Startseite Polylactic acid effectively reinforced with reduced graphitic oxide
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Polylactic acid effectively reinforced with reduced graphitic oxide

  • Alejandra De La Cruz Natera , Adriana Cordero García , Juan Restrepo Betancourt , Mary Judith Arias Tapia und Oscar Vargas Ceballos ORCID logo EMAIL logo
Veröffentlicht/Copyright: 27. Juni 2022
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Abstract

The present study was developed to reinforce a thermoplastic matrix with carbonaceous material to improve its thermal and mechanical properties. Composite materials formed from the homogenization of polylactic acid (PLA) and reduced graphitic oxide (RGO) were synthesized and characterized, reinforcement of the polymer’s thermomechanical properties and the adequate homogeneity ratio in the dispersion of the composite material were studied. Graphitic oxide (GO) was synthesized by the modified Hummers method, followed by thermal exfoliation. The chemical composition and the structure of RGO were studied by infrared (FT-IR) and Raman spectroscopies, respectively. PLA composites with different RGO contents (2 and 3% by weight) were prepared and compared in terms of distribution of RGO in the matrix and morphology, using scanning electron microscopy. The thermal stability of the composites was determined through thermogravimetric analysis. Torque of the different composites was measured, which increased at 21%; the tensile test showed an improvement in the mechanical parameters of the composites because the RGO favors the rigidity of the composite. In addition, the oxygenated functional groups present in the RGO allowed a more significant interaction with the PLA matrix, which results in an effective reinforcement of the mechanical properties of the composite material.


Corresponding author: Oscar Vargas Ceballos, Escuela de Ingeniería Metalúrgica y Ciencia de Materiales, Universidad Industrial de Santander, Bucaramanga 680002, Colombia, E-mail:

Award Identifier / Grant number: ING36-TGI2018

Award Identifier / Grant number: 2502

  1. Author contribution: All the authors have accepted responsibility for the entire content of this submitted manuscript and approved submission.

  2. Research funding: The authors acknowledge the different dependencies of the Universidad del Atlántico and the financial support from Universidad Industrial de Santander through the internal project 2502.

  3. Conflict of interest statement: The authors declare no conflicts of interest regarding this article.

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Received: 2022-01-07
Revised: 2022-04-05
Accepted: 2022-04-17
Published Online: 2022-06-27
Published in Print: 2022-09-27

© 2022 Walter de Gruyter GmbH, Berlin/Boston

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