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Microstructural characterization of nanostructured supersonic sprayed Ni–Sn coatings after wear tests at elevated temperature

Paper presented at “XV International Conference on Electron Microscopy”, 15–18 September 2014, Cracow, Poland
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Published/Copyright: July 9, 2015

Abstract

The paper presents results of the wear behavior, as well as the microstructural (scanning and transmission electron microscopy) and compositional (microanalysis with using energy dispersive and X-ray photon emission spectroscopy) characterization of nanostructured Ni-20Sn (wt.%) coatings, deposited on an Inconel 718 substrate by supersonic cold gas spraying at different spraying parameters. Coatings were examined in the as-deposited state and after testing in a linearly reciprocating sliding wear test at room temperature, 200, 400 and 550 °C. It was found that the Ni–Sn coatings exhibit superior wear resistance compared to benchmark materials. This is attributed to an appropriate balance of soft (Ni) and to hard (Ni3Sn – intermetallic) phases and to the nanostructure of the matrix, as well as to the presence of an NiO oxide tribo-layer, as revealed by the microanalysis and electron microscopy.


*Correspondence address, Prof. Jan Kusinski, AGH University of Science and Technology, 30 Mickiewicza Ave., 30-059 Krakow, Poland, Tel.: +48-12-617 3344, Fax: +48-12-617 2639, E-mail:

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Received: 2014-10-29
Accepted: 2015-01-27
Published Online: 2015-07-09
Published in Print: 2015-07-04

© 2015, Carl Hanser Verlag, München

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