Abstract
Statistical design of experiments was used for design and analysis of nickel extraction from hazardous waste. Sulphuric acid leaching of zinc plant residue has been performed for monitoring and evaluating the effects of process factors on the nickel leaching yield. Factorial design was planned first in order to study the effect of six process factors and screen main variables. These factors were reaction time, acid concentration, solid-liquid ratio % (w/v), particle size, stirring speed and reaction temperature. The main factors and their interaction were studied by analysis of variance (ANOVA), and the results showed that the reaction time, acid concentration and solid-liquid ratio were the most significant factors. In the second set of experiments, response surface methodology (RSM) was used for modelling and optimisation of significant factors. Quadratic model was derived for the prediction of nickel extraction. The optimum values for maximum nickel was identified to be a leaching time of 30 min, acid concentration 10% (V/V) and solid liquid ratio of 10%. Using these optimum conditions, more than 94% nickel was extracted. In addition the results of model equation showed a good agreement with the experimental data.
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©2016 by De Gruyter
Artikel in diesem Heft
- Frontmatter
- Review
- Novel Membrane Reactor Concepts for Hydrogen Production from Hydrocarbons: A Review
- Research Articles
- Modeling and Simulation Study of an Industrial Radial Moving Bed Reactor for Propane Dehydrogenation Process
- Oxidative Degradation of Methylene Blue in Aqueous Medium Catalyzed by Lab Prepared Nickel Hydroxide
- CFD Modelling of a Hollow Fibre Membrane for CO2 Removal by Aqueous Amine Solutions of MEA, DEA and MDEA
- Performance Study of a Thermally Double Coupled Multi-Tubular Reactor by Considering the Effect of Flow Type Patterns
- Radiative Three-Dimensional Flow with Chemical Reaction
- Three-Phase Model of a Fluidized-Bed Catalytic Reactor for Polyethylene Synthesis
- Study on the Effect of Nickel Doping on Mo-Bi Based Catalyst for Selective Oxidation of Isobutene to Methacrolein
- DM Water Plant Sedimentation as a Cheap and Waste Source of Catalyst for Biodiesel Production
- Recovery of Biogas from Meat Industry Wastewater Using Continuously Stirred Tank Reactor (CSTR): Modeling and Optimization
- Comparison of CFD Simulation and Simplified Modeling of a Fluidized Bed CO2 Capture Reactor
- Kinetic Study for Platinum Extraction from Spent Catalyst in Cyanide Solution at High Temperatures
- Hydroisomerization of Biomass Derived n-Hexadecane Towards Diesel Pool: Effect of Selective Removal External Surface Sites from Pt/ZSM-22
- Heat Flux and Variable Thermal Conductivity Effects on Casson Flow and Heat Transfer due to an Exponentially Stretching Sheet with Viscous Dissipation and Heat Generation
- Optimization of Nickel Chemical Extraction from Hazardous Residue
- Green Approach for Biodiesel Production from Jojoba Oil Supported by Process Modeling and Simulation
- Differentiating Process Performance of Various Coagulants in Removal of Congo red and Orange G Dyes
- CFD Simulation of Hydrodynamic of a Bubble Column Reactor Operating in Churn-Turbulent Regime and Effect of Gas Inlet Distribution on System Characteristics
- Transformation of Phenolic Compounds by Fe(III) in the Aqueous Solution in Dark and Under Irradiation
- Transient Predictive Model for Dynamic Analysis, Kinetic Study, and Reactor Design of Triglycerides Transesterification to Biodiesel
- Screening of Alternative Carbon Sources for Recombinant Protein Production in Pichia pastoris
- Optimization of a Large Scale Industrial Reactor Towards Tailor Made Polymers Using Genetic Algorithm
- Model of Reactive Transport within a Light Photocatalytic Textile
