Application of FT-NIR-DR and FT-IR-ATR spectroscopy to estimate the chemical composition of bamboo (Neosinocalamus affinis Keng)
-
Bailing Sun
,
Shujun Liu
Abstract
Neosinocalamus affinis Keng is widely grown in south-western China for pulp and paper production. Rapid assessment of the chemical properties of N. affinis is necessary for both bamboo breeding and industrial utilization. This study was performed to investigate the abilities of Fourier transform near-infrared spectroscopy in the diffuse reflectance mode (FT-NIR-DR) and Fourier transform infrared attenuated total reflectance (FT-IR-ATR) spectroscopy to predict the contents of holocellulose, α-cellulose, Klason lignin, and NaOH extractives in N. affinis. Partial least squares regression models based on the raw and preprocessed spectra, including multiplicative scatter correction (MSC) and Savitzky-Golay 1st and 2nd derivative spectra, were developed for the chemical components of bamboo. The NIR-based calibrations displayed better performance than those using FT-IR-ATR spectra. The best calibrations developed by both methods for properties all had satisfactory correlations, with coefficient of determination (R2c) values ranging from 0.81 (Klason lignin by FT-IR and MSC) to 0.98 (α-cellulose by FT-NIR and 2nd derivative), and root mean standard error of calibration between 0.50 and 1.47%. When applied to prediction sets, the correlations were good, with R2p above 0.68. The results demonstrate that both spectroscopic methods, combined with chemometric strategies, could rapidly predict the chemical composition of bamboo.
©2011 by Walter de Gruyter Berlin Boston
Articles in the same Issue
- Original Papers
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- Radical scavenging characteristics of condensed tannins from barks of various tree species compared with quebracho wood tannin
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- Effect of acetic acid addition on chemical conversion of woods as treated by semi-flow hot-compressed water
- Oxidative cleavage of non-phenolic β-O-4 lignin model dimers by an extracellular aromatic peroxygenase
- Surface chemistry of vessel elements by FE-SEM, μ-XPS and ToF-SIMS
- Application of FT-NIR-DR and FT-IR-ATR spectroscopy to estimate the chemical composition of bamboo (Neosinocalamus affinis Keng)
- Chemical modification of lignin assisted by microwave irradiation
- Acidic oxidation of kraft lignin into aromatic monomers catalyzed by transition metal salts
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- Effect of Physisporinus vitreus on wood properties of Norway spruce. Part 2: Aspects of microtensile strength and chemical changes
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- Effect of oxalic acid pretreatment of wood chips on manufacturing medium-density fiberboard
- Experimental investigation of stress wave propagation in standing trees
- Relationships between mechanical properties of oak timber (Quercus robur L.)
- Estimating mechanical properties and specific gravity for five-year-old Eucalyptus tereticornis having broad moisture content range by NIR spectroscopy
- Effect of morphological variability of incrusted pit membranes on efficiency of transverse compression to improve liquid uptake
- Short Notes
- Performance of biopolymer films with reinforcing cellulose-containing fillers from pine pulp and bark and birch sawdust
- Efficacy of two organic biocides with co-added antioxidants
Articles in the same Issue
- Original Papers
- Lignocellulosic biorefinery: process integration of hydrolysis and fermentation (SSF process)
- Study of stilbene and resin acid content of Scots pine heartwood by electrical impedance spectroscopy (EIS)
- Radical scavenging characteristics of condensed tannins from barks of various tree species compared with quebracho wood tannin
- Two-step hydrolysis of nipa (Nypa fruticans) frond as treated by semi-flow hot-compressed water
- Effect of acetic acid addition on chemical conversion of woods as treated by semi-flow hot-compressed water
- Oxidative cleavage of non-phenolic β-O-4 lignin model dimers by an extracellular aromatic peroxygenase
- Surface chemistry of vessel elements by FE-SEM, μ-XPS and ToF-SIMS
- Application of FT-NIR-DR and FT-IR-ATR spectroscopy to estimate the chemical composition of bamboo (Neosinocalamus affinis Keng)
- Chemical modification of lignin assisted by microwave irradiation
- Acidic oxidation of kraft lignin into aromatic monomers catalyzed by transition metal salts
- Effect of Physisporinus vitreus on wood properties of Norway spruce. Part 1: Aspects of delignification and surface hardness
- Effect of Physisporinus vitreus on wood properties of Norway spruce. Part 2: Aspects of microtensile strength and chemical changes
- Mode I critical stress intensity factor of wood and medium-density fiberboard measured by compact tension test
- Effect of oxalic acid pretreatment of wood chips on manufacturing medium-density fiberboard
- Experimental investigation of stress wave propagation in standing trees
- Relationships between mechanical properties of oak timber (Quercus robur L.)
- Estimating mechanical properties and specific gravity for five-year-old Eucalyptus tereticornis having broad moisture content range by NIR spectroscopy
- Effect of morphological variability of incrusted pit membranes on efficiency of transverse compression to improve liquid uptake
- Short Notes
- Performance of biopolymer films with reinforcing cellulose-containing fillers from pine pulp and bark and birch sawdust
- Efficacy of two organic biocides with co-added antioxidants
