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Textures and precipitates in Ti-stabilized interstitial-free steel

  • Eunjoo Shin , Baek-Seok Seong , Hee-Jae Kang and Moo-Young Huh EMAIL logo
Published/Copyright: February 5, 2022

Abstract

Samples of titanium-stabilized interstitial-free steel were coiled at 600 and 700 °C. The effect of the coiling temperature on the formation of textures and precipitates during coiling, cold rolling and recrystallization annealing was studied by means of neutron texture measurements, small angle neutron scattering analysis and transmission electron microscopy observations. Whereas coiling at the lower temperature resulted in an insufficient scavenging of carbon in solid solution, coiling at the higher temperature promoted scavenging of carbon in solid solution, and consequently the formation of a large number of precipitates. The large amount of carbon in solid solution caused the retardation of softening in the cold-rolled sample during annealing below 700 °C. Upon annealing above 700 °C the impact of the coiling temperature on grain size and precipitates was not observed. The samples coiled at different temperatures exhibited a nearly identical cold rolling texture. However, the cold-rolled sample having a large amount of carbon in solid solution displayed a weak recrystallization texture.


Prof. Dr. Moo-Young Huh Division of Materials Science and Engineering Korea University Seoul 136-701, Korea Tel.: +82 2 3290 3271 Fax: +82 2 928 3584

  1. Part of this work was supported by the HANARO Nuclear R & D Program of the Ministry of Science and Technology.

References

[1] R. Mendoza, J. Huante, M. Alanis, C. Gonzalez-Rivera, J.A. Juarez-Islas: Mater. Sci. Eng. A 276 (2000) 203.10.1016/S0921-5093(99)00267-1Search in Google Scholar

[2] S. Carabajar, J. Merlin, V. Massardier, S. Chabanet: Mater. Sci. Eng. A 281 (2000) 132.10.1016/S0921-5093(99)00737-6Search in Google Scholar

[3] C. Huang, E.B. Hawbolt, T.R. Meadowcroft: Canad. Metall. Quart. 39 (2000) 369.10.1179/cmq.2000.39.3.369Search in Google Scholar

[4] J.Y. Choi, B.S. Seong, S.C. Baik, H.C. Lee: ISIJ Int. 42 (2002) 889.10.2355/isijinternational.42.889Search in Google Scholar

[5] H.J. Bunge: Z. Metallkd. 70 (1979) 411.10.1515/ijmr-1979-700701Search in Google Scholar

[6] T. Senuma, K. Kawasaki: ISIJ Int. 34 (1994) 51.10.2355/isijinternational.34.51Search in Google Scholar

[7] A. Okamoto, N. Mizui, in: R. Pradhan (Ed.), Proc. Metallurgy of Vacuum-Degassed Products, The Minerals, Metals & Materials Society, Indianapolis (1990) 161.Search in Google Scholar

[8] S. Satoh, T. Obara, K. Tsunoyama: Trans. ISIJ 26 (1986) 737.10.2355/isijinternational1966.26.737Search in Google Scholar

[9] S.V. Subramaniam, M. Prikryl, B.D. Gaulin, D.D. Clifford, S. Benincasa, I. O’Reilly: ISIJ Int. 34 (1994) 61.10.2355/isijinternational.34.61Search in Google Scholar

[10] T. Matsumoto, S. Hamanaka, T. Yamada, T. Tanaka, in: Sheet steels, International Forum for Physical Metallurgy of IF Steels, ISIJ, Tokyo (1994) 269.Search in Google Scholar

[11] J. Shi, X. Wang: J. Mater. Eng. & Perf. 8 (1999) 641.10.1361/105994999770346396Search in Google Scholar

[12] W.B. Hutchinson, K. Ushioda: Scand. J. Metall. 13 (1984) 269.Search in Google Scholar

[13] K. Lücke, K. Detert: Acta metall. 5 (1957) 628.10.1016/0001-6160(57)90109-8Search in Google Scholar

[14] M.Y. Huh, D. Raabe, O. Engler: Steel Res. 66 (1995) 353.10.1002/srin.199501137Search in Google Scholar

[15] M.Y. Huh, H.C. Kim, O. Engler: Steel Res. 71 (2000) 239.10.1002/srin.200001223Search in Google Scholar

