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Facile Hydrothermal Synthesis of CoSO4ċH2O Nanoparticles and Barite Microcubes from Novel Precursors

  • Azam Sobhani and Masoud Salavati-Niasari EMAIL logo
Published/Copyright: December 13, 2012
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High Temperature Materials and Processes
From the journal High Temperature Materials and Processes Volume 31 Issue 6

Abstract

CoSO4ċH2O nanoparticles and barite (BaSO4) microcubes have been prepared by hydrothermal decomposition of new precursors [Co(tsc)2]Cl2 and [Ba(tsc)2]Cl2 (tsc =  thiosemicarbazide), respectively. The products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and Fourier transform infrared (FT-IR) spectroscopy. As a comparison between two methods, thermal decomposition of novel precursors in high temperature boiling organic solvents were examined.

Keywords: Nanoparticles; CoSO4ċH2O; BaSO4; hydrothermal; single-source precursor; thiosemicarbazide
Department of Inorganic Chemistry, Faculty of Chemistry, University of Kashan, Kashan, P. O. Box. 87317–51167, I. R. Iran
Received: 2011-12-24
Accepted: 2012-01-20
Published Online: 2012-12-13
Published in Print: 2012-12-14

©[2012] by Walter de Gruyter Berlin Boston

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  1. Masthead
  2. High Temperature Tensile Properties of Equal Channel Angular Pressed Al-Zn-Mg-Cu Alloy
  3. Hard Finish Turning Parameters Optimization for Machining of High Temperature Stainless Steel
  4. High Cycle Fatigue and Cyclic Plastic Deformation Behaviour of High Temperature Oxidation Resistant Titanium Aluminide Coated IMI 834 Alloy at 873 K
  5. Microstructural and Mechanical Properties of Er2O3-ZrO2 Ceramics with Different Er2O3 Contents
  6. Synthesis of Different Morphologies of PbS Nanostructures via Hydrothermal Process
  7. Facile Hydrothermal Synthesis of CoSO4ċH2O Nanoparticles and Barite Microcubes from Novel Precursors
  8. Hot Corrosion of Fe-Cr Alloys with 75 Na2SO4 + 25 NaCl Coating at 1173 K
  9. A Simple Method for Synthesis of PbS Nanoparticles Using 2-Mercaptoethanol as the Capping Agent
  10. Influence of Alloy Grain Size on High Temperature Corrosion Behavior of 2.25 Cr-1 Mo Steel in SO2 + O2 Atmosphere
  11. Encapsulation of Erbium(III) and Thulium(III) Nanocomplexes Containing 18- and 20-Membered Dioxa Tetraaza Macryclic Ligands Within the Framework of Zeolite
  12. Calculation of the Raman Linewidths of Lattice Modes Close to the α-β Transition in Quartz
  13. Production and Characterization of Hydroxyapatite-Zirconia Composites
  14. Influence of Long-term Aging on Microstructure and Creep Behaviors of FGH95 Nickel-based Superalloy
  15. Remnant Life Assessment and Microstructural Studies on Service Exposed Primary Reformer Tubes of a Catalytic Converter of an Ammonia Plant
  16. Preparation and Characterization of Poly Methyl Methacrylate-cadmium Sulfide Nanocomposite
  17. Oxidation Kinetics of Steels Utilized in the Production of Valves in Automobile Industry
https://doi.org/10.1515/htmp-2011-0153
Keywords for this article
Nanoparticles; CoSO4ċH2O; BaSO4; hydrothermal; single-source precursor; thiosemicarbazide

Articles in the same Issue

  1. Masthead
  2. High Temperature Tensile Properties of Equal Channel Angular Pressed Al-Zn-Mg-Cu Alloy
  3. Hard Finish Turning Parameters Optimization for Machining of High Temperature Stainless Steel
  4. High Cycle Fatigue and Cyclic Plastic Deformation Behaviour of High Temperature Oxidation Resistant Titanium Aluminide Coated IMI 834 Alloy at 873 K
  5. Microstructural and Mechanical Properties of Er2O3-ZrO2 Ceramics with Different Er2O3 Contents
  6. Synthesis of Different Morphologies of PbS Nanostructures via Hydrothermal Process
  7. Facile Hydrothermal Synthesis of CoSO4ċH2O Nanoparticles and Barite Microcubes from Novel Precursors
  8. Hot Corrosion of Fe-Cr Alloys with 75 Na2SO4 + 25 NaCl Coating at 1173 K
  9. A Simple Method for Synthesis of PbS Nanoparticles Using 2-Mercaptoethanol as the Capping Agent
  10. Influence of Alloy Grain Size on High Temperature Corrosion Behavior of 2.25 Cr-1 Mo Steel in SO2 + O2 Atmosphere
  11. Encapsulation of Erbium(III) and Thulium(III) Nanocomplexes Containing 18- and 20-Membered Dioxa Tetraaza Macryclic Ligands Within the Framework of Zeolite
  12. Calculation of the Raman Linewidths of Lattice Modes Close to the α-β Transition in Quartz
  13. Production and Characterization of Hydroxyapatite-Zirconia Composites
  14. Influence of Long-term Aging on Microstructure and Creep Behaviors of FGH95 Nickel-based Superalloy
  15. Remnant Life Assessment and Microstructural Studies on Service Exposed Primary Reformer Tubes of a Catalytic Converter of an Ammonia Plant
  16. Preparation and Characterization of Poly Methyl Methacrylate-cadmium Sulfide Nanocomposite
  17. Oxidation Kinetics of Steels Utilized in the Production of Valves in Automobile Industry
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