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Synthesis of Different Morphologies of PbS Nanostructures via Hydrothermal Process
-
Davood Ghanbari
,
Masoud Salavati-Niasari
Published/Copyright:
December 13, 2012
Abstract
Lead sulfide nanostructures with different morphologies and particle sizes were obtained via a simple hydrothermal reaction between lead salicylate (Pb(Hsal)2) and thioglycolic acid The novelty in this synthesis is using of thioglycolic acid as a sulfur source and stability agent simultaneously. Depending on the pH of the solution, morphologies of the PbS varied and crystals with shapes of nanoparticles, flower-like nanostructures and microrods were obtained. The effect of the reaction time on the morphology of the nanostructures has been investigated. Products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) ultraviolet-visible (UV-vis) and Fourier transform infrared (FT-IR) spectroscopy.
Received: 2011-12-24
Accepted: 2012-02-18
Published Online: 2012-12-13
Published in Print: 2012-12-14
©[2012] by Walter de Gruyter Berlin Boston
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- High Temperature Tensile Properties of Equal Channel Angular Pressed Al-Zn-Mg-Cu Alloy
- Hard Finish Turning Parameters Optimization for Machining of High Temperature Stainless Steel
- High Cycle Fatigue and Cyclic Plastic Deformation Behaviour of High Temperature Oxidation Resistant Titanium Aluminide Coated IMI 834 Alloy at 873 K
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- Hot Corrosion of Fe-Cr Alloys with 75 Na2SO4 + 25 NaCl Coating at 1173 K
- A Simple Method for Synthesis of PbS Nanoparticles Using 2-Mercaptoethanol as the Capping Agent
- Influence of Alloy Grain Size on High Temperature Corrosion Behavior of 2.25 Cr-1 Mo Steel in SO2 + O2 Atmosphere
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