Abstract
Collapsible soils are almost found in unsaturated states and involved significant engineering problems. Geotechnical challenges of such soils are represented by the hydro-mechanical behaviour during wetting–drying cycles due to the humidity and climate conditions. The main objective of this paper is to investigate the soil–water characteristic curve (SWCC) of unsaturated collapsible soils. In this study, three types of collapsible soils were investigated such as natural soils of sandy gypseous, silty loess, and artificial soil of gypsum–sand mixture. Determination of soil–water characteristic curve represented by wetting and drying paths has been done using a combination of the axis-translation technique (i.e. pressure plate device) and vapour equilibrium technique (i.e. salts solution desiccators) to cover a wide range of applied suction. The test results show that the air-entry value for all soils occurs at a very low suction range. At the boundary effect zone, the coarse grain size of the soil mass cannot hold the water molecules in the pore space, even with a low value of imposed suction. Moreover, the amount of hysteresis varied based on the geological formation and homogeneity of the soil fabric. Furthermore, SWCC has been interpreted by insignificant volume change and a slight reduction in void ratio, especially at high applied suction.
1 Introduction
In recent decades, many geotechnical problems such as collapse deformation and foundation failure were observed. Deformation of the engineering constructions is commonly occurred when carried out on collapsible soil layers, especially in unsaturated conditions [1]. The collapse deformation can be expected in single or multi-step wetting process. Soil wetting due to the reduction in suction pressure leads to particle softening, dissolution of cementing bonds, and hydro-mechanical changes within the soil skeleton [2,3].
Soil suction is a general term that is commonly associated with unsaturated soil mechanics and may be used when referring to matric suction, osmotic suction, or total suction [4,5]. Thus, the relationship between the suction types can be formulated as follows:
where
To study and solve the air and water flow problems and to analyse seepage, shear strength, and volume change behaviour involving unsaturated and saturated soils, the soil–water characteristic curve (SWCC) is required [5,6]. The SWCC is the denotation of the water content or degree of saturation of the soil corresponding to the soil suction [6,7]. A combination of two methods must be utilized to determine the SWCC because there is no unique technique or device that can cover the entire range of unsaturated soil suction values [6]. The most common laboratory technique is the axis-translation technique (ATT), which utilizes the porous ceramic disks in a pressure plate apparatus. This method can cover matric suction range equal to the maximum air-entry value of the ceramic disk of 1500 kPa. However, a controlled relative humidity environment (i.e. vapour equilibrium technique (VET)) is used to apply total suction up to more than 250000 kPa depending on the type and concentration of salt solutions used [2,6,8].
In general, the SWCC commonly consists of the drying path and the wetting path. To determine the drying path, the applied suction is increased incrementally on the initially fully saturated sample under zero net vertical stress. The volume and the amount of water in the saturated sample are slightly decreased as the suction increases until the air-entry value suction
2 Material, equipment, and techniques
2.1 Soil
Three types of soils were used: Gypseous sand soil of (70%) gypsum content from Al-Ramadi city, Iraq (GI); Loess silt soil from Dresden region, Germany (LG); and artificial sample of (70%) gypsum–(30%) Silber sand mixture (70G30S) [1,3]. The summary of the geotechnical properties of the soil samples is shown in Table 1.
Summary of the geotechnical properties of the soil samples
Property | Gypseous soil GI | Mixed soil 70G30S | Loess soil LG | Standard |
---|---|---|---|---|
Atterberg’s limits: LL, PL, PI (%) | NP | NP | 28.2, 16.8, 11.4 | ASTM D4318 |
Specific gravity (Gs) | 2.35 | 2.4 | 2.63 | ASTM D854 |
In place dry density (g/cm3) | 1.3 | — | 1.6 | ASTM D2937 |
Standard compaction test | ASTM D1557 | |||
Max.dry density (g/cm3) | 1.7 | 1.69 | 1.74 | |
Opt. moisture content (%) | 8.0 | 12.9 | 16.4 | |
Natural void ratio,
|
0.81 | — | 0.64 | |
Cu | 11.58 | 19.4 | — | ASTM D422 |
Cc | 0.33 | 0.16 | — | |
Passing sieve (75 µ) (%) | 22.1 | 35.5 | 98 | |
Initial suction
|
139280 | 198016 | 111311 | Chilled-Mirror [11] |
Collapse potential
|
9.3 | 11.1 | 5.4 | ASTM D5333 [1,2] |
2.2 Equipment and techniques
Two techniques were used during the determination of SWCC to cover wide range of imposed suction. The first technique is the axis-translation technique (ATT) using pressure plate apparatus, and the second is the vapour equilibrium technique (VET) using constant relative humidity desiccators with salt solutions.
2.2.1 Pressure plate apparatus
Pressure plate apparatus with ATT technique is used to determine parts of the drying and wetting paths of SWCC by applying matric suction range less than 1500 kPa as shown in Figure 1. The soil specimen was prepared in a Plexiglas plastic ring with a diameter of 50 mm and a height of 15 mm.

