Startseite Simple preperation of CuO nanoparticles and submicron spheres via ultrasonic spray pyrolysis (USP)
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Simple preperation of CuO nanoparticles and submicron spheres via ultrasonic spray pyrolysis (USP)

  • Burçak Ebin , Övgü Gençer und Sebahattin Gürmen
Veröffentlicht/Copyright: 17. August 2013
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International Journal of Materials Research
Aus der Zeitschrift International Journal of Materials Research Band 104 Heft 2

Abstract

Copper oxide nanoparticles and submicron size spheres were produced via the ultrasonic spray pyrolysis method using copper nitrate without any additives. The effects of the process temperature and solution concentration on the copper oxide particles were investigated. HSC software, differential scanning calorimetry and thermal gravimetric analysis were used for the thermodynamic investigation of the CuO formation by the decomposition reaction. Particle characterization studies were performed using X-ray diffraction, energy dispersive spectroscopy, scanning–and transmission–electron microscopy. The results show that spherical CuO nanoparticles having around 80 nm particle size were prepared at 400 °C and the submicron size CuO spheres were obtained by the aggregation of nanoparticles at elevated temperatures. The crystallite sizes of the particles ranged between 21 and 46 nm.

Keywords: Nanoparticles; Submicron spheres; Copper oxide; Ultrasonic spray pyrolysis
* Correspondence address, Prof. Dr. Sebahattin Gürmen, Metallurgical and Materials Eng. Dept. Istanbul Technical University, Ayazaga Campus 34469 Sariyer, Istanbul, Turkey; Tel.: +90 212 285 34 82, Fax: +90 212 285 34 27, E-mail:

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Received: 2012-2-5
Accepted: 2012-8-6
Published Online: 2013-08-17
Published in Print: 2013-02-15

© 2013, Carl Hanser Verlag, München

Artikel in diesem Heft

  1. Contents
  2. Contents
  3. Original Contributions
  4. Structure of composites consolidated from ball milled 7475 aluminum alloy and ZrO2 powders
  5. Isothermal section of the Al-Tb-V ternary system at 773 K
  6. Development of an atomic mobility database for disordered and ordered fcc phases in multicomponent Al alloys: focusing on binary systems
  7. Effect of additive and current density on microstructure and texture characteristics of copper electrodeposits
  8. Magnetic properties and microwave absorption properties of carbon fibers coated with FeCo alloy
  9. Effects of BN content on the structural and mechanical properties of a-SiBN ceramics
  10. Structural and relaxor characteristics of Ca0.18Sr0.226Ba0.594Nb2O6
  11. Study on the dielectric properties of CaCu3Ti4O12 ceramics using the one-dimensional Ising model
  12. Erosion wear performance of a surface diffusion alloyed coating on pure magnesium
  13. Evaluation of the quality of cladding deposited on continuous steel casting rolls
  14. Investigating the machinability of austempered ductile irons with dual matrix structures
  15. Simple preperation of CuO nanoparticles and submicron spheres via ultrasonic spray pyrolysis (USP)
  16. Fabrication of transparent Nd:YAG ceramic by vacuum sintering with CaF2 additive
  17. Synthesis and characterization of new Bi2FeNiO6 material using a citric acid assisted gel combustion technique
  18. Processing and characterization of up-converting Er3+ doped (Lu0.5Y0.5)2O3 nanophosphor
  19. People
  20. People
  21. DGM News
  22. DGM News
https://doi.org/10.3139/146.110853
Schlagwörter für diesen Artikel
Nanoparticles; Submicron spheres; Copper oxide; Ultrasonic spray pyrolysis

Artikel in diesem Heft

  1. Contents
  2. Contents
  3. Original Contributions
  4. Structure of composites consolidated from ball milled 7475 aluminum alloy and ZrO2 powders
  5. Isothermal section of the Al-Tb-V ternary system at 773 K
  6. Development of an atomic mobility database for disordered and ordered fcc phases in multicomponent Al alloys: focusing on binary systems
  7. Effect of additive and current density on microstructure and texture characteristics of copper electrodeposits
  8. Magnetic properties and microwave absorption properties of carbon fibers coated with FeCo alloy
  9. Effects of BN content on the structural and mechanical properties of a-SiBN ceramics
  10. Structural and relaxor characteristics of Ca0.18Sr0.226Ba0.594Nb2O6
  11. Study on the dielectric properties of CaCu3Ti4O12 ceramics using the one-dimensional Ising model
  12. Erosion wear performance of a surface diffusion alloyed coating on pure magnesium
  13. Evaluation of the quality of cladding deposited on continuous steel casting rolls
  14. Investigating the machinability of austempered ductile irons with dual matrix structures
  15. Simple preperation of CuO nanoparticles and submicron spheres via ultrasonic spray pyrolysis (USP)
  16. Fabrication of transparent Nd:YAG ceramic by vacuum sintering with CaF2 additive
  17. Synthesis and characterization of new Bi2FeNiO6 material using a citric acid assisted gel combustion technique
  18. Processing and characterization of up-converting Er3+ doped (Lu0.5Y0.5)2O3 nanophosphor
  19. People
  20. People
  21. DGM News
  22. DGM News
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