- Preparation of Chitosan based Nanofibers: Optimization and Modeling
- Adsorption of As (III) on Iron Coated Quartz Sand: Influence of Temperature on the Equilibrium Isotherm, Thermodynamics and Isosteric Heat of Adsorption Analysis
- Resistance Characteristics of Coal Slime in Pipe Flow at High Pressure
- Activity Comparison of Acidic Resins in the Production of Valuable Glycerol Acetates
- Bulk Polymerization of Styrene using Multifunctional Initiators in a Batch Reactor: A Comprehensive Mathematical Model
- An Effective Reaction Rate Model for Gas-Solid Reactions with High Intra-Particle Diffusion Resistance
- Heart-Like Micro-Flow Mixer
- Hydrogen Production by Hydrolysis of NaBH4 with Cr-Ni-W-B Catalyst: Effects of Cold Plasma and Chromium Content
- Prediction of Reactivity Ratios in Free Radical Copolymerization from Monomer Resonance–Polarity (Q–e) Parameters: Genetic Programming-Based Models
- Steady-State Modeling of Pt-Catalyzed H2 Combustion in a Monolithic Reactor: From Micro- to Macro-kinetics
- Premixed Methanol–Air Combustion Characteristics in a Mini-scale Catalytic Combustor
- Kinetic Modeling of VOC Photocatalytic Degradation Using a Process at Different Reactor Configurations and Scales
- Improvement of Activated Sludge Process Using a Nonlinear PI Controller Design via Adaptive Gain
- Modeling and Simulation of a Pilot-Scale Bubbling Fluidized Bed Gasifier for the Gasification of High Ash Indian Coal Using Eulerian Granular Approach
- Performance of a Catalytic Gas–Solid Fluidized Bed Reactor in the Presence of Interparticle Forces
- Mathematical Modeling of Biodiesel Production under Intense Agitation
- Extended Aeration Activated Sludge Reactor (EAASR) for Removal of Nitrobenzene: Air Stripped or Biologically Removed?
- CFD Modeling of Algae Flash Pyrolysis in the Batch Fluidized Bed Reactor Including Heat Carrier Particles
- A Robust Extended State Observer for the Estimation of Concentration and Kinetics in a CSTR
- Dynamic Modeling of CATOFIN® Fixed-Bed Iso-Butane Dehydrogenation Reactor for Operational Optimization
- Effect of Biomass Compositions on Combustion Kinetic Parameters using Response Surface Methodology
- Short Communications
- Discussions on Particle Flux Measurement in Gas-Solids Risers
- Use of New Regeneration Processes for Thermolabile Amines
- Oxidative-Extractive Desulfurization of Liquid Fuel by Dimethyl Sulfoxide and ZnCl2 Based Ionic Liquid
- Corrigendum
- Corrigendum to: Performance Analysis of Immobilized Enzyme Semifluidised Bed Bioreactors
Artikel in diesem Heft
- Frontmatter
- Review
- Novel Membrane Reactor Concepts for Hydrogen Production from Hydrocarbons: A Review
- Research Articles
- Modeling and Simulation Study of an Industrial Radial Moving Bed Reactor for Propane Dehydrogenation Process
- Oxidative Degradation of Methylene Blue in Aqueous Medium Catalyzed by Lab Prepared Nickel Hydroxide
- CFD Modelling of a Hollow Fibre Membrane for CO2 Removal by Aqueous Amine Solutions of MEA, DEA and MDEA
- Performance Study of a Thermally Double Coupled Multi-Tubular Reactor by Considering the Effect of Flow Type Patterns
- Radiative Three-Dimensional Flow with Chemical Reaction
- Three-Phase Model of a Fluidized-Bed Catalytic Reactor for Polyethylene Synthesis
- Study on the Effect of Nickel Doping on Mo-Bi Based Catalyst for Selective Oxidation of Isobutene to Methacrolein
- DM Water Plant Sedimentation as a Cheap and Waste Source of Catalyst for Biodiesel Production
- Recovery of Biogas from Meat Industry Wastewater Using Continuously Stirred Tank Reactor (CSTR): Modeling and Optimization
- Comparison of CFD Simulation and Simplified Modeling of a Fluidized Bed CO2 Capture Reactor
- Kinetic Study for Platinum Extraction from Spent Catalyst in Cyanide Solution at High Temperatures
