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Preparation and comparative evaluation of PVC/PbO and PVC/PbO/graphite based conductive nanocomposites

  • Junaid Raza , Abdul Hamid , Muhammad Khan EMAIL logo , Fakhar Hussain , Amir Zada EMAIL logo , Li Tiehu , Amjad Ali , Perveen Fazil and Zainul Wahab
Published/Copyright: August 17, 2022
Zeitschrift für Physikalische Chemie
From the journal Zeitschrift für Physikalische Chemie Volume 236 Issue 11-12

Abstract

Two series, A and B, of PVC based nanocomposite polymer membranes (nCPMs) were prepared using PbO only and PbO/graphite mixture as a filler by solution casting method. Seven samples with varying compositions (5–35%) of filler particles were prepared for each series and were compared by thickness measurements, porosity, water uptake, swelling degree, ionic conductivity, ion exchange capacity (IEC), membrane potential and transport number. The maximum values for these characteristics were observed as 0.402 mm, 0.77, 141.3%, 0.11, 0.0033 Scm−1, 8.6 milli-eq.g−1, 0.19 V and 0.01391 for series-A composites whereas that of 0.367 mm, 0.83, 63.4%, 0.019, 0.00981 Scm−1, 5.21 milli-eq.g−1, 0.13 V and 0.0108 for series-B nCPMs respectively. The SEM images of membranes showed greater voids produced in the series-B compared to series-A composites. The maximum Ionic conductivity, IEC, membrane potential and transport number were observed for membrane with 25% PbO/graphite, 20% PbO and 35% PbO particles respectively.

Keywords: conductivity; fuel cells; graphite nanocomposites; nanocomposites; PbO; PVC
Corresponding authors: Muhammad Khan, School of Materials Science and Engineering, Northwestern Polytechnical University, Xian, 710072, P.R. China; and Department of Chemistry, University of Okara, Punjab, Pakistan, E-mail: ; and Amir Zada, Department of Chemistry, Abdul Wali Khan University, Mardan, Khyber Pakhtunkhwa, 23200, Pakistan, E-mail:

Acknowledgments

We are also very thankful to the School of Materials Science and Engineering, Northwestern Polytechnical University, Xian, P.R. of China and Higher Education Commission (HEC) Pakistan for their financial support.

  1. Author contributions: All the authors have accepted responsibility for the entire content of this submitted manuscript and approved submission.

  2. Research funding: This research has been Financially Supported for the Postdoctoral study by the Shaanxi Province and Natural Science Foundation of China under the (Grant No: 2016JQ5108).

  3. Conflict of interest statement: On behalf of all authors, the corresponding author declared that this work is the original work of authors, and all standards were followed accordingly and there is no conflict of interest.

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Received: 2022-04-08
Accepted: 2022-07-21
Published Online: 2022-08-17
Published in Print: 2022-12-16

© 2022 Walter de Gruyter GmbH, Berlin/Boston

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https://doi.org/10.1515/zpch-2022-0051
Keywords for this article
conductivity; fuel cells; graphite nanocomposites; nanocomposites; PbO; PVC

Articles in the same Issue

  1. Frontmatter
  2. Original Papers
  3. Suppression of steel corrosion via some gemini cationic surfactant-based Schiff base: experimental and theoretical investigations
  4. Synthesis of poly (N-isopropyl acrylamide-co-2-acrylamido methylpropane sulfonic acid) hydrogel containing copper and nickel nanoparticles with easy recycling and efficient catalytic potential
  5. Eco-benign preparation of biosorbent using Momordica Charantia for the efficient removal of Cr(VI) ions from wastewater
  6. Oil mediated green synthesis of nano silver in the presence of surfactants for catalytic and food preservation application
  7. Adsorption properties of metal functionalized fullerene (C59Au, C59Hf, C59Ag, and C59Ir) nanoclusters for application as a biosensor for hydroxyurea (HXU): insight from theoretical computation
  8. Evaluation of diethylenetriaminepentaacetic acid modified chitosan immobilized in amino-carbmated alginate matrix as a low cost adsorbent for effective Cu(II) recovery
  9. Screening of four accelerated synthesized techniques in green fabrication of ZnO nanoparticles using Willow leaf extract
  10. Preparation and comparative evaluation of PVC/PbO and PVC/PbO/graphite based conductive nanocomposites
  11. Optical and topographic characteristics of silver films deposited from a colloidal solution on polyelectrolytes for IgG-FITC fluorescence analysis
  12. The three pyridazines, three naphthyridines and two azoles: effect of the position of the second heteroatom on pKaH of their eight conjugate acids
  13. Theoretical study on the origins of sildenafil tautomers’ relative stability
  14. Application of the Lennard-Jones potential for calculating the surface tension and the formation enthalpy of a binary solution
  15. Ultrasonic supported dye removal by a novel biomass
  16. A novel synthesis of graphene oxide-titanium dioxide (GO-TiO2) and graphene oxide-zinc oxide (GO-ZnO) nanocomposites and their application as effective, reusable photocatalysts for degradation of methylene blue (MB) dye
  17. Review Article
  18. Photocatalytic hydrogen generation using TiO2: a state-of-the-art review
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