Startseite Diffusion characteristics of plasma nitrided hard chromium on AISI 1010 steel
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Diffusion characteristics of plasma nitrided hard chromium on AISI 1010 steel

  • Murat Danışman , Mustafa Kocabaş und Nurhan Cansever
Veröffentlicht/Copyright: 21. April 2015
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Materials Testing
Aus der Zeitschrift Materials Testing Band 57 Heft 5

Abstract

In order to investigate the different Cr-N formation characteristics of plasma nitrided hard Cr coatings, Cr was electrodeposited on AISI 1010 steel and plasma nitrided at 600, 700 and 800 °C for 3 h, 5 h and 7 h, respectively. Phase analyses of resulting Cr-N phases and grain size of Cr layer before and after nitriding process were calculated by X-ray diffraction analysis. Structure of nitride layer and its thickness were analyzed using scanning electron microscopy micrographs. The micrographs indicated that samples consisted of three distinctive layers. In order to distinguish these layers, scanning electron microscopy and energy dispersive spectroscopy (EDX) analysis were used as well as elemental distribution versus depth was plotted. The Cr-N diffusion was investigated by layer thickness measurements, and diffusion coefficient as well as activation energies were calculated.

Kurzfassung

Um die verschiedenen Charakteristika der Cr-N-Bildung von plasmanitrierten Hartchromschichten zu untersuchen, wurde der Stahl AISI 1010 mit Chrom galvanisiert und bei 600, 700 bzw. 800 °C für 3 h, 5 h und 7 h plasmanitriert. Die Phasenanalyse der Cr-N-Phasen und die Korngröße der Chromschicht vor und nach dem Nitrierprozess wurden mittels Röntgendiffraktionsanalyse berechnet. Die Struktur der Nitridschicht und ihre Dicke wurden mittels Rasterlelektronenmikroskop analysiert. Die mikrostrukturellen Aufnahmen deuten darauf hin, dass die Proben aus drei verschiedenen Lagen bestehen. Um diese Lagen zu unterscheiden, wurden Rasterelektronenmikroskopie- und EDS-Analysen angewandt sowie die Elementverteilung über die Tiefe bestimmt. Die Cr-N-Diffusion wurde mit Schichtdickenmessungen untersucht und der Diffusionskoeffizient und die Aktivierungsenergien berechnet.

§Correspondence Address, Dr. Murat Danışman, Electronic Engineering Department, Faculty of Engineering, Gedik University, 34876 Yakacik, Istanbul, Turkey, E-mail:

Dr. Murat Danışman was born in 1977. After receiving his Bachelor's degree in Physics, he earned his MSc degree in Metallurgical and Materials Engineering in 2003. He holds a PhD in Metallurgical and Materials Engineering and is currently working as fulltime Assistant Professor Doctor in the Electrical and Electronic Engineering Department, Gedik University, Istanbul, Turkey. His research interests include materials science, surface engineering and semiconductor materials.

PhD candidate Mustafa Kocabaş, born in 1986, is currently working as Research Assistant at Yıldız Technical University, Istanbul, Turkey. His primary research interest is materials science, focusing on surface treatment. He began his PhD studies at Yıldız Technical University, Turkey, in 2012.

Prof. Dr. Nurhan Cansever, born in 1954, currently holds a full Professorship at Yıldız Technical University, Istanbul, Turkey. Her research focuses on corrosion, materials science and surface engineering.

References

1 T.Elangovan, P.Kuppusami, R.Thirumurugesan, V.Ganesan, E.Mohandas, D.Mangalaraj: Nanostructured CrN thin films prepared by reactive pulsed DC magnetron sputtering, Mater. Sci. Eng. B.167 (2010), pp. 17–2510.1016/j.mseb.2010.01.021Suche in Google Scholar

2 D.Kim, M.Kim, K. S.Nam, D.Chang, S. C.Kwon: Duplex coating for improvement of corrosion resistance in chromium deposit, Surf. Coat. Technol.169–170 (2003), pp. 650–65410.1016/S0257-8972(03)00107-5Suche in Google Scholar

3 L.Wang, K. S.Nam, S. C.Kwon: Effect of plasma nitriding of electroplated chromium coatings on the corrosion protection C45 mild steel, Surf. Coat. Technol.202 (2007), pp. 203–20710.1016/j.surfcoat.2007.05.027Suche in Google Scholar

4 L.Wang, D. S.Kim, K. S.Nam, M.Kim, S. C.Kwon: Microstructure of electroplated hard chromium coatings after plasma nitrocarburizing, Surf. Coat. Technol190 (2005), pp. 151–15410.1016/j.surfcoat.2004.08.213Suche in Google Scholar

5 J. G.Buijnsters, P.Shankar, J.Sietsma, J. J.Meulen: Gas nitriding of chromium in NH3- H2 atmosphere, Mater. Sci. Eng. A341 (2003), pp. 289–29510.1016/S0921-5093(02)00231-9Suche in Google Scholar

6 M. K.Hedayati, F.Mahboubi, T.Nickchi: Comparison of conventional and active screen plasma nitriding of hard chromium electroplated steel, Vacuum83 (2009), pp. 1123–112810.1016/j.vacuum.2009.02.005Suche in Google Scholar

7 A.El-Amoush, A.Abu-Rob, H.Edwan, K.Atrash, M.Igab: Tribological properties of hard chromium coated 1010 mild steel under different sliding distances, Solid State Sciences13–3 (2011), pp. 529–53310.1016/j.solidstatesciences.2010.12.020Suche in Google Scholar

