Startseite Two-Step Synthesis of Nano-Structured Carbon Phase
Artikel
Lizenziert
Nicht lizenziert Erfordert eine Authentifizierung

Two-Step Synthesis of Nano-Structured Carbon Phase

  • Nadir I. Seyidov , Musa I. Rustamov , Hikmet D. Ibrahimov , Eldar B. Zeynalov und Joerg F. Friedrich
Veröffentlicht/Copyright: 28. Mai 2013
Veröffentlichen auch Sie bei De Gruyter Brill

Abstract

This article describes in principal the possibility of nano-struc- tured carbon phase preparation through pyrolytic decomposition of a complex on the base of metallic Aluminium and Chlorohydrocarbons.

Kurzfassung

Im vorliegenden Beitrag wird die prinzipielle Möglichkeit beschrieben, nanostrukturierte Karbonphasen mittels pyrolytischem Zerfall eines auf metallischem Aluminium und Chlorkohlenwasserstoffen basierenden Komplexes zu präparieren.


Prof. Dr. sc. nat. Jörg F. Friedrich studied chemistry at the Humboldt Universität, Berlin, Germany. 1975 he acquired the Dr. rer. nat. (PhD) in Polymer Chemistry from the Academy of Sciences of GDR, Institute of Macromolecular Sciences, Berlin, as well as the Promotion B (Habilitation). 1982 he became Dr. sc. nat. in polymer and plasma chemistry. Ordinary habilitation (Dr. rer. nat. habil.) followed in 1991 from the TH Merseburg. Since 1996 he is Director and Professor at the Federal Institute of Materials Research and Testing, as well as Professor at the Technical University Berlin (2007).

Prof. Dr. sc. nat. Eldar B. Zeynalov studied chemistry at Azerbaijan State University, Baku (1966-1971). From 1971to 1976 he was post-graduate student and candidate of Chemical Sciences (Candidate=Dr. rer. nat.=PhD) at the Institute of Chemical Physics of the USSR Academy of Sciences, Moscow. Between 1976 and 1989, he was research officer, senior staff scientist, assistant professor, associate professor, Doctor of Chemical Sciences and scientific department leader at different institutes of the Azerbaijan Academy of Sciences, now in Baku. He is full professor since 2010.

Prof. Dr. sc. nat. Musa I. Rustamov, studied chemistry at the Azerbaijan Industrial Institute, Baku. He received his Doctor of Technical Sciences in 1968.Since 1973 he is Professor and since 1989 Academician and Director of the Institute of Petrochemical Processes of the Azerbaijan National Academy of Sciences, Baku.

Prof. Dr. sc. nat. Nadir I. Seyidov, studied at the Azerbaijan State University, Baku. He is Doctor of Chemical Sciences and since 1972 professor and academician since 2001. In 2007 he became head of the chemical department of Presidium of Azerbaijan National Academy of Sciences, Baku.

Dr. sc. nat. Hikmet D. Ibrahimov, studied at the Azerbaijan State University, Baku. In 2011 he received his Doctor of Technical Sciences and became deputy head of the laboratory at the Institute of Petrochemical Processes of the Azerbaijan National Academy of Sciences, Baku.


References

1 J.Barkauskas, I.Stankeviciene, A.Selskis: A novel purification of carbon nanotubes by high-temperature treatment with tetrachloromethane, Separation and Purification Technology71 (2010), pp. 33133610.1016/j.seppur.2009.12.019Suche in Google Scholar

2 S. J.Teng, X. X.Wang, B. Y.Xi, J.Na, Preparation of hollow carbon nanocages by iodine-assisted heat treatment, Journal of Power Sources195 (2010), pp. 1065107010.1016/j.jpowsour.2009.08.076Suche in Google Scholar

3 Q.Zhao, Y. H.Li, X. P.Zhou, T. S.Jiang, C. S.Li, H. B.Yin: Synthesis of multi-wall carbon nanotubes by the pyrolysis of ethanol on Fe/MCM-41 mesoporous molecular sieves, Superlattices and Microstructures47 (2010) pp. 43244110.1016/j.spmi.2009.11.003Suche in Google Scholar

4 S.Santangelo, C.Milone, M.Lanza, A.Pistone, G.Messina, G.Faggio: Scaling laws for multi-walled carbon nanotube growth by catalyzed chemical vapor deposition, Journal of Nanoscience and Nanotechnology10 (2010), pp. 1286129510.1166/jnn.2010.1823Suche in Google Scholar PubMed

5 S.Maghsoodi, A.Khodadadi, Y.Mortazavi: A novel continuous process for synthesis of carbon nanotubes using iron floating catalyst and MgO particles for CVD of methane in a fluidized bed reactor, Applied Surface Science256 (2010), pp. 2769277410.1016/j.apsusc.2009.11.026Suche in Google Scholar

6 M.Khavarian, S. P.Chai, S. H.Tan, A. R.Mohamed: Floating catalyst CVD synthesis of carbon nanotubes using iron (III) chloride: Influences of the growth parameters, Nano4 (2009), pp. 35936610.1142/S1793292009001939Suche in Google Scholar