[16] S. Abis, R. Caciuffo, F. Carsughi, R. Coppola, M. Magnani, F. Rustichelli, M. Stefanon: Phys. Rev. B 42 (1990) 2275.10.1103/PhysRevB.42.2275Search in Google Scholar

[17] P. Ancrenaz, C. Servant, O. Lyon: Acta Cryst. B 49 (1993) 458.10.1107/S0108768192011509Search in Google Scholar

[18] O.N. Yakubovsy, L.M. Storojeva, D.A. Burko, V.P. Barytinsky, J.I. Larin, in: 41ST MWSP CONF. ISS., Baltimore (1999) 245.Search in Google Scholar

[19] H.J. Bunge: Texture Analysis in Materials Science, Butterworths, London (1982).10.1016/B978-0-408-10642-9.50010-6Search in Google Scholar

[20] S.K. Chang, H.K. Kang: Steel Res. 66 (1995) 463.10.1002/srin.199501156Search in Google Scholar

[21] Y.B. Park, D.N. Lee, G. Gottstein: Acta. mater. 44 (1996) 3421.10.1016/1359-6454(95)00414-9Search in Google Scholar

[22] D. Raabe, K. Lücke: Mater. Sci. Technol. 9 (1993) 302.10.1179/mst.1993.9.4.302Search in Google Scholar

[23] M. Hölscher, D. Raabe, K. Lücke: Steel Res. 62 (1991) 567.10.1002/srin.199100451Search in Google Scholar

[24] R. Kern, P.H. Lee, H.J. Bunge: Steel Res. 57 (1986) 563.10.1002/srin.198600826Search in Google Scholar

[25] U. v. Schlippenbach, F. Emren, K. Lücke: Acta metall. 34 (1986) 1289.10.1016/0001-6160(86)90015-5Search in Google Scholar

[26] L.S. Tóth, J.J. Jonas, D. Daniel, R.K. Ray: Metall. Trans. A 21 (1990) 2985.10.1007/BF02647219Search in Google Scholar

[27] M.Y. Huh, O. Engler, D. Raabe: Textures and Microstructures 24 (1995) 225.10.1155/TSM.24.225Search in Google Scholar

[28] I. Samajdar, B. Verlinden, P. Van Houtte, D. Vanderschueren: Mater. Sci. Eng. A 238 (1997) 343.10.1016/S0921-5093(97)00455-3Search in Google Scholar

[29] C.G. Windsor: J. Appl. Cryst. 21 (1988) 582.10.1107/S0021889888008404Search in Google Scholar

[30] L.A. Feigin, D.I. Svergun: Structure Analysis by Small-Angle X-ray and Neutron Scattering, Plenum Press, New York (1987).10.1007/978-1-4757-6624-0Search in Google Scholar

[31] K. Usioda, N. Yoshinaga, O. Akisue, in: As Ref. [10], p. 227.Search in Google Scholar

[32] M. Hua, C.I. Garcia, A.J. Deardo: Metall. Mater. Trans. A 28 (1997) 1769.10.1007/s11661-997-0108-4Search in Google Scholar

[33] F. Emren, U. v. Schlippenbach, K. Lücke: Acta metall. 34 (1986) 2105.10.1016/0001-6160(86)90156-2Search in Google Scholar

[34] W. Lorenz, H.P. Hougardy: Z. Metallkd. 86 (1995) 164.10.1515/ijmr-1995-860304Search in Google Scholar

[35] O. Engler, K. Lücke, C. Pithan, in: J.A. Szpunar (Ed.) 12th Int. Conf. on Textures of Materials (ICOTOM-12), NRC Research Press, Ottawa, Ontario (1999) 842.Search in Google Scholar

[36] A.R. Jones, N. Hansen: Acta metall. 29 (1981) 589.10.1016/0001-6160(81)90140-1Search in Google Scholar

[37] P.A. Manohar, M. Ferry, T. Chandra: ISIJ Int. 38 (1998) 913.10.2355/isijinternational.38.913Search in Google Scholar

[38] F.J. Humphreys, M. Hatherly: Recrystallization and Related Annealing Phenomena, Elsevier Science, Oxford (1995).10.1016/B978-0-08-041884-1.50017-9Search in Google Scholar

Received: 2003-02-05
Published Online: 2022-02-05

© 2003 Carl Hanser Verlag, München

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