Startseite Effect of Co Addition to Heat- Treated P/M 316L Stainless Steel on α′-Martensite Formation and Mechanical Properties
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Effect of Co Addition to Heat- Treated P/M 316L Stainless Steel on α′-Martensite Formation and Mechanical Properties

  • Nantawan Pichaiwong , Panyawat Wangyao , Gobboon Lothongkum , Patama Visuttipitukul , Seksak Asavavisithchai , Ruangdaj Tongsri und Nutthita Chuankrerkkul
Veröffentlicht/Copyright: 26. Mai 2013
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Abstract

The effect of various Co additions to P/M 316L stainless steel on α ’-martensite formation and mechanical properties (bending strength and hardness) were investigated. Powder mixtures were compacted using a single action press at 498 MPa and sintered at 1,300°C for 30 min under hydrogen atmosphere, followed by heat-treating in air at 800°C and 900°C for 25 h, 50 h, 75 h, and 100 h, respectively. It is found that oxide formation in closed pores at high temperatures can induce the α ’-martensite formation and reduce the area fraction of porosities, resulting in higher hardness of the heat-treated specimens than that of the sintered specimens. The Co additions can also reduce the amount of α ’-martensite. Long-term heating results in a slight decrease of bending strength due to high connected oxide formation in the internal pores.

Kurzfassung

Die Wirkung verschieden großer Co-Zugaben zum hochlegierten Stahl P/M 316L auf die α’-Martensitausbildung und auf die mechanischen Eigenschaften (Biegefestigkeit und Härte) wurden in der diesem Beitrag zugrunde liegenden Studie untersucht. Hierzu wurden Pulvermischungen in einem Einmaldruckverfahren bei 498 MPa kompaktiert und bei 1300°C für 30 min in Wasserstoffatmosphäre gesintert und anschließend bei 800°C und 900°C über 25 h, 50 h, 75 h und 100 h an Luft behandelt. Es wurde herausgefunden, dass die Oxidausbildung in geschlossenen Poren bei hohen Temperaturen eine α’-Martensitausbildung auslösen kann und den Flächenanteil der Porösität reduzieren kann, woraus sich eine höhere Härte der wärmebehandelten gegenüber den gesinterten Proben ergibt. Die Co-Zugaben können auch den Gehalt an α’-Martensit reduzieren. Das Langzeitglühen führt zu einer leicht reduzierten Biegefestigkeit infolge der Ausbildung von komplex verbundenen Oxidstrukturen in den inneren Poren.


Nantawan Pichaiwong, born in 1987, is graduate student at the Department of Metallurgical Engineering, Faculty of Engineering, Chulalongkorn University, Thailand. She received a bachelor degree in metallurgical engineering from Chulalongkorn University, Thailand in 2010. Her research scope is related to development and characterizations of stainless steels at high temperatures.

Panyawat Wangyao, a corresponding author, received PhD (physical metallurgy) from Technical University, Kosice, Slovakia in 2002. He is lecturer and serving as head of Department of Metallurgical Engineering, Faculty of Engineering, Chulalongkorn University, Thailand, since 2011. His research areas of expertise include high temperature materials such as superalloys, superceramics, and supercomposites including superstainless steels as well as powder metallurgy of alloys.

Gobboon Lothongkum, a corresponding author, born 1960, is associate professor at Department of Metallurgical Engineering, Faculty of Engineering, Chulalongkorn University, Thailand. He received Dr.-Ing. degree from University of the Federal Armed Force Hamburg, Germany in 1994 and the International Welding Engineer Certificate of The International Welding Institute in 2006. His areas of expertise include corrosion of metals and alloys, welding and metal joining, high temperature materials and stainless steels.

Patama Visuttipitukul, PhD (metallurgy) from the University of Tokyo, Japan in 2003, is assistant professor at Department of Metallurgical Engineering, Faculty of Engineering, Chulalongkorn University, Thailand. She received bachelor and master degrees in metallurgical engineering from Chulalongkorn University, Thailand in 1998 and 2000. She received also the International Welding Engineer Certificate of The International Welding Institute in 2006. Her areas of expertise include Surface treatment, heat treatment and thin film.

Seksak Asavavisithchai, associate professor, works at the Department of Metallurgical Engineering, Faculty of Engineering, Chulalongkorn University, Thailand. He received his PhD from the University of Nottingham, UK in the field of materials design and engineering. His research interests are metallic foams, powder metallurgy, metal matrix composite (MMC) and failure analysis.

Dr. Ruangdaj Tongsri received PhD and DIC in 2000 from Imperial College of Science, Technology and Medicine. He graduated master of metallurgy (M. Met) from Sheffield University, UK, in 1995. Before that he graduated a master degree from Chulalongkorn University, Thailand in 1993 and a bachelor degree from Khon Kaen University in 1989, respectively. He works at National Metals and Materials Center of Thailand (MTEC). His areas of expertise include powder metallurgy, nanotechnology and energy management materials technology.

