Investigation of the influence of the energy conditions of pulsed plasma-chemical synthesis on the morphological and structural properties of copper-containing silica-based nanocomposites
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Denis Ponomarev
,
Roman Sazonov
Abstract
This paper presents the results of a study of the effect of energy conditions (additional heating of the walls of the reaction chamber and subsequent action of an electron beam on the synthesized powder) of pulsed plasma-chemical synthesis on the morphology, average geometric size, phase and chemical composition of copper-containing silica-based nanocomposites. The nanocomposites were synthesized using a TEA-500 pulsed electron accelerator. It was the first time that copper-containing silica-based nanocomposites had been prepared using the pulsed plasma-chemical synthesis. The values of the band gap for the as-prepared nanocomposites were calculated. The nanocomposites were characterized by means of transmission electron microscopy and X-ray diffraction. The analysis revealed the changes in the morphology and phase composition of the nanocomposites upon energy conditions.
Funding source: Russian Science FoundationTomsk Polytechnic University
Award Identifier / Grant number: Unassigned
Award Identifier / Grant number: Unassigned
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Author contribution: All the authors have accepted responsibility for the entire content of this submitted manuscript and approved submission.
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Research funding: This work was supported by the Russian Science Foundation, research project no. 18-73-10011. The chemical composition of the synthesized copper-containing silica-based nanocomposite was studied in the Scientific Analytical Center of Tomsk Polytechnic University.
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Conflict of interest statement: The authors declare no conflicts of interest regarding this article.
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Articles in the same Issue
- Frontmatter
- Original Papers
- Corrosion behavior of hydroxyapatite coated AZ31 and AZ91 Mg alloys by electrostatic spray coating
- Radiation synthesis and characterization of polymeric wet adhesives for attracting and trapping insects
- Promoting the effect of cationic substitution on thermal stability and redox properties of new synthesized Keggin type lacunary polyoxometalates (L-POMs) Ni2.5PMo11 M(H2O)O39 (M = Co, Fe, Cu, Zn)
- Investigation of the influence of the energy conditions of pulsed plasma-chemical synthesis on the morphological and structural properties of copper-containing silica-based nanocomposites
- A computational material study of HoB6 and Co/MgO–HoB6: heavy rare-earth metal hexaborides
- Effects of alloying elements on the microstructure and mechanical properties of as-cast Cr12MoV cold-working die steel
- The effects of rotational and traverse speeds and SiC particles on the microstructure and mechanical properties of AA 5052 in friction stir welding
- Influence of hot extrusion on the microstructure and mechanical properties of Al2O3/7075 aluminum matrix composites
- Short Communication
- Fabrication of magnetic core–shell Fe nanowires by electrochemical deposition
- News
- DGM – Deutsche Gesellschaft für Materialkunde
Articles in the same Issue
- Frontmatter
- Original Papers
- Corrosion behavior of hydroxyapatite coated AZ31 and AZ91 Mg alloys by electrostatic spray coating
- Radiation synthesis and characterization of polymeric wet adhesives for attracting and trapping insects
- Promoting the effect of cationic substitution on thermal stability and redox properties of new synthesized Keggin type lacunary polyoxometalates (L-POMs) Ni2.5PMo11 M(H2O)O39 (M = Co, Fe, Cu, Zn)
- Investigation of the influence of the energy conditions of pulsed plasma-chemical synthesis on the morphological and structural properties of copper-containing silica-based nanocomposites
- A computational material study of HoB6 and Co/MgO–HoB6: heavy rare-earth metal hexaborides
- Effects of alloying elements on the microstructure and mechanical properties of as-cast Cr12MoV cold-working die steel
- The effects of rotational and traverse speeds and SiC particles on the microstructure and mechanical properties of AA 5052 in friction stir welding
- Influence of hot extrusion on the microstructure and mechanical properties of Al2O3/7075 aluminum matrix composites
- Short Communication
- Fabrication of magnetic core–shell Fe nanowires by electrochemical deposition
- News
- DGM – Deutsche Gesellschaft für Materialkunde
