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12 Characterization and mechanical properties analysis of carbon nanotube and hydroxyapatite-modified polymethyl methacrylate bone cement for bio-nanocomposite

  • Rajesh Kumar Verma , Virat Mani Vidyasagar , Devendra Kumar Singh , Umang Dubey and Panagiotis Kyratsis
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Nanocomposite and Nanohybrid Materials
This chapter is in the book Nanocomposite and Nanohybrid Materials

Abstract

This article focuses on the significant increase in the mechanical strength of PMMA (polymethyl methacrylate) that was achieved through the incorporation of multiwall carbon nanotube (MWCNT) and nano-size hydroxyapatite (HA) powders at varied loadings ranging from 0.25 to 0.75 wt%. This study aimed to validate the potential applications of this modified bio-nanocomposite through mechanical investigation and characterization. According to the findings, the incorporation of 0.5 wt% of both HA and MWCNT nanoparticles into the PMMA bone cement powder resulted in increase in the flexural strength of 26.67%, the flexural modulus of 24.32%, the compression strength of 14.58%, and the compression modulus of 50.8%. Fourier-transform infrared spectroscopy (FTIR) and X-ray diffraction analysis (XRD) are used to investigate the distribution and interaction of reinforced nanoparticles within the PMMA polymer matrix further. Due to this compatibility between fillers and matrix, improvement in mechanical properties is observed in the developed bio-nanocomposite. Overall, the FTIR analysis provided valuable insights into the functional group composition and molecular interactions within the produced nanocomposites, confirming the presence of specific vibrational modes and demonstrating the compatibility between the filler materials and the polymeric matrix.

Abstract

This article focuses on the significant increase in the mechanical strength of PMMA (polymethyl methacrylate) that was achieved through the incorporation of multiwall carbon nanotube (MWCNT) and nano-size hydroxyapatite (HA) powders at varied loadings ranging from 0.25 to 0.75 wt%. This study aimed to validate the potential applications of this modified bio-nanocomposite through mechanical investigation and characterization. According to the findings, the incorporation of 0.5 wt% of both HA and MWCNT nanoparticles into the PMMA bone cement powder resulted in increase in the flexural strength of 26.67%, the flexural modulus of 24.32%, the compression strength of 14.58%, and the compression modulus of 50.8%. Fourier-transform infrared spectroscopy (FTIR) and X-ray diffraction analysis (XRD) are used to investigate the distribution and interaction of reinforced nanoparticles within the PMMA polymer matrix further. Due to this compatibility between fillers and matrix, improvement in mechanical properties is observed in the developed bio-nanocomposite. Overall, the FTIR analysis provided valuable insights into the functional group composition and molecular interactions within the produced nanocomposites, confirming the presence of specific vibrational modes and demonstrating the compatibility between the filler materials and the polymeric matrix.

Chapters in this book

  1. Frontmatter I
  2. Preface V
  3. Acknowledgments VII
  4. Contents IX
  5. 1 The current scenario in nanocomposite and nanohybrid materials 1
  6. 2 A current perspective on nanocomposite and nanohybrid material: developments and trends 29
  7. 3 Synthetic nanomaterials: fabrication, development, and characterization 55
  8. 4 Advances in fabrication, development, and characterization of synthetic nanomaterials 85
  9. 5 Structural, morphological, thermal, and long persistent properties of synthesized nanostructured phosphor 99
  10. 6 Mechanical characteristics and surface roughness testing of nanomaterials in enhancing the discharge over spillways 117
  11. 7 Biomedical considerations of nanomaterials based on biological aspects in biomedical field 139
  12. 8 Nanomaterial-based molecular imaging and targeted cancer therapy: current progress and limitations 161
  13. 9 Emerging perspectives of nanoparticles to treat neurodegenerative diseases 179
  14. 10 Understanding antibacterial disinfection mechanisms of oxide-based photocatalytic materials 195
  15. 11 Nanocomposites and nanohybrids in additive manufacturing 223
  16. 12 Characterization and mechanical properties analysis of carbon nanotube and hydroxyapatite-modified polymethyl methacrylate bone cement for bio-nanocomposite 237
  17. 13 Role of nanomaterials in enhancing the performance of polymer composite materials 259
  18. 14 Nanotechnology: a novel weapon for insect pest and vector management 277
  19. 15 Effect of carbon nanotubes, aluminum hydroxide, and zinc borate on the mechanical and fire properties of epoxy nanocomposite 297
  20. 16 Recent advancements in polymer nanocomposites-based adsorbents for chromium removal 315
  21. About the editors 337
  22. List of contributors 339
  23. Index 343
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