Nutthita Chuankrerkkul, PhD, is lecturer at Metallurgy and Materials Science Research Institute, Chulalongkorn University, Thailand. She received bachelor degree in materials science and master degree in ceramic technology both from Chulalongkorn University, Thailand and received doctor of philosophy in engineering materials from the University of Sheffield, UK. Her research interest is particulate materials processing, especially in powder injection molding of metals, ceramics, and composites.


References

1 H.Buscail, S.El Messki, F.Riffard, S.Perrier, R.Cueff, E.Caudron, C.Issartel: Characterization of the oxides formed at 1000 C on the AISI 316L stainless steel-role of molybdenum, Materials Chemistry and Physics111 (2008), pp. 491496Suche in Google Scholar

2 Stainless Steel: Specialist Course, International Stainless Steel Forum (ISSF), Training notes 16, 1 st Edition (2002)Suche in Google Scholar

3 D.Peckner, I. M.Bernstein: Handbook of Stainless Steels, McGraw-Hill, New York (1997)Suche in Google Scholar

4 J. R.Davis: Stainless Steels, ASM Specialty Handbook, ASM International, Materials Park, OH (1994)Suche in Google Scholar

5 Metals Handbook, Powder Metallurgy, American Society for Metals, 9th Edition, Metals Park, OH (1984)Suche in Google Scholar

6 N.Kurgan, R.Varol: Mechanical properties of P/M 316L stainless steel materials, Powder Technology201 (2010), pp. 242247Suche in Google Scholar

7 S. K.Ghosh, P.Mallick, P. P.Chattopadhyay: Effect of Cold Deformation on Phase Evolution and Mechanical Properties in an Austenitic Stainless Steel for Structural and Safety Applications, Journal of Iron and Steel Research International 19, Issue 4 (April 2012), pp. 63–6810.1016/S1006-706X(12)60089-2Suche in Google Scholar

8 P.Hedström, U.LienertJ.Almer, M.Oden: Stepwise transformation behaviour of the strain induced martensitic transformation in a metastable stainless steel, Scripta Materialia56 (2007), pp. 213216Suche in Google Scholar

9 A.Kurc-Lisiecka, E.Kalinowska-Ozgowicz: Structure and mechanical properties of austenitic steel after cold rolling, Journal of Achievements in Materials and Manufacturing Engineering44 (2011), pp. 148153Suche in Google Scholar

10 A.Kurc, Z.Stoklosa: The effect of γ-α— phase transformation on microstructure and properties of austenitic Cr-Ni steel, Journal of Achievements in Materials and Manufacturing Engineering41 (2010), pp. 8594Suche in Google Scholar

11 J.Talonen, H.Hänninen: Formation of shear bands and strain induced martensite during plastic deformation of metastable austenitic stainless steels, Acta Materialia55 (2007), pp. 61086118Suche in Google Scholar

12 T.Shyr, J.Shie, S.Huang, S.Yang, W.Hwang: Phase transformation of 316L stainless steel from wire to fiber, Materials Chemistry and Physics122 (2010), pp. 273277Suche in Google Scholar

13 S.Hong, S.Lee, T.Byun: Temperature effect on the low cycle fatigue behaviour of type 316L stainless steel: Cyclic non-stabilization and an invariable fatigue parameter, Materials Science and Engineering: A457 (2007), pp. 139147Suche in Google Scholar

14 A.Bautista, F.Velasco, M.Campos, M. E.Rabanal, J. M.Torralba: Oxidation Behaviour at 900 C of Austenitic, Ferritic and Duplex Stainless Steels Manufactured By Powder Metallurgy, Oxidation of Metals59 (2002), pp. 37339310.1023/A:1023000329514Suche in Google Scholar

15 F. B.Pickering: The Metallurgical Evolution of Stainless Steels, American Society for Metals/the Metals Society, OH (1979)Suche in Google Scholar

16 A.Buatista, C.Moral, F.Velasco, C.Simal, S.Guzman: Density improved powder metallurgical ferritic stainless steels for high-temperature applications, Journal of Material Processing Technology189 (2007), pp. 344351Suche in Google Scholar

17 S.Dai, F.Shen, A.Yu: Granule Size Distribution and Porosity of Granule Packing, Journal of Iron and Steel Research International 15, Issue 5 (September 2008), pp. 1–510.1016/S1006-706X(08)60238-1Suche in Google Scholar

18 J.Ma, L. C.Lim: Effect of particle size distribution on sintering of agglomerate free submicron alumina powder compacts, Journal of European Ceramic Society22 (2002), pp. 21972208Suche in Google Scholar

Published Online: 2013-05-26
Published in Print: 2012-11-01

© 2012, Carl Hanser Verlag, München

Heruntergeladen am 6.10.2025 von https://www.degruyterbrill.com/document/doi/10.3139/120.110389/html
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