7 S.Ratkovic, E.Kiss, G.Boscovic: Synthesis of high-purity carbon nanotubes over alumina and silica supported bimetallic catalysts, Chemical Industry and Chemical Engineering Quarterly, 15 (2009), pp. 26327010.2298/CICEQ0904263RSuche in Google Scholar

8 M. H.Xu, X. S.Qi, W.Zhong, X. J.Ye, Y.Deng, C. T.Au, C. Q.Jin, Z. X.Yang, Y. W.Du: Synthesis and properties of magnetic composites of carbon nanotubes/Fe nanoparticle, Chinese Physics Letters26 (2009), article No.116103Suche in Google Scholar

9 T.Somanathan, A.Pandurangan: Direct synthesis of vanadium substituted mesoporous MCM-41 molecular sieves: a systematic study for the growth of SWNTs, Journal of Porous Materials16 (2009), pp. 65766510.1007/s10934-008-9246-3Suche in Google Scholar

10 K. N.Patil, C. S.Solanki: Precursor to high purity carbon nanotubes: a step by step evaluation of carbon yield, Journal of Nano Research6 (2009), pp. 758710.4028/www.scientific.net/JNanoR.6.75Suche in Google Scholar

11 N.Tang, J. F.Wen, Y.Zhang, F. X.Liu, K. J.Lin, Y. W.Du: Helical Carbon Nanotubes: Catalytic Particle Size-Dependent Growth and Magnetic Properties, ACS Nano4 (2010), pp. 24125010.1021/nn901425rSuche in Google Scholar PubMed

12 X. S.Qi, W.Zhong, Y.Deng, C. T.Au, Y. W.Du: Synthesis of helical carbon nanotubes, worm-like carbon nanotubes and nanocoils at 450 degrees C and their magnetic properties, Carbon48 (2010), pp. 36537610.1016/j.carbon.2009.09.038Suche in Google Scholar

13 S.Lyu, D.Jung, K.Ahn, H.Lee, N.Lee, Y.Park, J.Sok: Purification of Single-walled Carbon Nanotubes by HCl Treatment and Analysis of the Field Emission Property, Korean Journal of Metals and Materials48 (2010), pp. 33534110.3365/KJMM.2010.48.04.335Suche in Google Scholar

14 Q. J.Nie, W. Z.Qian, Q.Zhang, Q.Wen, F.Wie: Very High-Quality Single-Walled Carbon Nanotubes Grown Using a Structured and Tunable Porous Fe/MgO Catalyst, Journal of Physical Chemistry 113 C (2009), pp. 2017820183Suche in Google Scholar

15 Y.Ando, Carbon Nanotube: The Inside Story, Journal of Nanoscience and Nanotechnology, 10 (2010), pp. 3726373810.1166/jnn.2010.2017Suche in Google Scholar PubMed

16 M. H.Ruemmeli, F.Schaeffel, A.Bachmatiuk, G.Trotter, D.Adebimpe, G.Sim-ha-Martynkova, D.Placha, B.Rellinghaus, P. G.McCormick, E.Borowiak-Palen, P.Ayala, T.Pichler, R.Klingeler, M.Knupfer, B.Buechner: Oxide catalysts for carbon nanotube and few layer graphene formation, Physica Status Solidi B-Basic Solid State Physics246 (2009), pp. 2530253310.1002/pssb.200982259Suche in Google Scholar

17 S.Costa, E.Borowiak-Palen, A.Bachmatiuk, M. H.Ruemmeli, T.Gemming, R. J.Kalenczuk: Iron filled carbon nanostructures from different precursors, Energy Conversion and Management, 49 (2008), pp. 2483248610.1016/j.enconman.2008.01.040Suche in Google Scholar

18 J.Liu, A. T.Harris: Synthesis of coiled carbon nanotubes on Co/Al2O3 catalysts in a fluidised-bed, Journal of Nanoparticle Research12 (2010), pp. 64565310.1007/s11051-009-9634-xSuche in Google Scholar

19 Z.Sadeghian, J. G.Heinrich: Growth of carbon nanotubes with different morphologies by pyrolising acetylene: Advances in Applied Ceramics109 (2010), pp. 3944Suche in Google Scholar

20 E. F.Antunes, E. C.Almeida, C. B. F.Rosa, L. I.de Medeiros, L. C.Pardini, M.Massi, E. J.Corat: Thermal Annealing and Electrochemical Purification of Multi-Walled Carbon Nanotubes Produced by Camphor/Ferrocene Mixtures, Journal of Nano-science and Nanotechnology, 10 (2010), pp. 1296130310.1166/jnn.2010.1830Suche in Google Scholar PubMed

21 E.Borowiak-Palen, A.Steplewska, M. H.Ruemmeli: On the use of Cu catalysts for tailoring carbon nanostructures in alcohol-CVD, Physica Status Solidi B-Basic Solid State Physics246 (2009), pp. 2448245310.1002/pssb.200982263Suche in Google Scholar

Published Online: 2013-05-28
Published in Print: 2011-04-01

© 2011, Carl Hanser Verlag, München

Heruntergeladen am 23.10.2025 von https://www.degruyterbrill.com/document/doi/10.3139/120.110217/html?lang=de
Button zum nach oben scrollen