Suche in Google Scholar

[3] EU Contract G6RD-CT2000-00418, “Development of Certified Reference Materials for Depth Sensing Indentation (DESIRED)”.Suche in Google Scholar

[4] ISO 14577. Metallic Materials – Instrumented Indentation Test for Hardness and Materials Parameters. Part 1: Test Method; Part 2: Verification and Calibration of Testing Machines; Part 3: Calibration of Reference Blocks; Part 4: Properties of Coatings (Committee Draft).Suche in Google Scholar

[5] P.M. Harris, I.M. Smith: NPL Report CMSC 48/04, NPL, Teddington, Middlesex, ISSN 1471-0005, 2004.Suche in Google Scholar

[6] N.M. Jennett, G. Shafirstein, S. Saunders: VDI-Berichte, Düsseldorf, 1995, p. 201.Suche in Google Scholar

[7] The Expression of Uncertainty and Confidence in Measurement, M3003, United Kingdom Accreditation Service, Feltham, Middlesex, 1997.Suche in Google Scholar

Received: 2005-02-04
Accepted: 2005-03-11
Published Online: 2022-02-04

© 2005 Carl Hanser Verlag, München

Artikel in diesem Heft

  1. Frontmatter
  2. Editorial
  3. nanomech 5
  4. Articles Basic
  5. Quantitative evaluation of nanoindents: Do we need more reliable mechanical parameters for the characterization of materials?
  6. Nanoindentation investigation of solid-solution strengthening in III-V semiconductor alloys
  7. Comparison between conventional Vickers hardness and indentation hardness obtained with different instruments
  8. On the pressure dependence of the indentation modulus
  9. A review on the reverse analysis for the extraction of mechanical properties using instrumented Vickers indentation
  10. Articles Applied
  11. Quasi-static and dynamic depth-sensing indentation measurements to characterize wear and mar resistance of coating–polymer systems
  12. Obtaining mechanical parameters for metallisation stress sensor design using nanoindentation
  13. Direct measurement of nanoindentation area function by metrological AFM
  14. A usable concept for the indentation of thin porous films
  15. Analysis of the ductile/brittle transition during a scratch test performed into polymeric film deposited on a PMMA substrate
  16. Nanomechanical and nanotribological properties of polymeric ultrathin films for nanoimprint lithography
  17. Adhesive and nanomechanical properties of polymeric films deposited on silicon
  18. Modelling of the nanoindentation process of ultrathin films
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  21. Thermodynamic assessment of the Ca–Sn system
  22. Interfacial reaction between Cu and Ti2SnC during processing of Cu–Ti2SnC composite
  23. Effects of heat treatment on the lubricated sliding wear behaviour of zinc-based alloy containing nickel under varying test conditions
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  25. Notifications/Mitteilungen
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  27. Press/Presse
Heruntergeladen am 16.11.2025 von https://www.degruyterbrill.com/document/doi/10.1515/ijmr-2005-0221/pdf
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