Pressure plate apparatus with axis-translation technique (ATT): (a) device set up; (b) schematic plot.
Three types of saturated and air-flushed ceramic disks with different air-entry values
2.2.2 Constant relative humidity desiccators
The constant relative humidity desiccators with the VET technique are utilized for continuing the determination of the rest parts of the drying and wetting paths of the SWCC. Many large and leak-proof desiccators containing different concentrations of salt solutions were used to apply total suction range >2000 kPa on the soil specimens, as shown in Figure 2. The actual total suction based on the relative humidity of the salt solutions was measured at the beginning and the end of the test using the chilled-mirror hygrometer technique [11]. The isolated chamber of constant temperature (22 ± 0.5°C) is used to conduct the test.

Constant relative humidity desiccators with vapour equilibrium technique (VET): (a) desiccators set up; (b) schematic plot.
3 Best-fit laboratory data for the SWCC
3.1 Van Genuchten (1980)–Mualem (1976) model
Van Genuchten [12] proposed a mathematical function which connected the soil suction and the water content as demonstrated in Eq. (2). In order to unify (n and m) parameters in a single variable, Van Genuchten (1980) used Mualem's (1976) relationship between (n and m) as shown in Eq. (3):
where
3.2 Fredlund and Xing (1994) model
The Fredlund and Xing [10] SWCC equation which expressed in Eqs. (4) or (8) is used the correction factor
or
If the SWCC is required to fit only between saturated conditions and residual conditions, another form of Eq. (6) can be used to obtain best fit for the experimental data as follows:
where
The fitting parameters (a, m, and n) used to obtain the best fit for SWCC as well as the standard regression (R 2) are illustrated in Table 2.
Fitting parameters for drying and wetting paths of SWCCs of GI, 70G30S, and LG soils
Model | Van Genuchten (1980)–Mualem (1976) | Fredlund and Xing (1994) | ||||||
---|---|---|---|---|---|---|---|---|
Parameter | a | m | n | R 2 | a | m | n | R 2 |
GI | ||||||||
Drying-w | 0.55 | 0.26 | 1.35 | 0.990 | 5.5 | 1.2 | 1.2 | 0.974 |
Drying-Sr | 0.3 | 0.31 | 1.44 | 0.980 | 4.5 | 1.0 | 1.4 | 0.984 |
Wetting-w | 0.7 | 0.26 | 1.35 | 0.902 | 3.0 | 0.58 | 5.0 | 0.982 |
Wetting-Sr | 0.7 | 0.26 | 1.35 | 0.903 | 3.0 | 0.58 | 5.0 | 0.981 |
70G30S | ||||||||
Drying-w | 0.15 | 0.35 | 1.55 | 0.994 | 13.0 | 1.75 | 1.0 | 0.996 |
Drying-Sr | 0.12 | 0.35 | 1.54 | 0.993 | 20.0 | 1.85 | 1.0 | 0.993 |
Wetting-w | 0.45 | 0.37 | 1.58 | 0.985 | 3.5 | 0.85 | 4.0 | 0.993 |
Wetting-Sr | 0.45 | 0.37 | 1.58 | 0.985 | 3.5 | 0.85 | 4.0 | 0.993 |
LG | ||||||||
Drying-w | 0.042 | 0.26 | 1.35 | 0.993 | 50 | 1.1 | 1.0 | 0.994 |
Drying-Sr | 0.032 | 0.25 | 1.33 | 0.990 | 50 | 1.0 | 0.9 | 0.992 |
Wetting-w | 0.4 | 0.17 | 1.21 | 0.981 | 4.0 | 0.43 | 1.9 | 0.994 |
Wetting-Sr | 0.4 | 0.17 | 1.21 | 0.987 | 5.0 | 0.5 | 1.7 | 0.993 |
4 Results and discussion
Figure 3 shows the variation of void ratio with applied suction in SWCC test-Drying path results for GI, 70G30S, and LG soil samples, while Figures 4–9 and Table 3 demonstrate the results of gravimetric water content versus suction and degree of saturation versus suction, respectively (i.e. SWCCs). Figures 10–12 indicate the verification of experimental data with predicted data.

Variation of void ratio with applied suction in SWCC test-drying path results for GI, 70G30S, and LG soil samples.

Soil–water characteristic curve, gravimetric water content versus suction for GI soil.

Soil–water characteristic curve, gravimetric water content versus suction for 70G30Ssoil.

Soil–water characteristic curve, gravimetric water content versus suction for LG soil.

Soil–water characteristic curve (SWCC), degree of saturation versus suction for GI soil.

Soil–water characteristic SWCC, degree of saturation versus suction for 70G30S soil.

