Startseite Direct observation of phase transformations in the simulated heat-affected zone of a 9Cr martensitic steel
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Direct observation of phase transformations in the simulated heat-affected zone of a 9Cr martensitic steel

  • Peter Mayr , Todd A. Palmer , John W. Elmer und Eliot D. Specht
Veröffentlicht/Copyright: 11. Juni 2013
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International Journal of Materials Research
Aus der Zeitschrift International Journal of Materials Research Band 99 Heft 4

Abstract

An experimental test melt of a boron alloyed 9Cr-3W-3Co-V,Nb steel for high temperature applications in the thermal power generation industry was produced by vacuum induction melting. This grade of steel typically displays a homogeneous tempered martensitic microstructure in the as-received, i. e. normalised and tempered, condition. However, after welding, this microstructure is significantly altered, resulting in a loss of its desired properties. The phase transformations during simulated thermal cycles typical of those experienced in the weld heat-affected zone were directly observed by in-situ X-ray diffraction experiments using synchrotron radiation. Heating rates of 10 K s−1 and 100 K s−1 up to a peak temperature of 1300°C are investigated here. The final microstructures observed after both simulated weld thermal cycles are primarily composed of martensite with approximately 4% retained delta ferrite and 4% retained austenite, by volume. With the temporal resolution of the in-situ X-ray diffraction technique, phase transformations from tempered martensite to austenite to delta ferrite during heating and to martensite during cooling were monitored. With this technique, the evolution of the final microstructure through both heating and cooling is monitored, providing additional context to the microstructural observations.

Keywords: Chromium steels; Heat-affected zone; Phase transformations; Delta ferrite; Retained austenite
* Correspondence address, Dr. Peter Mayr, Graz University of Technology, Institute for Materials Science, Welding and Forming, Kopernikusgasse 24, A-8010 Graz, Austria, Tel.: +43 316 873 7186, Fax: +43 316 873 7187, E-mail:

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Received: 2007-11-13
Accepted: 2008-1-21
Published Online: 2013-06-11
Published in Print: 2008-04-01

© 2008, Carl Hanser Verlag, München

Artikel in diesem Heft

  1. Contents
  2. Contents
  3. Editorial
  4. Horst Cerjak – Emeritus Professor
  5. Review
  6. Calculation of crystallographic texture due to displacive transformations
  7. Basic
  8. Ferrite transformation from oxide–steel interface in HAZ-simulated C–Mn steel
  9. Influence of metastable tetragonal ZrO2-reinforcements on the properties of MoSi2-composites
  10. Joining strategies for open-porous metallic foams
  11. Precipitation behaviour of an Fe–Co–Mo-alloy during non-isothermal ageing
  12. Characterization of δ-phase in superalloy Allvac 718PlusTM
  13. Direct observation of phase transformations in the simulated heat-affected zone of a 9Cr martensitic steel
  14. Effect of boron on creep deformation behavior and microstructure evolution in 9% Cr steel at 650°C
  15. Effect of stress on the creep deformation of ASME Grade P92/T92 steels
  16. Applied
  17. Assessment of creep rupture life of weldments of martensitic steels
  18. Computational analysis of the precipitation kinetics in a complex tool steel
  19. Predicted precipitate back-stress and creep rupture strength of the advanced 9–12% Cr steel COST E2
  20. Compositional characterisation and thermodynamic modelling of nitride precipitates in a 12% Cr steel
  21. The L2 norm of the deviation between the measured and computed transient displacement field in a test weld
  22. Toward reliable calculations of heat and plastic flow during friction stir welding of Ti-6Al-4V alloy
  23. Notifications
  24. DGM News
https://doi.org/10.3139/146.101649
Schlagwörter für diesen Artikel
Chromium steels; Heat-affected zone; Phase transformations; Delta ferrite; Retained austenite

Artikel in diesem Heft

  1. Contents
  2. Contents
  3. Editorial
  4. Horst Cerjak – Emeritus Professor
  5. Review
  6. Calculation of crystallographic texture due to displacive transformations
  7. Basic
  8. Ferrite transformation from oxide–steel interface in HAZ-simulated C–Mn steel
  9. Influence of metastable tetragonal ZrO2-reinforcements on the properties of MoSi2-composites
  10. Joining strategies for open-porous metallic foams
  11. Precipitation behaviour of an Fe–Co–Mo-alloy during non-isothermal ageing
  12. Characterization of δ-phase in superalloy Allvac 718PlusTM
  13. Direct observation of phase transformations in the simulated heat-affected zone of a 9Cr martensitic steel
  14. Effect of boron on creep deformation behavior and microstructure evolution in 9% Cr steel at 650°C
  15. Effect of stress on the creep deformation of ASME Grade P92/T92 steels
  16. Applied
  17. Assessment of creep rupture life of weldments of martensitic steels
  18. Computational analysis of the precipitation kinetics in a complex tool steel
  19. Predicted precipitate back-stress and creep rupture strength of the advanced 9–12% Cr steel COST E2
  20. Compositional characterisation and thermodynamic modelling of nitride precipitates in a 12% Cr steel
  21. The L2 norm of the deviation between the measured and computed transient displacement field in a test weld
  22. Toward reliable calculations of heat and plastic flow during friction stir welding of Ti-6Al-4V alloy
  23. Notifications
  24. DGM News
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