- Hydroisomerization of Biomass Derived n-Hexadecane Towards Diesel Pool: Effect of Selective Removal External Surface Sites from Pt/ZSM-22
- Heat Flux and Variable Thermal Conductivity Effects on Casson Flow and Heat Transfer due to an Exponentially Stretching Sheet with Viscous Dissipation and Heat Generation
- Optimization of Nickel Chemical Extraction from Hazardous Residue
- Green Approach for Biodiesel Production from Jojoba Oil Supported by Process Modeling and Simulation
- Differentiating Process Performance of Various Coagulants in Removal of Congo red and Orange G Dyes
- CFD Simulation of Hydrodynamic of a Bubble Column Reactor Operating in Churn-Turbulent Regime and Effect of Gas Inlet Distribution on System Characteristics
- Transformation of Phenolic Compounds by Fe(III) in the Aqueous Solution in Dark and Under Irradiation
- Transient Predictive Model for Dynamic Analysis, Kinetic Study, and Reactor Design of Triglycerides Transesterification to Biodiesel
- Screening of Alternative Carbon Sources for Recombinant Protein Production in Pichia pastoris
- Optimization of a Large Scale Industrial Reactor Towards Tailor Made Polymers Using Genetic Algorithm
- Model of Reactive Transport within a Light Photocatalytic Textile
- Preparation of Chitosan based Nanofibers: Optimization and Modeling
- Adsorption of As (III) on Iron Coated Quartz Sand: Influence of Temperature on the Equilibrium Isotherm, Thermodynamics and Isosteric Heat of Adsorption Analysis
- Resistance Characteristics of Coal Slime in Pipe Flow at High Pressure
- Activity Comparison of Acidic Resins in the Production of Valuable Glycerol Acetates
- Bulk Polymerization of Styrene using Multifunctional Initiators in a Batch Reactor: A Comprehensive Mathematical Model
- An Effective Reaction Rate Model for Gas-Solid Reactions with High Intra-Particle Diffusion Resistance
- Heart-Like Micro-Flow Mixer
- Hydrogen Production by Hydrolysis of NaBH4 with Cr-Ni-W-B Catalyst: Effects of Cold Plasma and Chromium Content
- Prediction of Reactivity Ratios in Free Radical Copolymerization from Monomer Resonance–Polarity (Q–e) Parameters: Genetic Programming-Based Models
- Steady-State Modeling of Pt-Catalyzed H2 Combustion in a Monolithic Reactor: From Micro- to Macro-kinetics
- Premixed Methanol–Air Combustion Characteristics in a Mini-scale Catalytic Combustor
- Kinetic Modeling of VOC Photocatalytic Degradation Using a Process at Different Reactor Configurations and Scales
- Improvement of Activated Sludge Process Using a Nonlinear PI Controller Design via Adaptive Gain
- Modeling and Simulation of a Pilot-Scale Bubbling Fluidized Bed Gasifier for the Gasification of High Ash Indian Coal Using Eulerian Granular Approach
- Performance of a Catalytic Gas–Solid Fluidized Bed Reactor in the Presence of Interparticle Forces
- Mathematical Modeling of Biodiesel Production under Intense Agitation
- Extended Aeration Activated Sludge Reactor (EAASR) for Removal of Nitrobenzene: Air Stripped or Biologically Removed?
- CFD Modeling of Algae Flash Pyrolysis in the Batch Fluidized Bed Reactor Including Heat Carrier Particles
- A Robust Extended State Observer for the Estimation of Concentration and Kinetics in a CSTR
- Dynamic Modeling of CATOFIN® Fixed-Bed Iso-Butane Dehydrogenation Reactor for Operational Optimization
- Effect of Biomass Compositions on Combustion Kinetic Parameters using Response Surface Methodology
- Short Communications
- Discussions on Particle Flux Measurement in Gas-Solids Risers
- Use of New Regeneration Processes for Thermolabile Amines
- Oxidative-Extractive Desulfurization of Liquid Fuel by Dimethyl Sulfoxide and ZnCl2 Based Ionic Liquid
- Corrigendum
- Corrigendum to: Performance Analysis of Immobilized Enzyme Semifluidised Bed Bioreactors