Soil–water characteristic curve (SWCC), degree of saturation versus suction for LG soil.
Initial suction, air entry value and residual suction of SWCC
Soil sample | Initial suction
|
Air entry value (
|
Residual suction (
|
---|---|---|---|
GI | 139280 | 2 | 70 |
70G30S | 198016 | 4 | 250 |
LG | 111311 | 15 | 2000 |

Verification of experimental with predicted data of SWCC: (left) gravimetric water content (w) results and (right) degree of saturation (Sr) results for GI soil.

Verification of experimental with predicted data of SWCC: (left) gravimetric water content (w) results and (right) degree of saturation (Sr) results for 70G30S soil.

Verification of experimental with predicted data of SWCC: (left) gravimetric water content (w) results and (right) degree of saturation (Sr) results for LG soil.
From Figure 3, it can be noticed that the SWCC has been interpreted by insignificant volume change throughout the test, especially at high applied suction. However, slight reduction in void ratio is observed during the drying path when for suction values lower than 1500 kPa. This behaviour can be attributed to shrinkage of the soil mass due to an increase in the rate of desorption as well as increasing suction application.
From the SWCCs of both GI (Figures 4 and 6) and 70G30S (Figures 5 and 8) soils, it can be observed that the air-entry value
By comparing the SWCCs for both GI (Figures 4 and 6) and 70G30S (Figures 5 and 8) soils, the transition zone of 70G30S soil was greater and flatter than the transition zone of GI soil, where the residual suction of 70G30S soil exceeded the residual suction of GI soil by approximately five times. However, the gypsum cementing structure showed considerable hysteresis on its SWCC with a clear increase in the magnitude of hysteresis for 70G30S soil. This behaviour can be related to the type and the difference in geological formation and homogeneity of soil fabric and gypsum bonds.
For LG soil, the
In general, hysteresis in SWCCs for all soil specimens exists. This can be related to two reasons: first, the difference in the contact angles and/or open end pores because of cementing bonds dissolution. This action occurred when withdrawing the soil–water interface during drying and when proceeding during wetting, such as in Gypseous soils (GI and 70G30S). Second, the non-uniformity formation of the individual trapped air and pores media causes an ‘ink bottle’ effect phenomenon [13] such as in Loess soil (LG).
It is worth mentioning that the slope of the SWCCs of the three samples at boundary effect zone is not straight. They show a slight desaturation where the capillary suction in this range is less than the
On the other hand, the drying path of SWCCs for all samples showed also a curvature shape after the residual condition even with a high range of applied suction as in LG soil (Figures 6 and 9). Significant moisture in the microscope level of soil structure is the reason behind this behaviour.
Figures 10–12 show the verification results of experimental data with the predicted data of the SWCCs. Regression analysis for the experimental results using the Van Genuchten (1980)–Mualem (1976) and Fredlund and Xing models reveal the high accuracy of these results in comparison with the predicted data of the SWCCs (Table 2).
The Fredlund and Xing [10] model provided reliable closeness of fit with experimental data sets and more flexibility, particularly at the residual zone of the wetting part at the point of the inflection of the SWCC as confirmed by many researchers such as [5,14].
5 Conclusions
The SWCC has been interpreted by insignificant volume change especially at high applied suction. However, a slight reduction in the void ratio during the drying path is observed. The shrinkage of the soil mass has occurred as a result of increasing the rate of desorption simultaneously with increasing suction application.
The air-entry value for all soils occurs at a low suction range. The residual suction value for gypseous soils occurs at low suction while for loess soil occurs at a relatively high suction range.
At the boundary effect zone, the coarse grain size of the soil mass cannot hold the water molecules in the pore space, even with a low value of imposed suction due to the high permeability and weak interparticle tension forces of the metastable soil.
The hysteresis in SWCC is presented for the three soil samples. The amount of hysteresis varied based on the geological formation and homogeneity of the soil fabric.
Hysteresis in SWCCs caused by the differences in the contact angles; open end pores at the withdrawing and proceeding of soil–water interface as in Gypseous soils. And/or to the non-uniformity of the individual pores and trapped air as in Loess soil.
The slope of the SWCCs at the boundary effect zone for the three soil samples is not straight and shows a slight desaturation where the capillary suction in this range is less than the air entry value.
At the boundary effect zone, the air has not yet completely penetrated into the soil pores. The observed slight desaturation is due to the increase in the applied capillary force (i.e. suction pressure) towards the air-entry value. It caused successive loss of water within the soil mass.
Significant moisture in the microscope level of soil structure is the reason behind the curvature of the drying path of SWCC after the residual condition.
Acknowledgements
I hereby would like to express my gratitude and appreciation to the Chair of Soil Mechanics, Foundation Engineering and Environmental Engineering, Department of Civil and Environmental Engineering, Ruhr-Universität Bochum, Bochum, Germany and German Academic Exchange Service DAAD for their support and cooperation.
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Funding information: The authors state no funding involved.
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Author contributions: All authors have accepted responsibility for the entire content of this manuscript and approved its submission.
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Conflict of interest: The authors state no conflict of interest.
References
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