8 M.Soltanieh, H.Mahboubi, F.Nekouee: Surface characterization of multiple coated H11 hot work tool steel by plasma nitriding and hard chromium electroplated processes, Vacuum86 (2012), pp. 1470–147610.1016/j.vacuum.2012.01.003Suche in Google Scholar

9 E.Menthe, K. T.Rie: Plasma nitriding and plasma nitrocarburizing of electroplated hard chromium to increase the wear and the corrosion properties, Surf. Coat. Technol.112 (1999), pp. 217–22010.1016/S0257-8972(98)00793-2Suche in Google Scholar

10 A.Basu, J. D.Majumdar, S. G.Chowdhury, P. K.Ajikumar, P.Shankar, A. K.Tyagi: Microstructural and texture studies of gasnitrided, Surf. Coat. Technol.201 (2007), pp. 6985–699210.1016/j.surfcoat.2007.01.004Suche in Google Scholar

11 B. D.Cullity: Elements of X-ray Diffraction, Addison-Wesley Publishing Company Inc.Massachusetts, USA (1956)Suche in Google Scholar

12 S. W.Russell, J.Li, T. L.Alford, P. R.Oakey, S. C.Shatas: Rapid thermal nitridation of thin chromium films, Appl. Surf. Sci.90 (1995), pp. 455–46310.1016/0169-4332(95)00161-1Suche in Google Scholar

13 F.Fazlalipour: Kinetics of V (N, C) coating produced by a duplex surface treatment, Surf. Coat. Technol.202 (2008), pp. 4107–411310.1016/j.surfcoat.2008.02.027Suche in Google Scholar

14 S.Sen, U.Sen, C.Bindal: The growth kinetics of borides formed on boronized AISI 4140 steel, Vacuum77 (2005), pp. 195–20210.1016/j.vacuum.2004.09.005Suche in Google Scholar

15 C. E.Pinedo, W. A.Monteiro: On the kinetics of plasma nitriding a martensitic stainless steel type AISI 420, Surf. Coat. Technol.179 (2004), pp. 119–12310.1016/S0257-8972(03)00853-3Suche in Google Scholar

Published Online: 2015-04-21
Published in Print: 2015-04-30

© 2015, Carl Hanser Verlag, München

Artikel in diesem Heft

  1. Inhalt/Contents
  2. Inhalt
  3. Fachbeiträge/Technical Contributions
  4. Effects of the thickness on the microstructure and corrosion behavior of a TiAlN film on 4140 steel
  5. The effect of anodizing conditions on the corrosion resistance of Ti6Al4V titanium alloy
  6. Frequency analysis of volumetric porosity in aluminum castings at high and low cooling rates
  7. Corrosion resistance of nanosilicasilicate conversion coatings on aluminum prepared by the dip immersion method
  8. Corrosion behavior of Haynes® 556® Fe-Ni-Cr-Co alloy for integrated coal gasification combined cycle syngas plants: A plant exposure study*
  9. Effects of Y2O3 and Al2O3 sintering additives on the hot pressing behavior of AlN ceramics
  10. Einfluss der Klebschichtdicke auf Kopplungsfaktor und Lebensdauer beim Bekleben von piezoelektrischen Flächenwandlern mit Epoxykleber
  11. Influence of the heat treatment on hardness and adhesive wear performance of Ni-P deposit with low phosphorus content
  12. Effect of plasma nitriding time on surface properties of hard chromium electroplated AISI 1010 steel
  13. Diffusion characteristics of plasma nitrided hard chromium on AISI 1010 steel
  14. Estimation of the mechanical properties of nanocomposites based on the properties prediction of single wall carbon nanotubes (SWCNT)
  15. Investigation of joints between polypropylene and polybutylene terephthalate
  16. Parametric optimization of seam welding of stainless steel (SS 304) sheets
  17. Effect of the powder particle size on the wear behavior of boronized AISI 304 stainless steel
  18. Optimum buckling design of axially layered graded uniform columns
  19. Kalender/Calendar
  20. Kalender
https://doi.org/10.3139/120.110736

Artikel in diesem Heft

  1. Inhalt/Contents
  2. Inhalt
  3. Fachbeiträge/Technical Contributions
  4. Effects of the thickness on the microstructure and corrosion behavior of a TiAlN film on 4140 steel
  5. The effect of anodizing conditions on the corrosion resistance of Ti6Al4V titanium alloy
  6. Frequency analysis of volumetric porosity in aluminum castings at high and low cooling rates
  7. Corrosion resistance of nanosilicasilicate conversion coatings on aluminum prepared by the dip immersion method
  8. Corrosion behavior of Haynes® 556® Fe-Ni-Cr-Co alloy for integrated coal gasification combined cycle syngas plants: A plant exposure study*
  9. Effects of Y2O3 and Al2O3 sintering additives on the hot pressing behavior of AlN ceramics
  10. Einfluss der Klebschichtdicke auf Kopplungsfaktor und Lebensdauer beim Bekleben von piezoelektrischen Flächenwandlern mit Epoxykleber
  11. Influence of the heat treatment on hardness and adhesive wear performance of Ni-P deposit with low phosphorus content
  12. Effect of plasma nitriding time on surface properties of hard chromium electroplated AISI 1010 steel
  13. Diffusion characteristics of plasma nitrided hard chromium on AISI 1010 steel
  14. Estimation of the mechanical properties of nanocomposites based on the properties prediction of single wall carbon nanotubes (SWCNT)
  15. Investigation of joints between polypropylene and polybutylene terephthalate
  16. Parametric optimization of seam welding of stainless steel (SS 304) sheets
  17. Effect of the powder particle size on the wear behavior of boronized AISI 304 stainless steel
  18. Optimum buckling design of axially layered graded uniform columns
  19. Kalender/Calendar
  20. Kalender
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